CN110236990A - Hydrolyze jojoba ester shin moisturizer and facial mask - Google Patents
Hydrolyze jojoba ester shin moisturizer and facial mask Download PDFInfo
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- CN110236990A CN110236990A CN201910682711.4A CN201910682711A CN110236990A CN 110236990 A CN110236990 A CN 110236990A CN 201910682711 A CN201910682711 A CN 201910682711A CN 110236990 A CN110236990 A CN 110236990A
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/9794—Liliopsida [monocotyledons]
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The invention discloses a kind of hydrolysis jojoba ester shin moisturizer comprising each component of following mass parts: 10 parts ~ 15 parts of water, 6 parts ~ 13 parts of Gotu Kola P.E, 6 parts ~ 10 parts of bladder-wrack extract, 8 parts ~ 12 parts of American aloe leaf extract, 14 parts ~ 20 parts of jojoba ester of hydrolysis, 5 parts ~ 12 parts of hyaluronic acid, 10 parts ~ 15 parts of glycerol, 6 parts ~ 10 parts of butanediol, 6 parts ~ 10 parts of citric acid and 6 parts ~ 10 parts of sodium citrate.The present invention also provides a kind of facial mask, which includes above-mentioned hydrolysis jojoba ester shin moisturizer.Above-mentioned hydrolysis jojoba ester shin moisturizer and facial mask, jojoba ester is replaced to be added using hydrolysis jojoba ester, hydrolysis jojoba ester is small-molecule substance, its soothing effect more persistence, so that the moistening effect of shin moisturizer and facial mask is more long-acting, to solve the problems, such as that the existing shin moisturizer containing jojoba ester or facial mask soothing effect are poor, the competitiveness of product in market is improved.
Description
Technical field
The present invention relates to daily chemical product technical fields, more particularly to a kind of hydrolysis jojoba ester shin moisturizer and facial mask.
Background technique
Jojoba ester is to be esterified Ester obtained after pulverizing purification by liquid extraction by the seed of Jojoba, is mended because it has
It fills the functions such as skin sebum, balance skin water loss and softening skin cutin and is widely used in shin moisturizer and facial mask, so that
It obtains skin to keep soft, there is elasticity and be chronically at the moist state of nature, while reaching and soothing the skin and improve skin sensitivity
The purpose of problem.
However, jojoba ester is long-chain unsaturated acid ester, molecular weight is larger, and jojoba ester penetrates the speed of skin surface
Relatively slow, the soothing effect duration is shorter, therefore, when jojoba ester is added to shin moisturizer or facial mask, applies shin moisturizer or makes
It can be come into force with long period product is needed after facial mask, and the soothing effect persistence of product is poor, to cause shin moisturizer and face
The overall skin effect of film is insufficient.
Summary of the invention
Based on this, it is necessary to for the technical problem of skin effect deficiency, provide a kind of hydrolysis jojoba ester shin moisturizer and
Facial mask.
A kind of hydrolysis jojoba ester shin moisturizer, the hydrolysis jojoba ester shin moisturizer include each component of following mass parts: water
10 parts ~ 15 parts, 6 parts ~ 13 parts of Gotu Kola P.E, 6 parts ~ 10 parts of bladder-wrack extract, 8 parts of American aloe leaf extract ~ 12 parts, water
14 parts ~ 20 parts of jojoba ester of solution, 5 parts ~ 12 parts of hyaluronic acid, 10 parts ~ 15 parts of glycerol, 6 parts ~ 10 parts of butanediol, 6 parts of citric acid ~
10 parts and 6 parts ~ 10 parts of sodium citrate.
Water is deionized water in one of the embodiments,.
In one of the embodiments, hydrolysis jojoba ester be jojoba ester hydrolysate through emulsification manufactured cream
Body.
The hydrolysate of jojoba ester is hydrolyzed system by jojoba ester under basic catalyst in one of the embodiments,
?.
Basic catalyst is one of sodium hydroxide, potassium hydroxide or calcium hydroxide in one of the embodiments,.
The hydrolysis temperature for hydrolyzing operation in one of the embodiments, is 80oC~100oC。
The concentration of hyaluronic acid is 0.05% ~ 0.5% in one of the embodiments,.
The concentration of citric acid is 1% ~ 2% in one of the embodiments,.
Hydrolysis jojoba ester shin moisturizer further includes 3 parts ~ 5 parts of aloe extract in one of the embodiments,.
The present invention also provides a kind of facial mask, which includes above-mentioned hydrolysis jojoba ester shin moisturizer.
Above-mentioned hydrolysis jojoba ester shin moisturizer and facial mask replace jojoba ester to be added, water using hydrolysis jojoba ester
Solution jojoba ester is small-molecule substance, soothing effect more persistence, even if still having height texture after water rinses, making
The moistening effect for obtaining shin moisturizer and facial mask is more long-acting, to solve the existing shin moisturizer containing jojoba ester or facial mask moisturizing
The problem of effect difference, improves the competitiveness of product in market.
Detailed description of the invention
Fig. 1 is the flow chart that the preparation method of jojoba ester is hydrolyzed in embodiment 1；
Fig. 2 is the flow chart that the preparation method of jojoba ester is hydrolyzed in embodiment 2；
Fig. 3 is the flow chart that the preparation method of jojoba ester is hydrolyzed in embodiment 3.
Specific embodiment
In order to make the foregoing objectives, features and advantages of the present invention clearer and more comprehensible, with reference to the accompanying drawing to the present invention
Specific embodiment be described in detail.Many details are explained in the following description in order to fully understand this hair
It is bright.But the invention can be embodied in many other ways as described herein, those skilled in the art can be not
Similar improvement is done in the case where violating intension of the present invention, therefore the present invention is not limited by the specific embodiments disclosed below.
Embodiment 1
The present invention provides a kind of hydrolysis jojoba ester shin moisturizer, which includes each group of following mass parts
Point: 10 parts of water, 13 parts of Gotu Kola P.E, 10 parts of bladder-wrack extract, 8 parts of American aloe leaf extract, hydrolysis jojoba ester 15
Part, 12 parts of hyaluronic acid, 10 parts of glycerol, 10 parts of butanediol, 6 parts of citric acid and 6 parts of sodium citrate.
Above-mentioned hydrolysis jojoba ester shin moisturizer replaces the biggish Jojoba of molecular weight using the hydrolysis jojoba ester of small molecule
Ester is added, and the hydrolysis jojoba ester of small molecule is easier to penetrate skin surface, in this way, after shin moisturizer is applied to skin, shield
Hydrolysis jojoba ester onset time in skin liquid is short, to accelerate the moisturizing rate of shin moisturizer.In addition, hydrolysis jojoba ester body
Product is smaller, easily in conjunction with keratoderma, even if skin surface still retains a large amount of small point of jojoba ester of hydrolysis after water flow is rinsed
The moistening effect of son, such shin moisturizer is more long-acting, to solve the soothing effect of the existing shin moisturizer containing jojoba ester
The problem of difference, to improve the competitiveness of product in market.It should be noted that hydrolysis jojoba ester shin moisturizer of the invention is not only
For being applied to human body face, moisturizing is continued to skin, so as to improve the skin quality of human body face, it may also be used for be applied to human body hand
Portion reduces the microgroove of hand to moisten hand skin.
Above-mentioned hydrolysis jojoba ester shin moisturizer the preparation method comprises the following steps: above-mentioned each component is added to heat preservation according to corresponding proportion
In bucket, the temperature of insulation barrel is increased to 75oC, and each component substance in insulation barrel is held with the stirring rate of 800r/min
Continuous stirring 30min, so that each component uniformly mixes, so that the hydrolysis jojoba ester shin moisturizer that property is uniform, stable is obtained, with
Guarantee the quality of product.
Water is mainly used as solvent, in order to which the extract of each component dissolves mixing in water, so that output is uniform, stable
Jojoba ester shin moisturizer is hydrolyzed, in this way, each section property is identical in hydrolysis jojoba ester shin moisturizer, in favor of controlling product matter
Amount.In the present embodiment, used water is deionized water, and deionized water refers to pure after eliminating the impurity in ionic species
In other words water eliminates mineral ion and the acid ion etc. in water, so that the pH value of water is maintained at 7, to eliminate mineral
The influence of each component in ion pair shin moisturizer can also prevent and generate precipitating in conjunction with acid ion because of mineral ion, in turn
The problem of causing clogging of pores.In addition, the acid-base property of solvent is made to keep neutral, solvent can be also reduced to the shadow of shin moisturizer pH value
It rings, in order to adjust the acid-base property of shin moisturizer by control each component content, in this way, passing through the shin moisturizer of same proportion production
Property it is identical, to ensure that the stability of product quality.
Centella, which has, helps skin growth, and collagen in skin corium is promoted to be formed, and realizes fibrin regeneration connection
The effect of.Specifically, by the way that Gotu Kola P.E is added in shin moisturizer, can firm skin epidermis and corium coupling part,
So that skin is limbered up, to improve cutis laxa phenomenon, achievees the effect that skin compact smooth.In addition, centella can also inhibit
The increase of fat cell prevents hydroderma, obesity occurs, that is to say, that hydrolysis jojoba ester shin moisturizer also has weight reducing function
Effect.
There are humectant properties to be therefore added to when by bladder-wrack extract for bladder-wrack glutamic acid rich in, glutamic acid
When shin moisturizer is smeared, the pliability and smoothness of skin can be improved, so that skin of releiving, achievees the purpose that improve skin quality.
The extract of American aloe is inhibited to hyaluronidase, and the decomposition of hyaluronic acid can be effectively suppressed, and saturating
Bright matter acid belongs to a kind of ingredient of human body, and with special Water-saving effect, in other words, American aloe can keep hyaluronidase
Activity reach skin effect to prevent skin water loss.In addition, American aloe extracting solution also acts as the moisturizing of cosmetics
Agent has the shin moisturizer of American aloe extracting solution by applying, can increase the water content of cuticula, further skin to be promoted to protect
It is wet, so as to improve skin state.
The hydrolysate that jojoba ester is jojoba ester is hydrolyzed, with jojoba ester supplement skin sebum, balance skin
The effect of skin water loss, can softening skin cutin, make skin keep soft, there is elasticity and be chronically at nature to moisten shape
State can also soothe the skin, and improve skin sensitivity problem.Due to hydrolyzing molecule of the strand compared to jojoba ester of jojoba ester
Chain is shorter, and molecular weight is smaller, is easier to mix with water, when that will hydrolyze jojoba ester and be added to shin moisturizer and applied, hydrolyzes
Jojoba ester is easier to go deep into skin corium by skin surface, and with skin corium cell combination, in this way, shin moisturizer be coated on skin surface
Afterwards, can quick acting, to improve the soothing effect of shin moisturizer.In addition, the substantial amounts of hydrolysis jojoba ester small molecule,
It is larger with the quantity of skin corium cell combination, it is not easy in a short time all failures, that is to say, that the moisturizing of shin moisturizer can be extended
Time, corresponding, it after shin moisturizer is coated on skin surface, is rinsed even across water flow, has still retained a large amount of water on skin
Jojoba ester is solved, to realize the long-acting moisturizing to skin.
Hyaluronic acid also known as sodium hyaluronate are a kind of acid mucopolysaccharides.Hyaluronic acid is to maintain the tender important foundation of skin water
Substance, while being also a kind of ingredient of human body, with special water retention, deal is more up to 100 times of itself weight,
It is the substance that moisture retention is best in presently found nature, referred to as ideal natural moisturizing factor.By by hyaluronic acid
It is added to shin moisturizer to be smeared, skin-nourishing metabolism can be improved, skin is made to become tender and smooth, skin is removed in realization
Wrinkle increases elasticity and prevents aging, can promote the absorption of skin moisturizing and skin to shin moisturizer, to improve the skin care of shin moisturizer
Effect.
It should be noted that, if the additive amount of hyaluronic acid is too low, easily causing skin care in the use process of hyaluronic acid
The moistening effect of liquid is insufficient, if counter osmosis easily occurs for the adding too much of hyaluronic acid, skin surface, so that skin table
The moisture of layer is flowed out through space between cells, to cause skin water shortage, deteriorates skin.In the present embodiment, use concentration for
0.05% middle-molecular-weihydroxyethyl hyaluronic acid is added.Middle-molecular-weihydroxyethyl hyaluronic acid has the effect of firm skin, long-acting moisturizing,
It can gradually form one layer of film for being rich in moisture in cuticula coated on after skin surface, to reduce the evaporation of moisture of skin,
Realize the moisturizing to skin.
Glycerol also known as glycerine, glycerol can dissolve part inorganic matter, therefore can be used as solvent and be added in shin moisturizer, with
Dissolution part is insoluble in the skin care components of water.Skin is carried out moist in addition, the glycerol of low concentration is alternatively arranged as lubricating oil, prevented
There is microgroove in turn in chapped skin.
Butanediol is a kind of polyalcohol, is used in cosmetics frequently as moisturizer and solvent.Since butanediol belongs to
Small-molecule substance, structure is relatively simple, and butanediol is compared with the macromolecular alcohol substance of equal quality, moisture in combination
Son amount is less, in this way, the water that can provide life condition for bacterium and impurity is less, that is to say, that bacterium in butanediol solvent
Amount is few, to reach the inhibiting effect to bacterium.In view of such characteristic of butanediol, it is added in shin moisturizer when by butanediol
Afterwards, it can inhibit the growth of bacterium in shin moisturizer, equally to guarantee safety that shin moisturizer uses.
Citric acid belongs to one kind of tartaric acid, is mainly used for accelerating cuticula update, is usually used in lotion, creams, shampoo, beauty
White articles, anti-aging articles, Acne etc..The update of cuticula facilitates the peeling of the middle melanin of skin, pore
Receive thin and dissolution of blackhead etc., that is to say, that by using citric acid, skin metabolism can be accelerated, assist in removing skin keratin,
To make skin become soft clean.But since citric acid belongs to acidic materials, if excessive addition, citric acid will burn skin
Skin causes keratoderma excessively thin, so that skin of face is red and swollen, is unfavorable for the health of skin.Therefore, in actual production, lemon
The concentration of lemon acid is no more than 4%, to prevent citric acid from excessively updating to skin.The concentration of citric acid used by the present embodiment
It is 1%, while guaranteeing that citric acid promotes cuticula to update, reduces it and burn to skin, to improve what skin care item used
Safety.
Sodium citrate is a kind of weak acid strong alkali salt, stronger pH buffer is constituted with citric acid cooperation, to solution
PH value is adjusted.Specifically, the skin of human body face is between 7.2 to 7.8, if the pH value and human body of used shin moisturizer
Face pH value difference it is larger when, the acid-base balance of human body face script will be destroyed, in this way, the flora type of human body face and
Quantity will change, to influence the skin quality of human body face.In the present embodiment, by adjusting the dense of citric acid and sodium citrate
Degree, is adjusted the pH value of shin moisturizer, so that initial pH value of the pH value of shin moisturizer as close as human body face, to subtract
Adverse effect of the small shin moisturizer to facial skin quality.
It should be noted that hydrolysis jojoba ester shin moisturizer further includes 5 parts of aloe extracts in an embodiment.In aloe
Polysaccharide and vitamin rich in, these polysaccharide and vitamin can provide human skin nutrition and moisten, and may additionally facilitate black
The decomposition of pigment, so that whiteness of skin.In addition, aloe also has the function of pore refining, cutin-softening layer and anti-inflammatory, aloe
In contain large quantity of moisture, it is sustainable to provide moisture for skin, realize the moisturizing to skin, help to prevent small wrinkle, eye pouch and
The problems such as cutis laxa.By the way that aloe extract to be added in shin moisturizer, while skin moisture-keeping is moistened in realization, may be used also
Anti-inflammatory is carried out to skin, to remove the small pox and acne on skin, realizes and the deep layer of skin is nursed.
Referring to Fig. 1, hydrolysis jojoba ester preparation method 10 the following steps are included:
Step S101: at room temperature, the jojoba ester and water that mass ratio is 1:5 is added in a kettle, forms jojoba ester and water
Mixed liquor.
Specifically, in the present embodiment, major ingredient of the jojoba ester as hydrolysis hydrolyzes jojoba ester for product
It generates and fatty acid radical ion is provided, water is used to provide hydrogen ion and hydroxide ion, the two and fat for hydrolysis
Acid ion combines, and generates the preferable fatty acid of dissolubility and alcohols material respectively.
Step S102: basic catalyst being added into mixed liquor, starts the blender of reaction kettle, stirs mixed liquor
It mixes.
Specifically, basic catalyst is used to provide hydroxide ion to mixed liquor, by destroying the acid-base balance of mixed liquor,
Promote the progress of hydrolysis.Under room temperature, slight ionization will occur in water for jojoba ester, generate a small amount of fatty acid radical from
Son, after basic catalyst is added in mixed liquor, basic catalyst will ionization generate free metal cation and hydroxyl from
Son, free hydroxide ion have broken the acid-base balance of mixed liquor, promote the water power in mixed liquor from generation hydrogen ion and hydrogen
Oxygen radical ion.The fatty acid radical ions binding that the hydrogen ion and hydroxide ion of generation will be generated with jojoba ester ionization, generates
Fatty acid substance and alcohols material dissociate jojoba ester further in conjunction with hydrogen ion and hydroxide ion, realize flash
The purpose of bar ester continued hydrolysis.In addition, neutralization reaction will occur with fatty acid for basic catalyst in hydrolysis reaction, generate
Fatty acid substance removes excessive hydroxide ion in mixed liquor, the safety used with guarantee hydrolysis jojoba ester.This reality
It applies in example, selects and be added to jojoba ester and water as basic catalyst for the sodium hydroxide of 1:1 with the molar ratio of jojoba ester
Mixed liquor in, the ionizing power of sodium hydroxide is strong, after being added to the water can fast dissociation generate a large amount of hydroxide ions, to promote
Into Jojoba ester hydrolysis, the content of jojoba ester is less in the present embodiment, hydrogen ion needed for hydrolysis and hydroxyl
Ion is also relatively fewer, therefore the sodium hydroxide by adding smaller concentration is the progress that can trigger hydrolysis.
Step S103: after stirring, starting the heater of reaction kettle, and the mixed liquor in reaction kettle is at the uniform velocity warming up to 80oC,
Heating-up time continues 1h.
Specifically, since hydrolysis is endothermic process, for the disconnected of the strand of promotion jojoba ester molecule and hydrone
Split and recombinate, the temperature of mixed liquor need to be improved, for hydrolysis carry out energy is provided.It in the present embodiment, will be in reaction kettle
The temperature of mixed liquor is at the uniform velocity warming up to 80oC, at this temperature, the covalent bond of jojoba ester molecule and the covalent bond of hydrone are obtained
It takes energy to be broken, then freely recombinates, generate various fatty acid and alcohols material.In addition, passing through the temperature for improving mixed liquor
Degree, can accelerate the movement velocity of fatty acid radical ion, hydrogen ion and hydroxide ion in mixed liquor, increase and collide between ion
The chance of contact further promotes the generation of hydrolysate.It is heated evenly for the mixed liquor in guarantee reaction kettle and improves water
The efficiency of reaction is solved, in the present embodiment, mixed liquor persistently overheating 1h, with this condition, mixeding liquid temperature Quick uniform rise,
Each section temperature is consistent in reaction kettle, effectively prevent heating rate is too fast to cause mixed liquor uneven heating problem and liter in reaction kettle
Warm rate reduces the appearance of hydrolysis efficiency slowly excessively.
Step S104: make mixed liquor 80oSustained response 6h at a temperature of C.
Specifically, sustained response for a period of time, jojoba ester need to be made at such a temperature after mixed liquor is warming up to steady temperature
It is sufficiently broken and recombinates with the strand of water, the content of jojoba ester as far as possible in reduction product, to improve the production of product
Efficiency guarantees the soothing effect of product.Smaller by jojoba ester concentration in this present embodiment, jojoba ester is 80oIt is held at a temperature of C
Continuous hydrolysis 6h can be depleted, and jojoba ester is completely converted into hydrolysis jojoba ester, ensure that product quality, improves utilization
The conversion ratio of jojoba ester production hydrolysis jojoba ester.
Step S105: after the completion of jojoba ester hydrolysis, starting the refrigerator of reaction kettle, and mixed liquor in reaction kettle is even
Speed is cooled to 50oC, temperature fall time continue 2h.
Specifically, by the way that the mixed liquor after hydrolysis to be adjusted to suitable emulsifying temperature, being subsequent in the present embodiment
Emulsion reaction provide condition, emulsion reaction process, and emulsifying device only needs to maintain the temperature is i.e. sustainable to be emulsified
Reaction, reduces equipment loss caused by the frequent heating and cooling of emulsifying device, extends the service life of emulsifying device.
Step S106: the mixed liquor after cooling down in reaction kettle is passed through in vacuum homogeneous emulsifying machine, 50oTo mixing under C
Liquid persistently emulsifies 60min.
Specifically, including fatty acid, alcohols material in the hydrolysis jojoba ester mixed liquor that reaction kettle is released after hydrolysis
And water, since the polarity of fatty acid, alcohols material and water is different, the substance in mixed liquor can not mutually fuse, at mixed liquor
In the state of water-oil separating, property is simultaneously unstable, affects the normal use of hydrolysis jojoba ester.Mixed liquor is in grease point
When from state, each liquid phase is immiscible each other, and there are interface, the molecule in same phase is difficult to shake off intermolecular two-phase adjacent
Active force and moved in adjacent phase, the surface tension overcome needed for molecule is larger, therefore need to provide energy for molecule to promote
The emulsification of mixed liquor is realized in the movement of different phase molecules.The present embodiment is using vacuum homogeneous emulsifying machine at relatively high temperatures to water
Solution jojoba ester mixed liquor is emulsified, and covers it by the high-speed rotating cutting wheel and fixed cutting of vacuum homogeneous emulsifying machine
Between generate the cutting of strength, impact and sinuous flow effect, cut mixed liquor in shearing seam, mixed liquor is broken into rapidly nanometer
The particle of grade, forms structure and the stable paste body shape of property hydrolyzes jojoba ester.Specifically, vacuum homogeneous emulsifying machine is 50oC item
Under part, cutting wheel cuts mixed liquor with the revolving speed of 15000r/min, higher emulsifying temperature and high-speed rotating cuts
It cuts the constraint that wheel shakes off surface tension for molecule and provides energy, so that molecule is shaken off the constraint of hydrogen bond, quickly enter other phases
It is interior in the phase in conjunction with molecule, molecule is difficult to restore to initial shape after leaving original phase under the premise of noenergy supply
State, to form stable paste body shape substance.
Step S107: will emulsify at a high speed post-job paste body shape collecting material into hydrops bucket, labelled, in sterile item
It is dried in the air naturally under part to room temperature to get hydrolysis jojoba ester is arrived.
Specifically, the hydrolysis jojoba ester lotion of preparation for being added in shin moisturizer, is imitated with improving the moisturizing of shin moisturizer
Fruit.It, need to be 5 after the completion of hydrolyzing the preparation of jojoba ester lotionoC to 15oIt stores or transports at a temperature of C, to prevent lotion temperature too low
And harden or lotion because temperature be too high softening decompose, formed grease, and then influence hydrolysis jojoba ester addition and make
With.It should be noted that shading treatment preferably is carried out to hydrolysis jojoba ester lotion in the storage and transport process of hydrolysis jojoba ester,
To prevent water solution jojoba ester from decomposing under action of ultraviolet radiation, to guarantee the quality of hydrolysis jojoba ester lotion.
Embodiment 2
The present invention provides a kind of hydrolysis jojoba ester shin moisturizer, which includes each group of following mass parts
Point: 12 parts of water, 7 parts of Gotu Kola P.E, 7 parts of bladder-wrack extract, 11 parts of American aloe leaf extract, hydrolysis jojoba ester 14
Part, 10 parts of hyaluronic acid, 13 parts of glycerol, 7 parts of butanediol, 8 parts of citric acid, 8 parts of sodium citrate and 3 parts of aloe extract.
Referring to Fig. 2, hydrolysis jojoba ester preparation method 20 the following steps are included:
Step S201: at room temperature, opening the feed inlet of reaction kettle, into reaction kettle be added mass ratio be 1:4 jojoba ester with
Water forms the mixed liquor of jojoba ester and water.
Step S202: the potassium hydroxide for being 1.8:1 with jojoba ester molar ratio is added into mixed liquor, then to mixed liquor
It is stirred.
Specifically, opening the blender of reaction kettle after potassium hydroxide is added to reaction kettle, making blender with 100r/min
Mixing speed 20min is persistently stirred to mixed liquor.Concentration by jojoba ester in this present embodiment is higher, triggers it and water occurs
The content of basic catalyst needed for solution reaction is also relatively high, and being chosen in the present embodiment with jojoba ester molar ratio is 1.8:1
Potassium hydroxide as basic catalyst.In actual production, the stronger lithium hydroxide of alkalinity also can be selected as base catalysis
Agent triggers the hydrolysis of jojoba ester, repeats no more in this.Ionization generates more hydrogen-oxygen after mixed liquor is added in potassium hydroxide
Radical ion and metal cation, and promote the hydrolytic dissociation generation in mixed liquor and the hydrogen ion of hydroxide ion equivalent, hydrogen ion
And the fatty acid radical ions binding that hydroxide ion continues and jojoba ester dissociation generates, fatty acid radical ion is consumed, quilt is balanced
Break, thus promotes the lasting progress of hydrolysis.Under the conditions of jojoba ester concentration is biggish, more jojoba ester molecules
Together by hydrogen bond firm connection, it so that jojoba ester is not easy to mix haptoreaction with water, in the present embodiment, is stirred by improving
It mixes the stirring rate of device and extends its mixing time, the stirring blade of blender beats jojoba ester micel under higher rotation speed
It dissipates, mixes jojoba ester uniformly in water, form jojoba ester solution.The extension of mixing time is conducive to water flow and smashes suddenly
Bar ester molecule group suddenly, prevents jojoba ester from failing to be dispersed in water, causes hydrolysis insufficient, in product it is remaining flash
The phenomenon that bar ester, occurs.
Step S203: mixed liquor after mixing evenly, starts the heater of reaction kettle, rises the mixed liquor in reaction kettle at the uniform velocity
Temperature is to 87oC, temperature-rise period continue 1.5h.
Specifically, larger by the concentration of jojoba ester in this present embodiment, the rate of hydrolysis is slower, therefore at this
In embodiment, the temperature in mixed liquor is at the uniform velocity warming up to 87oC, with this condition, jojoba ester molecule and hydrone heat absorption are more
Conversion of heat into kinetic energy that are more, obtaining, promote breaking of covalent bonds and the recombination of jojoba ester molecule and hydrone, are conducive to add
The progress of fast hydrolysis, improves the production efficiency of product.For guarantee mixed liquor the at the uniform velocity stable rising of temperature, in the present embodiment
In, the temperature-rise period of mixed liquor continues 1.5h, in the case, can prevent because mixed liquor heat up overrun, uneven heating occur heat
Liquid spattering problem improves the safety of operation.
Step S204: make mixed liquor 87oSustained response 10h at a temperature of C.
Specifically, the jojoba ester content due to the present embodiment is higher, to be fully hydrolyzed jojoba ester, product water is reduced
The residual of jojoba ester in jojoba ester is solved, to improve the soothing effect of product, in the present embodiment, hydrolysis is persistently carried out
10h guarantees product quality to guarantee the hydrolysis of the jojoba ester in mixed liquor totally.The fatty acid that jojoba ester hydrolysis generates will
Neutralization reaction occurs with the potassium hydroxide in mixed liquor, reduces the pH value of mixed liquor, prevents remaining in hydrolysis jojoba ester
Potassium hydroxide skin ambustion ensure that the safety that hydrolysis jojoba ester uses.
Step S205: after the completion of jojoba ester hydrolysis, start the refrigerator of reaction kettle, keep mixed liquor in reaction kettle even
Speed is cooled to 60oC, temperature fall time continue 1.8h.
Specifically, compared with Example 1, the temperature drop of mixed liquor is smaller in the present embodiment, therefore can suitably shorten cooling
Time with improve cooling operation efficiency.In the present embodiment, the predetermined temperature of mixed liquor cooling is the emulsification temperature of emulsion reaction
Degree provides energy by adjusting the temperature of mixed liquor for the constraint that all kinds of molecules in mixed liquor shake off congeneric elements, and adds
Moving freely for molecule of speed, and then improve the operating efficiency of subsequent emulsion reaction.
Step S206: opening reaction kettle, and the mixed liquor after cooling down in reaction kettle is passed through in vacuum homogeneous emulsifying machine,
60o50min is persistently emulsified to mixed liquor under C.
Specifically, in the present embodiment, the cutting wheel of vacuum homogeneous emulsifying machine with the revolving speed of 17000r/min to mixed liquor into
Row cutting, effectively increases the kinetic energy of molecular motion in each phase, and molecule is easier to shake off the constraint of congeneric elements and out-phase molecule knot
It closes, each component uniformly mixes in mixed liquor, forms homogeneous paste body shape substance, realizes the emulsification of hydrolysis jojoba ester.Pass through raising
The emulsifying temperature of jojoba ester is hydrolyzed, higher thermal energy is obtained convenient for molecule, is then changed into the kinetic energy of molecule, accelerates emulsification anti-
The progress answered, so the present embodiment, which only needs 50min can be completed, emulsifies operation to the high speed of hydrolysis jojoba ester.
Step S207: will emulsify at a high speed post-job paste body shape collecting material into hydrops bucket, labelled, in sterile item
It is dried in the air naturally under part to room temperature to get hydrolysis jojoba ester is arrived.
Hydrolyzed as made from above-mentioned condition jojoba ester concentration be higher than obtained hydrolysis under the conditions of embodiment 1 flash
The concentration of bar ester, therefore, the present embodiment only need the paste hydrolysis jojoba ester of addition less volume that can meet matching for shin moisturizer
Than requiring, to realize the nursing efficacy to skin.
In one embodiment, the concentration of hyaluronic acid is 0.3%.By improving the concentration of hyaluronic acid, shin moisturizer pair can be reinforced
The moistening effect of skin further promotes the skin-care effect of shin moisturizer.It should be noted that in the present embodiment, citric acid it is dense
Degree is 1.8%.By the concentration of raising citric acid, skin metabolism can be further speeded up, quickly removes the cutin of skin surface,
That is the dead skin of skin surface quickly can be removed, thus the effect of reaching cleaning skin, softening skin.
Embodiment 3
The present invention provides a kind of hydrolysis jojoba ester shin moisturizer, which includes each group of following mass parts
Point: 15 parts of water, 6 parts of Gotu Kola P.E, 6 parts of bladder-wrack extract, 12 parts of American aloe leaf extract, hydrolysis jojoba ester 20
Part, 5 parts of hyaluronic acid, 10 parts of glycerol, 6 parts of butanediol, 10 parts of citric acid and 10 parts of sodium citrate.
Referring to Fig. 3, hydrolysis jojoba ester preparation method 30 the following steps are included:
Step S301: at room temperature, opening the feed inlet of reaction kettle, into reaction kettle be added mass ratio be 1:3 jojoba ester with
Water forms the mixed liquor of jojoba ester and water.
Step S302: the calcium hydroxide for being 2.2:1 with jojoba ester molar ratio is added into mixed liquor, then to mixed liquor
It is stirred.
Specifically, opening the blender of reaction kettle after calcium hydroxide is added to reaction kettle, making blender with 120r/min
Mixing speed 25min is persistently stirred to mixed liquor.Basic catalyst used by the present embodiment is calcium hydroxide, calcium hydroxide
It is completely dissociated into after being dissolved in water, provides hydroxide ion for Jojoba ester hydrolysis, to trigger the progress of hydrolysis, and it is produced
Cost is relatively low, simple and easy to get, can effectively reduce the production cost of hydrolysis jojoba ester.In the present embodiment jojoba ester concentration compared with
Greatly, a large amount of jojoba ester molecules are firmly combined together by hydrogen bond, so that jojoba ester is not easy to mix haptoreaction with water, lead to
The stirring rate for improving blender is crossed, the stirring blade of blender breaks up jojoba ester micel under higher rotation speed, shortens
Jojoba ester and the distance between hydrone and basic catalyst, dissociate fatty acid radical ion, hydrogen ion and the hydrogen-oxygen of generation
Radical ion can combine rapidly recombination, effectively increase the production efficiency of hydrolysis jojoba ester.
Step S303: mixed liquor after mixing evenly, starts the heater of reaction kettle, rises the mixed liquor in reaction kettle at the uniform velocity
Temperature is to 100oC, temperature-rise period continue 1.8h.
Specifically, jojoba ester all in mixed liquor point can be made by the reaction temperature for further increasing jojoba ester
Son and hydrone obtain biggish kinetic energy to shake off the constraint of covalent bond, and then fracture recombination, is fully hydrolyzed jojoba ester.For
Prevent heating from overrunning, hydrothermal solution spattering problem caused by mixed liquor uneven heating, temperature-rise period continues 1.8h in the present embodiment, herein
Under the conditions of can guarantee the at the uniform velocity stable rising of mixeding liquid temperature, improve the safety of operation.
Step S304: make mixed liquor 100oSustained response 14h at a temperature of C.
Specifically, in the present embodiment, extend the time of jojoba ester hydrolysis, be conducive to make in mixed liquor everywhere flash
Bar ester is fully hydrolyzed, and prevents from carrying unhydrolysed jojoba ester in product secretly, ensure that the quality of product hydrolysis jojoba ester.
Step S305: after the completion of hydrolysis, start the refrigerator of reaction kettle, be cooled to mixed liquor in reaction kettle at the uniform velocity
70oC, temperature fall time continue 1.5h.
Specifically, the temperature drop for the operation that cools down in the present embodiment further decreases, if sharply cooling down to mixed liquor, hydrolysis is suddenly
Esterification is occurred for part by bar ester suddenly, influences the hydrolysis effect of jojoba ester, it is difficult to be guaranteed the quality of hydrolysis jojoba ester, be led to
The 1.5h that at the uniform velocity cools down to mixed liquor is crossed to emulsifying temperature, is conducive to while guaranteeing that hydrolysis jojoba ester mixed liquor characteristics are stablized
Improve the efficiency of cooling operation.
Step S306: opening reaction kettle, and the mixed liquor after cooling down in reaction kettle is passed through in vacuum homogeneous emulsifying machine,
70o40min is persistently emulsified to mixed liquor under C.
Specifically, the concentration of the jojoba ester of the present embodiment is larger, that is, the content for hydrolyzing jojoba ester is higher, to promote
It hydrolyzes jojoba ester mixed liquor each component and forms isotropic stable structure, guarantee the quality of hydrolysis jojoba ester, in the present embodiment,
The cutting wheel of vacuum homogeneous emulsifying machine cuts mixed liquor with the revolving speed of 20000r/min, makes the individual molecule in mixed liquor
High-energy can be obtained to shake off the constraint of congeneric elements, out of phase molecule is mutually fused, forms the stable cream of structural property
Body shape substance realizes the emulsification of hydrolysis jojoba ester.The emulsifying temperature as provided by the present embodiment further increases, and single point
The energy that son obtains greatly improves, and is easier to leave this mutually in conjunction with out-phase molecule, therefore the present embodiment only needs 40min can be completed
Operation is emulsified to the high speed of hydrolysis jojoba ester.
Step S307: will emulsify at a high speed post-job paste body shape collecting material into hydrops bucket, labelled, in sterile item
It is dried in the air naturally under part to room temperature to get hydrolysis jojoba ester is arrived.
Specifically, the concentration for hydrolyzing jojoba ester as made from above-mentioned condition is higher than under the conditions of embodiment 1 and embodiment 2
The concentration of obtained hydrolysis jojoba ester, therefore, the present embodiment only need the paste hydrolysis jojoba ester of addition less volume i.e.
The ratio requirement of shin moisturizer can be met, to realize the nursing efficacy to skin.
In one embodiment, the concentration of hyaluronic acid is 0.5%.By further promoting the concentration of hyaluronic acid, shield can be promoted
The moistening effect of skin liquid, however, counter osmosis will occur for skin surface if the concentration of constantly improve hyaluronic acid, so that skin
The moisture of skin script is flowed out via skin surface cell gap, skin water shortage will be so caused, to influence the skin care of shin moisturizer
Therefore effect should not continue the concentration for improving hyaluronic acid.
In one embodiment, the concentration of citric acid is 2%.By further promoting the concentration of citric acid, shin moisturizer pair can be reinforced
The renewal rate of skin, but since citric acid is acidic materials, and the pH value meta-alkalescence of human body face, if continuing to improve citric acid
Concentration, citric acid will generate neutralization reaction with the substance on human body face surface layer, and then ablation skin influences skin health, because
This, should not continue the concentration for improving citric acid.
The present invention also provides a kind of facial mask, which includes above-mentioned hydrolysis jojoba ester shin moisturizer, by non-woven fabrics in water
It solves to impregnate in jojoba ester shin moisturizer and be made.
Specifically, non-woven fabrics is cut to predetermined size, which can be completely covered human body face with non-woven fabrics and be
Standard then further cuts on the non-woven fabrics of predetermined size, reserves hole, to obtain facial mask cloth.By in non-woven fabrics
Upper reserving hole, the corresponding sites such as eyes, nose and the mouth of such human body expose, and object is breathed or normally regarded in order to user,
Guarantee that the safety of facial-care carries out.It after facial mask cloth is tailored, by facial mask cloth retort sterilization, and dries, to remove facial mask cloth
On bacteria impurities, realize to the aseptic process of facial mask.After facial mask cloth aseptic process, facial mask cloth is soaked in hydrolysis jojoba ester
In shin moisturizer, make hydrolyze jojoba ester shin moisturizer complete wetting facial mask cloth, then by the facial mask after infiltration be distributed into bag encapsulation to get
To facial mask.
Above-mentioned facial mask replaces jojoba ester to be added using hydrolysis jojoba ester, and hydrolysis jojoba ester is small molecule object
Matter, soothing effect more persistence, even if still there is height texture, so that the moistening effect of facial mask is more after water rinses
It is long-acting, to solve the problems, such as that the existing facial mask soothing effect containing jojoba ester is poor, improve the competitiveness of product in market.
Each technical characteristic of embodiment described above can be combined arbitrarily, for simplicity of description, not to above-mentioned reality
It applies all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited
In contradiction, all should be considered as described in this specification.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously
It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art
It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection of the invention
Range.Therefore, the scope of protection of the patent of the invention shall be subject to the appended claims.
Claims (10)
1. a kind of hydrolysis jojoba ester shin moisturizer, which is characterized in that each component including following mass parts: 10 parts ~ 15 parts of water, product
Avenge careless 6 parts ~ 13 parts of extract, 6 parts ~ 10 parts of bladder-wrack extract, 8 parts ~ 12 parts of American aloe leaf extract, hydrolysis jojoba ester 14
Part ~ 20 parts, 5 parts ~ 12 parts of hyaluronic acid, 10 parts ~ 15 parts of glycerol, 6 parts ~ 10 parts of butanediol, 6 parts ~ 10 parts of citric acid and citric acid
6 parts ~ 10 parts of sodium.
2. hydrolysis jojoba ester shin moisturizer according to claim 1, which is characterized in that the water is deionized water.
3. hydrolysis jojoba ester shin moisturizer according to claim 1, which is characterized in that the hydrolysis jojoba ester be flash
Bar ester hydrolysis product manufactured lotion through emulsification.
4. hydrolysis jojoba ester shin moisturizer according to claim 3, which is characterized in that the hydrolysate of the jojoba ester
It is hydrolyzed and is made under basic catalyst by jojoba ester.
5. hydrolysis jojoba ester shin moisturizer according to claim 4, which is characterized in that the basic catalyst is hydroxide
One of sodium, potassium hydroxide or calcium hydroxide.
6. hydrolysis jojoba ester shin moisturizer according to claim 4, which is characterized in that the hydrolysis temperature of the hydrolysis operation
It is 80oC~100oC。
7. hydrolysis jojoba ester shin moisturizer according to claim 1, which is characterized in that the concentration of the hyaluronic acid is
0.05%~0.5%。
8. hydrolysis jojoba ester shin moisturizer according to claim 1, which is characterized in that the concentration of the citric acid be 1% ~
2%。
9. hydrolysis jojoba ester shin moisturizer according to claim 1, which is characterized in that the hydrolysis jojoba ester shin moisturizer
It further include 3 parts ~ 5 parts of aloe extract.
10. a kind of facial mask, which is characterized in that including the described in any item hydrolysis jojoba ester shin moisturizer of claim 1 to 9.
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Cited By (1)
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| CN111568807A (en) * | 2020-04-20 | 2020-08-25 | 上海九乙生物科技有限公司 | Preparation process and application of hydrolyzed jojoba ester semitransparent system |
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Application publication date: 20190917 |