CN110243978A - A kind of chromatograph - Google Patents
A kind of chromatograph Download PDFInfo
- Publication number
- CN110243978A CN110243978A CN201910655487.XA CN201910655487A CN110243978A CN 110243978 A CN110243978 A CN 110243978A CN 201910655487 A CN201910655487 A CN 201910655487A CN 110243978 A CN110243978 A CN 110243978A
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- Prior art keywords
- chromatograph
- plate
- gear
- case
- fixedly installed
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Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/16—Injection
- G01N30/18—Injection using a septum or microsyringe
Abstract
The present invention relates to chromatograph fields, specifically a kind of chromatograph, including chromatograph case, top plate, sample placement mechanism, dust-proof mechanism, supporting leg, mobile mechanism and handwheel, top plate is fixedly installed at the top of chromatograph case, the side of chromatograph case is movably set with the sample displacement structure for storing samples.A kind of chromatograph of the invention, when using the chromatograph, when needing to place stable, rotate the rotation of hand wheeling driving gear, rack-plate is driven to move upwards in gear rotation process, to drive movable pulley to move upwards, so that movable pulley is received into the inside of supporting leg, so that supporting leg and ground face contact, it is supported using supporting leg, achieve the purpose that place when use stable, simultaneously but also fixed plate is moved downward under the drive that gear rotates, so that dust excluding plate leaves the side of heat release hole, allow to carry out radiating treatment using heat release hole, placement can be reached to stablize, it can achieve the purpose that synchronous heat dissipation again.
Description
Technical field
The present invention relates to chromatograph field, specifically a kind of chromatograph.
Background technique
Chromatograph, for the device for carrying out chromatographic isolation analysis, including at sampling system, detection system, record and data
Reason system, temperature control system and mobile phase control system etc., modern chromatograph have stability, sensitivity, versatility and from
The features such as dynamicization degree is high has gas chromatograph, liquid chromatograph and gel permeation chrommatograph etc., these being widely used for of chromatograph
Product, the analysis of certain content of high molecular material are learned, gel chromatography can also measure the molecular weight of high molecular material and its divide
Cloth, chromatographic earliest application are for separating plant pigment, and method is such that be put into calcium carbonate in a glass tube,
To be poured into pipe containing the petroleum ether of phytochrome (extracting solution of leaves of plants), at this point, the upper end of glass tube occur immediately it is several
Then the mixed spectrum band of color is rinsed with pure petroleum ether, with the addition of petroleum ether, bands of a spectrum are constantly moved down, and gradually
Be separated into the bands of a spectrum of several different colours, continue to rinse can connect respectively various colors pigment, and can be identified respectively,
Chromatography is also gained the name therefrom.
Gas chromatograph refers to the chromatography instrument for using gas as mobile phase, and principle is mainly to utilize the boiling of substance
The difference of point, polarity and adsorption property realizes the separation of mixture, and sample to be analysed is after vaporizer gasification by inert gas band
Enter in chromatographic column, liquid or solid stationary phase is contained in column, each component tends between mobile phase and stationary phase in sample
Form distribution or adsorption equilibrium, with the flowing of carrier gas, sample component carry out during exercise repeated multiple times distribution or absorption and
Desorption distributes the big component of concentration in carrier gas and first flows out chromatographic column, and flows out after distributing the big component of concentration in stationary phase,
Traditional gas chromatograph is not readily portable, needs user to clasp and moves, however consumes manpower and material resources excessively, is not easy to
The use of user solves the problems, such as mobile if installation universal wheel etc. mobile mechanisms, and there is also propped up using universal wheel
Support is unstable in the presence of placing, and particular for using under outdoor environment, when encountering outdoor ground out-of-flatness, then will appear placement
Unstable, placing unstable rule causes to be unfavorable for sample to carry out injection work, is easy so that leakage problem occurs when sample injects,
And when injecting sample, syringe is not easy to place, and when outdoor, majority is placed using manpower, is more unfavorable for sampling analysis, no
Easily take, cause using effect bad, and traditional gas chromatograph there is a problem of radiate dedusting be difficult to it is compatible.
Summary of the invention
For the problems of the prior art, the present invention provides a kind of chromatographs.
The technical solution adopted by the present invention to solve the technical problems is: a kind of chromatograph, including chromatograph case, top plate,
Sample placement mechanism, dust-proof mechanism, supporting leg, mobile mechanism and handwheel are fixedly installed top at the top of the chromatograph case
Plate, the side of the chromatograph case are movably set with the sample displacement structure for storing samples, the surface of the chromatograph case
It is provided with for dust-proof dustproof construction, the bottom of the chromatograph case is fixedly installed the supporting leg being used to support, the branch
Support leg is internally provided with for the mobile mobile mechanism carried, and the bottom on chromatograph case surface is provided with to be moved for controlling
The handwheel of motivation structure;
The mobile mechanism includes gear, and gear is located at the inside of chromatograph case, and the side of the gear is engaged
There is rack-plate, the bottom of the rack-plate is fixedly installed movable pulley by telescopic sleeving rod, and the other side engagement of the gear is set
It is equipped with fixed plate, the fixed plate is fixedly installed dust excluding plate far from the side of gear, and the side of the dust excluding plate is provided with position
Heat release hole in chromatograph case surface.
Specifically, the surface of the top plate is turned left from the right side is disposed with sample injector and hydrogen flame ionization detector, and
It is arranged in parallel between sample injector and hydrogen flame ionization detector.
Specifically, the sample placement mechanism includes fixed frame, the bottom of the fixed frame is fixedly installed fixture block, described
It is fixedly installed placement block at the top of fixed frame, placing groove, the upper table of the chromatograph case are offered at the top of the placement block
Face offers card slot, and the inside of the card slot is connected with fixture block.
Specifically, the dust-proof mechanism includes sliding rail, the sliding rail is fixedly mounted on the side of chromatograph case, the cunning
The internal slide of rail is connected with sliding block, and the side of the sliding block is fixedly connected with Air Filter, between the heat release hole and Air Filter
To be vertically arranged in parallel, i.e., the inside immediately below Air Filter is arranged in heat release hole, and the top and bottom of the sliding rail are fixed
It is connected with gag lever post.
Specifically, the two sides of chromatograph box cavity bottom are fixedly installed with guide rail, the internal slide of the guide rail
It is connected with movable block, the side of the movable block is fixedly connected with rack-plate, and the rack-plate is provided with close to the side of gear
Tooth socket, and gear engages connection with tooth socket.
Specifically, the fixed plate is provided with connection tooth socket close to the side of gear, and connects and nibbled between tooth socket and gear
Connection is closed, the bottom of the fixed plate offers fixing groove, and the internal activity of the fixing groove is connected with guide rod, the guide rod
Surface is socketed with adjustable spring.
Specifically, the fixed plate is fixedly connected with dust excluding plate, the outside setting of the dust excluding plate far from the side of gear
There is heat release hole, the dust excluding plate, heat release hole and Air Filter are arranged from inside to outside.
Beneficial effects of the present invention:
(1), a kind of chromatograph of the present invention exists mobile in outdoor application for outdoor chromatograph and places steady
Surely it is difficult to compatible problem, while for the problem compatible with being difficult between dedusting that radiate, passing through setting supporting leg and movement
Mechanism, when using the chromatograph, when needing to place stable, rotation hand wheeling driving gear is rotated, band movable tooth in gear rotation process
Batten moves upwards, so that movable pulley be driven to move upwards so that movable pulley is received into the inside of supporting leg so that supporting leg with
Ground face contact, is supported using supporting leg, achieve the purpose that place when use it is stable, while but also fixed plate gear turn
It is moved downward under dynamic drive, so that dust excluding plate leaves the side of heat release hole, allows to radiate using heat release hole
Processing can reach placement and stablize and achieve the purpose that synchronous heat dissipation, substantially increase using effect, while by Air Filter
It pulls downward on, Air Filter is moved to the front side of heat release hole, play dust-proof purpose, dust is avoided to enter the interior of chromatograph case
Portion is dusted processing while so that reaching stable placement and heat dissipation.
(2), a kind of chromatograph of the present invention, for outdoor chromatograph in use, existing because outdoor placement is unstable
Surely it will lead to and be unfavorable for sample and carry out injection work, be easy so that leakage problem occurs when sample injects, and in injection sample
When, syringe problem not easy to place, by the way that sample placement mechanism is arranged, in use, the fixture block grafting of fixed frame bottom is arranged
In the inside of card slot, portable installation is carried out to fixed frame to realize, while syringe being inserted into placing groove, when taking
It only needs to extract sample injector out, it is simple and convenient, and also placing groove is vertical direction setting, be can effectively prevent
Sample injector, which occurs to roll, to be dropped, and is taken conveniently, to solve to lead to be unfavorable for sample note because outdoor placement is unstable
Enter work, leakage problem occurs.
Detailed description of the invention
Present invention will be further explained below with reference to the attached drawings and examples.
Fig. 1 is a kind of chromatographic structural schematic diagram provided by the invention;
Fig. 2 is a kind of chromatographic schematic cross-sectional view provided by the invention;
Fig. 3 is a kind of chromatographic sample placement mechanism schematic diagram provided by the invention;
Fig. 4 is a kind of chromatographic dust-proof mechanism schematic diagram provided by the invention;
Fig. 5 is the portion A enlarged structure schematic diagram in a kind of chromatographic Fig. 2 provided by the invention.
In figure: 1, chromatograph case;101, card slot;102, heat release hole;2, top plate;21, sample injector;22, hydrogen flame ion is examined
Survey device;3, sample placement mechanism;31, fixed frame;32, fixture block;33, block is placed;34, placing groove;4, dust-proof mechanism;41, sliding rail;
42, sliding block;43, Air Filter;44, gag lever post;5, supporting leg;6, mobile mechanism;61, gear;62, rack-plate;63, telescopic
Bar;64, buffer spring;65, movable pulley;66, fixed plate;661, tooth socket is connected;662, fixing groove;663, guide rod;664, it stretches
Spring;67, dust excluding plate;68, guide rail;69, movable block;7, handwheel.
Specific embodiment
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed, the present invention is further explained.
As Figure 1-Figure 5, a kind of chromatograph of the present invention, including chromatograph case 1, top plate 2, sample placement mechanism
3, dust-proof mechanism 4, supporting leg 5, mobile mechanism 6 and handwheel 7, the top of the chromatograph case 1 are fixedly installed top plate 2, institute
The side for stating chromatograph case 1 is movably set with sample displacement structure 3 for storing samples, and the surface of the chromatograph case 1 is set
It is equipped with for dust-proof dustproof construction 4, the bottom of the chromatograph case 1 is fixedly installed the supporting leg 5 being used to support, the branch
Support leg 5 is internally provided with for the mobile mobile mechanism 6 carried, and the bottom on 1 surface of chromatograph case is provided with for controlling
The handwheel 7 of mobile mechanism 6 processed;
The mobile mechanism 6 includes gear 61, and gear 61 is located at the inside of chromatograph case 1, the side of the gear 61
It is engaged rack-plate 62, the bottom of the rack-plate 62 is fixedly installed movable pulley 65, the tooth by telescopic sleeving rod 63
The other side of wheel 61 has been engaged fixed plate 66, and the fixed plate 66 is fixedly installed dust excluding plate far from the side of gear 61
67, the side of the dust excluding plate 67 is provided with the heat release hole 102 positioned at 1 surface of chromatograph case.
Specifically, the surface of the top plate 2 turns left from the right side and is disposed with sample injector 21 and hydrogen flame ionization detector
22, and be arranged in parallel between sample injector 21 and hydrogen flame ionization detector 22, the underface of sample injector 21 is provided with positioned at chromatography
Burner hearth inside instrument case 1 can effectively detect sample using hydrogen flame ionization detector 22.
Specifically, the sample placement mechanism 3 includes fixed frame 31, the bottom of the fixed frame 31 is fixedly installed fixture block
32, the top of the fixed frame 31, which is fixedly installed, places block 33, and the top for placing block 33 offers placing groove 34, described
The upper surface of chromatograph case 1 offers card slot 101, and the inside of the card slot 101 is connected with fixture block 32, and the inside for placing block 33 is opened
Equipped with the placing groove 34 for being inserted into syringe, in use, card slot 101 is arranged in 32 grafting of fixture block of 31 bottom of fixed frame
Inside carries out portable installation to fixed frame 31 to realize, while syringe being inserted into placing groove 34, only needs when taking
Extract sample injector out, it is simple and convenient, and also placing groove is vertical direction setting, can effectively prevent sample
Syringe, which occurs to roll, to be dropped, and is taken conveniently.
Specifically, the dust-proof mechanism 4 includes sliding rail 41, the sliding rail 41 is fixedly mounted on the side of chromatograph case 1,
The internal slide of the sliding rail 41 is connected with sliding block 42, and the side of the sliding block 42 is fixedly connected with Air Filter 43, the heat dissipation
It is vertically to be arranged in parallel between hole 102 and Air Filter 43, i.e., the inside immediately below Air Filter 43 is arranged in heat release hole 102, described
The top and bottom of sliding rail 41 are fixedly connected to gag lever post 44, can be effectively in chromatograph case 1 using heat release hole 102
Portion radiates, when the chromatograph does not need in use, Air Filter 43 can then be pulled downward on, so that Air Filter 43 is in sliding block
42 allow to utilize Air Filter 43 with slide downward under the cooperation of sliding rail 41 using the gear of Air Filter 43 in 102 front side of heat release hole
Dust-proof processing is carried out, simultaneously as the outside of chromatograph case 1 is arranged in Air Filter 43, it is periodically clear convenient for being carried out to Air Filter 43
Reason.
Specifically, the two sides of 1 intracavity bottom of chromatograph case are fixedly installed with guide rail 68, the inside of the guide rail 68
Slidably connect movable block 69, the side of the movable block 69 is fixedly connected with rack-plate 62, and the rack-plate 62 is close to gear
61 side is provided with tooth socket, and gear 61 engages connection with tooth socket, drives rack-plate 62 to carry out in 61 rotation process of gear
Lower movement so that movable block 69 moves up and down under the action of guide rail 68, movable block 69 guide rail 68 effect into
Row sliding, can play guiding role to rack-plate 62, avoid rack-plate 62 during up and down motion because vibration leads to tooth
Batten 62 and gear 61 are displaced or damage, to improve using effect.
Specifically, the fixed plate 66 close to the side of gear 61 be provided with connection tooth socket 661, and connect tooth socket 661 with
Connection is engaged between gear 61, the bottom of the fixed plate 66 offers fixing groove 662, the internal activity of the fixing groove 662
It is connected with guide rod 663, the surface of the guide rod 663 is socketed with adjustable spring 664, drives fixed plate 66 in 61 rotation process of gear
Move up and down, the adjustable spring 664 on 663 surface of guide rod allowed to carry out stretching motion, be both avoided that fixed plate 66 to
It is contacted in lower motion process with 1 bottom rigid of chromatograph case, plays the role of protecting fixed plate 66, while can also play to fixation
The purpose of damping is played in the effect that plate 66 is buffered.
Specifically, the fixed plate 66 is fixedly connected with dust excluding plate 67 far from the side of gear 61, the dust excluding plate 67
Outside is provided with heat release hole 102, and the dust excluding plate 67, heat release hole 102 and Air Filter 43 are arranged from inside to outside, when the chromatograph
In use, rotation handwheel 7 is rotated with moving gear 61, rack-plate 62 is driven to move upwards in 61 rotation process of gear, to drive
Movable pulley 65 moves upwards, so that movable pulley 65 is received into the inside of supporting leg 5, so that supporting leg 5 and ground face contact, reaching makes
Used time places stable purpose, while but also fixed plate 66 is moved downward under the drive that gear 61 rotates, so that anti-
Dirt plate 67 leaves the side of heat release hole 102, allows to carry out radiating treatment using heat release hole 102, can reach placement and stablize,
It can achieve the purpose that synchronous heat dissipation again, substantially increase using effect.
When in use, using the chromatograph, when needing to place stable, rotation handwheel 7 is rotated with moving gear 61, gear 61
Rack-plate 62 is driven to move upwards in rotation process, to drive movable pulley 65 to move upwards, so that movable pulley 65 is received into branch
The inside of support leg 5, so that supporting leg 5 and ground face contact, are supported using supporting leg 5, reach and place stable mesh when use
, while but also fixed plate 66 is moved downward under the drive that gear 61 rotates, so that dust excluding plate 67 leaves heat release hole
102 side allows to carry out radiating treatment using heat release hole 102, can reach placement and stablize and reach synchronous heat dissipation
Purpose, substantially increase using effect, while Air Filter 43 being pulled downward on, Air Filter 43 be moved to heat release hole 102
Dust-proof purpose is played in front side, and dust is avoided to enter the inside of chromatograph case 1, so that it is stable same with heat dissipation to reach placement
When, it is dusted processing, while in use, 32 grafting of fixture block of 31 bottom of fixed frame to be arranged in the inside of card slot 101, thus
It realizes and portable installation is carried out to fixed frame 31, while syringe being inserted into placing groove 34, only need to extract sample out when taking
Product syringe, it is simple and convenient, and also placing groove is vertical direction setting, can effectively prevent sample injector hair
Raw roll is dropped, and takes conveniently, to solve to lead to be unfavorable for sample injection work because outdoor placement is unstable, leaks
Liquid problem rotates backward handwheel 7 and rotates with moving gear 61, rack-plate 62 is driven in 61 rotation process of gear when needing mobile
It moves downward, to drive movable pulley 65 to move downward, so that movable pulley 65 is moved to the bottom of supporting leg 5, so that movable pulley
65 with ground face contact, moved using movable pulley 65, accomplished it is easy to remove, while but also fixed plate 66 at 61 turns of gear
It is moved upwards under dynamic drive, so that dust excluding plate 67 moves to the side of heat release hole 102, allows to utilize dust excluding plate 67
Baffle lives heat release hole 102 and carries out dissipating dust-proof processing, avoids dust from entering the inside of chromatograph case 1 by heat release hole 102, reaches
Mobile convenient and dust-proof processing is run simultaneously.
The basic principles, main features and advantages of the invention have been shown and described above.The technical staff of the industry should
Understand, the present invention is not limited to the above embodiments, and the description in above embodiment and specification only illustrates the present invention
Principle, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these variation and
Improvement is both fallen in the scope of protection of present invention.The claimed scope of the invention is by appended claims and its equivalent
Object defines.
Claims (7)
1. a kind of chromatograph, including chromatograph case (1), top plate (2), sample placement mechanism (3), dust-proof mechanism (4), supporting leg
(5), mobile mechanism (6) and handwheel (7), it is characterised in that: top plate (2) are fixedly installed at the top of the chromatograph case (1),
The side of the chromatograph case (1) is movably set with the sample displacement structure (3) for storing samples, the chromatograph case (1)
Surface be provided with for dust-proof dustproof construction (4), the bottom of the chromatograph case (1) is fixedly installed the branch being used to support
Support leg (5), the supporting leg (5) are internally provided with for the mobile mobile mechanism (6) carried, chromatograph case (1) table
The bottom in face is provided with the handwheel (7) for controlling mobile mechanism (6);
The mobile mechanism (6) includes gear (61), and gear (61) is located at the inside of chromatograph case (1), the gear (61)
Side be engaged rack-plate (62), the bottom of the rack-plate (62) is fixedly installed movement by telescopic sleeving rod (63)
It takes turns (65), the other side of the gear (61) has been engaged fixed plate (66), and the fixed plate (66) is far from gear (61)
Side is fixedly installed dust excluding plate (67), and the side of the dust excluding plate (67) is provided with the heat dissipation positioned at chromatograph case (1) surface
Hole (102).
2. a kind of chromatograph according to claim 1, it is characterised in that: turn left successively from the right side on the surface of the top plate (2)
Be provided with sample injector (21) and hydrogen flame ionization detector (22), and sample injector (21) and hydrogen flame ionization detector (22) it
Between be arranged in parallel.
3. a kind of chromatograph according to claim 1, it is characterised in that: the sample placement mechanism (3) includes fixed frame
(31), the bottom of the fixed frame (31) is fixedly installed fixture block (32), is fixedly installed and is put at the top of the fixed frame (31)
It sets block (33), is offered placing groove (34) at the top of the placement block (33), the upper surface of the chromatograph case (1) offers card
The inside of slot (101), the card slot (101) is connected with fixture block (32).
4. a kind of chromatograph according to claim 1, it is characterised in that: the dust-proof mechanism (4) includes sliding rail (41), institute
Sliding rail (41) to be stated to be fixedly mounted on the side of chromatograph case (1), the internal slide of the sliding rail (41) is connected with sliding block (42),
The side of the sliding block (42) is fixedly connected with Air Filter (43), is vertical between the heat release hole (102) and Air Filter (43)
It is arranged in parallel, i.e. inside of heat release hole (102) setting immediately below Air Filter (43), the top and bottom of the sliding rail (41)
It is fixedly connected to gag lever post (44).
5. a kind of chromatograph according to claim 1, it is characterised in that: the two sides of chromatograph case (1) intracavity bottom
It is fixedly installed with guide rail (68), the internal slide of the guide rail (68) is connected with movable block (69), the movable block (69)
Side is fixedly connected with rack-plate (62), and the rack-plate (62) is provided with tooth socket, and gear close to the side of gear (61)
(61) connection is engaged with tooth socket.
6. a kind of chromatograph according to claim 1, it is characterised in that: the one of the fixed plate (66) close gear (61)
Side is provided with connection tooth socket (661), and connects and engage connection between tooth socket (661) and gear (61), the fixed plate (66)
Bottom offers fixing groove (662), and the internal activity of the fixing groove (662) is connected with guide rod (663), the guide rod (663)
Surface be socketed with adjustable spring (664).
7. a kind of chromatograph according to claim 1, it is characterised in that: the one of the fixed plate (66) separate gear (61)
Side is fixedly connected with dust excluding plate (67), is provided with heat release hole (102) on the outside of the dust excluding plate (67), the dust excluding plate (67),
Heat release hole (102) and Air Filter (43) are arranged from inside to outside.
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CN201910655487.XA CN110243978B (en) | 2019-07-19 | 2019-07-19 | Chromatograph |
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CN201910655487.XA CN110243978B (en) | 2019-07-19 | 2019-07-19 | Chromatograph |
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CN110243978B CN110243978B (en) | 2022-04-26 |
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CN111307970A (en) * | 2020-03-06 | 2020-06-19 | 福建日新检测技术服务有限公司 | Workshop-based hexane concentration detection device and detection method thereof |
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CN112834667A (en) * | 2020-12-31 | 2021-05-25 | 贵州电网有限责任公司 | Transformer oil chromatogram sampling device |
CN116183776A (en) * | 2023-03-29 | 2023-05-30 | 山东千河环境科技有限公司 | Chromatograph for gas monitoring and monitoring method thereof |
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CN112834667A (en) * | 2020-12-31 | 2021-05-25 | 贵州电网有限责任公司 | Transformer oil chromatogram sampling device |
CN116183776A (en) * | 2023-03-29 | 2023-05-30 | 山东千河环境科技有限公司 | Chromatograph for gas monitoring and monitoring method thereof |
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