CN110230216A - A kind of Lyocell fibers fabric of natural dye dying and preparation method thereof - Google Patents
A kind of Lyocell fibers fabric of natural dye dying and preparation method thereof Download PDFInfo
- Publication number
- CN110230216A CN110230216A CN201910463379.2A CN201910463379A CN110230216A CN 110230216 A CN110230216 A CN 110230216A CN 201910463379 A CN201910463379 A CN 201910463379A CN 110230216 A CN110230216 A CN 110230216A
- Authority
- CN
- China
- Prior art keywords
- lyocell fibers
- natural dye
- fibers fabric
- fabric
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000004744 fabric Substances 0.000 title claims abstract description 83
- 229920000433 Lyocell Polymers 0.000 title claims abstract description 78
- 229930182559 Natural dye Natural products 0.000 title claims abstract description 46
- 239000000978 natural dye Substances 0.000 title claims abstract description 46
- 238000002360 preparation method Methods 0.000 title claims abstract description 31
- 238000004043 dyeing Methods 0.000 claims abstract description 31
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 20
- 235000004256 Buglossoides arvense Nutrition 0.000 claims abstract description 11
- 235000000177 Indigofera tinctoria Nutrition 0.000 claims abstract description 11
- 241000118841 Lithospermum incisum Species 0.000 claims abstract description 11
- 229940097275 indigo Drugs 0.000 claims abstract description 11
- COHYTHOBJLSHDF-UHFFFAOYSA-N indigo powder Natural products N1C2=CC=CC=C2C(=O)C1=C1C(=O)C2=CC=CC=C2N1 COHYTHOBJLSHDF-UHFFFAOYSA-N 0.000 claims abstract description 11
- 241000123069 Ocyurus chrysurus Species 0.000 claims abstract description 10
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 28
- 239000000975 dye Substances 0.000 claims description 24
- 238000003756 stirring Methods 0.000 claims description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 21
- 150000001768 cations Chemical class 0.000 claims description 19
- 239000000243 solution Substances 0.000 claims description 19
- 239000003607 modifier Substances 0.000 claims description 18
- XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 claims description 16
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 claims description 16
- CTKINSOISVBQLD-UHFFFAOYSA-N Glycidol Chemical compound OCC1CO1 CTKINSOISVBQLD-UHFFFAOYSA-N 0.000 claims description 14
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- -1 Polyethylene Polymers 0.000 claims description 12
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 12
- 238000001035 drying Methods 0.000 claims description 12
- 239000007864 aqueous solution Substances 0.000 claims description 10
- 239000004698 Polyethylene Substances 0.000 claims description 8
- NJSSICCENMLTKO-HRCBOCMUSA-N [(1r,2s,4r,5r)-3-hydroxy-4-(4-methylphenyl)sulfonyloxy-6,8-dioxabicyclo[3.2.1]octan-2-yl] 4-methylbenzenesulfonate Chemical compound C1=CC(C)=CC=C1S(=O)(=O)O[C@H]1C(O)[C@@H](OS(=O)(=O)C=2C=CC(C)=CC=2)[C@@H]2OC[C@H]1O2 NJSSICCENMLTKO-HRCBOCMUSA-N 0.000 claims description 8
- 229910001870 ammonium persulfate Inorganic materials 0.000 claims description 8
- 239000003999 initiator Substances 0.000 claims description 8
- 239000007788 liquid Substances 0.000 claims description 8
- 239000011259 mixed solution Substances 0.000 claims description 8
- 229960000583 acetic acid Drugs 0.000 claims description 6
- FPCJKVGGYOAWIZ-UHFFFAOYSA-N butan-1-ol;titanium Chemical compound [Ti].CCCCO.CCCCO.CCCCO.CCCCO FPCJKVGGYOAWIZ-UHFFFAOYSA-N 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 6
- 239000012362 glacial acetic acid Substances 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 6
- 238000007654 immersion Methods 0.000 claims description 6
- 238000002386 leaching Methods 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 6
- 238000012545 processing Methods 0.000 claims description 6
- 239000002202 Polyethylene glycol Substances 0.000 claims description 5
- 229920001223 polyethylene glycol Polymers 0.000 claims description 5
- 239000008367 deionised water Substances 0.000 claims description 2
- 229910021641 deionized water Inorganic materials 0.000 claims description 2
- 229920000573 polyethylene Polymers 0.000 claims description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- 238000005406 washing Methods 0.000 abstract description 3
- 230000009467 reduction Effects 0.000 abstract description 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 11
- 229910017604 nitric acid Inorganic materials 0.000 description 10
- 235000011121 sodium hydroxide Nutrition 0.000 description 5
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 4
- 230000008859 change Effects 0.000 description 4
- 239000000835 fiber Substances 0.000 description 4
- 230000005484 gravity Effects 0.000 description 4
- 229940068918 polyethylene glycol 400 Drugs 0.000 description 3
- 229920003043 Cellulose fiber Polymers 0.000 description 2
- RGCKGOZRHPZPFP-UHFFFAOYSA-N alizarin Chemical compound C1=CC=C2C(=O)C3=C(O)C(O)=CC=C3C(=O)C2=C1 RGCKGOZRHPZPFP-UHFFFAOYSA-N 0.000 description 2
- 229920002678 cellulose Polymers 0.000 description 2
- 239000001913 cellulose Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 231100001261 hazardous Toxicity 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012805 post-processing Methods 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
- D06P1/5207—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- D06P1/5214—Polymers of unsaturated compounds containing no COOH groups or functional derivatives thereof
- D06P1/5242—Polymers of unsaturated N-containing compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/002—Locally enhancing dye affinity of a textile material by chemical means
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/10—After-treatment with compounds containing metal
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Coloring (AREA)
Abstract
Description
Claims (7)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201910463379.2A CN110230216B (en) | 2019-05-30 | 2019-05-30 | Lyocell fiber fabric dyed by natural dye and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201910463379.2A CN110230216B (en) | 2019-05-30 | 2019-05-30 | Lyocell fiber fabric dyed by natural dye and preparation method thereof |
Publications (2)
Publication Number | Publication Date |
---|---|
CN110230216A true CN110230216A (en) | 2019-09-13 |
CN110230216B CN110230216B (en) | 2020-07-28 |
Family
ID=67858230
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201910463379.2A Active CN110230216B (en) | 2019-05-30 | 2019-05-30 | Lyocell fiber fabric dyed by natural dye and preparation method thereof |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN110230216B (en) |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111471316A (en) * | 2020-03-19 | 2020-07-31 | 当阳市鸿阳新材料科技有限公司 | Extraction method of microbial pigment and method for dyeing lyocell fibers by using microbial pigment |
CN112252054A (en) * | 2020-09-22 | 2021-01-22 | 鲁泰纺织股份有限公司 | Method for dyeing pure cotton yarn on line by vegetable dye |
CN112323513A (en) * | 2020-10-13 | 2021-02-05 | 武汉纺织大学 | Blue Lyocell fabric prepared by dyeing plant dye hyacinth and preparation method thereof |
CN112411202A (en) * | 2020-10-13 | 2021-02-26 | 武汉纺织大学 | Black lyocell fabric prepared by dyeing plant dye black fig and preparation method thereof |
CN112482052A (en) * | 2020-10-13 | 2021-03-12 | 武汉纺织大学 | Green lyocell fabric prepared by dyeing with rosemary serving as vegetable dye and preparation method of green lyocell fabric |
CN112501925A (en) * | 2020-10-13 | 2021-03-16 | 武汉纺织大学 | Brown Lyocell fabric prepared by dyeing chestnut peels with vegetable dye and preparation method thereof |
CN112680971A (en) * | 2020-12-24 | 2021-04-20 | 创姿服饰(上海)有限公司 | Fabric with excellent performance and application thereof in field of clothes |
CN114703688A (en) * | 2022-04-29 | 2022-07-05 | 武汉纺织大学 | Black lyocell fabric prepared by dyeing animal dye gallnut and preparation method thereof |
WO2024038442A1 (en) * | 2022-08-14 | 2024-02-22 | Sonoviatech Ltd. | Compositions and methods for indigo dyeing |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103015239A (en) * | 2012-12-29 | 2013-04-03 | 福建清源科技有限公司 | Polydimethyldiallylammonium chloride modified color fixing agent and preparation method thereof |
CN105648745A (en) * | 2016-04-01 | 2016-06-08 | 陕西科技大学 | Polymer-based cerium-doped nano zinc oxide compound antibacterial agent for fabric and preparation method thereof |
CN106283617A (en) * | 2016-09-13 | 2017-01-04 | 陕西科技大学 | Bafta polymer/Ag dopen Nano ZnO long acting antibiotic mildew-proofing finishing agent and preparation method thereof |
-
2019
- 2019-05-30 CN CN201910463379.2A patent/CN110230216B/en active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103015239A (en) * | 2012-12-29 | 2013-04-03 | 福建清源科技有限公司 | Polydimethyldiallylammonium chloride modified color fixing agent and preparation method thereof |
CN105648745A (en) * | 2016-04-01 | 2016-06-08 | 陕西科技大学 | Polymer-based cerium-doped nano zinc oxide compound antibacterial agent for fabric and preparation method thereof |
CN106283617A (en) * | 2016-09-13 | 2017-01-04 | 陕西科技大学 | Bafta polymer/Ag dopen Nano ZnO long acting antibiotic mildew-proofing finishing agent and preparation method thereof |
Non-Patent Citations (3)
Title |
---|
任安民等: "天然染料对阳离子改性棉针织物的无媒染色实践", 《印染》 * |
朱敏等: "AM-AGE-DMDAAC 共聚阳离子改性剂的合成及应用", 《印染》 * |
路艳华: "《天然染料在真丝染色中的应用》", 31 January 2017, 中国纺织出版社 * |
Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111471316A (en) * | 2020-03-19 | 2020-07-31 | 当阳市鸿阳新材料科技有限公司 | Extraction method of microbial pigment and method for dyeing lyocell fibers by using microbial pigment |
CN112252054A (en) * | 2020-09-22 | 2021-01-22 | 鲁泰纺织股份有限公司 | Method for dyeing pure cotton yarn on line by vegetable dye |
CN112323513A (en) * | 2020-10-13 | 2021-02-05 | 武汉纺织大学 | Blue Lyocell fabric prepared by dyeing plant dye hyacinth and preparation method thereof |
CN112411202A (en) * | 2020-10-13 | 2021-02-26 | 武汉纺织大学 | Black lyocell fabric prepared by dyeing plant dye black fig and preparation method thereof |
CN112482052A (en) * | 2020-10-13 | 2021-03-12 | 武汉纺织大学 | Green lyocell fabric prepared by dyeing with rosemary serving as vegetable dye and preparation method of green lyocell fabric |
CN112501925A (en) * | 2020-10-13 | 2021-03-16 | 武汉纺织大学 | Brown Lyocell fabric prepared by dyeing chestnut peels with vegetable dye and preparation method thereof |
CN112501925B (en) * | 2020-10-13 | 2022-09-09 | 江苏苏美达轻纺科技产业有限公司 | Brown Lyocell fabric prepared by dyeing chestnut peels with vegetable dye and preparation method thereof |
CN112323513B (en) * | 2020-10-13 | 2023-02-28 | 武汉纺织大学 | Blue Lyocell fabric prepared by dyeing plant dye hyacinth and preparation method thereof |
CN112411202B (en) * | 2020-10-13 | 2023-02-28 | 武汉纺织大学 | Black Lyocell fabric prepared by dyeing plant dye black cone and preparation method thereof |
CN112680971A (en) * | 2020-12-24 | 2021-04-20 | 创姿服饰(上海)有限公司 | Fabric with excellent performance and application thereof in field of clothes |
CN114703688A (en) * | 2022-04-29 | 2022-07-05 | 武汉纺织大学 | Black lyocell fabric prepared by dyeing animal dye gallnut and preparation method thereof |
WO2024038442A1 (en) * | 2022-08-14 | 2024-02-22 | Sonoviatech Ltd. | Compositions and methods for indigo dyeing |
Also Published As
Publication number | Publication date |
---|---|
CN110230216B (en) | 2020-07-28 |
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Legal Events
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PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
TA01 | Transfer of patent application right | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20200630 Address after: 444199 No. 333 Changban Road, Dangyang City, Yichang City, Hubei Province (Jinqiao Industrial Park) Applicant after: Dangyang Hongyang New Material Technology Co.,Ltd. Address before: 444199 No. 333 Changban Road, Dangyang City, Yichang City, Hubei Province (Jinqiao Industrial Park) Applicant before: Dangyang Hongyang New Material Technology Co.,Ltd. Applicant before: Wuhan Textile University |
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GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20240614 Address after: 444100 Baling Village, Baling Office, Dangyang City, Yichang City, Hubei Province Patentee after: HUBEI XINYANG SPECIAL FIBER Co.,Ltd. Country or region after: China Address before: 444199 333 changchangban Road, Dangyang city, Yichang City, Hubei Province (Jinqiao Industrial Park) Patentee before: Dangyang Hongyang New Material Technology Co.,Ltd. Country or region before: China |