CN110205064A - A kind of disposable sanitary articles scrape gluing method with impervious hot melt adhesive and coating - Google Patents
A kind of disposable sanitary articles scrape gluing method with impervious hot melt adhesive and coating Download PDFInfo
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- CN110205064A CN110205064A CN201910489257.0A CN201910489257A CN110205064A CN 110205064 A CN110205064 A CN 110205064A CN 201910489257 A CN201910489257 A CN 201910489257A CN 110205064 A CN110205064 A CN 110205064A
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- CN
- China
- Prior art keywords
- hot melt
- melt adhesive
- disposable sanitary
- sanitary articles
- impervious
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J157/00—Adhesives based on unspecified polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C09J157/02—Copolymers of mineral oil hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Absorbent Articles And Supports Therefor (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
The invention discloses a kind of disposable sanitary articles to scrape gluing method with impervious hot melt adhesive and coating, the hot melt adhesive is made of main polymer, tackifying resin, White Mineral Oil, processing aid and antioxidant, the coating scrapes gluing method the following steps are included: being added in size applicator after above-mentioned disposable sanitary articles are melted with impervious hot melt adhesive, sizing face on size applicator matches with substrate surface structure, glue is coated on making hole film or non-woven fabrics base material again, substrate is bonded again, is bonded.Gluing method is scraped in the impervious hot melt adhesive of disposable sanitary articles of the invention and coating can substantially reduce strike-through in Process of Applying Glue, improve product quality, while not will increase production cost and technology difficulty, will not impact to adhesive property.
Description
Technical field
The present invention relates to a kind of disposable sanitary articles to scrape gluing method with impervious hot melt adhesive and coating.
Background technique
Hot melt adhesive is a kind of adhesive of plasticity, its physical state changes with temperature and changed in certain temperature range
Become, and chemical characteristic is constant, it is non-toxic and tasteless, belong to environmental-protecting chemical product, is widely used in hygienic articles, packaging, book
Nationality bookbinding, clothes, adhesive tape, shoemaking, refrigerator, cable, automobile and other industries.
It is hygienic articles, clothes, glue stick, books and packaging respectively that domestic hot melt adhesive market, which accounts for former industries, wherein
Hygienic articles are ranked first with glue, and in hygienic articles accounting it is maximum be sanitary napkin and baby paper diaper both disposably defend
Raw articles.Disposable sanitary articles are the market of a high speed development with hot melt adhesive market, and the past 10 years fitting growth rates are high
Up to 16%.In order to meet the great market demand of disposable sanitary articles, sanitary napkin, diaper production lines linear speed need to improve
Even higher to 800~1000 pieces/minute, the ground that hot melt adhesive is bonded is also more and more thinner, and the use of perforated material is got over
Come more frequent, leads to that it is easy to appear strike-throughs.Strike-through not only will affect the normal operation of production line, reduce production efficiency, and
Can also make a big impact to the quality of product (such as: strike-through will cause adhesion between product, and when use can only tear viscous by force
Product even, it is easy to lead to product breakage).
Currently, solving the problems, such as the method for strike-through mainly include the following types: 1) being adjusted to product core；2) to heat
Melten gel formula is adjusted, and adjusts curing time；3) glue consumption is reduced.Although three of the above method can be to a certain extent
Strike-through is reduced, but also results in the problems such as the production cost increases, technology difficulty increases, cohesive force is inadequate simultaneously.
Summary of the invention
The purpose of the present invention is to provide a kind of disposable sanitary articles to scrape gluing method with impervious hot melt adhesive and coating.
The technical solution used in the present invention is:
A kind of impervious hot melt adhesive of disposable sanitary articles, consists of the following mass percentage components:
Main polymer: 10%~20%；
Tackifying resin: 45%~55%；
White Mineral Oil: 15%~25%；
Processing aid: 5%~10%；
Antioxidant: 0.1%~0.5%.
Preferably, the impervious hot melt adhesive of a kind of disposable sanitary articles, consists of the following mass percentage components:
Main polymer: 14%~20%；
Tackifying resin: 50%~55%；
White Mineral Oil: 20%~25%；
Processing aid: 5%~10%；
Antioxidant: 0.1%~0.5%.
Preferably, the main polymer is that Styrene-Butadiene-Styrene Block Copolymer (SBS), styrene-are different
Isoprene-styrene block copolymer (SIS), styrene-ethylene-butylene-styrene block copolymer (SEBS), ethylene-vinegar
At least one of sour ethylene copolymer (EVA).
Preferably, diblock is free of in the Styrene-Butadiene-Styrene Block Copolymer.
Preferably, the mass percentage of styrene is in the styrene-isoprene-styrene block copolymer
35%~40%.
Preferably, the tackifying resin is at least one of Petropols, hydrogenated petroleum resin.
Preferably, the Petropols are at least one of C5 Petropols, C9 Petropols, DCPD Petropols.
Preferably, the hydrogenated petroleum resin is C5 hydrogenated petroleum resin, C9 hydrogenated petroleum resin, DCPD hydrotreated petroleum tree
At least one of rouge.
Preferably, the mass percentage of cycloalkane is greater than 40% in the White Mineral Oil.
Preferably, the processing aid is at least one of linear low density polyethylene, Fischer-Tropsch wax, PE wax, PP wax.
Preferably, the antioxidant is antioxidant 1010, irgasfos 168, antioxidant CA, at least one in antioxidant BHT
Kind.
The preparation method of the impervious hot melt adhesive of above-mentioned disposable sanitary articles is the following steps are included: by main polymer, increase
Viscosity resin, White Mineral Oil, processing aid and antioxidant are uniformly mixed, and are again heated to 145~160 DEG C, and it is complete to material to vacuumize stirring
Full-fusing, then stop stirring, it is evacuated to bubble-free in material, obtains disposable sanitary articles with impervious hot melt adhesive.
A kind of coating of disposable sanitary articles scrapes gluing method the following steps are included: by above-mentioned disposable sanitary articles with anti-
It is added in size applicator, then glue is coated on making hole film or non-woven fabrics base material, then substrate is bonded after seeping hot melt adhesive melting, into
Row bonding；The sizing face of the size applicator matches with substrate surface structure.
Preferably, the size applicator is made of two application rolls, and it is convex that the surface staggered row of an application roll shows diamond shape
It rises, and is additionally provided with several micropores between adjacent diamond shape protrusion, the surface staggered row of another application roll is shown convex with diamond shape
The diamond sunk to match is acted, and is additionally provided with several micropores between adjacent diamond sunk.
The beneficial effects of the present invention are: disposable sanitary articles of the invention scrape gluing method with impervious hot melt adhesive and coating can
To substantially reduce the strike-through in Process of Applying Glue, product quality is improved, while not will increase production cost and technology difficulty, also not
Adhesive property can be impacted.
1) the initial bonding force of the impervious hot melt adhesive of disposable sanitary articles of the invention is big, and curing time is moderate, even if
It carries out high speed sizing and is also not easy strike-through occur；
2) coating of the invention is scraped gluing method and is simple and efficient, and can not only effectively reduce the strike-through in Process of Applying Glue, and not
It needs to reduce resin added and adjustment product core, and then cohesive force will not be reduced and increase production cost.
Detailed description of the invention
Fig. 1 is the infrared spectrogram of the impervious hot melt adhesive of disposable sanitary articles of embodiment 1.
Fig. 2 is the structural schematic diagram of two application rolls in size applicator of the invention.
Specific embodiment
The present invention will be further explained combined with specific embodiments below and explanation.
Embodiment 1:
A kind of impervious hot melt adhesive of disposable sanitary articles, raw material composition are as shown in the table:
A kind of raw material of the impervious hot melt adhesive of the disposable sanitary articles of table 1 forms table
The preparation method of the impervious hot melt adhesive of above-mentioned disposable sanitary articles is the following steps are included: by styrene-butadiene-
Styrene block copolymer, C5 Petropols, White Mineral Oil, PE wax and antioxidant 1010 are uniformly mixed, and are again heated to 155 DEG C, are taken out
Vacuum stirring melts completely to material, then stops stirring, and is evacuated to bubble-free in material, and it is anti-to obtain disposable sanitary articles use
It seeps hot melt adhesive (infrared spectrogram is as shown in Figure 1).
Above-mentioned disposable sanitary articles are tested for the property with impervious hot melt adhesive, test result is as follows shown in table:
The performance test results of the impervious hot melt adhesive of 2 disposable sanitary articles of table
Note:
Glue applying method is as follows: being added in size applicator after above-mentioned disposable sanitary articles are melted with impervious hot melt adhesive, sizing
Sizing face on device matches with hole drilling ventilation membrane superficial tissue, then glue is coated on hole drilling ventilation film, then will punch saturating
Air film and water repellent nonwovens fitting, are bonded；The size applicator is made of two application rolls (structure is as shown in Figure 2), and one
The surface staggered row of a application roll shows diamond shape protrusion, and is additionally provided with several micropores between adjacent diamond shape protrusion, another
The surface staggered row of application roll shows the diamond sunk to match with diamond shape protrusion, and is additionally provided between adjacent diamond sunk
Several micropores.
SUMMIT: spiral glue spraying mode.
Test discovery scrapes gluing method production using the impervious hot melt adhesive of disposable sanitary articles and coating of the present embodiment
Sanitary napkin and baby paper diaper are without adhesion problems caused by strike-through.
Embodiment 2:
A kind of impervious hot melt adhesive of disposable sanitary articles, raw material composition are as shown in the table:
A kind of raw material of the impervious hot melt adhesive of the disposable sanitary articles of table 3 forms table
The preparation method of the impervious hot melt adhesive of above-mentioned disposable sanitary articles is the following steps are included: by styrene-isoamyl two
Alkene-styrene block copolymer, C5 Petropols, C9 hydrogenated petroleum resin, White Mineral Oil, PE wax and antioxidant 1010 mixing are equal
It is even, 150 DEG C are again heated to, stirring is vacuumized and is melted completely to material, then stop stirring, be evacuated to bubble-free in material, obtain
To the impervious hot melt adhesive of disposable sanitary articles.
Above-mentioned disposable sanitary articles are tested for the property with impervious hot melt adhesive, test result is as follows shown in table:
The performance test results of the impervious hot melt adhesive of 4 disposable sanitary articles of table
Note:
Glue applying method is as follows: being added in size applicator, applies after above-mentioned disposable sanitary articles are melted with impervious hot melt adhesive
Sizing face on adhesive dispenser matches with hole drilling ventilation membrane superficial tissue, then glue is coated on hole drilling ventilation film, then will punching
Ventilated membrane and water repellent nonwovens fitting, are bonded；The size applicator is made of two application rolls (structure is as shown in Figure 2),
The surface staggered row of one application roll shows diamond shape protrusion, and is additionally provided with several micropores between adjacent diamond shape protrusion, another
The surface staggered row of a application roll shows the diamond sunk to match with diamond shape protrusion, and also sets up between adjacent diamond sunk
There are several micropores.
SUMMIT: spiral glue spraying mode.
Test discovery scrapes gluing method production using the impervious hot melt adhesive of disposable sanitary articles and coating of the present embodiment
Sanitary napkin and baby paper diaper are without adhesion problems caused by strike-through.
Embodiment 3:
A kind of impervious hot melt adhesive of disposable sanitary articles, raw material composition are as shown in the table:
A kind of raw material of the impervious hot melt adhesive of the disposable sanitary articles of table 5 forms table
The preparation method of the impervious hot melt adhesive of above-mentioned disposable sanitary articles is the following steps are included: by ethene-vinyl acetate
Copolymer, C5 hydrogenated petroleum resin, White Mineral Oil, Fischer-Tropsch wax and antioxidant 1010 are uniformly mixed, and are again heated to 155 DEG C, are vacuumized
Stirring melts completely to material, then stops stirring, and is evacuated to bubble-free in material, obtains disposable sanitary articles with impervious heat
Melten gel.
Above-mentioned disposable sanitary articles are tested for the property with impervious hot melt adhesive, test result is as follows shown in table:
The performance test results of the impervious hot melt adhesive of 6 disposable sanitary articles of table
Note:
Glue applying method is as follows: being added in size applicator, applies after above-mentioned disposable sanitary articles are melted with impervious hot melt adhesive
Sizing face on adhesive dispenser matches with hole drilling ventilation membrane superficial tissue, then glue is coated on hole drilling ventilation film, then will punching
Ventilated membrane and water repellent nonwovens fitting, are bonded；The size applicator is made of two application rolls (structure is as shown in Figure 2),
The surface staggered row of one application roll shows diamond shape protrusion, and is additionally provided with several micropores between adjacent diamond shape protrusion, another
The surface staggered row of a application roll shows the diamond sunk to match with diamond shape protrusion, and also sets up between adjacent diamond sunk
There are several micropores.
SUMMIT: spiral glue spraying mode.
Test discovery scrapes gluing method production using the impervious hot melt adhesive of disposable sanitary articles and coating of the present embodiment
Sanitary napkin and baby paper diaper are without adhesion problems caused by strike-through.
Embodiment 4:
A kind of impervious hot melt adhesive of disposable sanitary articles, raw material composition are as shown in the table:
A kind of raw material of the impervious hot melt adhesive of the disposable sanitary articles of table 7 forms table
The preparation method of the impervious hot melt adhesive of above-mentioned disposable sanitary articles is the following steps are included: by styrene-butadiene-
It is styrene block copolymer, styrene-ethylene-butylene-styrene block copolymer, DCPD Petropols, White Mineral Oil, linear low
Density polyethylene and antioxidant 1010 are uniformly mixed, and are again heated to 160 DEG C, are vacuumized stirring and are melted completely to material, then stop
Stirring, is evacuated to bubble-free in material, obtains disposable sanitary articles with impervious hot melt adhesive.
Above-mentioned disposable sanitary articles are tested for the property with impervious hot melt adhesive, test result is as follows shown in table:
The performance test results of the impervious hot melt adhesive of 8 disposable sanitary articles of table
Note:
Glue applying method is as follows: being added in size applicator, applies after above-mentioned disposable sanitary articles are melted with impervious hot melt adhesive
Sizing face on adhesive dispenser matches with hole drilling ventilation membrane superficial tissue, then glue is coated on hole drilling ventilation film, then will punching
Ventilated membrane and water repellent nonwovens fitting, are bonded；The size applicator is made of two application rolls (structure is as shown in Figure 2),
The surface staggered row of one application roll shows diamond shape protrusion, and is additionally provided with several micropores between adjacent diamond shape protrusion, another
The surface staggered row of a application roll shows the diamond sunk to match with diamond shape protrusion, and also sets up between adjacent diamond sunk
There are several micropores.
SUMMIT: spiral glue spraying mode.
Test discovery scrapes gluing method production using the impervious hot melt adhesive of disposable sanitary articles and coating of the present embodiment
Sanitary napkin and baby paper diaper are without adhesion problems caused by strike-through.
The above embodiment is a preferred embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment
Limitation, other any changes, modifications, substitutions, combinations, simplifications made without departing from the spirit and principles of the present invention,
It should be equivalent substitute mode, be included within the scope of the present invention.
Claims (10)
1. a kind of impervious hot melt adhesive of disposable sanitary articles, it is characterised in that: consist of the following mass percentage components:
Main polymer: 10%~20%；
Tackifying resin: 45%~55%；
White Mineral Oil: 15%~25%；
Processing aid: 5%~10%；
Antioxidant: 0.1%~0.5%.
2. the impervious hot melt adhesive of disposable sanitary articles according to claim 1, it is characterised in that: the main polymer
For Styrene-Butadiene-Styrene Block Copolymer, styrene-isoprene-styrene block copolymer, styrene-second
At least one of alkene-butylene-styrene block copolymer, ethylene-vinyl acetate copolymer.
3. the impervious hot melt adhesive of disposable sanitary articles according to claim 2, it is characterised in that: the styrene-fourth
Diblock is free of in styrene block copolymer；Benzene second in the styrene-isoprene-styrene block copolymer
The mass percentage of alkene is 35%~40%.
4. the impervious hot melt adhesive of disposable sanitary articles according to claim 1, it is characterised in that: the tackifying resin is
At least one of Petropols, hydrogenated petroleum resin.
5. the impervious hot melt adhesive of disposable sanitary articles according to claim 4, it is characterised in that: the Petropols are
At least one of C5 Petropols, C9 Petropols, DCPD Petropols；The hydrogenated petroleum resin is C5 hydrotreated petroleum tree
At least one of rouge, C9 hydrogenated petroleum resin, DCPD hydrogenated petroleum resin.
6. the impervious hot melt adhesive of disposable sanitary articles described according to claim 1~any one of 4, it is characterised in that:
The mass percentage of cycloalkane is greater than 40% in the White Mineral Oil.
7. the impervious hot melt adhesive of disposable sanitary articles described according to claim 1~any one of 4, it is characterised in that:
The processing aid is at least one of linear low density polyethylene, Fischer-Tropsch wax, PE wax, PP wax.
8. the preparation method of impervious hot melt adhesive of disposable sanitary articles described in any one of claim 1~7, feature
It is: the following steps are included: main polymer, tackifying resin, White Mineral Oil, processing aid and antioxidant are uniformly mixed, then plus
Heat vacuumizes stirring and melts completely to material to 145~160 DEG C, then stops stirring, and is evacuated to bubble-free in material, obtains
The impervious hot melt adhesive of disposable sanitary articles.
9. gluing method is scraped in a kind of disposable sanitary articles coating, it is characterised in that: the following steps are included: by claim 1~7
Any one of described in disposable sanitary articles with impervious hot melt adhesive melt after be added size applicator in, then by glue be coated on beat
On pore membrane or non-woven fabrics base material, then substrate is bonded, is bonded；The sizing face of the size applicator and substrate surface structure phase
It coincide.
10. gluing method is scraped in disposable sanitary articles coating according to claim 9, it is characterised in that: the sizing dress
It sets and is made of two application rolls, the surface staggered row of an application roll shows diamond shape protrusion, and between adjacent diamond shape protrusion also
Several micropores are provided with, the surface staggered row of another application roll shows the diamond sunk to match with diamond shape protrusion, and adjacent
Diamond sunk between be additionally provided with several micropores.
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| CN201910489257.0A CN110205064B (en) | 2019-06-06 | 2019-06-06 | Impervious hot melt adhesive for disposable hygienic product and coating and frictioning method |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910489257.0A CN110205064B (en) | 2019-06-06 | 2019-06-06 | Impervious hot melt adhesive for disposable hygienic product and coating and frictioning method |
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Cited By (2)
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| CN110791239A (en) * | 2019-10-11 | 2020-02-14 | 东莞市成铭胶粘剂有限公司 | Low-odor strong-adhesiveness hot melt adhesive for sanitary materials |
| CN113999615A (en) * | 2021-11-22 | 2022-02-01 | 新乡市华洋粘合剂有限公司 | Hot melt adhesive for cigarette filter stick |
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| CN113999615A (en) * | 2021-11-22 | 2022-02-01 | 新乡市华洋粘合剂有限公司 | Hot melt adhesive for cigarette filter stick |
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| Publication number | Publication date |
|---|---|
| CN110205064B (en) | 2021-07-06 |
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Address after: 511335 first floor of ganggushan (plant A1), Shajiao village, Xiancun East Industrial Park, Xintang Town, Zengcheng, Guangzhou, Guangdong Patentee after: Poly glue New Material Co.,Ltd. Address before: 511335 Guangdong Province Guangzhou Zengcheng Xintang Town Xiancun East Industrial Park Shajiao village Ganggu Shandong Fanglong workshop A1 Patentee before: GUANGDONG POLY ADHESIVE Co.,Ltd. |