CN110251714A - A kind of water solubility solid-state fragrant product and preparation method thereof - Google Patents
A kind of water solubility solid-state fragrant product and preparation method thereof Download PDFInfo
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- CN110251714A CN110251714A CN201910606604.3A CN201910606604A CN110251714A CN 110251714 A CN110251714 A CN 110251714A CN 201910606604 A CN201910606604 A CN 201910606604A CN 110251714 A CN110251714 A CN 110251714A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/012—Deodorant compositions characterised by being in a special form, e.g. gels, emulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/14—Disinfection, sterilisation or deodorisation of air using sprayed or atomised substances including air-liquid contact processes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
- A61L2209/20—Method-related aspects
- A61L2209/21—Use of chemical compounds for treating air or the like
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Abstract
The present invention relates to a kind of water-soluble solid-state fragrant products and preparation method thereof, belong to daily-use chemical industry technical field；Water-soluble solid-state fragrant product of the invention includes the raw material components of following parts by weight: 10~20 parts of fragrance, sour 20~40 parts of agent, 5~20 parts of sodium bicarbonate, 20~50 parts of lactose, 1~5 part of mannitol, 1~5 part of PEG, the fragrance are essence or essential oil；Water-soluble solid-state fragrant product fragrance bearing capacity of the invention is high, easy to use, effect is good, uses the water-soluble solid-state fragrant product of of long duration, convenient transportation and safety.
Description
Technical field
The invention belongs to daily-use chemical industry technical fields, are related to a kind of preparation method of solid-state champignon ball.
Background technique
Rattan champignon is the articles with fresh air and furniture daily necessities of the country such as America and Europe, Japan and Korea S environmental protection all the fashion,
Champignon liquid finished product is diffused into air by certain carrier (such as rattan, the showy flowers of herbaceous plants, cotton cord) in fact.Air is set to diffuse virtue
Perfume (or spice), reaching improves air, pleasant mental and body and other effects.China is always the main processing base of global rattan champignon, most early in number
Just there is Hong Kong client to process champignon product in continent before 10 years.It is in addition modern as modern increasingly payes attention to quality of the life
Rhythm of life is getting faster, and people's lives are more nervous, increased pressure, and champignon product, which has, mitigates operating pressure, conversion mood
The effect of, help to improve thought concentrated force and working efficiency.Thus champignon product using more and more.However traditional champignon
Volatilization liquid is by natural essential oil or artificial essential oil by obtaining after dilution dilution agent, and diluent uses the organic solvents such as alcohol more,
It is inconvenient to carry such as to board a plane due to being liquid, and the organic solvent diluting agent used some with combustible nature, using
There is also security risks in transportational process.
Also there is solid scent product currently on the market, but be usually directly to use in solid form, there are no be directed to rattan
The solid-state fragrant product of champignon, this is for being a kind of sorry for getting used to the people of rattan champignon.Meanwhile existing solid
Fragrant product fragrance bearing capacity is often lower, influences using effect and long-lasting use property, and the use of a large amount of auxiliary materials is also a kind of money
Source waste.It is fragrant to substitute traditional liquid it is therefore desirable to develop a kind of fragrant product that conveniently, safely transports, can persistently use
Smoke product.
Summary of the invention
The purpose of the present invention is in view of the above-mentioned problems existing in the prior art, proposing, a kind of fragrance bearing capacity is high, uses
Facilitate, effect is good, water-soluble solid-state fragrant product using of long duration, convenient transportation and safety.
A kind of water solubility solid-state fragrant product, the water solubility solid-state fragrant product include the raw material group of following parts by weight
Point:
10~20 parts of fragrance,
20~40 parts of sour agent,
5~20 parts of sodium bicarbonate,
20~50 parts of lactose,
1~5 part of mannitol,
1~5 part of PEG,
The fragrance is essence or essential oil.
According to the champignon of rattan champignon in the prior art volatilization liquid, not portable, transport has asking for security risk to the present invention
Topic, addition auxiliary material is made water-soluble solid-state fragrant product in the raw material essence or essential oil of champignon volatilization liquid, very convenient carrying,
And soluble easily in water, the uses such as rattan can be added i.e. according to the application method of traditional rattan champignon when in use by being dissolved in water
Can, not dangerous organic solvent substantially increases the safety in utilization of fragrant product.
But solid-state fragrant product has that fragrance bearing capacity is not high, and generally only 3~5% or so, lead to fragrance
It is thin, influence using effect.The present invention passes through the raw material components of reasonable compatibility water solubility solid-state fragrant product, so that fragrant in product
Smart bearing capacity can reach 10~20%, substantially increase the using effect of solid-state fragrant product, extends using the time, also reduces
Transport pressure；And sticking problem will not occur during the preparation process.
The present invention joined sour agent, sodium bicarbonate in solid-state fragrant product, can when solid-state fragrant product is dissolved in water
Bubble is generated, product is quickly dissolved and is dispersed in water；The PEG being added in the present invention can effectively increase essence or essence
The solubility of oil in water, to improve the concentration and persistence of fragrance.
Preferably, the acid agent includes citric acid, malic acid, fumaric acid or tartaric acid.
Preferably, the fragrance is esters essence or/and essential oil containing hydrophobic grouping.
Preferably, the esters essence or essential oil containing hydrophobic grouping includes lavender oil, rosemary oil, spearmint
Oil, sage clary oil, basil, orange oil, tea oil, sage oil, geranium oil, peppermint oil, Java Cananga Oil, lemon oil, jasmine oil,
Attar of rose, Rome oil of chamomile, sandalwood oil, neroli oil, cypress oil, frankincense oil, carrot seed oil, deodar essential oil or Patchouli
Oil.
Part material component (sour agent, sodium bicarbonate) of the invention meets water and can react, and causes fragrant product of the present invention
It deliquesces, the present invention, which uses, has esters essence or essential oil containing hydrophobic grouping, can effectively control fragrant product to environment
The sucking of middle moisture, thus the persistence that guarantees properties of product, but also can tart up.
Preferably, the water solubility solid-state fragrant product includes the raw material components of following parts by weight:
Fragrance 20%,
Sour agent 22.5%,
Sodium bicarbonate 17.5%,
Lactose 35%,
Mannitol 2%,
PEG-6000 3%.
The present invention by the further preferred of fragrant product raw material components, by the bearing capacity of essence or essential oil improve to
20%, effectively increase the using effect and long-lasting use property of product.
Preferably, the raw material components of the water solubility solid-state fragrant product further include for the poly- of 0.3~0.8 parts by weight
Tie up ketone-ethanol solution.
Preferably, the weight percent of povidone is 3~7% in the povidone-ethanol solution.
The present invention adds a small amount of povidone-ethanol solution in water-soluble solid-state fragrant product can significantly improve product
Adhesive property, improve the compressibility of product, assign the higher hardness of product and preferable appearance property.
Preferably, the PEG includes PEG-800, PEG-1000, PEG-1500, PEG-2000, PEG-4000, PEG-
6000 or PEG-8000.
Preferably, it is 100~200 mesh powders that the sour agent and sodium bicarbonate in the raw material components, which are particle size range,
Shape solid.
The present invention significantly improves the operability of compression moulding by limiting the particle size range of sour agent and sodium bicarbonate, acid
Compression moulding is not easy when agent and excessive sodium bicarbonate partial size.
Another object of the present invention is to provide a kind of preparation method of water-soluble solid-state fragrant product, the preparation methods
The following steps are included:
Prepare raw material components in proportion, after sour agent, sodium bicarbonate, lactose and mannitol are mixed in proportion, fragrance be added,
It mixes, is eventually adding PEG, is then pressed into type, drying, packaging.
Preferably, the preparation method further includes the steps that povidone-ethanol solution is added after fragrance is added.
Preferably, each step in the preparation method is in addition to drying steps 15~30 DEG C of temperature, 30~50%
It is carried out under conditions of humidity, constant temperature and humidity.
The present invention guarantees that fragrant product is producing by controlling the conditions such as temperature, humidity in fragrant product production process
Deliquescence phenomenon will not be generated in the process, guarantee product quality.And in finally addition fragrance, to prevent fragrance emission.The present invention is raw
Otherwise humidity during production can occur acid-base neutralization reaction and deliquescence, make product failure not above 50%.
Preferably, the drying is to dry 10~14h at a temperature of 50~55 DEG C.
Preferably, the acid agent and sodium bicarbonate are first ground into powdery, and screening of sifting out, 100~200 mesh partial sizes are taken
The pulverulent solids acid agent of range and sodium bicarbonate use.
Preferably, described be packaged as shrink-packaging, so as to moisture-proof.
Compared with prior art, the invention has the following advantages:
1, fragrance bearing capacity is high, reduces the usage amount of auxiliary material, has saved cost, aromatic flavour is lasting, and using effect is good；
2, water-soluble and solute effect is good, solution rate is fast, can be used as existing solvent borne rattan champignon liquid after molten water
Substitute also can be used as spray product use, safe to use；
3, small in size, solid forms convenient transportation and carrying, there is no Transport Safety problems and certain occasions to be refused
The problem of carrying absolutely
Specific embodiment
The following is specific embodiments of the present invention, and technical scheme of the present invention will be further described, but the present invention is simultaneously
It is not limited to these embodiments.
Embodiment 1
Citric acid and sodium bicarbonate are first first ground into powdery, and screening of sifting out, take 100~200 mesh particle size ranges
The agent of pulverulent solids acid and sodium bicarbonate use, then by weight, by 22.5 parts of citric acids, 17.5 parts of sodium bicarbonates, 35
After part lactose and 2 parts of mannitol mixing, 20 parts of essential oils are added, mix, are eventually adding 3 parts of PEG-6000, mixing is placed on mold
Middle compression moulding, drying, shrink-packaging.
Wherein, 20 parts of essential oils include 5 parts of lavender oils and 15 parts of spearmint oils；Above steps exists in addition to drying steps
22 DEG C of temperature, 40% humidity constant temperature and humidity under the conditions of carry out, it is dry to dry 12h at a temperature of 52 DEG C.
Embodiment 2
Citric acid and sodium bicarbonate are first first ground into powdery, and screening of sifting out, take 100~200 mesh particle size ranges
The agent of pulverulent solids acid and sodium bicarbonate use, then by weight, by 25 parts of citric acids, 20 parts of sodium bicarbonates, 33 parts of creams
After sugar and 4 parts of mannitol mixing, 13 parts of essential oils are added, mix, are eventually adding 5 parts of PEG-6000, mixing, which is placed in mold, presses
Type, drying, shrink-packaging is made.
It wherein, include 3 parts of orange oils and 10 parts of attars of rose in 13 parts of essential oils；Above steps is in addition to drying steps 26
DEG C temperature, 43% humidity constant temperature and humidity under the conditions of carry out, it is dry to dry 12h at a temperature of 53 DEG C.
Embodiment 3
Citric acid and sodium bicarbonate are first first ground into powdery, and screening of sifting out, take 100~200 mesh particle size ranges
The agent of pulverulent solids acid and sodium bicarbonate use, then by weight, by 21 parts of citric acids, 17 parts of sodium bicarbonates, 40 parts of creams
After sugar and 3 parts of mannitol mixing, 16 parts of essential oils are added, mix, are eventually adding 3 parts of PEG-6000, mixing, which is placed in mold, presses
Type, drying, shrink-packaging is made.
It wherein, include 15 parts of orange oils and 1 part of tea oil in 16 parts of essential oils；Above steps is in addition to drying steps 21
DEG C temperature, 35% humidity constant temperature and humidity under the conditions of carry out, it is dry to dry 13h at a temperature of 51 DEG C.
Embodiment 4
Malic acid and sodium bicarbonate are first first ground into powdery, and screening of sifting out, take 100~200 mesh particle size ranges
The agent of pulverulent solids acid and sodium bicarbonate use, then by weight, by 20 parts of malic acid, 16 parts of sodium bicarbonates, 39 parts of creams
After sugar and 5 parts of mannitol mixing, 12 parts of fragrance are added, mix, are eventually adding 3 parts of PEG-2000, mixing, which is placed in mold, presses
Type, drying, shrink-packaging is made.
It wherein, include 1 part of sandalwood oil and 11 parts of Java Cananga Oils in 12 parts of fragrance；Above steps is in addition to drying steps 15
DEG C temperature, 30% humidity constant temperature and humidity under the conditions of carry out, it is dry to dry 14h at 50 °C.
Embodiment 5
Tartaric acid and sodium bicarbonate are first first ground into powdery, and screening of sifting out, take 100~200 mesh particle size ranges
The agent of pulverulent solids acid and sodium bicarbonate use, then by weight, by 28 parts of tartaric acid, 20 parts of sodium bicarbonates, 30 parts of creams
After sugar and 3 parts of mannitol mixing, 17 parts of fragrance are added, mix, are eventually adding 2 parts of PEG-6000, mixing, which is placed in mold, presses
Type, drying, shrink-packaging is made.
It wherein, include 15 parts of attars of rose and 2 parts of deodar essential oils in 17 parts of fragrance；Above steps exists in addition to drying steps
30 DEG C of temperature, 50% humidity constant temperature and humidity under the conditions of carry out, it is dry to dry 10h at a temperature of 55 DEG C.
Embodiment 6
Being distinguished as after adding essential oil for the present embodiment and embodiment 1 is also molten added with 0.3 parts by weight povidone-ethyl alcohol
Liquid, the weight percent of povidone is 7% in povidone-ethanol solution, other are same as Example 1.
Embodiment 7
Being distinguished as after adding essential oil for the present embodiment and embodiment 1 is also molten added with 0.6 parts by weight povidone-ethyl alcohol
Liquid, the weight percent of povidone is 5% in povidone-ethanol solution, other are same as Example 1.
Comparative example 1
Lactose is replaced with equivalent sucrose, other are same as Example 1.
Comparative example 2
Lactose is replaced with equivalent soluble starch, other are same as Example 1.
Comparative example 3
Citric acid and sodium bicarbonate are ground to thicker partial size, select particle size range for the lemon of 30~50 mesh after sieving
Acid and sodium bicarbonate use.
In the alternative of other embodiment and above-described embodiment of the invention, sour agent can also be fumaric acid；It is fragrant
Material can also use the mixing of essence or essence and essential oil, and the esters essence or essential oil used in fragrance containing hydrophobic grouping may be used also
To be other essence or essential oil described in description of the invention or in which two or more compounding and other are unlisted
The esters essence or essential oil containing hydrophobic grouping；PEG can also be PEG-800, PEG-1000, PEG-1500, PEG-4000 or
PEG-8000；Povidone-ethanol solution parts by weight can also be 0.4 part, 0.5 part, 0.7 part, 0.8 part and 0.3~0.8
Any value between part；In povidone-ethanol solution the weight percent of povidone can also be for 3%, 4%, 6%, 7% with
And 3~7% any value.
Fragrant product progress product test obtained, test method are as follows in Example 1~7, comparative example 1~3:
50ml distilled water is taken, the fragrant product (about 5g) made is added, measures its dissolution time, then shifts solution
It is put into medium of the fiber stick as solution fragrance emission into fragrance bottle, is placed in 12 square metres of air environment and distributes perfume (or spice)
Gas records the volatilization time thin out to fragrance, during fragrance is thin out, since the evaporating solution change of solvent gradually becomes muddy
It is turbid.
Table 1: the comparison of fragrant product performance in Examples 1 to 7, comparative example 1~3
In conclusion the present invention passes through the composition of raw materials of reasonable compatibility fragrant product, and by specific preparation method, make
Fragrant product obtained can be rapidly and efficiently soluble in water, and alternative existing solvent type fragrant product, convenient transportation uses peace
Quan Xinggao, it is thin out in 7d or so fragrance, since solution becomes cloudy in solution.
Specific embodiment described herein is only an example for the spirit of the invention.The neck of technology belonging to the present invention
The technical staff in domain can make various modifications or additions to the described embodiments or replace by a similar method
In generation, however, it does not deviate from the spirit of the invention or beyond the scope of the appended claims.
Claims (9)
1. a kind of water solubility solid-state fragrant product, which is characterized in that the water solubility solid-state fragrant product includes following parts by weight
Several raw material components:
10~20 parts of fragrance,
20~40 parts of sour agent,
5~20 parts of sodium bicarbonate,
20~50 parts of lactose,
1~5 part of mannitol,
1~5 part of PEG,
The fragrance is essence or essential oil.
2. water solubility solid-state fragrant product according to claim 1, which is characterized in that the acid agent includes citric acid, apple
Tartaric acid, fumaric acid or tartaric acid.
3. water solubility solid-state fragrant product according to claim 1, which is characterized in that the fragrance is containing hydrophobic grouping
Esters essence or essential oil.
4. water solubility solid-state fragrant product according to claim 1, which is characterized in that the water solubility solid-state fragrant product
Raw material components including following parts by weight:
20 parts of fragrance,
22.5 parts of sour agent,
17.5 parts of sodium bicarbonate,
35 parts of lactose,
2 parts of mannitol,
3 parts of PEG-6000.
5. water solubility solid-state fragrant product according to claim 1 or 4, which is characterized in that the water solubility solid-state champignon
The raw material components of product further include povidone-ethanol solution that parts by weight are 0.3~0.8 part.
6. a kind of preparation method of water solubility solid-state fragrant product, which is characterized in that the preparation method comprises the following steps:
Prepare raw material components in the ratio of any claim in Claims 1 to 5, by sour agent, sodium bicarbonate, lactose and sweet dew
After alcohol mixes in proportion, fragrance is added, mixes, is eventually adding PEG, is then pressed into type, drying, packaging.
7. the preparation method of water solubility solid-state fragrant product according to claim 6, which is characterized in that the preparation method
Further include the steps that povidone-ethanol solution is added after fragrance is added.
8. the preparation method of water solubility solid-state fragrant product according to claim 6, which is characterized in that the preparation method
In each step carried out under conditions of 15~30 DEG C of temperature, 30~50% humidity, constant temperature and humidity in addition to drying steps.
9. the preparation method of water solubility solid-state fragrant product according to claim 6, which is characterized in that the drying be
10~14h is dried at a temperature of 50~55 DEG C.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111840621A (en) * | 2020-08-04 | 2020-10-30 | 安徽克菱保健科技有限公司 | Water-meeting self-heating aromatherapy bath tablet |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111840621A (en) * | 2020-08-04 | 2020-10-30 | 安徽克菱保健科技有限公司 | Water-meeting self-heating aromatherapy bath tablet |
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Application publication date: 20190920 |