CN110280756A - Add the diamond engineering thin-walled drill and its preparation process of cubic boron nitride - Google Patents

Add the diamond engineering thin-walled drill and its preparation process of cubic boron nitride Download PDF

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Publication number
CN110280756A
CN110280756A CN201910635953.8A CN201910635953A CN110280756A CN 110280756 A CN110280756 A CN 110280756A CN 201910635953 A CN201910635953 A CN 201910635953A CN 110280756 A CN110280756 A CN 110280756A
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diamond
boron nitride
cubic boron
engineering thin
powder
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CN110280756B (en
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栾会生
马永德
刘冰
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Shijiazhuang Oceanpower Tools Co Ltd
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Shijiazhuang Oceanpower Tools Co Ltd
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    • B22F1/0003
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/16Metallic particles coated with a non-metal
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F5/00Manufacture of workpieces or articles from metallic powder characterised by the special shape of the product
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C1/00Making non-ferrous alloys
    • C22C1/04Making non-ferrous alloys by powder metallurgy
    • C22C1/05Mixtures of metal powder with non-metallic powder
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C26/00Alloys containing diamond or cubic or wurtzitic boron nitride, fullerenes or carbon nanotubes
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C30/00Alloys containing less than 50% by weight of each constituent
    • C22C30/02Alloys containing less than 50% by weight of each constituent containing copper
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C30/00Alloys containing less than 50% by weight of each constituent
    • C22C30/04Alloys containing less than 50% by weight of each constituent containing tin or lead
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F5/00Manufacture of workpieces or articles from metallic powder characterised by the special shape of the product
    • B22F2005/001Cutting tools, earth boring or grinding tool other than table ware

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Polishing Bodies And Polishing Tools (AREA)
  • Cutting Tools, Boring Holders, And Turrets (AREA)
  • Drilling Tools (AREA)

Abstract

The invention discloses a kind of diamond engineering thin-walled drills for adding cubic boron nitride, it is made of raw material components such as metal powder, diamond and cubic boron nitrides, wherein metal powder includes FeCu30 prealloy powder, CuSn15 prealloy powder, am1 alloy powder, cobalt powder, the addition of the cubic boron nitride, which is taken, is first coated diamond and cubic boron nitride with covering, then the mode with metal powder mixture.The diamond engineering thin-walled drill of acquisition not only has the performance advantages such as toughness is high, thermal stability is strong, wearability is good, also greatly improves the service life and drilling hardness, speed of diamond engineering thin-walled drill.Furthermore, the preparation process of diamond engineering thin-walled drill provided by the invention, compound material is formed using special cladding process cladding diamond and cubic boron nitride, mixed metal powder again, and treatment conditions are limited, and to guarantee the high-quality and high-performance of diamond engineering thin wall drill, the preparation process Portable safety, high production efficiency, at low cost, product quality is excellent and stablizes.

Description

Add the diamond engineering thin-walled drill and its preparation process of cubic boron nitride
Technical field
The present invention relates to diamond engineering thin-walled drill technical field more particularly to a kind of diamonds for adding cubic boron nitride The preparation process of engineering thin wall drill and diamond core drill bit.
Background technique
Engineering thin wall drill is chiefly used in concrete sampling, building drilling burrows, when carrying out drilling concrete work, meeting Because operation needs to carry out drilling to metal products such as reinforcing bars in concrete with drill bit, although carrying out adding water cooling in drilling process But, but still it is not avoided that the high temperature generated by frictional heating.
Engineering thin wall drilling bit is mostly prepared by diamond at present, and diamond is mainly used for such as hard alloy, glass, pottery The processing of the hard brittle materials such as porcelain, stone material, concrete, building materials, since diamond is the allotrope of carbon, diamond bit is in height It is easily chemically reacted with the iron family element in steel under temperature, causes strong chemical abrasion, such as produced in drilling bar material Raw high temperature can make diamond be carbonized, and cause tool bit abrasion fast, influence sharpness, cutting effect and service life.
Summary of the invention
To solve the shortcomings of the prior art, the present invention provides a kind of diamond engineering for adding cubic boron nitride is thin Wall bores, and cutter head has toughness, thermal stability and the service life significantly improved.
To achieve the above object, the diamond engineering thin-walled drill of addition cubic boron nitride provided by the invention, including it is following Mass parts raw material components:
92~98 parts of metal powder;
1.5~4.5 parts of diamond;
0.5~3.5 part of cubic boron nitride;
Wherein, metal powder includes following mass parts raw material components per hundred parts:
The addition of the cubic boron nitride, which is taken, is first wrapped up diamond and cubic boron nitride with covering, then with gold Belong to powder mixture mode, the cladding process the following steps are included:
A1, it obtains covering: taking 1.5~3.0 parts of granulating agent (ws-180), 25~30 parts of cobalt powder, 32~38 parts of isopropanol, It 32~45 parts of acetone, is stirred evenly under the conditions of 50~70 DEG C of temperature, obtains covering;
A2, gluing, pre-coated and drying and processing: the diamond cleaned up and cubic boron nitride are proportioned It is even, gluing is then mixed and carried out with covering made from step a1, after gluing processing after by material be then added in cobalt powder into Row pre-coated obtains cobalt powder and coats 10~50 μm of thickness, then dries;
The painting jelly that the gluing processing uses is granulating agent ws-180;
A3, cladding and reduction treatment: the pre-coated material after drying is coated again with covering in coating machine, is obtained To cladding 100~500 μm of thickness, finally by after cladding diamond and cubic boron nitride carry out reduction treatment.
Diamond engineering thin-walled drill of the invention, by being modified to cutter head, the addition cube in cutter head material formula The metal powder prepared by prealloy powder is compounded while boron nitride, and to give full play to the performance of cubic boron nitride, general cube Boron nitride is wrapped by agent package with elder generation together with diamond, then feeds with the mode of metal powder mixture, exists to assign cutter head Higher toughness under high temperature, and to the chemical stability of iron family element, significantly improve service performance and service life.
Cubic boron nitride, has very high hardness, thermal stability and chemical inertness, and hardness is only second to diamond, but heat Stability is much higher than diamond, and is known as biggish chemical stability to Ferrious material member.By in diamond engineering thin-walled drill Although cutter head material in be added cubic boron nitride it is helpful for cutter head toughness, chemical stability at high temperature, for The hardness of cutter head, drilling can but be influenced, therefore addition of the present invention for cubic boron nitride, first to use specific cladding Diamond and cubic boron nitride are bundled together by technique, then the mode of the metal powder mixture compounded with by prealloy powder, are made Cubic boron nitride and diamond further generate synergistic effect between metal powder, obtain not only being remarkably improved at high temperature Toughness, chemical stability, and the unaffected diamond engineering thin-walled drill enhanced instead in terms of drilling hardness, speed Cutter head extends cutter head service life to improve cutter head service performance comprehensively.In addition, diamond and cubic boron nitride are carrying out When package, gluing, pre-coated and drying and processing need to be first carried out, to reduce the cladding difficulty to diamond and cubic boron nitride, is come Guarantee the package quality and thickness of diamond and cubic boron nitride;Reduction treatment is carried out after also cubic boron nitride is wrapped up, and is reinforced Bond strength between cobalt powder and diamond and cubic boron nitride, and guarantee that cobalt powder is to diamond in cutter head subsequent processes With the holding power of cubic boron nitride, to significantly improve the service performance and service life of cutter head.
As the restriction to above-mentioned technical proposal, the granularity of the metal powder is 100~400 mesh, the diamond Granularity is 25~70 mesh, and the granularity of the cubic boron nitride is 25~70 mesh.
As the restriction to above-mentioned technical proposal, the FeCu30 prealloy powder, CuSn15 prealloy powder, am1 alloyed powder Expect, the granularity of cobalt powder is 100~400 mesh.
As the restriction to above-mentioned technical proposal, the speed of agitator for preparing of the covering is 150~350 turns/min.
As the restriction to above-mentioned technical proposal, the reduction treatment condition is reduction temperature 800 under an atmosphere of hydrogen ~900 DEG C.
The granularity of metal powder, diamond and cubic boron nitride is further limited, the grain of each raw material component in metal powder Degree, the reduction treatment condition of covering prepared after revolving speed, and cladding, to make the diamond engineering thin-walled drill performance obtained It is more excellent.
Meanwhile the present invention also provides a kind of preparation processes of diamond engineering thin-walled for adding cubic boron nitride, including Following steps:
A, coat: cladding process according to claim 1 prepares the package compound material of diamond and cubic boron nitride;
B, mixture: the package compound material of step a being mixed with metal powder, adds the wetting agent of 0.3~2g/kg, It is formed in batch mixer and blendes together material;
C, cold pressing compacting, sintering: will blend together in material investment cold stamping die, obtains cold pressing green compact through cold pressing compacting, places into It is sintered to obtain cutter head prefabrication in agglomerating plant;
D, it post-processes: will be welded on drilling rod after the processing of cutter head prefabrication, obtain diamond engineering thin-walled drill.
As the restriction to above scheme, every hundred mass parts of wetting agent include 39~45 parts of glycerol, zinc stearate 7~ 12 parts, remaining be isopropanol.
As the restriction to above scheme, batch mixer described in step b uses three-dimensional material mixer, and the mixing condition is normal Temperature, relative humidity 30% are hereinafter, 1~3h of incorporation time.
As the restriction to above scheme, cold pressing pressing conditions described in step c is in will in the 2s time in cold stamping die Pressing pressure rises to 5t/cm by normal pressure2Pressure.
As the restriction to above scheme, sintering condition described in step c be in hot press in the 5min time by temperature 820~950 DEG C are risen to, this temperature 10min is then maintained, is subsequently reduced to room temperature.
Further limit effective composition of wetting agent during mixture, the type of batch mixer, mixing condition, cold pressing compacting item Part and sintering condition, to obtain the more optimized diamond engineering thin-walled drill of performance, to be conducive to diamond engineering thin-walled drill It uses.
The diamond engineering thin-walled drill of addition cubic boron nitride provided by the invention is wrapped by limiting during the preparation process The condition of mixture sequence and cold pressing compacting, sintering and post-processing after wrapping up in compound material, cladding, to guarantee in diamond engineering The performance of each raw material component can be combined effectively in the preparation process of thin-walled drill, promote the formation of preparation process cutter head overall performance, It realizes the optimization to performances such as diamond core drill bit toughness, thermal stability, wearabilities, meets the diamond engineering of high performance requirements Thin-walled drill.
In conclusion the diamond engineering thin-walled drill obtained using technical solution of the present invention, utilizes cubic boron nitride knot Alloy hard rock compounds the metal powder prepared by prealloy powder, and is fed in a manner of first wrapping up mixture again, significantly improves knife Toughness, chemical stability and the service performance and service life of head at high temperature.Diamond engineering thin-walled provided by the invention The preparation process of brill using special cladding process cladding diamond and cubic boron nitride, and further limits mixture, cold pressing pressure System, the treatment conditions of sintering, to guarantee the high-quality and high-performance of diamond engineering thin wall drill, the preparation process Portable safety, High production efficiency, at low cost, product quality is excellent and stablizes.
Specific embodiment
Below in conjunction with embodiment, technical solution of the present invention is clearly and completely described, it is clear that described Embodiment is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field Those of ordinary skill's every other embodiment obtained without making creative work, belongs to protection of the present invention Range.
Embodiment one
The present embodiment is related to a kind of diamond engineering thin-walled drill and its preparation process for adding cubic boron nitride.
A kind of diamond engineering thin-walled drill, including following mass parts raw material components:
92~98 parts of metal powder, 1.5~4.5 parts of diamond, 0.5~3.5 part of cubic boron nitride;The metal powder Granularity is 100~400 mesh, and the granularity of the diamond is 25~70 mesh, and the granularity of the cubic boron nitride is 25~70 mesh;
Wherein, metal powder includes following quality powder raw material component per hundred parts: 35~55 parts of FeCu30 prealloy powder, 20~30 parts of CuSn15 prealloy powder, 3~8 parts of am1 alloy powder, 13~27 parts of cobalt powder;The FeCu30 prealloy powder, CuSn15 prealloy powder, am1 alloy powder, the granularity of cobalt powder are 100~400 mesh;
In each embodiment shown in raw material components table specific as follows:
In upper table the diamond engineering thin-walled drill of each embodiment prepare it is as follows:
A, it coats: preparing the package compound material of diamond and cubic boron nitride by following cladding process;
A1, it obtains covering: taking granulating agent ws-1801.5~3.0 part, 25~30 parts of cobalt powder, 32~38 parts of isopropanol, third It 32~45 parts of ketone, is stirred evenly under the conditions of 150~350 turns 50~70 DEG C of temperature, speed of agitator/min, obtains covering;
A2, gluing, pre-coated and drying and processing: the diamond cleaned up and cubic boron nitride are proportioned It is even, gluing is then mixed and carried out with covering made from step a1, after gluing processing after by material be then added in cobalt powder into Row pre-coated obtains cobalt powder and coats 10~50 μm of thickness, then dries;
The painting jelly that the gluing processing uses is granulating agent ws-180;
A3, cladding and reduction treatment: the pre-coated material after drying is coated again with covering in coating machine, is obtained To cladding 100~500 μm of thickness, finally by after cladding diamond and cubic boron nitride under an atmosphere of hydrogen, reduction temperature is Reduction treatment is carried out under conditions of 800~900 DEG C;
B, mixture: the package compound material of step a is mixed with metal powder, the wetting agent of 0.3~2g/kg is added, adopts With three-dimensional material mixer, material is blended together hereinafter, being formed in 1~3h of incorporation time in room temperature, relative humidity 30%;
Every hundred mass parts of wetting agent include 39~45 parts of glycerol, 7~12 parts of zinc stearate, remaining be isopropanol;
C, cold pressing compacting, sintering: it will blend together in material investment cold stamping die, rise to pressing pressure by normal pressure in the 2s time 5t/cm2Pressure, through cold pressing compacting obtain cold pressing green compact, place into agglomerating plant and be sintered, will be hot in the 5min time Temperature in press rises to 820~950 DEG C, then maintains this temperature 10min, is subsequently reduced to room temperature, so that it is prefabricated to obtain cutter head Product;
D, it post-processes: will be welded on drilling rod after the processing of cutter head prefabrication, obtain diamond engineering thin-walled drill.
Auxiliary material and dosage that the preparation process of the various embodiments described above is related to, technological parameter are as shown in the table:
Embodiment two
The present embodiment is related to the using effect of diamond engineering thin-walled drill.
The performance of diamond engineering thin-walled drill prepared by embodiment 1.1~1.4 is tested, using effect is tested such as Under:
The diamond engineering thin wall drilling bit that embodiment 1.1 obtains, sample specification are as follows: φ 76-380, wherein cutter head height 10mm, cutter head is with a thickness of 3.6mm.It is obtained using test drilling block (standard c40 cement, thickness 240mm, 4 32mm reinforcing bars) Diamond engineering thin-walled drill is tested, and drilling speed can reach the hole 6min/, and service life is up to 40 holes.
The diamond engineering thin wall drilling bit that embodiment 1.2 obtains, sample specification are as follows: φ 76-380, wherein cutter head height 10mm, cutter head is with a thickness of 3.6mm.It is obtained using test drilling block (standard c40 cement, thickness 240mm, 4 32mm reinforcing bars) Diamond engineering thin-walled drill is tested, and drilling speed can reach the hole 5.6min/, and service life is up to 36 holes.
The diamond engineering thin wall drilling bit that embodiment 1.3 obtains, sample specification are as follows: φ 76-380, wherein cutter head height 10mm, cutter head is with a thickness of 3.6mm.It is obtained using test drilling block (standard c40 cement, thickness 240mm, 4 32mm reinforcing bars) Diamond engineering thin-walled drill is tested, and drilling speed can reach the hole 5.2min/, and service life is up to 33 holes.
The diamond engineering thin wall drilling bit that embodiment 1.4 obtains, sample specification are as follows: φ 76-380, wherein cutter head height 10mm, cutter head is with a thickness of 3.6mm.It is obtained using test drilling block (standard c40 cement, thickness 240mm, 4 32mm reinforcing bars) Diamond engineering thin-walled drill is tested, and drilling speed can reach the hole 5min/, and service life is up to 31 holes.
Comparative example one
This comparative example is related to influence of the cubic boron nitride to diamond engineering thin-walled drill.
One diamond engineering thin-walled drill, raw material components include metal powder 1000g (i.e. FeCu30 prealloy powder 370g, CuSn15 prealloy powder 300g, am1 metal powder 80g, cobalt powder 250g), diamond 250ct;By the diamond in raw material components It after first being wrapped up, remixes by the metal powder of prealloy powder compounding preparation, then successively carries out mixture, cold pressing compacting, burns Knot and post-processing.
The above-mentioned diamond engineering thin-walled drill being prepared is tested for the property, sample specification are as follows: φ 76-380, wherein Cutter head height 10mm, cutter head is with a thickness of 3.6mm.It is right using test drilling block (standard c40 cement, thickness 240mm, 4 32mm reinforcing bars) Its obtained diamond engineering thin-walled drill is tested, and drilling speed can reach the hole 10min/, and service life is up to 25 holes.
Comparative example two
This comparative example is related to influence of the metal powder to diamond engineering thin-walled drill.
One diamond engineering thin-walled drill, raw material components include metal powder 1000g (i.e. Fe powder 280g, Cu powder 300g, Sn Powder 90g, cobalt powder 250g, am1 metal powder 80g), cubic boron nitride 40ct, diamond 210ct;By cube in raw material components Boron nitride and diamond first carry out cladding processing, remix the metal powder prepared by common metal powder, are then successively mixed Match, be cold-pressed compacting, sintering and post-processing.
The above-mentioned diamond engineering thin-walled drill being prepared is tested for the property, sample specification are as follows: φ 76-380, wherein Cutter head height 10mm, cutter head is with a thickness of 3.6mm.It is right using test drilling block (standard c40 cement, thickness 240mm, 4 32mm reinforcing bars) Its obtained diamond engineering thin-walled drill is tested, and drilling speed can reach the hole 8.9min/, and service life is up to 27 holes.
Comparative example three
This comparative example is related to influence of the cladding process to diamond engineering thin-walled drill.
One diamond engineering thin-walled drill, raw material components include metal powder 1000g (i.e. FeCu30 prealloy powder 370g, CuSn15 prealloy powder 300g, am1 metal powder 80g, cobalt powder 250g), cubic boron nitride 40ct, diamond 210ct;By raw material Diamond and cubic boron nitride in component first carry out mixture, remix by the metal powder of prealloy powder compounding preparation, then Successively carry out mixture, cold pressing compacting, sintering and post-processing.
The above-mentioned diamond engineering thin-walled drill being prepared is tested for the property, sample specification are as follows: φ 76-380, wherein Cutter head height 10mm, cutter head is with a thickness of 3.6mm.It is right using test drilling block (standard c40 cement, thickness 240mm, 4 32mm reinforcing bars) Its obtained diamond engineering thin-walled drill is tested, and drilling speed can reach the hole 13min/, and service life is up to 20 holes.
In conclusion diamond engineering thin wall drilling bit of the invention, in terms of raw material components and cladding process two simultaneously into Row optimization, makes the diamond engineering thin-walled drill obtained have the performance advantages such as extremely excellent toughness, thermal stability, wearability, To improve the service life of diamond engineering thin-walled drill, production cost is reduced, and improve diamond engineering thin-walled drill Drilling speed.

Claims (10)

1. a kind of diamond engineering thin-walled drill for adding cubic boron nitride, which is characterized in that including following mass parts raw material components:
92~98 parts of metal powder;
1.5~4.5 parts of diamond;
0.5~3.5 part of cubic boron nitride;
Wherein, metal powder includes following mass parts raw material components per hundred parts:
The addition of the cubic boron nitride, which is taken, is first wrapped up diamond and cubic boron nitride with covering, then with metal powder The mode of last mixture, the cladding process the following steps are included:
A1, it obtains covering: taking 1.5~3.0 parts of granulating agent ws-180,25~30 parts of cobalt powder, 32~38 parts of isopropanol, acetone It 32~45 parts, is stirred evenly under the conditions of 50~70 DEG C of temperature, obtains covering;
A2, gluing, pre-coated and drying and processing: by the diamond cleaned up and cubic boron nitride grinding human bone ash, so Gluing is mixed and carried out with covering made from step a1 afterwards, material is then added in cobalt powder after gluing processing and is wrapped in advance It covers, obtains cobalt powder and coat 10~50 μm of thickness, then dry;
The painting jelly that the gluing processing uses is granulating agent ws-180;
A3, cladding and reduction treatment: the pre-coated material after drying is coated again with covering in coating machine, is wrapped Cover 100~500 μm of thickness, finally by after cladding diamond and cubic boron nitride carry out reduction treatment.
2. the diamond engineering thin-walled drill of addition cubic boron nitride according to claim 1, it is characterised in that: the metal The granularity of powder is 100~400 mesh, and the granularity of the diamond is 25~70 mesh, the granularity of the cubic boron nitride is 25~ 70 mesh.
3. the diamond engineering thin-walled drill of addition cubic boron nitride according to claim 2, it is characterised in that: described FeCu30 prealloy powder, CuSn15 prealloy powder, am1 alloy powder, the granularity of cobalt powder are 100~400 mesh.
4. the diamond engineering thin-walled drill of addition cubic boron nitride according to claim 1, it is characterised in that: the cladding The speed of agitator for preparing of agent is 150~350 turns/min.
5. the diamond engineering thin-walled drill of addition cubic boron nitride according to claim 1, it is characterised in that: the reduction Treatment conditions are that under an atmosphere of hydrogen, reduction temperature is 800~900 DEG C.
6. a kind of preparation process of the diamond engineering thin-walled drill of addition cubic boron nitride as described in claim 1, feature It is: the following steps are included:
A, coat: cladding process according to claim 1 prepares the package compound material of diamond and cubic boron nitride;
B, mixture: the package compound material of step a is mixed with metal powder, the wetting agent of 0.3~2g/kg is added, in mixing It is formed in machine and blendes together material;
C, cold pressing compacting, sintering: will blend together in material investment cold stamping die, obtains cold pressing green compact through cold pressing compacting, places into sintering It is sintered to obtain cutter head prefabrication in equipment;
D, it post-processes: will be welded on drilling rod after the processing of cutter head prefabrication, obtain diamond engineering thin-walled drill.
7. the preparation process of the diamond engineering thin-walled drill of addition cubic boron nitride according to claim 6, feature exist In: every hundred mass parts of wetting agent include 39~45 parts of glycerol, 7~12 parts of zinc stearate, remaining be isopropanol.
8. the preparation process of the diamond engineering thin-walled drill of addition cubic boron nitride according to claim 6, feature exist In: batch mixer described in step b uses three-dimensional material mixer, and the mixing condition is in room temperature, relative humidity 30% hereinafter, when mixing Between 1~3h.
9. the preparation process of the diamond engineering thin-walled drill of addition cubic boron nitride according to claim 6, feature exist In: cold pressing pressing conditions described in step c is in pressing pressure is risen to 5t/cm by normal pressure in the 2s time in cold stamping die2's Pressure.
10. the preparation process of the diamond engineering thin-walled drill of addition cubic boron nitride according to claim 6, feature exist In: sintering condition described in step c is then to maintain this temperature in temperature is risen to 820~950 DEG C in the 5min time in hot press 10min is spent, room temperature is subsequently reduced to.
CN201910635953.8A 2019-07-15 2019-07-15 Diamond engineering thin-wall drill added with cubic boron nitride and preparation process thereof Active CN110280756B (en)

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