CN110270212A - A kind of bactericidal deodorant and preparation method thereof - Google Patents
A kind of bactericidal deodorant and preparation method thereof Download PDFInfo
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- CN110270212A CN110270212A CN201810220697.1A CN201810220697A CN110270212A CN 110270212 A CN110270212 A CN 110270212A CN 201810220697 A CN201810220697 A CN 201810220697A CN 110270212 A CN110270212 A CN 110270212A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/77—Liquid phase processes
- B01D53/78—Liquid phase processes with gas-liquid contact
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2257/00—Components to be removed
- B01D2257/91—Bacteria; Microorganisms
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Environmental & Geological Engineering (AREA)
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- Dentistry (AREA)
- Plant Pathology (AREA)
- Pest Control & Pesticides (AREA)
- Inorganic Chemistry (AREA)
- Biomedical Technology (AREA)
- General Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Toxicology (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
The present invention relates to a kind of bactericidal deodorants and preparation method thereof, including following component: hypochloric acid water solution, disodium phosphate soln, sodium dihydrogen phosphate, sodium citrate solution；Wherein, the concentration of hypochloric acid water solution is 0.5~1.0mol/L；The concentration of disodium phosphate soln is 2.8-3.2mol/L；The concentration of sodium dihydrogen phosphate is 4.8-5.2mol/L, and sodium citrate solution concentration is 5.6-6.2mol/L；Hypochloric acid water solution, disodium phosphate soln, sodium dihydrogen phosphate, sodium citrate solution mass percent be 3-6:1-2:1-2:0.2-0.5.Bactericidal deodorant provided by the invention, it is efficient, inexpensive, nontoxic, harmless, without side-effects, without screening agent, noresidue, without secondary pollution.
Description
Technical field
The present invention relates to a kind of bactericidal deodorants and preparation method thereof, and in particular to a kind of efficient, inexpensive, nontoxic, nothing
It is harmful, without side-effects, without screening agent, noresidue, bactericidal deodorant without secondary pollution and preparation method thereof.
Background technique
In recent years, with urbanization, industrialized fast development, in garbage transfer station, slaughterhouse, farm, Industry Waste
A large amount of poisonous and hazardous foul gas are generated at sewage sludge accumulation, human survival and environment sustainable development may be caused seriously
It influences.General deodorizing methods has physical method, traditional chemical oxidizing process and bioanalysis.Physical method is easy to operate, but effect is poor；
Traditional chemical oxidizing process is high-efficient, still chemicals risk is larger and is harmful to the human body；Bioanalysis is high-efficient, but at
This height.A kind of cheap, efficient, easy to operate, non-toxic to humans deodorant becomes one of research hotspot.
In the present invention, a kind of efficient, cheap, easy behaviour is produced by production equipment by halite and pure water
Make, deodorant non-toxic to humans, and is widely used in garbage transfer station, slaughterhouse, farm and industrial wastewater sludge
At accumulation, good deodorizing effect is achieved.
Summary of the invention
In view of the above-mentioned problems, the main purpose of the present invention is to provide it is a kind of it is efficient, inexpensive, nontoxic, harmless, without secondary work
With, without screening agent, noresidue, bactericidal deodorant without secondary pollution and preparation method thereof.
The present invention is to solve above-mentioned technical problem by following technical proposals: a kind of bactericidal deodorant, the sterilization
Deodorant includes following component: hypochloric acid water solution, disodium phosphate soln, sodium dihydrogen phosphate, sodium citrate solution.
Wherein, the concentration of hypochloric acid water solution is 0.5~1.0mol/L；The concentration of disodium phosphate soln is 2.8-
3.2mol/L；The concentration of sodium dihydrogen phosphate is 4.8-5.2mol/L, and sodium citrate solution concentration is 5.6-6.2mol/L；It is secondary
Chloric acid aqueous solution, disodium phosphate soln, sodium dihydrogen phosphate, sodium citrate solution mass percent be 3-6:1-2:1-
2:0.2-0.5.
A kind of preparation method of bactericidal deodorant: the preparation method of the bactericidal deodorant includes the following steps:
(1), saturated sodium-chloride water solution and pure water pass through electrolysis under the conditions of 10-30 DEG C, relative humidity 50-80%rh
Equipment prepares the hypochloric acid water solution of 0.5~1.0mol/L, and the hypochlorite solution of preparation is placed in the 1# with glass lining and is stirred
It mixes in kettle；
(2), the disodium hydrogen phosphate that 2.8-3.2mol/L is prepared under the conditions of 10-30 DEG C, relative humidity 50-80%rh is molten
Liquid is placed in plastic containers；
(3), the sodium dihydrogen phosphate that 4.8-5.2mol/L is prepared under the conditions of 10-30 DEG C, relative humidity 50-80%rh is molten
Liquid is placed in plastic containers；
(4), the sodium citrate solution of 5.6-6.2mol/L is prepared under the conditions of 10-30 DEG C, relative humidity 50-80%rh,
It places in plastic containers；
(5), first three kinds of solution in step (2), (3), (4) are pumped into respectively in 2# stirred tank with vacuum pump, setting is stirred
It mixes 10-30 DEG C of temperature, mixing time 2-10 minutes, mixes them thoroughly uniformly, then by the solution vacuum pumping in step (1)
Into in 2# stirred tank, 10-30 DEG C of whipping temp is set, mixing time 5-15 minutes, is uniformly mixed it；
Hypochloric acid water solution, disodium phosphate soln, sodium dihydrogen phosphate, sodium citrate solution mass percent be
3-6:1-2:1-2:0.2-0.5.
In specific embodiments of the present invention, the preparation method of bactericidal deodorant includes the following steps:
(1), saturated sodium-chloride water solution and pure water prepare hypochloric acid water solution by electrolysis installation, by the 300- of preparation
The hypochlorite solution of 600mL, 0.7mol/L are placed in 1000mL beaker；
(2), the disodium phosphate soln 100-200mL of 3.0mol/L is weighed；
(3), the sodium dihydrogen phosphate 100-200mL of 5.0mol/L is weighed；
(4), the sodium citrate solution 20-50mL of 6.0mol/L is weighed；
(5), first three kinds of solution in step (2), (3), (4) after mixing, then with the solution in step (1) are mixed
Uniformly.
In specific embodiments of the present invention, the preparation method of the bactericidal deodorant includes the following steps:
(1), saturated sodium-chloride water solution and pure water prepare hypochloric acid water solution by electrolysis installation, by the 300- of preparation
The hypochlorite solution of 600mL, 0.5mol/L are placed in 1000mL beaker；
(2), the disodium phosphate soln 100-200mL of 2.8mol/L is weighed；
(3), the sodium dihydrogen phosphate 100-200mL of 4.8mol/L is weighed；
(4), the sodium citrate solution 20-50mL of 6.2mol/L is weighed；
(5), first three kinds of solution in step (2), (3), (4) after mixing, then with the solution in step (1) are mixed
Uniformly.
In specific embodiments of the present invention, the preparation method of the bactericidal deodorant includes the following steps:
(1), saturated sodium-chloride water solution and pure water prepare hypochloric acid water solution by electrolysis installation, by preparation
The hypochlorite solution of 100mL, 1.0mol/L are placed in 500mL beaker；
(2), the disodium phosphate soln 100-200mL of 3.2mol/L is weighed；
(3), the sodium dihydrogen phosphate 100-200mL of 5.2mol/L is weighed；
(4), the sodium citrate solution 20-50mL of 5.6mol/L is weighed；
(5), first three kinds of solution in step (2), (3), (4) after mixing, then with the solution in step (1) are mixed
Uniformly.
The positive effect of the present invention is that: bactericidal deodorant provided by the invention and preparation method thereof, deodorization and sterilization
Agent is efficient, it is inexpensive, nontoxic, harmless, without side-effects, without screening agent, noresidue, without secondary pollution.
Specific embodiment
Present pre-ferred embodiments are given below, in order to explain the technical scheme of the invention in detail.
Bactericidal deodorant provided by the invention, including following component: hypochloric acid water solution, disodium phosphate soln, phosphoric acid
Dihydro sodium solution, sodium citrate solution.
Wherein, the concentration of hypochloric acid water solution is 0.5~1.0mol/L；The concentration of disodium phosphate soln is 2.8-
3.2mol/L；The concentration of sodium dihydrogen phosphate is 4.8-5.2mol/L, and sodium citrate solution concentration is 5.6-6.2mol/L；It is secondary
Chloric acid aqueous solution, disodium phosphate soln, sodium dihydrogen phosphate, sodium citrate solution mass percent be 3-6:1-2:1-
2:0.2-0.5.
Stabilizer as pH value after disodium hydrogen phosphate of the present invention is mixed with sodium dihydrogen phosphate, so that pH value of solution is stablized
In 6.8-7.2, sodium citrate solution is used as stable and preservative, while also being had the function of to pH stable.
The preparation method of bactericidal deodorant includes the following steps:
(1), saturated sodium-chloride water solution and pure water pass through electrolysis under the conditions of 10-30 DEG C, relative humidity 50-80%rh
Equipment prepares the hypochloric acid water solution of 0.5~1.0mol/L, and the hypochlorite solution of preparation is placed in the 1# with glass lining and is stirred
It mixes in kettle；
(2), the disodium hydrogen phosphate that 2.8-3.2mol/L is prepared under the conditions of 10-30 DEG C, relative humidity 50-80%rh is molten
Liquid is placed in plastic containers；
(3), the sodium dihydrogen phosphate that 4.8-5.2mol/L is prepared under the conditions of 10-30 DEG C, relative humidity 50-80%rh is molten
Liquid is placed in plastic containers；
(4), the sodium citrate solution of 5.6-6.2mol/L is prepared under the conditions of 10-30 DEG C, relative humidity 50-80%rh,
It places in plastic containers；
(5), first three kinds of solution in step (2), (3), (4) are pumped into respectively in 2# stirred tank with vacuum pump, setting is stirred
It mixes 10-30 DEG C of temperature, mixing time 2-10 minutes, mixes them thoroughly uniformly, then by the solution vacuum pumping in step (1)
Into in 2# stirred tank, 10-30 DEG C of whipping temp is set, mixing time 5-15 minutes, is uniformly mixed it；
Hypochloric acid water solution, disodium phosphate soln, sodium dihydrogen phosphate, sodium citrate solution mass percent be
3-6:1-2:1-2:0.2-0.5.
Here is some specifically to prepare example:
Example 1:
The preparation method of bactericidal deodorant includes the following steps:
(1), saturated sodium-chloride water solution and pure water prepare hypochloric acid water solution by electrolysis installation, by the 300- of preparation
The hypochlorite solution of 600mL, 0.7mol/L are placed in 1000mL beaker；
(2), the disodium phosphate soln 100mL of 3.0mol/L is weighed；
(3), the sodium dihydrogen phosphate 100mL of 5.0mol/L is weighed；
(4), the sodium citrate solution 20mL of 6.0mol/L is weighed；
(5), first three kinds of solution in step (2), (3), (4) after mixing, then with the solution in step (1) are mixed
Uniformly.
Example 2:
The preparation method of bactericidal deodorant includes the following steps:
(1), saturated sodium-chloride water solution and pure water prepare hypochloric acid water solution by electrolysis installation, by the 300- of preparation
The hypochlorite solution of 600mL, 0.5mol/L are placed in 1000mL beaker；
(2), the disodium phosphate soln 150mL of 2.8mol/L is weighed；
(3), the sodium dihydrogen phosphate 200mL of 4.8mol/L is weighed；
(4), the sodium citrate solution 50mL of 6.2mol/L is weighed；
(5), first three kinds of solution in step (2), (3), (4) after mixing, then with the solution in step (1) are mixed
Uniformly.
Example 3:
The preparation method of bactericidal deodorant includes the following steps:
(1), saturated sodium-chloride water solution and pure water prepare hypochloric acid water solution by electrolysis installation, by preparation
The hypochlorite solution of 100mL, 1.0mol/L are placed in 500mL beaker；
(2), the disodium phosphate soln 200mL of 3.2mol/L is weighed；
(3), the sodium dihydrogen phosphate 180mL of 5.2mol/L is weighed；
(4), the sodium citrate solution 35mL of 5.6mol/L is weighed；
(5), first three kinds of solution in step (2), (3), (4) after mixing, then with the solution in step (1) are mixed
Uniformly.
Product main ingredient provided by the invention is neutrality hypochlorous acid (HClO), is that white blood cell kills bacterium production in human body
Raw substance.By its Strong oxdiative ability come decomposition smell source, it is nontoxic, harmless, without side-effects, without screening agent, noresidue, without two
Secondary pollution, safety and environmental protection.
Function: the stink as caused by hydrogen sulfide, mercaptan, thioether, ammonia nitrogen, trimethylamine etc. is quickly removed, while can be located
Process gases, liquid, solid tri-state pollutant.
Use scope: garbage transfer station, sludge stockyard, pulping and paper-making, sewage treatment, food processing.
Application method: this product is diluted 5-20 times with clean water, cooperates little Wu company high-pressure fog device, exists to foul smell
Space and source all standing.If stink or pollutant concentration are larger, dosage can be improved or improve concentration.
Points for attention: avoiding acutely shaking when transport as far as possible, and when storage is protected from light, forbids to be exposed to the sun.
Product characteristic: this product mainly becomes neutral hypochlorous acid (HClO), is that white blood cell killing is bacteriogenic in human body
Substance.By its extremely strong oxidability come decomposition smell source, compared with the general biological deodorant in market, when being reacted with source of odor
There is no absorption and the process decomposed, but directly quickly chemically react with it, quickly remove stink.
Advantage: efficient, inexpensive, nontoxic, harmless, without side-effects, without screening agent, noresidue, without secondary pollution.
Deodorizing device feature: automation control is saved artificial, guarantee continuous operation product provided by the invention and is quickly removed
The stink as caused by hydrogen sulfide, mercaptan, thioether, ammonia nitrogen, trimethylamine etc..
Present invention can be suitably applied to garbage loading embeading factory, sorting processing workshop, garbage power plant, the market of farm produce, garbage of residential areas bucket,
Kitchen, garbage transfer station, garbage transporting vehicle behind restaurant.
The application method of product provided by the invention: this product is diluted 5-20 times with clean water, cooperates little Wu company high pressure
Micro- mist device, to space existing for foul smell and source all standing.If stink or pollutant concentration are larger, dosage or raising can be improved
Concentration.
The ground such as garbage disposal, slaughterhouse, farm are used in, the growth for being not only able to deodorization, mosquito, fly can also being prevented.
Product line device in the present invention solves problem wide in variety, batch is small, syringe dosage is small, metering is unstable.
The present invention uses totally enclosed pipeline, and not only producing efficiency is high, but also does not pollute the environment.
Table 1 is the comparison (comparison of concentration of hydrogen sulfide) of using effect and product common at present of the invention:
As can be seen that effect is clearly using after product provided by the invention.
Table 2 is the comparison (comparison of ammonia concentration) of using effect and product common at present of the invention:
As can be seen that effect is clearly using after product provided by the invention.
Table 3 asks the sodium citrate solution being added in the application and the comparison without adding sodium citrate solution
As can be seen that stability greatly enhances after being added to sodium citrate solution.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention, the claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (5)
1. a kind of bactericidal deodorant, it is characterised in that: the bactericidal deodorant includes following component: hypochloric acid water solution, phosphoric acid
Disodium hydrogen solution, sodium dihydrogen phosphate, sodium citrate solution；
Wherein, the concentration of hypochloric acid water solution is 0.5~1.0mol/L；The concentration of disodium phosphate soln is 2.8-3.2mol/
L；The concentration of sodium dihydrogen phosphate is 4.8-5.2mol/L, and sodium citrate solution concentration is 5.6-6.2mol/L；Hypochloric acid water
Solution, disodium phosphate soln, sodium dihydrogen phosphate, sodium citrate solution mass percent be 3-6:1-2:1-2:0.2-
0.5。
2. a kind of preparation method of bactericidal deodorant: it is characterized by: the preparation method of the bactericidal deodorant includes following step
It is rapid:
(1), saturated sodium-chloride water solution and pure water pass through electrolysis installation under the conditions of 10-30 DEG C, relative humidity 50-80%rh
The hypochlorite solution of preparation, is placed in the 1# stirred tank with glass lining by the hypochloric acid water solution for preparing 0.5~1.0mol/L
In；
(2), the disodium phosphate soln that 2.8-3.2mol/L is prepared under the conditions of 10-30 DEG C, relative humidity 50-80%rh, puts
It sets in plastic containers；
(3), the sodium dihydrogen phosphate that 4.8-5.2mol/L is prepared under the conditions of 10-30 DEG C, relative humidity 50-80%rh, puts
It sets in plastic containers；
(4), the sodium citrate solution of 5.6-6.2mol/L is prepared under the conditions of 10-30 DEG C, relative humidity 50-80%rh, is placed
In plastic containers；
(5), first three kinds of solution in step (2), (3), (4) are pumped into respectively in 2# stirred tank with vacuum pump, setting stirring temperature
10-30 DEG C of degree mixing time 2-10 minutes, mixes them thoroughly uniformly, then the solution in step (1) is pumped into 2# with vacuum pump
In stirred tank, 10-30 DEG C of whipping temp is set, mixing time 5-15 minutes, is uniformly mixed it；
Hypochloric acid water solution, disodium phosphate soln, sodium dihydrogen phosphate, sodium citrate solution mass percent be 3-6:
1-2:1-2:0.2-0.5.
3. the preparation method of bactericidal deodorant according to claim 2, it is characterised in that: the preparation of the bactericidal deodorant
Method includes the following steps:
(1), saturated sodium-chloride water solution and pure water prepare hypochloric acid water solution by electrolysis installation, by the 300- of preparation
The hypochlorite solution of 600mL, 0.7mol/L are placed in 1000mL beaker；
(2), the disodium phosphate soln 100-200mL of 3.0mol/L is weighed；
(3), the sodium dihydrogen phosphate 100-200mL of 5.0mol/L is weighed；
(4), the sodium citrate solution 20-50mL of 6.0mol/L is weighed；
(5), first three kinds of solution in step (2), (3), (4) after mixing, then with the solution in step (1) are mixed
It is even.
4. the preparation method of bactericidal deodorant according to claim 2, it is characterised in that: the preparation of the bactericidal deodorant
Method includes the following steps:
(1), saturated sodium-chloride water solution and pure water prepare hypochloric acid water solution by electrolysis installation, by the 300- of preparation
The hypochlorite solution of 600mL, 0.5mol/L are placed in 1000mL beaker；
(2), the disodium phosphate soln 100-200mL of 2.8mol/L is weighed；
(3), the sodium dihydrogen phosphate 100-200mL of 4.8mol/L is weighed；
(4), the sodium citrate solution 20-50mL of 6.2mol/L is weighed；
(5), first three kinds of solution in step (2), (3), (4) after mixing, then with the solution in step (1) are mixed
It is even.
5. the preparation method of bactericidal deodorant according to claim 2, it is characterised in that: the preparation of the bactericidal deodorant
Method includes the following steps:
(1), saturated sodium-chloride water solution and pure water prepare hypochloric acid water solution by electrolysis installation, by the 100mL of preparation,
The hypochlorite solution of 1.0mol/L is placed in 500mL beaker；
(2), the disodium phosphate soln 100-200mL of 3.2mol/L is weighed；
(3), the sodium dihydrogen phosphate 100-200mL of 5.2mol/L is weighed；
(4), the sodium citrate solution 20-50mL of 5.6mol/L is weighed；
(5), first three kinds of solution in step (2), (3), (4) after mixing, then with the solution in step (1) are mixed
It is even.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810220697.1A CN110270212A (en) | 2018-03-16 | 2018-03-16 | A kind of bactericidal deodorant and preparation method thereof |
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| CN201810220697.1A CN110270212A (en) | 2018-03-16 | 2018-03-16 | A kind of bactericidal deodorant and preparation method thereof |
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| CN110270212A true CN110270212A (en) | 2019-09-24 |
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ID=67957865
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112042667A (en) * | 2020-08-21 | 2020-12-08 | 山东知能环保科技有限公司 | Stable hypochlorous acid disinfectant and preparation method thereof |
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| JP2002360689A (en) * | 2001-06-13 | 2002-12-17 | Clean Chemical Kk | Cleaning method of artificial dialyzer |
| CN103314996A (en) * | 2006-08-28 | 2013-09-25 | 本部三庆株式会社 | Process for producing aqueous chlorous acid solution for use as bactericide |
| CN102480972A (en) * | 2009-06-15 | 2012-05-30 | 奥古露丝创新科学公司 | Solution Containing Hypochlorous Acid And Methods Of Using Same |
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| CN112042667A (en) * | 2020-08-21 | 2020-12-08 | 山东知能环保科技有限公司 | Stable hypochlorous acid disinfectant and preparation method thereof |
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