CN110279618A - A kind of preparation method of the oleogel of immobilized Co-Q10 - Google Patents
A kind of preparation method of the oleogel of immobilized Co-Q10 Download PDFInfo
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- CN110279618A CN110279618A CN201910747494.2A CN201910747494A CN110279618A CN 110279618 A CN110279618 A CN 110279618A CN 201910747494 A CN201910747494 A CN 201910747494A CN 110279618 A CN110279618 A CN 110279618A
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- oleogel
- immobilized
- preparation
- sunflower oil
- added
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- ACTIUHUUMQJHFO-UPTCCGCDSA-N coenzyme Q10 Chemical compound COC1=C(OC)C(=O)C(C\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CCC=C(C)C)=C(C)C1=O ACTIUHUUMQJHFO-UPTCCGCDSA-N 0.000 title claims abstract description 56
- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- 235000019486 Sunflower oil Nutrition 0.000 claims abstract description 20
- 239000002600 sunflower oil Substances 0.000 claims abstract description 20
- -1 stearic acid ethylene glycol ester Chemical class 0.000 claims abstract description 19
- 239000000203 mixture Substances 0.000 claims abstract description 9
- 238000003756 stirring Methods 0.000 claims abstract description 8
- 238000010438 heat treatment Methods 0.000 claims abstract description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 8
- 239000003349 gelling agent Substances 0.000 abstract description 8
- 239000004519 grease Substances 0.000 abstract description 7
- 230000000694 effects Effects 0.000 abstract description 5
- 239000003795 chemical substances by application Substances 0.000 abstract description 3
- 239000002537 cosmetic Substances 0.000 description 8
- 239000000499 gel Substances 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- 235000019198 oils Nutrition 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000007767 bonding agent Substances 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 239000003995 emulsifying agent Substances 0.000 description 2
- 235000013376 functional food Nutrition 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 238000001338 self-assembly Methods 0.000 description 2
- 239000002453 shampoo Substances 0.000 description 2
- 235000020238 sunflower seed Nutrition 0.000 description 2
- 235000015112 vegetable and seed oil Nutrition 0.000 description 2
- 230000002407 ATP formation Effects 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 235000019483 Peanut oil Nutrition 0.000 description 1
- 235000019484 Rapeseed oil Nutrition 0.000 description 1
- 239000012190 activator Substances 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
- 235000019438 castor oil Nutrition 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- 230000019522 cellular metabolic process Effects 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 235000019441 ethanol Nutrition 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
- 239000000017 hydrogel Substances 0.000 description 1
- 239000000944 linseed oil Substances 0.000 description 1
- 235000021388 linseed oil Nutrition 0.000 description 1
- 210000003470 mitochondria Anatomy 0.000 description 1
- 210000001700 mitochondrial membrane Anatomy 0.000 description 1
- 239000000312 peanut oil Substances 0.000 description 1
- 150000004053 quinones Chemical class 0.000 description 1
- 239000008159 sesame oil Substances 0.000 description 1
- 235000011803 sesame oil Nutrition 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000003549 soybean oil Substances 0.000 description 1
- 235000012424 soybean oil Nutrition 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 235000019871 vegetable fat Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/042—Gels
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
- A61K8/355—Quinones
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Emergency Medicine (AREA)
- Mycology (AREA)
- Nutrition Science (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Dispersion Chemistry (AREA)
- Dermatology (AREA)
- Fats And Perfumes (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of preparation methods of the oleogel of immobilized Co-Q10, it is under conditions of room temperature, being protected from light, the Co-Q10 that the 0.5-5% of sunflower oil quality will be accounted for is added in sunflower oil, Co-Q10 is dissolved in sunflower oil by the stirring of 100-500rpm, the gelling agent stearic acid ethylene glycol ester for accounting for the 2-10% of sunflower oil quality is then added, first in 60-90 DEG C of heating 0.5-1h, 4-25 DEG C is cooled to again with the rate of 1-10 DEG C/min, mixture is stood into 12-24h, obtains a kind of oleogel of immobilized Co-Q10.At low cost using stearic acid ethylene glycol ester as gelling agent, dosage is few, effect is good, and has no publication, extends the selection of grease gel agent, with the oleogel of the immobilized Co-Q10 of technical solution disclosed by the invention preparation, the storage stability and bioavilability of Co-Q10 are improved.
Description
Technical field
The present invention relates to functional foods and cosmetics preparation field, and in particular to a kind of oleogel of immobilized Co-Q10
Preparation method.
Background technique
Co-Q10 is a kind of natural fat-soluble quinones, is distributed mainly in the mitochondria of biological cell, is line
A kind of important electron transit mediator, antioxidant and cell metabolism activator on mitochondrial membrane, the transmitting for internal signal
Play a significant role with ATP synthesis, therefore it all has biggish answer in medicine, cosmetic field and field of functional food
Use potentiality.
Co-Q10 is soluble in organic solvent, is slightly soluble in ethyl alcohol, not soluble in water and methanol, although there is application in terms of drug,
But be difficult to add and apply in various foods and cosmetics, therefore, how Co-Q10 to be effectively added to food and change
In cosmetic and improve the hot spot that its bioavilability is current research.
Currently, stearic acid ethylene glycol ester is mainly used for assigning the pearly-lustres colors such as shampoo, bath foam, while head can also be made
Conditioner is sent out, pearly-lustre color is improved stearic as obtained from controlling its crystallization degree and crystalline state in shampoo
The crystalline condition of sour ethylene glycol ester is that original very thin flat crystal becomes relatively large platelet, can enhance pearl effect,
In addition, stearic acid ethylene glycol ester can be used as emulsifier, dispersing agent, solubilizer in cosmetics, plays emulsification, solubilising, resists
The effect of electrostatic.
Application No. is the patents of invention of CN201610001647.5 to disclose a kind of pair based on organogel and hydrogel
The preparation of gel cosmetic products.The technical solution is that organic gel agent, vegetable oil, Co-Q10 are mixed with oily phase, reuses water
Gelling agent, glycerol, emulsifier prepare water phase, and uniform miscella phase, water phase obtain double gel cosmetic products.But its gel for providing
The dosage of bonding agent is larger, higher cost, and effect is not outstanding.
Therefore, it is necessary to find a kind of preparation method of the oleogel of efficient, low cost immobilized Co-Q10.
Summary of the invention
In order to achieve the purpose that for Co-Q10 to be added in foods and cosmetics and improve its bioavilability, one is found out
The kind gel bonding agent that dosage is few, effect is good, The present invention gives a kind of preparation methods of the oleogel of immobilized Co-Q10.
A kind of preparation method of the oleogel of immobilized Co-Q10 includes the following steps:
S1: Co-Q10 is added in sunflower oil, is dissolved in Co-Q10 in sunflower oil by stirring；
S2: it is rear to cool down to, dissolved with stearic acid ethylene glycol ester is added in the sunflower oil of Co-Q10, first being heated obtained in S1,
Mixture is stood, the oleogel of immobilized Co-Q10 is obtained.
Further, under conditions of room temperature, being protected from light, the operation that Co-Q10 is added to sunflower oil is carried out.
Further, it is dissolved in Co-Q10 in sunflower oil with the stirring rate of 100-500rpm.
Further, the addition quality of Co-Q10 accounts for the 0.5-5% of sunflower oil quality.
Further, the quality of the stearic acid ethylene glycol ester of addition is the 2%-10% of sunflower oil quality.
Further, after stearic acid ethylene glycol ester being added, under conditions of 60-90 DEG C, to the heating duration of mixture
For 0.5-1.5h.
Further, after the mixture of addition stearic acid ethylene glycol ester is heated, rate of temperature fall is 1-10 DEG C/min, drop
Temperature is to 4-25 DEG C.
Further, be cooled to 4-25 DEG C mixture it is quiet should set 12-24h, obtain a kind of oleogel of immobilized Co-Q10
Preparation method.
Since oleogel is usually using gelling agent to be self-assembly of a three-dimensional network to fix grease, grease gel pair
Active constituent contained by it has protection and slow releasing function, and therefore, Co-Q10 is directly dissolved in edible sunflower oil by the present invention
In, three-dimensional network is self-assembly of as gelling agent using stearic acid ethylene glycol ester and is solidified, the oil for preparing immobilized Co-Q10 is solidifying
Glue.
In addition, being soluble in many vegetable fat since Co-Q10 is soluble in organic solvent, therefore, certain herbaceous plants with big flowers not only can be used
Flower seed oil dissolves Co-Q10, and such as soybean oil, sesame oil, peanut oil, castor oil, linseed oil, rapeseed oil can also be used to dissolve
Co-Q10, and be gelling agent using stearic acid ethylene glycol ester, the oleogel of immobilized Co-Q10 is made.
Compared with prior art, the invention has the following beneficial effects:
1. the present invention prepares the oleogel of immobilized Co-Q10 using stearic acid ethylene glycol ester as gelling agent, gelling agent dosage is few,
Gel process is simple, at low cost, and has no publication, extends the selection of grease gel agent.
2. improving the storage of Co-Q10 with the oleogel of the immobilized Co-Q10 of technical solution disclosed by the invention preparation
Stability and bioavilability.
Specific embodiment
Combined with specific embodiments below, explanation is further explained to the present invention.But embodiment is only to the present invention
Explanation, rather than be to be defined.
Embodiment 1
0.45 g Co-Q10 is accurately weighed, lower 100 rpm stirring is protected from light in room temperature, Co-Q10 is made to be completely dissolved in 90 g sunflower seeds
In oil, 1.8g stearic acid ethylene glycol ester is then added into grease, 0.5 h is heated under conditions of 60 DEG C, then with 1
DEG C/cooling rate of min is cooled to 4 DEG C, constant temperature stands 12 h, and the oleogel of immobilized Co-Q10 can be obtained.
Embodiment 2
2.85 g Co-Q10s are accurately weighed, lower 250 rpm stirring is protected from light in room temperature, Co-Q10 is made to be completely dissolved in 95 g sunflower seeds
In oil, then into grease add 5.7g stearic acid ethylene glycol ester, heat 1 h under conditions of 75 DEG C, then with 6 DEG C/
The cooling rate of min is cooled to 15 DEG C, and constant temperature stands 18h, and the oleogel of immobilized Co-Q10 can be obtained.
Embodiment 3
5 g Co-Q10s are accurately weighed, lower 500 rpm stirring is protected from light in room temperature, Co-Q10 is made to be completely dissolved in 100 g sunflower oils
In, then into grease add 10g stearic acid ethylene glycol ester, heat 1.5 h under conditions of 90 DEG C, then with 10 DEG C/
The cooling rate of min is cooled to 25 DEG C, and the oleogel of immobilized Co-Q10 can be obtained in static 24 h of constant temperature.
Part not in the detailed description of the invention is the prior art.
Claims (8)
1. a kind of preparation method of the oleogel of immobilized Co-Q10, it is characterised in that: preparation method includes the following steps:
S1: Co-Q10 is added in sunflower oil, is dissolved in Co-Q10 in sunflower oil by stirring；
S2: it is rear to cool down to, dissolved with stearic acid ethylene glycol ester is added in the sunflower oil of Co-Q10, first being heated obtained in S1,
Mixture is stood, the oleogel of immobilized Co-Q10 is obtained.
2. a kind of preparation method of the oleogel of immobilized Co-Q10 as described in claim 1, it is characterised in that: in room temperature, keep away
Under conditions of light, the operation that Co-Q10 is added to sunflower oil is carried out.
3. a kind of preparation method of the oleogel of immobilized Co-Q10 as claimed in claim 2, it is characterised in that: with 100-
The stirring rate of 500rpm is dissolved in Co-Q10 in sunflower oil.
4. a kind of preparation method of the oleogel of immobilized Co-Q10 as described in claim 1, it is characterised in that: Co-Q10
The 0.5-5% that quality accounts for sunflower oil quality is added.
5. a kind of preparation method of the oleogel of immobilized Co-Q10 as claimed in claim 4, it is characterised in that: addition it is hard
The quality of resin acid ethylene glycol ester is the 2%-10% of sunflower oil quality.
6. a kind of preparation method of the oleogel of immobilized Co-Q10 as claimed in claim 5, it is characterised in that: be added stearic
After sour ethylene glycol ester, under conditions of 60-90 DEG C, a length of 0.5-1.5h when to the heating of mixture.
7. a kind of preparation method of the oleogel of immobilized Co-Q10 as described in claim 1, it is characterised in that: be added stearic
After the mixture of sour ethylene glycol ester is heated, rate of temperature fall is 1-10 DEG C/min, is cooled to 4-25 DEG C.
8. a kind of preparation method of the oleogel of immobilized Co-Q10 as claimed in claim 7, it is characterised in that: mixture is quiet
12-24h should be set.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910747494.2A CN110279618A (en) | 2019-08-14 | 2019-08-14 | A kind of preparation method of the oleogel of immobilized Co-Q10 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910747494.2A CN110279618A (en) | 2019-08-14 | 2019-08-14 | A kind of preparation method of the oleogel of immobilized Co-Q10 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110279618A true CN110279618A (en) | 2019-09-27 |
Family
ID=68025228
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910747494.2A Pending CN110279618A (en) | 2019-08-14 | 2019-08-14 | A kind of preparation method of the oleogel of immobilized Co-Q10 |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110279618A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114854469A (en) * | 2022-04-28 | 2022-08-05 | 西安工业大学 | Waste edible oleogel and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101732201A (en) * | 2009-12-31 | 2010-06-16 | 玉溪健坤生物药业有限公司 | Reduced coenzyme Q10 essence oil and preparation method thereof |
| CN103859395A (en) * | 2014-01-24 | 2014-06-18 | 天津科技大学 | Self-emulsifying drug release system of coenzyme Q10 with high absorptivity and preparation method and application thereof |
| CN103976901A (en) * | 2014-05-22 | 2014-08-13 | 东南大学 | Coenzyme Q10 and tea polyphenol loaded micro-nano carrier, as well as preparation and application methods thereof |
| CN104855548A (en) * | 2015-05-25 | 2015-08-26 | 华南理工大学 | Preparation method of fat gel capable of loading carotene |
| CN106172898A (en) * | 2016-07-27 | 2016-12-07 | 安徽国香粮油有限公司 | A kind of Semen Allii Tuberosi gel oil with high immune effect and preparation method thereof |
| CN106937917A (en) * | 2016-01-05 | 2017-07-11 | 河南工业大学 | A kind of preparation of double gel cosmetic products based on organogel and hydrogel |
| CN109170890A (en) * | 2018-09-21 | 2019-01-11 | 河南科技学院 | A kind of method of immobilized Turmeric P.E |
| CN109588497A (en) * | 2018-12-26 | 2019-04-09 | 淮阴工学院 | A kind of antioxidant and edible oleogel and preparation method thereof |
-
2019
- 2019-08-14 CN CN201910747494.2A patent/CN110279618A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101732201A (en) * | 2009-12-31 | 2010-06-16 | 玉溪健坤生物药业有限公司 | Reduced coenzyme Q10 essence oil and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114854469A (en) * | 2022-04-28 | 2022-08-05 | 西安工业大学 | Waste edible oleogel and preparation method thereof |
| CN114854469B (en) * | 2022-04-28 | 2023-11-21 | 西安工业大学 | Abandoned edible oil gel and preparation method thereof |
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