CN110250556A - Improve the preparation method for heating the cigarette core material moisture pick-up properties that do not burn - Google Patents

Improve the preparation method for heating the cigarette core material moisture pick-up properties that do not burn Download PDF

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Publication number
CN110250556A
CN110250556A CN201910539180.3A CN201910539180A CN110250556A CN 110250556 A CN110250556 A CN 110250556A CN 201910539180 A CN201910539180 A CN 201910539180A CN 110250556 A CN110250556 A CN 110250556A
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CN
China
Prior art keywords
preparation
burn
core material
heating
properties
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910539180.3A
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Chinese (zh)
Inventor
陈绍全
李锐
冯涛
吴建霖
陈宇超
周俊
周潇
王艳红
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Tobacco Shi Weice (yunnan) Reconstituted Tobacco Co Ltd
Original Assignee
China Tobacco Shi Weice (yunnan) Reconstituted Tobacco Co Ltd
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Publication date
Application filed by China Tobacco Shi Weice (yunnan) Reconstituted Tobacco Co Ltd filed Critical China Tobacco Shi Weice (yunnan) Reconstituted Tobacco Co Ltd
Priority to CN201910539180.3A priority Critical patent/CN110250556A/en
Publication of CN110250556A publication Critical patent/CN110250556A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/12Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/14Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Abstract

The invention belongs to new tobacco products fields, and in particular to improve the preparation method for heating the cigarette core material moisture pick-up properties that do not burn;This method comprises the following steps: (1) raw material extracts;(2) preparation of chip base;(3) concentration of extracting solution;(4) one times sample preparation is deployed and be once coated with to coating fluid;(5) sample is wound;(6) secondary coating fluid allotment and secondary coating sample preparation;(7) sample calendering and rewinding;It is simple that the present invention provides a kind of method, and the preparation method for the cigarette core material moisture pick-up properties that do not burn is heated in improvement at low cost.Prepared by this method, the do not burn hygroscopicity of cigarette core material of resulting heating is decreased obviously, aesthetic quality be improved significantly.

Description

Improve the preparation method for heating the cigarette core material moisture pick-up properties that do not burn
Technical field
The invention belongs to new tobacco products fields, and in particular to a kind of improvement heating is not burnt cigarette core material moisture pick-up properties Preparation method.
Background technique
Key of the research for the cigarette cigarette core that do not burn as new tobacco products is heated, has tobacco product heating non-ignitable It burns, burning is avoided to generate harmful components, meanwhile, it is capable to be effectively prevented the generation of secondhand smoke, protect environment.But heating is not Burning is insufficient because burning, and causes sensory evaluating smoking's effect not ideal enough, then, how effectively to promote exhaust gas volumn, reduce heating Do not burn water imbibition, promote its aesthetic quality and become the key for heating incombustible field.
CN201610131559 discloses a kind of heating and does not burn cigarette cigarette core material processing method, with anaerobic glowing furnace, It heats in an inert gas atmosphere and cools down tobacco material in an inert gas atmosphere, then flavoring processing, obtain heating non-ignitable Burn cigarette cigarette core material.Treated tobacco material can be released effectively flue gas in the case where heating non-burning state, have good sense Official's quality.
Heating cigarette core material of not burning is mostly reconstituted tobacco product, the auxiliary material raw material added in preparation process, moisture absorption Property is stronger, and then influences the release of its fragrance and flue gas during heating, and aesthetic quality's effect is impacted larger.Therefore, have Effect reduces the hygroscopicity for heating cigarette core material of not burning, and for promoting smoke delivery, it is very crucial to promote its aesthetic quality.
Summary of the invention
It is of the invention the purpose of the present invention is to provide the preparation method that the cigarette core material moisture pick-up properties that do not burn is heated in improvement Purpose is the demand of the novel tobacco for market trend exploitation, provides that a kind of method is simple, improvement hygroscopicity at low cost Can heating do not burn cigarette core material preparation method for material.It is prepared by this method, the resulting moisture absorption for heating cigarette core material of not burning Property is decreased obviously, aesthetic quality be improved significantly.
The present invention solves the above problems the scheme of use are as follows:
The heating for improving moisture pick-up properties is not burnt cigarette core material preparation method for material, and this method comprises the following steps: (1) raw material extracts; (2) preparation of chip base;(3) concentration of extracting solution;(4) one times sample preparation is deployed and be once coated with to coating fluid;(5) sample is wound;(6) Secondary coating fluid allotment and secondary coating sample preparation;(7) sample calendering and rewinding.
Further, step (4) is allocated as with coating fluid described in step (6) by concentrate: hydrophobic material 20:1 The ratio of~10:1 is coated liquid allotment.
Further, step (4) and step (6) middle coating sample preparation drying moisture are 9~12%.
Further, the addition manner of addition hydrophobic material is a kind of or more in step (2), step (4) or step (6) Kind.
Further, hydrophobic material described in step (2), step (4) or step (6) includes intermixture or powder.
Further, the solute of intermixture and solvent ratio are 1:3~1:5.
Further, the solute of the intermixture is sodium alginate, tamarind seed polysaccharide glue, chitosan, casein, cation One or more combinations of guar gum, carragheen, modified starch adhesive and carboxymethyl cellulose, solvent be water, ethyl alcohol, propylene glycol, Glycerol, acetic acid are one or more.
The present invention provides a kind of method for beneficial the having the technical effect that of the present invention simply, improvement moisture pick-up properties at low cost Heat the cigarette core material preparation method for material that do not burn.It is prepared by this method, the resulting hygroscopicity for heating cigarette core material of not burning is bright Aobvious decline, aesthetic quality be improved significantly.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to the present invention It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to Limit the present invention.
Embodiment 1
Improve the preparation method for heating the cigarette core material moisture pick-up properties that do not burn, this method comprises the following steps: (1) raw material extracts; (2) preparation of chip base;(3) concentration of extracting solution;(4) one times sample preparation is deployed and be once coated with to coating fluid;(5) sample is wound;(6) Secondary coating fluid allotment and secondary coating sample preparation;(7) sample calendering and rewinding, provide that a kind of method is simple, improvement at low cost The heating of moisture pick-up properties is not burnt cigarette core material preparation method for material.It is prepared by this method, it is resulting to heat cigarette core material of not burning Hygroscopicity be decreased obviously, aesthetic quality be improved significantly.
Embodiment 2
On the basis of embodiment 1, step (4) is allocated as with coating fluid described in step (6) by concentrate: hydrophobic material It is coated liquid allotment for the ratio of 20:1, reconstituted tobacco rower is based on, it is right during the preparation process to heat cigarette core material of not burning All the components have the proportion on basis, then also there is certain requirement to additive.And the one kind of hydrophobic material as additive, Total component ratio has control.Test proves, is lower than this ratio, and will affect it improves hygroscopic effect, is higher than this ratio, then can It influences it and inhales taste and aesthetic quality.
Embodiment 3
On the basis of embodiment 1, step (4) is allocated as with coating fluid described in step (6) by concentrate: hydrophobic material It is coated liquid allotment for the ratio of 15:1, reconstituted tobacco rower is based on, it is right during the preparation process to heat cigarette core material of not burning All the components have the proportion on basis, then also there is certain requirement to additive.And the one kind of hydrophobic material as additive, Total component ratio has control.Test proves, is lower than this ratio, and will affect it improves hygroscopic effect, is higher than this ratio, then can It influences it and inhales taste and aesthetic quality.
Embodiment 4
On the basis of embodiment 1, step (4) is allocated as with coating fluid described in step (6) by concentrate: hydrophobic material It is coated liquid allotment for the ratio of 10:1, reconstituted tobacco rower is based on, it is right during the preparation process to heat cigarette core material of not burning All the components have the proportion on basis, then also there is certain requirement to additive.And the one kind of hydrophobic material as additive, Total component ratio has control.Test proves, is lower than this ratio, and will affect it improves hygroscopic effect, is higher than this ratio, then can It influences it and inhales taste and aesthetic quality.
Embodiment 4
On the basis of embodiment 1, step (4) and step (6) middle coating sample preparation drying moisture are 9%, enable to the production of preparation Product conform to quality requirements.
Embodiment 5
On the basis of embodiment 1, step (4) and step (6) middle coating sample preparation drying moisture are 10%, enable to preparation Product conforms to quality requirements.
Embodiment 6
On the basis of embodiment 1, step (4) and step (6) middle coating sample preparation drying moisture are 12%, enable to preparation Product conforms to quality requirements.
Embodiment 7
On the basis of embodiment 1, the addition manner of addition hydrophobic material is one in step (2), step (4) or step (6) Kind is a variety of.
Embodiment 8
On the basis of embodiment 1, hydrophobic material described in step (2), step (4) or step (6) include intermixture or Powder, intermixture are chiefly used in adding in wet end position, such as coating link, and dissolubility is preferable, in coating link addition, dosage It is few, but effect is preferable;Intermixture powder is chiefly used in adding in slurrying link, and dosage is larger.
Embodiment 9
On the basis of embodiment 8, the solute and solvent ratio of intermixture are 1:3, are obtained according to solute and solvent solubility, this ratio Example can obtain the suitable solution of concentration.
Embodiment 10
On the basis of embodiment 8, the solute and solvent ratio of intermixture are 1:4, are obtained according to solute and solvent solubility, this ratio Example can obtain the suitable solution of concentration.
Embodiment 11
On the basis of embodiment 8, the solute and solvent ratio of intermixture are 1:5, are obtained according to solute and solvent solubility, this Ratio can obtain the suitable solution of concentration.
Embodiment 12
On the basis of embodiment 8-11, the solute of the intermixture is sodium alginate, tamarind seed polysaccharide glue, chitosan, does One or more combinations of casein, cation guar gum, carragheen, modified starch adhesive and carboxymethyl cellulose, solvent are water, second Alcohol, propylene glycol, glycerol, acetic acid are one or more.
Embodiment 13
Tobacco material 63g, additional pulp fiber 25g are taken, 900g water is added, 60 DEG C of extraction 40min are separated by solid-liquid separation, according to Same proportion reextraction, separation of solid and liquid obtain solid and liquid.Solid after extraction is subjected to defibrination and manufactures paper with pulp into chip base.It mentions The liquid obtained carries out being concentrated into density 1.1g/cm3, obtain concentrate.
Take sodium alginate, chitosan, cation guar gum, carragheen and each 0.5g of carboxymethyl cellulose, be added glycerol, Each 1g of propylene glycol deploys to obtain hydrophobicity intermixture, and the hydrophobicity intermixture that allotment is obtained is added in concentrate, is added simultaneously Perfume material 2g, allotment obtain coating fluid.
Coating fluid is coated on and is prepared in resulting chip base, moisture 10% is dried to, a coated sample is obtained, by above-mentioned Method deploys secondary hydrophobicity intermixture, secondary coating fluid and carries out secondary coating, obtains secondary coated sample.
Resulting secondary coated sample is subjected to two-sided calendering using calender, rewinding is carried out using rewinding machine later and is obtained Heat the cigarette core material material products that do not burn.
With above-mentioned processing, preparing the obtained cigarette core material water content of not burning that heats is 10% non-ignitable with conventional heating Burning cigarette core material water content is 10%, between 25 DEG C, the constant temperature and humidity of 60% humidity it is middle carry out 48 hours balances after, measure water Point, the results showed that the heating cigarette core moisture content of not burning for adding hydrophobic material is only 13%, and conventional heating does not burn cigarette core material Expect that moisture content is 19%.
Experimental analysis:
Under conditions of other steps are identical, hydrophobic material is added in a kind of cigarette core material, another kind is not added, carried out flat After weighing apparatus, compare as follows:
Added the product of hydrophobic material, moisture is from 9.03%, and middle between 25 DEG C, the constant temperature and humidity of 60% humidity to carry out 48 small After Shi Pingheng, moisture is to 10.92%, and moisture absorption increases 20.90%;
It is un-added from 9.03%, between 25 DEG C, the constant temperature and humidity of 60% humidity it is middle carry out 48 hours balances after, moisture is reachable To 17.36%, wetting rate 92.25%.
The present invention is not limited by examples detailed above, describes the principle of the present invention and operation side in examples detailed above and specification Method, various changes and improvements may be made to the invention, these changes and improvements will be fallen into scope of the claimed invention.

Claims (7)

1. improving the preparation method for heating the cigarette core material moisture pick-up properties that do not burn, it is characterised in that: this method comprises the following steps: (1) raw material extracts;(2) preparation of chip base;(3) concentration of extracting solution;(4) one times sample preparation is deployed and be once coated with to coating fluid;(5) Sample winding;(6) secondary coating fluid allotment and secondary coating sample preparation;(7) sample calendering and rewinding.
2. according to claim 1 improve the preparation method for heating the cigarette core material moisture pick-up properties that do not burn, it is characterised in that: Coating fluid described in step (4) and step (6) is allocated as in concentrate: the ratio that hydrophobic material is 20:1~10:1 carries out Coating fluid allotment.
3. according to claim 1 improve the preparation method for heating the cigarette core material moisture pick-up properties that do not burn, it is characterised in that: Coating sample preparation drying moisture is 9~12% in step (4) and step (6).
4. according to claim 1 improve the preparation method for heating the cigarette core material moisture pick-up properties that do not burn, it is characterised in that: The addition manner of addition hydrophobic material is one or more in step (2), step (4) or step (6).
5. according to claim 1 improve the preparation method for heating the cigarette core material moisture pick-up properties that do not burn, it is characterised in that: Hydrophobic material described in step (2), step (4) or step (6) includes intermixture or powder.
6. according to claim 5 improve the preparation method for heating the cigarette core material moisture pick-up properties that do not burn, it is characterised in that: The solute and solvent ratio of intermixture are 1:3~1:5.
7. according to claim 4 or 5 improve the preparation method for heating the cigarette core material moisture pick-up properties that do not burn, feature exists In: the solute of the intermixture is sodium alginate, tamarind seed polysaccharide glue, chitosan, casein, cation guar gum, OK a karaoke club One or more combinations of glue, modified starch adhesive and carboxymethyl cellulose, solvent are water, ethyl alcohol, propylene glycol, glycerol, acetic acid one Kind is a variety of.
CN201910539180.3A 2019-06-20 2019-06-20 Improve the preparation method for heating the cigarette core material moisture pick-up properties that do not burn Pending CN110250556A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114098134A (en) * 2021-12-15 2022-03-01 云南中烟新材料科技有限公司 Heating cigarette core material and preparation method thereof
CN114886139A (en) * 2022-06-30 2022-08-12 福建金闽再造烟叶发展有限公司 Method for perfuming reconstituted tobacco by paper-making process
WO2023012304A1 (en) * 2021-08-04 2023-02-09 Nicoventures Trading Limited Aerosol-generating material comprising guar gum and starch or modified starch
WO2023012303A1 (en) * 2021-08-04 2023-02-09 Nicoventures Trading Limited Aerosol-generating material comprising chitosan and an additional binder

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CN1565285A (en) * 2003-06-13 2005-01-19 广东省金叶烟草薄片技术开发有限公司 Remaking tobacco leaf applying reduction process using paper making method
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2023012304A1 (en) * 2021-08-04 2023-02-09 Nicoventures Trading Limited Aerosol-generating material comprising guar gum and starch or modified starch
WO2023012303A1 (en) * 2021-08-04 2023-02-09 Nicoventures Trading Limited Aerosol-generating material comprising chitosan and an additional binder
CN114098134A (en) * 2021-12-15 2022-03-01 云南中烟新材料科技有限公司 Heating cigarette core material and preparation method thereof
CN114886139A (en) * 2022-06-30 2022-08-12 福建金闽再造烟叶发展有限公司 Method for perfuming reconstituted tobacco by paper-making process

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Application publication date: 20190920