CN110251635A - A kind of black plaster and preparation method thereof - Google Patents

A kind of black plaster and preparation method thereof Download PDF

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Publication number
CN110251635A
CN110251635A CN201910661834.XA CN201910661834A CN110251635A CN 110251635 A CN110251635 A CN 110251635A CN 201910661834 A CN201910661834 A CN 201910661834A CN 110251635 A CN110251635 A CN 110251635A
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parts
oil
spare
rhizome
plaster
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张云举
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00—Medicinal preparations containing organic active ingredients
    • A61K31/045—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K33/00—Medicinal preparations containing inorganic active ingredients
    • A61K33/24—Heavy metals; Compounds thereof
    • A61K33/36—Arsenic; Compounds thereof
    • A—HUMAN NECESSITIES
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    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
    • A61K35/12—Materials from mammals; Compositions comprising non-specified tissues or cells; Compositions comprising non-embryonic stem cells; Genetically modified cells
    • A61K35/55—Glands not provided for in groups A61K35/22 - A61K35/545, e.g. thyroids, parathyroids or pineal glands
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A—HUMAN NECESSITIES
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    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
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    • A61K36/36—Caryophyllaceae (Pink family), e.g. babysbreath or soapwort
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    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
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    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
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Abstract

The invention discloses a kind of black plasters and preparation method thereof, are grouped as by each group of following parts by weight: 400~900 parts of vegetable oil, 120~260 parts of yellow lead, 5~20 parts of leaf of elm tree, 5~20 parts of elm bark, 3~12 parts of red bean, 3~12 parts of soya bean, 5~15 parts of realgar, 5~15 parts of Herba Anemones vitifoliae, 5~15 parts of Giantleaf Ardisia Rhizome, 5~15 parts of folium photiniae, 3~12 parts of berba aristolochiae mollissimae, 3~12 parts of Aralia wood, 5~15 parts of tuniclike psammosilene root, 5~15 parts of Moschus, 3~12 parts of tsaoko, 3~12 parts of mountain spicy tree root and rhizome, 3~12 parts of myrrh, 3~12 parts of olibanum and 3~12 parts of borneol.Black plaster of the invention the major functions: the illnesss such as waist is de-, cervical spondylosis, scapulohumeral periarthritis, arthritis, heel infection, synovitis and cold and cool gas old complaint, quick, the efficacy of a drug is lasting, and curative effect is good, and cure rate is high, and without side-effects.

Description

A kind of black plaster and preparation method thereof
Technical field
The present invention relates to pharmaceutical technology field, specifically a kind of black plaster and preparation method thereof.
Background technique
Plaster has long history in China, continued to use practice by 1,100, sufficiently proves that drug external therapy has The features such as " simple row, price low, significant in efficacy, marvellous quick ", is very suitable in " people that be unwilling to take medicine cannot take medicine it Disease ".Especially cureless difficult and complicated cases are more shown with unique effect.
The dosage form that plaster includes mainly has a black plaster and white plaster, " black plaster " of civil widespread mainly with sesame oil with Yellow lead is as matrix, and " white plaster " is then using oily and palace powder as matrix.
Plaster dosage forms of medicine on domestic market still continues to use vegetable oil and red lead as matrix, by drug through height Temperature refining (270 DEG C) is process.Specific method is prescription medicine and oil setting high temperature frying in fried batch can, temperature control together System is at 200~220 DEG C, until withered and yellow, after filtration is removed slag, oil refining, temperature is controlled at 270~300 DEG C, twice-cooked stir-frying after lower red, releasing fire-toxin Contributory plan obtains.
The patent of notification number CN103330913A discloses a kind of Traditional Chinese herbal medicinal plaster, which includes ford dutchmanspipe root or herb, radix aconiti agrestis, river Crow, asarum, the root of Chinese clematis, pericarpium zanthoxyli, turmeric, the root of Dahurain angelica, olibanum, myrrh, ground bettle, trigone, corydalis tuber, camphor.The plaster can play Certain detumescence, analgesic, dehumidifying effect.
The patent of notification number CN102698242A discloses a kind of black plaster for treating waist and knee joints pain, and the medicine is to waist and knee Pain caused by joint injury, sciatica, hyperosteogeny etc. has relative remission curative effect.
But can not completely remove currently on the market rheumatism, rheumatoid arthritis, waist de-, cervical spondylosis, scapulohumeral periarthritis, Protrusion of lumber intervertebral disc, osteoproliferation, traumatic injury, arteriosclerosis and obstruction of lower limbs pain, synovitis and dispel the illnesss such as cold and cool gas old complaint ointment, It can also be recurred after some treatments；And the expenses for medicine of Western medicine is expensive, it is also difficult to remove root.
Summary of the invention
The purpose of the present invention is to overcome the deficiency in the prior art, tetra- generation of Jing Chengchuan bone fracture folk secret handed down from one's ancestors and long-term special Pharmaceutical developments research and clinical practice of practising medicine, provide a kind of easy osmotic absorption, quick, curative effect is good, and cure rate is high, no secondary to make Treatment waist is de-, cervical spondylosis, scapulohumeral periarthritis, arthritis, heel infection, synovitis and the old complaint for dispelling the illnesss such as cold and cool gas black cream Medicine and preparation method thereof.
In order to achieve the above objectives, The technical solution adopted by the invention is as follows:
A kind of black plaster is grouped as by each group of following parts by weight: 400~900 parts of vegetable oil, 120~260 parts of yellow lead, 5~20 parts of leaf of elm tree, 5~20 parts of elm bark, 3~12 parts of red bean, 3~12 parts of soya bean, 5~15 parts of realgar, Herba Anemones vitifoliae 5~15 Part, 5~15 parts of Giantleaf Ardisia Rhizome, 5~15 parts of folium photiniae, 3~12 3~12 parts of Fen, Aralia wood of berba aristolochiae mollissimae, 5~15 parts of tuniclike psammosilene root, Moschus 5 ~15 parts, 3~12 parts of tsaoko, 3~12 parts of mountain spicy tree root and rhizome, 3~12 parts of myrrh, 3~12 parts of olibanum and 3~12 parts of borneol.
It is preferred to above scheme, it is grouped as by each group of following parts by weight: 500~800 parts of vegetable oil, yellow lead 150~240 Part, 10~15 parts of leaf of elm tree, 10~15 parts of elm bark, 5~10 parts of red bean, 5~10 parts of soya bean, 8~12 parts of realgar, Herba Anemones vitifoliae 8 ~12 parts, 8~12 parts of Giantleaf Ardisia Rhizome, 8~12 parts of folium photiniae, 5~10 5~10 parts of Fen, Aralia wood of berba aristolochiae mollissimae, 8~12 parts of tuniclike psammosilene root, musk deer 8~12 parts fragrant, 5~10 parts of tsaoko, 5~10 parts of mountain spicy tree root and rhizome, 5~10 parts of myrrh, 5~10 parts of olibanum and 5~10 parts of borneol.
It is preferred to above scheme, it is grouped as by each group of following parts by weight: 750 parts of vegetable oil, 220 parts of yellow lead, leaf of elm tree 12 parts, 12 parts of elm bark, 8 parts of red bean, 8 parts of soya bean, 10 parts of realgar, 10 parts of Herba Anemones vitifoliae, 10 parts of Giantleaf Ardisia Rhizome, 10 parts of folium photiniae, seek 88 parts of Fen, Aralia wood of bone wind, 10 parts of tuniclike psammosilene root, 10 parts of Moschus, 8 parts of tsaoko, 8 parts of mountain spicy tree root and rhizome, 8 parts of myrrh, 8 parts of olibanum and borneol 8 Part.
Preferred to above scheme, the vegetable oil is selected from one of sesame oil, cottonseed oil, rapeseed oil or peanut oil.
Preferred to above scheme, the lead tolerance of the yellow lead is no less than 95%.
The preparation method of above-mentioned black plaster, includes the following steps:
(1) by leaf of elm tree, elm bark, Herba Anemones vitifoliae, Giantleaf Ardisia Rhizome, folium photiniae, berba aristolochiae mollissimae, Aralia wood and tuniclike psammosilene root selected impurity elimination Matter, dry, crushing are spare；
(2) red bean and soya bean are cleaned, is dry, mixed together with realgar, it is spare；
(3) yellow lead is dry, be ground to 100~120 mesh fine powders, it is spare；
(4) Moschus is ground to 100~200 mesh fine powders, it is spare；
(5) by tsaoko, mountain spicy tree root and rhizome, myrrh, olibanum and borneol and grinding to 100~200 mesh fine powders, mixing is spare；
(6) vegetable oil is placed in copper pot, intense fire is heated to 100~105 DEG C, spare thick of investment step (1) and (2) Material is adjusted to mild fire and carries out frying, lasting stirring and 90~120min of frying, up to coarse fodder frying to outer withered interior coke, oil temperature at this time To 210~220 DEG C, stop heating, be cooled to 40~60 DEG C, medicine oil is collected in residual oil separation；
(7) step (6) medicine oil intense fire is heated to 320 DEG C, is adjusted to moderate heat, decocted to no moisture and oily become drops into a bead, Medicine oil is smelt；
(8) the spare yellow lead of step (3) is equably sprinkled into the medicine oil being smelt to step (7) several times, ceaselessly towards same Direction stirs into sticky lotion, until lotion is tack-free, wire drawing is constantly made；
(9) plaster made of step (8) is poured into cold water, impregnates releasing fire-toxin；
(10) it takes group as in container on ointment made of step (9), is melted on water-bath or mild fire, then step (5) is standby Fines is blended into, and is stirred evenly, and the uniform stall with goods spread out on the ground for sale of ointment is coated on plaster paper or dedicated medicated plaster cloth, sprinkles step (4) Spare Moschus, is made black plaster.
Preferred to above scheme, step (9) impregnates releasing fire-toxin, changes 1 water daily, ointment was made on 7th.
The black plaster that the present invention protects the preparation method of above-mentioned black plaster to prepare simultaneously.
Step (6) medicine oil intense fire is heated to 320 DEG C, as core by the preparation method of black plaster of the present invention, step (7) Step, control method is with emphasis on following four aspect: 1. reaching predetermined temperature by thermometer judgement；2. seeing oil smoke, start to be shallow Cyan is gradually black and dense, and then is white dense smoke, when calm white cigarette it is straight on；3. seeing oil bloom, when boiling starts, oil bloom are mostly in pot Wall periphery, when oil bloom assemble Shi Weidu to pot center；It is dropped into a bead 4. seeing: taking a little medicine oil drop Yu Shuizhong, be not shattered into Pearl is degree.
Black plaster of the invention is the major functions: waist is de-, cervical spondylosis, scapulohumeral periarthritis, arthritis, heel infection, synovitis and cold and cool gas etc. The old complaint of illness.
The pharmacology and nature,taste and action of composition used in the present invention:
Leaf of elm tree, in the age of past drug scarcity, leaf of elm tree can be picked and be smashed to pieces by people, be added suitable white Wine is tuned into paste, is applied on wound, can play the role of hemostasis and pain-relieving.In addition, clinical research find this method for The patient of fracture also has good therapeutic effect, can accelerate the regeneration of bone while analgesic.Brainstrust passes through research discovery Leaf of elm tree food full of nutrition, people, which often eat, can play the role of powerful physique, improve the disease resistance of human body.Separately Outside, leaf of elm tree can also inducing diuresis for removing edema, difficult urination and edema of the body to the mankind have good alleviation effect.In treatment body When body edema, eaten after elm leaf being cooked congee.
Elm bark can be used as medicine, and treat neurasthenia, and relieving insomnia can have simultaneously with strengthening spleen and nourishing stomach, pure and fresh fall fire There is the effect of relieving cough and reducing sputum, reducing fever and causing diuresis detumescence desinsection.
Red bean, mild-natured, bitter.Return large intestine channel, stomach meridian, the heart channel of Hang-Shaoyin.The glycosides of triterpene containing jequirity A, jequirity triterpene glycosides B, yearning between lovers Sub- triterpene glycosides C, jequirity triterpene glycosides D, abrus agglutinin-a, abrus agglutinin-b, abrulin I, jequirity poison Protein I I, abrulin III, abrine, abraline, abrine, choline, gynesin, N, N- diformazan primary colours The methocation of propylhomoserin methyl esters, lower didactic literary composition erythrine etc., abrus agglutinin have very strong cause erythroagglutination.Have anti-swollen The effects of tumor, antiallergy, antihistamine.
Soya bean, it is bitter, pungent, it is cool.Inducing diaphoresis, relieving restlessness, a surname sends out hot and suffocating.It can be used for catching a cold, fever and chills headache, fidgety uncomfortable in chest, dysphoria is not It sleeps.
Realgar, warm-natured, acrid flavour are toxic.Return liver warp, large intestine channel.Have the function of antibacterial, anti-schistosome.Experiment shows hero Huang has inhibiting effect to staphylococcus aureus, Pseudomonas aeruginosa, a variety of dermatophytes and human-like, bacillus tuberculosis bovis.Clinic is used There is significant curative effect in treatment shingles zoster, chronic myelocytic leukemia and chronic bronchitis.
Herba Anemones vitifoliae, warm-natured, acrid flavour, micro-puckery.Wind analgesic, it is promoting blood circulation and removing obstruction in channels.Belong to the wind-damp dispelling strengthening the bones and muscles classified under medicine for rheumatism Medicine.External application: it is appropriate, decoct washing；Or mill juice applies；Or it mashes deposited.Cure mainly rheumatic arthralgia, apoplexy and hemiplegia, migraine and general headache, postpartum Blood stasis, agglomeration in stomache, traumatic injury, carbuncle sore tumefacting virus, unhealing ulcer.
Giantleaf Ardisia Rhizome, warm-natured, acrid flavour.Return liver warp, the spleen channel.Wind-damp dispelling strengthens the bone, promoting blood circulation.Belong to medicine for rheumatism subordinate point The wind-damp dispelling strengthening the bones and muscles medicine of class.
Folium photiniae, mild-natured, acrid flavour, hardship.Return liver warp, kidney channel.Wind-damp dispelling, antipruritic, strengthening the bones and muscles, liver and kidney benefiting.Belong to medicine for rheumatism The wind-damp dispelling strengthening the bones and muscles medicine of subordinate's classification.Cure mainly rheumatic arthralgia, cold and headache, rubeola, flaccidity of feet and knees, lumbago due to the kidney deficiency, impotence, something lost Essence.
Berba aristolochiae mollissimae, mild-natured, acrid flavour, hardship.Return liver warp, stomach meridian.Dispelling wind and removing obstruction in the meridians, promoting qi circulation and relieving pain.Belong under medicine for rheumatism classification Wind-damp dispelling strengthening the bones and muscles medicine.With controlling rheumatic arthralgia, extremity numbness, muscles and bones muscular constricture, traumatic injury pain, stomachache, toothache, colic etc.. Contained ethereal oil and alkaloid has apparent detumescence and prevention effect to rat formaldehyde or albumen arthritis；To rheumatism Property, rheumatoid arthritis play the role of obviously relieve pain, improve function of joint.
Aralia wood, acrid flavour；It is bitter；It is mild-natured.Return liver；Stomach；Kidney channel.Dispelling wind and eliminating dampness；Water profitting；Promoting blood circulation and detoxication.Medicine for the treatment of rheumatism and arthritis； Water profitting medicine；Promoting blood circulation and detoxication medicine.Cure mainly rheumatic arthritis；Waist and leg ache；Edema due to deficiency of the kidney；It quenches one's thirst；Epigastric pain；Traumatic injury； Fracture；It spits blood；Bleeding from five sense organs or subcutaneous tissue；Malaria；Dermatitis rhus；Osteomyelitis；Deep purulence ulcer.
Tuniclike psammosilene root, temperature are bitter, pungent.Return liver warp.Dispelling wind and eliminating dampness, removing blood stasis and acesodyne, removing toxicity for detumescence.Belong to medicine for rheumatism subordinate point The wind-damp-dispelling and cold-dissipating medicinal of class.Suitable amount used externally.With controlling rheumatic arthralgia, stomachache with cool feeling, traumatic injury, traumatic hemorrhage；Boil, snake are controlled outside Insect bite.
Moschus, the secretion of the glandular sac between the navel and genitals of male musk deer, is in granular form or blocky after dry, there is spy Different fragrance, there is bitter taste, and fragrance can be made, and can also be used as medicine；It is central nervous excitation agent, external application can ease pain, reduce swelling；For Blood stasis levies lump in the abdomen, trusted subordinate sudden and violent pain, traumatic injury, the card such as wind-cold-dampness arthralgia；Product Xin Xiang, opens away and alters, can the stasis of blood in promoting circulation of blood Stagnant, the heap soil or fertilizer over and around the roots for opening channels and collaterals is held back, and is used for sore swollen toxin, abscess of throat with promoting menstruation eliminating stagnation to stop pain, and the pungent fragrant row of the product dissipates, and has good promoting blood circulation Dissipating bind, swelling and pain relieving effect, oral administration and externally have good effect.
Tsaoko, warm-natured, acrid flavour.Converge to the spleen channel, stomach meridian.Eliminating dampness middle benefit gas, eliminating phlegm preventing malaria.Belong to damp-resolving medicinal.With controlling internal retention of cold wetness, gastral cavity Abdominal distention and pain, feeling of fullness vomiting, malaria fever and chills.
Mountain spicy tree root and rhizome, acrid flavour, hardship are warm-natured.Return stomach meridian, the spleen channel, Liver Channel.Dispelling wind and eliminating dampness, warming spleen and stomach for dispelling cold, the promoting flow of qi and blood circulation.Category is dispelled The wind-damp-dispelling and cold-dissipating medicinal of medicine for rheumatism subordinate classification.This product contain volatile oil, and oil principal component have linalool, citronellal, australene, Amphene, citronellol, beta-terpineol etc..
Myrrh also known as myrrh bright do not have there is also the vinegar-fried myrrh Myrrha of bright myrrh myrrh myrrh myrrh stir-baked MYRRHA with vinegar is raw Medicine etc. is also known as.For olive subject plant Chinese violet tree or the dry resin of Ha Didingshu.Main product in African Somalia, Ethiopia with And the ground such as India.The white oleo-gum-resin oozed out by bark crack is acquired, becomes rufous and hard round block in air. After smashing, fry to coke black application.Cure mainly chest and abdomen stasis caused pain, dysmenorrhea, menostasis, abdominal mass, traumatic injury, carbuncle swells sore, acute appendicitis, hot eyes Swelling and pain.There are promoting blood circulation and stopping pain, detumescence and promoting granulation and other effects.In the Chinese medicine that east is a kind of promoting blood circulation, stagnation resolvation, analgesic, stomach invigorating, the place of production is come from Ancient times are Arabic and one band of East Africa.It is i.e. on the books in " northern history ", say it is from Western Regions mortise state.In west, it is said that myrrh is a kind of There is the drug of magical curative effect.Myrrh branch is fabricated to various aromatic, preservative and analgesic by Hebrew.Old Testament period, Often it is made into ointment, is applied to wound, promotes wound healing.
Olibanum, dry gum resin, Duo Cheng little shape mamillary, teardrop shaped particle or irregular fritter are 0.5~3 centimetre long, Sometimes adhesion is at agglomerate.It is faint yellow, often with slight green, blue or brownish red；Translucent, there is one layer of off-white color powder on surface Dirt, after removing dust, surface is still matt；Matter heavily fortified point is crisp, and section is waxy, unglazed to select, and also has a small number of in hyaloid gloss；The micro- virtue of gas Perfume (or spice), mildly bitter flavor；Chew it, be just broken into fritter, immediately soften into blob of viscose, adhere to tooth, saliva becomes emulsus, and it is micro- have it is spicy Sense；Heat then softens, micro- aromatic (but should not have rosin gas) of burning, over-emitting black exhaust, and leaves black residue；It is total with a small amount of water It grinds, white " milky " liquid can be formed；With faint yellow, graininess, it is translucent, glue hand, gas fragrance person without sandstone bark impurity, powder and be It is good.Resinous 60~70%, natural gum 27~35%, volatile oil 3~8%.The main component of resin is free α, β-boswellic acid 33%, in conjunction with boswellic acid 1.5%, olibanoresene 33%.Natural gum is the calcium salt and magnesium salts 20% of arabitic acid, and tragacanth is viscous Element 6%；In addition, still containing amaroid 0.5%.Volatile oil has fragrance in faint yellow, contains firpene, racemization-limonene and α, β-Chinese celery Alkene.The major functions: regulating qi and activating blood, analgesic therapy chase after poison.Control qi and blood stagnation, trusted subordinate's pain, ulcerative carbuncle pyogenic infections, traumatic injury, dysmenorrhea, the postpartum stasis of blood Blood shouting pain.
Borneol, cold in nature, acrid flavour, hardship.Thoughts of returning home warp, the spleen channel, lung channel.Inducing resuscitation of having one's ideas straightened out, clearing away heat to and alleviating pain.Belong to awaking drug.External application is suitable Amount.With control heat close coma, close in phlegm heat, hot summer weather soldier faints, child convulsion and various sore, carbuncle and painful swellings, burst after do not hold back, burn and scald, throat Swelling and pain, sore throat, red eye, swell pain, aphthae etc..
Each medicament respectively has unique effects and an effect in above-mentioned formula, can more preferable interworking mutual tolerance, mutual compatibility is fabulous, collaboration Effect is significant, and easily in the iuntercellular of lesions position, permeability is strong for infiltration, is easily absorbed by cell, rapidly until lesion, such as damaged At bone tissue joint office film, amendment or reparation damage, the tissue of jackknifing or cold-dispelling, dehumidifying etc., quick, the efficacy of a drug Persistently, curative effect is good, and cure rate is high, and without side-effects.
Specific embodiment
It elaborates below to specific embodiments of the present invention.
Embodiment 1
A kind of black plaster is grouped as by each group of following parts by weight: 750 parts of sesame oil, 220 parts of yellow lead, 12 parts of leaf of elm tree, elm 12 parts of bark, 8 parts of red bean, 8 parts of soya bean, 10 parts of realgar, 10 parts of Herba Anemones vitifoliae, 10 parts of Giantleaf Ardisia Rhizome, 10 parts of folium photiniae, 8 parts of berba aristolochiae mollissimae, 8 parts of Aralia wood, 10 parts of tuniclike psammosilene root, 10 parts of Moschus, 8 parts of tsaoko, 8 parts of mountain spicy tree root and rhizome, 8 parts of myrrh, 8 parts of olibanum and 8 parts of borneol.
The lead tolerance of the yellow lead is no less than 95%, purchased from large-scale pharmacy.
The preparation method of above-mentioned black plaster, includes the following steps:
(1) by leaf of elm tree, elm bark, Herba Anemones vitifoliae, Giantleaf Ardisia Rhizome, folium photiniae, berba aristolochiae mollissimae, Aralia wood and tuniclike psammosilene root selected impurity elimination Matter, dry, crushing are spare；
(2) red bean and soya bean are cleaned, is dry, mixed together with realgar, it is spare；
(3) yellow lead is dry, be ground to 120 mesh fine powders, it is spare；
(4) Moschus is ground to 120 mesh fine powders, it is spare；
(5) by tsaoko, mountain spicy tree root and rhizome, myrrh, olibanum and borneol and grinding to 120 mesh fine powders, mixing is spare；
(6) vegetable oil is placed in copper pot, intense fire is heated to 100~105 DEG C, spare thick of investment step (1) and (2) Material is adjusted to mild fire and carries out frying, lasting stirring and frying 100min, and up to coarse fodder frying to outer withered interior coke, oil temperature is extremely at this time 220 DEG C, stop heating, be cooled to 50 DEG C, medicine oil is collected in residual oil separation；
(7) step (6) medicine oil intense fire is heated to 320 DEG C, is adjusted to moderate heat, decocted to no moisture and oily become drops into a bead, Medicine oil is smelt；
(8) the spare yellow lead of step (3) is equably sprinkled into the medicine oil being smelt to step (7) several times, ceaselessly towards same Direction stirs into sticky lotion, until lotion is tack-free, wire drawing is constantly made；
(9) plaster made of step (8) is poured into cold water, impregnates releasing fire-toxin, changes 1 water daily, ointment was made on 7th；
(10) it takes group as in container on ointment made of step (9), is melted on water-bath or mild fire, then step (5) is standby Fines is blended into, and is stirred evenly, and the uniform stall with goods spread out on the ground for sale of ointment is coated on plaster paper or dedicated medicated plaster cloth, sprinkles step (4) Spare Moschus, is made black plaster.
Patient clinical case 1: Li Nanshi, 45 years old, people from Shenyang City, Liaoning Province, taxi driver drove age 18 years, because hiring out Industry has very heavy professional cervical spondylosis, and cervical intervertebral disk CT shows: prominent, C4-5 intervertebral disc protrusion after C4-5 interverbebral disc is right arrives Pharmacy has purchased many patch plaster, and cooperation massage is only alleviated, and it is marvellous to hear the close black plaster effect processed handed down from one's ancestors, then purchases Enter three patches, after continuous use 3 days, symptom mitigates, and then buys 30 patches again, and feedback after being used continuously, cervical vertebra does not ache not yet Acid, cervical vertebra disease symptoms disappear, rehabilitation, and then follow-up recovery from illness is as usual, have no recurrence.
Patient clinical case 2: Zhao Nvshi, 50 years old, Liaoning Province Heng Renxian people, because of school lunch service's long-term work in the county Heng Ren Amount is big, causes body illness, scapulohumeral periarthritis, cold air and cold air, and the pack grabbed through pharmacy's purchase plaster and traditional Chinese medical science is only alleviated, Old complaint is not gone, is introduced by friend and uses black plaster of the invention, be used for two acupuncture points of shoulder, left and right shoulder one every time Four positions are pasted altogether, are continuously finished 20 patches, shoulder not ache, and continue to take 50 patch of purchase, shoulder restores normal, cold air and cold air It goes.
Embodiment 2
A kind of black plaster is grouped as by each group of following parts by weight: 800 parts of cottonseed oil, 240 parts of yellow lead, 15 parts of leaf of elm tree, 15 parts of elm bark, 10 parts of red bean, 10 parts of soya bean, 12 parts of realgar, 12 parts of Herba Anemones vitifoliae, 12 parts of Giantleaf Ardisia Rhizome, 12 parts of folium photiniae, berba aristolochiae mollissimae 10 10 parts of Fen, Aralia woods, 12 parts of tuniclike psammosilene root, 12 parts of Moschus, 10 parts of tsaoko, 10 parts of mountain spicy tree root and rhizome, 10 parts of myrrh, 10 parts of olibanum and borneol 10 parts.
The lead tolerance of the yellow lead is no less than 95%, purchased from large-scale pharmacy.
The preparation method of above-mentioned black plaster, includes the following steps:
(1) by leaf of elm tree, elm bark, Herba Anemones vitifoliae, Giantleaf Ardisia Rhizome, folium photiniae, berba aristolochiae mollissimae, Aralia wood and tuniclike psammosilene root selected impurity elimination Matter, dry, crushing are spare；
(2) red bean and soya bean are cleaned, is dry, mixed together with realgar, it is spare；
(3) yellow lead is dry, be ground to 100 mesh fine powders, it is spare；
(4) Moschus is ground to 120 mesh fine powders, it is spare；
(5) by tsaoko, mountain spicy tree root and rhizome, myrrh, olibanum and borneol and grinding to 150 mesh fine powders, mixing is spare；
(6) vegetable oil is placed in copper pot, intense fire is heated to 100~105 DEG C, spare thick of investment step (1) and (2) Material is adjusted to mild fire and carries out frying, lasting stirring and frying 120min, and up to coarse fodder frying to outer withered interior coke, oil temperature is extremely at this time 215 DEG C, stop heating, be cooled to 55 DEG C, medicine oil is collected in residual oil separation；
(7) step (6) medicine oil intense fire is heated to 320 DEG C, is adjusted to moderate heat, decocted to no moisture and oily become drops into a bead, Medicine oil is smelt；
(8) the spare yellow lead of step (3) is equably sprinkled into the medicine oil being smelt to step (7) several times, ceaselessly towards same Direction stirs into sticky lotion, until lotion is tack-free, wire drawing is constantly made；
(9) plaster made of step (8) is poured into cold water, impregnates releasing fire-toxin, changes 1 water daily, ointment was made on 7th；
(10) it takes group as in container on ointment made of step (9), is melted on water-bath or mild fire, then step (5) is standby Fines is blended into, and is stirred evenly, and the uniform stall with goods spread out on the ground for sale of ointment is coated on plaster paper or dedicated medicated plaster cloth, sprinkles step (4) Spare Moschus, is made black plaster.
Patient clinical case 3: Lv Nanshi, 54 years old, cook suffered from protrusion of lumber intervertebral disc, and need of work is stood for a long time, then Aggravation can not work normally, in great pain, can not normally fall asleep at night.Medical readme pain in waist and lower extremities is as pierced, leg raising straight examination The positive is tested, knee, Achilles jerk weaken, and big toe dorsiflexion power weakens.And dark purple tongue, there is ecchymosis, stringy and tense pulse is puckery.Diagnosis: between lumbar vertebrae Disk protrudes syndrome of blood stasis.Continuously stick black plaster of the present invention 14 days, pain is substantially reduced, and waist movable function improves, and symptom is obvious It improves.Continue after sticking 21 days, pain disappears, and 70 ° of leg raising straight or more, can work normally.
Embodiment 3
A kind of black plaster is grouped as by each group of following parts by weight: 900 parts of rapeseed oil, 260 parts of yellow lead, 20 parts of leaf of elm tree, 20 parts of elm bark, 12 parts of red bean, 12 parts of soya bean, 15 parts of realgar, 15 parts of Herba Anemones vitifoliae, 15 parts of Giantleaf Ardisia Rhizome, 15 parts of folium photiniae, berba aristolochiae mollissimae 12 12 parts of Fen, Aralia woods, 15 parts of tuniclike psammosilene root, 15 parts of Moschus, 12 parts of tsaoko, 12 parts of mountain spicy tree root and rhizome, 12 parts of myrrh, 12 parts of olibanum and borneol 12 parts.
The lead tolerance of the yellow lead is no less than 95%, purchased from large-scale pharmacy.
The preparation method of above-mentioned black plaster, includes the following steps:
(1) by leaf of elm tree, elm bark, Herba Anemones vitifoliae, Giantleaf Ardisia Rhizome, folium photiniae, berba aristolochiae mollissimae, Aralia wood and tuniclike psammosilene root selected impurity elimination Matter, dry, crushing are spare；
(2) red bean and soya bean are cleaned, is dry, mixed together with realgar, it is spare；
(3) yellow lead is dry, be ground to 120 mesh fine powders, it is spare；
(4) Moschus is ground to 200 mesh fine powders, it is spare；
(5) by tsaoko, mountain spicy tree root and rhizome, myrrh, olibanum and borneol and grinding to 120 mesh fine powders, mixing is spare；
(6) vegetable oil is placed in copper pot, intense fire is heated to 100~105 DEG C, spare thick of investment step (1) and (2) Material is adjusted to mild fire and carries out frying, lasting stirring and frying 120min, and up to coarse fodder frying to outer withered interior coke, oil temperature is extremely at this time 210 DEG C, stop heating, be cooled to 45 DEG C, medicine oil is collected in residual oil separation；
(7) step (6) medicine oil intense fire is heated to 320 DEG C, is adjusted to moderate heat, decocted to no moisture and oily become drops into a bead, Medicine oil is smelt；
(8) the spare yellow lead of step (3) is equably sprinkled into the medicine oil being smelt to step (7) several times, ceaselessly towards same Direction stirs into sticky lotion, until lotion is tack-free, wire drawing is constantly made；
(9) plaster made of step (8) is poured into cold water, impregnates releasing fire-toxin, changes 1 water daily, ointment was made on 7th；
(10) it takes group as in container on ointment made of step (9), is melted on water-bath or mild fire, then step (5) is standby Fines is blended into, and is stirred evenly, and the uniform stall with goods spread out on the ground for sale of ointment is coated on plaster paper or dedicated medicated plaster cloth, sprinkles step (4) Spare Moschus, is made black plaster.
Patient clinical case 4: Yu Nvshi 47 years old, suffers from knee joint hypertrophic synovitis, and part has pain, oedema, has work Dynamic obstacle.Sticking black plaster treatment of the present invention after two weeks, knee joint fever, feeling of pain obviously decreases, and continual cure three weeks Edematous condition greatly improves afterwards, and feeling of pain disappears substantially, and treats all symptoms at knee joint after three weeks and disappear, and body is extensive Multiple normal, follow-up later is over one year without recurrence.
Patient clinical case 5: Wu Nanshi 56 years old, leads to left foot injury of ankle because cycling tumble injury, local swelling pain, living Dynamic inconvenience, making a definite diagnosis is traumatic synovitis, sticks black plaster of the present invention after a week, and local swelling pain sense greatly improves, limbs Activity condition also makes moderate progress, and is further continued for sticking the present invention and fully recovers after a week, and patient consolidates again have been sticked one week, and drug withdrawal is over one year Limbs situation is normally without recurrence.
Embodiment 4
A kind of black plaster is grouped as by each group of following parts by weight: 500 parts of peanut oil, 150 parts of yellow lead, 10 parts of leaf of elm tree, 10 parts of elm bark, 5 parts of red bean, 5 parts of soya bean, 8 parts of realgar, 8 parts of Herba Anemones vitifoliae, 8 parts of Giantleaf Ardisia Rhizome, 8 parts of folium photiniae, 5 Fen, Aralia of berba aristolochiae mollissimae 5 parts of wood, 8 parts of tuniclike psammosilene root, 8 parts of Moschus, 5 parts of tsaoko, 5 parts of mountain spicy tree root and rhizome, 5 parts of myrrh, 5 parts of olibanum and 5 parts of borneol.
The lead tolerance of the yellow lead is no less than 95%, purchased from large-scale pharmacy.
The preparation method of above-mentioned black plaster, includes the following steps:
(1) by leaf of elm tree, elm bark, Herba Anemones vitifoliae, Giantleaf Ardisia Rhizome, folium photiniae, berba aristolochiae mollissimae, Aralia wood and tuniclike psammosilene root selected impurity elimination Matter, dry, crushing are spare；
(2) red bean and soya bean are cleaned, is dry, mixed together with realgar, it is spare；
(3) yellow lead is dry, be ground to 100 mesh fine powders, it is spare；
(4) Moschus is ground to 150 mesh fine powders, it is spare；
(5) by tsaoko, mountain spicy tree root and rhizome, myrrh, olibanum and borneol and grinding to 110 mesh fine powders, mixing is spare；
(6) vegetable oil is placed in copper pot, intense fire is heated to 100~105 DEG C, spare thick of investment step (1) and (2) Material is adjusted to mild fire and carries out frying, lasting stirring and frying 110min, and up to coarse fodder frying to outer withered interior coke, oil temperature is extremely at this time 215 DEG C, stop heating, be cooled to 50 DEG C, medicine oil is collected in residual oil separation；
(7) step (6) medicine oil intense fire is heated to 320 DEG C, is adjusted to moderate heat, decocted to no moisture and oily become drops into a bead, Medicine oil is smelt；
(8) the spare yellow lead of step (3) is equably sprinkled into the medicine oil being smelt to step (7) several times, ceaselessly towards same Direction stirs into sticky lotion, until lotion is tack-free, wire drawing is constantly made；
(9) plaster made of step (8) is poured into cold water, impregnates releasing fire-toxin, changes 1 water daily, ointment was made on 7th；
(10) it takes group as in container on ointment made of step (9), is melted on water-bath or mild fire, then step (5) is standby Fines is blended into, and is stirred evenly, and the uniform stall with goods spread out on the ground for sale of ointment is coated on plaster paper or dedicated medicated plaster cloth, sprinkles step (4) Spare Moschus, is made black plaster.
Patient clinical case 6: Chen Nvshi, 42 years old, there is flank pain without obvious inducement at the beginning of 2015 in patient's private prosecution, Limitation of activity is still endured, tired standing activity and meet it is cold after aggravate, alleviate after lying up.It drenched with rain before 1 week rear waist of suffering from cold Pain aggravates, and lower limb rediating pain to the right, and when cough and abdomen are exerted oneself, the pain increased, cannot turn over.Symptoms include: waist-leg portion crymodynia It weighs, it is unfavorable to change one's position, fixed pain, does not also subtract or aggravates instead though reposing, and light night day weight, pain increase in intensity under coldness obtains hot, subtracts.Lumbar vertebrae MRI shows: lumbar retrogression, L5/S1 disc herniation.DR (l spine ap & lat+mistake extends through position in the wrong+left and right loxosis) shows: lumbar vertebrae Front and rear edge degree of taking a favourable turn hyperostosis osteosclerosis, lumbar vertebrae Osteoarthritis.Diagnosis: the L5/S1 protrusion of the intervertebral disc (acute stage) -- cold-dampness Numbness resistance card.Black plaster Local out dressing of the invention is given, one time a day, is used continuously 1 week, patient tells that the miserable discomfort of flank pain subtracts Gently, functional activity improves；Continue to use drug therapy of the invention, totally 32 days, patient's pain in the loins was removed to the greatest extent, right lower extremity without sense of discomfort, Activity is obviously improved, and there has been no recurrence since follow-up.
Embodiment 5
A kind of black plaster is grouped as by each group of following parts by weight: 400 parts of sesame oil, 120 parts of yellow lead, 5 parts of leaf of elm tree, elm 5 parts of bark, 3 parts of red bean, 3 parts of soya bean, 5 parts of realgar, 5 parts of Herba Anemones vitifoliae, 5 parts of Giantleaf Ardisia Rhizome, 5 parts of folium photiniae, 3 Fen, Aralia wood 3 of berba aristolochiae mollissimae Part, 5 parts of tuniclike psammosilene root, 5 parts of Moschus, 3 parts of tsaoko, 3 parts of mountain spicy tree root and rhizome, 3 parts of myrrh, 3 parts of olibanum and 3 parts of borneol.
The lead tolerance of the yellow lead is no less than 95%, purchased from large-scale pharmacy.
The preparation method of above-mentioned black plaster, includes the following steps:
(1) by leaf of elm tree, elm bark, Herba Anemones vitifoliae, Giantleaf Ardisia Rhizome, folium photiniae, berba aristolochiae mollissimae, Aralia wood and tuniclike psammosilene root selected impurity elimination Matter, dry, crushing are spare；
(2) red bean and soya bean are cleaned, is dry, mixed together with realgar, it is spare；
(3) yellow lead is dry, be ground to 120 mesh fine powders, it is spare；
(4) Moschus is ground to 200 mesh fine powders, it is spare；
(5) by tsaoko, mountain spicy tree root and rhizome, myrrh, olibanum and borneol and grinding to 200 mesh fine powders, mixing is spare；
(6) vegetable oil is placed in copper pot, intense fire is heated to 100~105 DEG C, spare thick of investment step (1) and (2) Material is adjusted to mild fire and carries out frying, lasting stirring and frying 90min, and up to coarse fodder frying to outer withered interior coke, oil temperature is extremely at this time 220 DEG C, stop heating, be cooled to 40 DEG C, medicine oil is collected in residual oil separation；
(7) step (6) medicine oil intense fire is heated to 320 DEG C, is adjusted to moderate heat, decocted to no moisture and oily become drops into a bead, Medicine oil is smelt；
(8) the spare yellow lead of step (3) is equably sprinkled into the medicine oil being smelt to step (7) several times, ceaselessly towards same Direction stirs into sticky lotion, until lotion is tack-free, wire drawing is constantly made；
(9) plaster made of step (8) is poured into cold water, impregnates releasing fire-toxin, changes 1 water daily, ointment was made on 7th；
(10) it takes group as in container on ointment made of step (9), is melted on water-bath or mild fire, then step (5) is standby Fines is blended into, and is stirred evenly, and the uniform stall with goods spread out on the ground for sale of ointment is coated on plaster paper or dedicated medicated plaster cloth, sprinkles step (4) Spare Moschus, is made black plaster.
Patient clinical case 7: Huang Nanshi, 43 years old, Liaoning Province Fushun Qing Yuanxian people, because working in freezer throughout the year, frequent stomach Ache, have a pain in the leg and abdomen pain, checks that making a definite diagnosis is that cold air, cold air are too heavy, causes above-mentioned pain, takes many drugs not to hospital It gets better and turns, give black plaster Local out dressing of the invention, one time a day, be used continuously 1 week, patient's pleadings condition improves, and continues to use this The drug therapy of invention, totally 21 days, patient is cold and cool to be removed to the greatest extent.
Medicine Clinical Practice statistics is analyzed as follows shown:
Above-described embodiment is only more excellent embodiment of the invention, is implemented according to the technical essence of the invention to above Any simple modification, modification and the alternate variation that example is made, belong in the range of technical solution of the present invention.

Claims (8)

1. a kind of black plaster, which is characterized in that be grouped as by each group of following parts by weight: 400~900 parts of vegetable oil, yellow lead 120 ~260 parts, 5~20 parts of leaf of elm tree, 5~20 parts of elm bark, 3~12 parts of red bean, 3~12 parts of soya bean, 5~15 parts of realgar, strong wind 5~15 parts of rattan, 5~15 parts of Giantleaf Ardisia Rhizome, 5~15 parts of folium photiniae, 3~12 3~12 parts of Fen, Aralia wood of berba aristolochiae mollissimae, tuniclike psammosilene root 5~15 Part, 5~15 parts of Moschus, 3~12 parts of tsaoko, 3~12 parts of mountain spicy tree root and rhizome, 3~12 parts of myrrh, 3~12 parts of olibanum and borneol 3~12 Part.
2. a kind of black plaster according to claim 1, which is characterized in that 500~800 parts of vegetable oil, yellow lead 150~240 Part, 10~15 parts of leaf of elm tree, 10~15 parts of elm bark, 5~10 parts of red bean, 5~10 parts of soya bean, 8~12 parts of realgar, Herba Anemones vitifoliae 8 ~12 parts, 8~12 parts of Giantleaf Ardisia Rhizome, 8~12 parts of folium photiniae, 5~10 5~10 parts of Fen, Aralia wood of berba aristolochiae mollissimae, 8~12 parts of tuniclike psammosilene root, musk deer 8~12 parts fragrant, 5~10 parts of tsaoko, 5~10 parts of mountain spicy tree root and rhizome, 5~10 parts of myrrh, 5~10 parts of olibanum and 5~10 parts of borneol.
3. a kind of black plaster according to claim 1, which is characterized in that be grouped as by each group of following parts by weight: plant Oil 750 parts, 220 parts of yellow lead, 12 parts of leaf of elm tree, 12 parts of elm bark, 8 parts of red bean, 8 parts of soya bean, 10 parts of realgar, 10 parts of Herba Anemones vitifoliae, 10 parts of Giantleaf Ardisia Rhizome, 10 parts of folium photiniae, 88 parts of Fen, Aralia wood of berba aristolochiae mollissimae, 10 parts of tuniclike psammosilene root, 10 parts of Moschus, 8 parts of tsaoko, mountain spicy tree root and rhizome 8 Part, 8 parts of myrrh, 8 parts of olibanum and 8 parts of borneol.
4. a kind of black plaster according to any one of claims 1 to 3, which is characterized in that the vegetable oil be selected from sesame oil, One of cottonseed oil, rapeseed oil or peanut oil.
5. a kind of black plaster according to any one of claims 1 to 3, which is characterized in that the lead tolerance of the yellow lead is not Less than 95%.
6. the preparation method of black plaster as described in claims 1 to 3 any one, which comprises the steps of:
(1) it by leaf of elm tree, elm bark, Herba Anemones vitifoliae, Giantleaf Ardisia Rhizome, folium photiniae, berba aristolochiae mollissimae, Aralia wood and tuniclike psammosilene root selected impurity elimination matter, does Dry, crushing, it is spare；
(2) red bean and soya bean are cleaned, is dry, mixed together with realgar, it is spare；
(3) yellow lead is dry, be ground to 100~120 mesh fine powders, it is spare；
(4) Moschus is ground to 100~200 mesh fine powders, it is spare；
(5) by tsaoko, mountain spicy tree root and rhizome, myrrh, olibanum and borneol and grinding to 100~200 mesh fine powders, mixing is spare；
(6) vegetable oil is placed in copper pot, intense fire is heated to 100~105 DEG C, and the spare coarse fodder of investment step (1) and (2) is adjusted Frying, lasting stirring and 90~120min of frying are carried out to mild fire, up to coarse fodder frying to outer withered interior coke, oil temperature is extremely at this time 210~220 DEG C, stop heating, be cooled to 40~60 DEG C, medicine oil is collected in residual oil separation；
(7) step (6) medicine oil intense fire is heated to 320 DEG C, is adjusted to moderate heat, decocted to no moisture and oily become drops into a bead, medicine oil It is smelt；
(8) the spare yellow lead of step (3) is equably sprinkled into the medicine oil being smelt to step (7) several times, ceaselessly towards equidirectional Sticky lotion is stirred into, until lotion is tack-free, wire drawing is constantly made；
(9) plaster made of step (8) is poured into cold water, impregnates releasing fire-toxin；
(10) it takes group as in container on ointment made of step (9), is melted on water-bath or mild fire, then step (5) is spare Fines is blended into, and is stirred evenly, and the uniform stall with goods spread out on the ground for sale of ointment is coated on plaster paper or dedicated medicated plaster cloth, and it is spare to sprinkle step (4) Moschus, black plaster is made.
7. the preparation method of black plaster according to claim 6, which is characterized in that step (9) impregnates releasing fire-toxin, changes daily 1 water, ointment was made on 7th.
8. black plaster prepared by the preparation method of black plaster as claimed in claim 6.
CN201910661834.XA 2019-07-22 2019-07-22 A kind of black plaster and preparation method thereof Withdrawn CN110251635A (en)

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Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1282587A (en) * 2000-01-27 2001-02-07 王福真 Musk ointment (exterior application)

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1282587A (en) * 2000-01-27 2001-02-07 王福真 Musk ointment (exterior application)

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Application publication date: 20190920