CN110184486A - A kind of method of sheet billet continuous casting and rolling production high-performance aluminium alloy Strip - Google Patents

A kind of method of sheet billet continuous casting and rolling production high-performance aluminium alloy Strip Download PDF

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Publication number
CN110184486A
CN110184486A CN201910577706.7A CN201910577706A CN110184486A CN 110184486 A CN110184486 A CN 110184486A CN 201910577706 A CN201910577706 A CN 201910577706A CN 110184486 A CN110184486 A CN 110184486A
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casting
rolling
temperature
hot
sheet billet
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李勇
贺晨
许光明
李家栋
田勇
王丙兴
韩毅
付天亮
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Northeastern University China
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Northeastern University China
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Priority to CN201910804548.4A priority patent/CN110373560B/en
Publication of CN110184486A publication Critical patent/CN110184486A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B1/00Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations
    • B21B1/22Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling plates, strips, bands or sheets of indefinite length
    • B21B1/24Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling plates, strips, bands or sheets of indefinite length in a continuous or semi-continuous process
    • B21B1/26Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling plates, strips, bands or sheets of indefinite length in a continuous or semi-continuous process by hot-rolling, e.g. Steckel hot mill
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B3/00Rolling materials of special alloys so far as the composition of the alloy requires or permits special rolling methods or sequences ; Rolling of aluminium, copper, zinc or other non-ferrous metals
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C1/00Making non-ferrous alloys
    • C22C1/02Making non-ferrous alloys by melting
    • C22C1/026Alloys based on aluminium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C1/00Making non-ferrous alloys
    • C22C1/02Making non-ferrous alloys by melting
    • C22C1/03Making non-ferrous alloys by melting using master alloys
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C21/00Alloys based on aluminium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/04Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B1/00Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations
    • B21B1/22Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling plates, strips, bands or sheets of indefinite length
    • B21B2001/225Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling plates, strips, bands or sheets of indefinite length by hot-rolling
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B3/00Rolling materials of special alloys so far as the composition of the alloy requires or permits special rolling methods or sequences ; Rolling of aluminium, copper, zinc or other non-ferrous metals
    • B21B2003/001Aluminium or its alloys

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Continuous Casting (AREA)
  • Metal Rolling (AREA)

Abstract

The present invention relates to a kind of methods of sheet billet continuous casting and rolling production high-performance aluminium alloy Strip, this method is first refining aluminium alloy melt, double-roll type sheet billet continuous casting and rolling is carried out to it using the water-cooled casting rolls that surface has nano-graphite coating to lubricate, and obtains continuous casting and rolling sheet billet;Carry out hot-leveling, the processing of concurrent heating samming, heat preservation, uncoiling progress hot finishing.Method of the invention saves the processes such as semi-continuous casting, milling face, homogenization heat treatment, hot roughing, the intermediate annealing of traditional slab hot-rolling cogging method, aluminum alloy strip lumber recovery significantly improves 20% or more, production cycle was shortened to 0.5 day or so by original 20 days, and production efficiency significantly improves;Improving, production technology is successional while reducing by 30% or more production cost, reduce 50% or more the pollutant emissions such as carbon/sulfide, generates big economic benefit and social benefit.

Description

A kind of method of sheet billet continuous casting and rolling production high-performance aluminium alloy Strip
Technical field
The present invention relates to a kind of methods of sheet billet continuous casting and rolling production high-performance aluminium alloy Strip, belong to material metallurgy Technical field.
Background technique
In recent decades, domestic and international intermetallic composite coating circle all around it is energy saving, reduce discharge, reduce production cost, Production efficiency and lumber recovery are improved, is improved production quality to develop new technology, to reach long-term and constantly energy-saving and emission-reduction, raising The purpose of quality.It is obtained currently, aluminum alloy slab mainly uses semi-continuous casting method to prepare big slab ingot by rolling, ingot casting is thick Degree is more than 600mm, and length about 6-8m, this big inside ingot homogeneity of ingredients is poor, and the production cycle is long, the processes such as cutting head, milling face Lumber recovery is less than 70% afterwards, and heat treatment energy consumption is high, pollutant emission is mostly the huge barrier for improving aluminium quality, reducing production cost Hinder.
Sheet billet continuous casting rolling technology is that liquid metal is directly injected into the Casting Roller and casting cooling by two internal water flowings In the closing roll casting zone that mouth is constituted, and a kind of technique of semifinished or finished goods slab is directly prepared with the rotation of Casting Roller, spy Point is the quick nonequilibrium solidification process in Asia completed in a very short period of time from liquid metal to solid-state slab, and liquid metal exists Pressure processing and plastic deformation are born while crystallization and freezing.Sheet billet continuous casting rolling technology is considered as most possibly overturning biography Uniting, metal material manufacturing process is long, at high cost, energy consumption is high, of poor quality, discharge more, the low status of lumber recovery one revolutionary skills Art, compared with traditional strip production procedure, sheet billet casting-rolling technology can save producing line investment 80%, reduce production energy consumption 50%, COx, NO are reducedX、SOXEqual 50% or more noxious gas emissions save 30% or more production cost, improve lumber recovery 20% More than.At the same time, sheet billet rolling casting technology provides a kind of extreme preparation condition with industrial applications prospect, is based on The non-equilibrium microstructure feature of Sub realizable fuzzy matrix, the super saturated solid solution of alloying element and special homogenization institutional framework are work Wide cut, homogeneous, high quality, low cost, the alloy strip steel rolled stock for being easy to be further processed are developed and designed under industry scale to provide entirely New technological means, and completely new possibility is provided for the design and being substantially improved for performance of novel alloy.But current ingot casting- That there are large-sized aluminium alloy plate ingot thickness direction component differences is big for hot rolling technology, microstructure is uneven, lumber recovery is low etc. lacks Falling into is that there is an urgent need for solutions.
Summary of the invention
(1) technical problems to be solved
In order to solve prior art large-sized aluminium alloy plate ingot thickness direction component difference is big, microstructure is uneven, at The low problem of material rate, the present invention provide a kind of method of sheet billet continuous casting and rolling production high-performance aluminium alloy Strip, this method Process flow it is short, cost of investment is low, and energy consumption discharge is low, the aluminum alloy sheets and strips producer that slab quality is high and lumber recovery is high Method.
(2) technical solution
In order to achieve the above object, the main technical schemes that the present invention uses include:
A kind of method of sheet billet continuous casting and rolling production high-performance aluminium alloy Strip comprising following steps:
S1, according to the standard analysis ingredient of institute's cast aluminium alloy sheet billet, first by aluminium ingot all fusing after, sequentially add needed for Aluminum water, is then transferred in heat preservation standing furnace and carries out stewing process by intermediate alloy, and the stable refined aluminum of temperature is obtained after cooling Alloy melt;
S2, the water-cooled casting rolls for having nano-graphite coating to lubricate using surface carry out double-roll type to the refining aluminium alloy melt Sheet billet continuous casting and rolling obtains the continuous casting and rolling sheet billet with a thickness of 15~100mm;
S3, the pinch roller in the exit of casting and rolling machine setting a pair with hot-leveling function are thin to obtained continuous casting and rolling Slab carries out hot-leveling, obtains the good sheet billet casting volume of plate shape, thickness;
S4, sheet billet casting volume is subjected to the processing of concurrent heating samming in continuous tunnel furnace or holding furnace,
After S5, sheet billet casting volume are kept the temperature in continuous tunnel furnace, uncoiling carries out hot finishing.
Be preferably carried out in scheme one, in step sl, the aluminum alloy thin slab include 1100,3003,5182, 6022,7075 line aluminium alloy sheet billet.
It is preferably carried out in scheme one, in step sl, the cleaning molten processing refers specifically to rotate using SNIF Blowing carries out degassing processing;It is filtered using ceramic wafer except Slag treatment.
It is preferably carried out in scheme one, in step sl, the temperature of the heat preservation standing furnace is 710~750 DEG C, is stood Time is 0.5~1.5h.
Be preferably carried out in scheme one, in step s 2, the roller diameters of the water-cooled casting rolls be Φ 500~ 1200mm, roller set are 25 DEG C~35 DEG C with a thickness of 20~40mm, the temperature of roll Inlet water, the temperature setting 30 of roll exit water ~35 DEG C, cooling water pressure is set as 0.2Mpa~0.4Mpa, and the pouring temperature of the refining aluminium alloy melt is 650~730 DEG C, roll casting speed is 0.3~35m/min.
Further, it is preferable that the pouring temperature of the refining aluminium alloy melt is 675~720 DEG C, roll casting speed 0.3 ~1.5m/min.
It is preferably carried out in scheme one, in step s3, the temperature of institute's hot-leveling is 200~600 DEG C, smooth drafts It is up to 3%~20%.
It is preferably carried out in scheme one, in step s3, the temperature of institute's hot-leveling is preferably 300~500 DEG C, smooth pressure Lower amount maximum is preferably 5%~10%.
It is preferably carried out in scheme one, in step s 4, the holding temperature 300 DEG C~600 of the concurrent heating samming processing DEG C, temperature-controlled precision ± 3~5 DEG C, quantity volume 10~20 of storage volume, 30~35m of effective length.
It is preferably carried out in scheme one, in step s 5, the uncoiling carries out the start rolling temperature 340~350 of hot finishing DEG C, 180~200 DEG C of finishing temperature, hot rolling deformation amount 70%~90%, percentage pass reduction is up to 50%, obtain with a thickness of 2~ The finished product of 10mm/semi-finished product hot rolled coil.
(3) beneficial effect
Compared with prior art, the features of the present invention and beneficial effect are:
Sheet billet continuous casting and rolling provided by the invention produces high-performance aluminium alloy Strip method, is the essence that temperature is stable Aluminium metallurgy water produces the sheet billet with a thickness of 15~100mm using Horizontal double roller casting equipment, while during continuous casting and rolling Realizing has the casting for stablizing liquid level, and being involved in for aluminium oxide is reduced while not destroying liquid level surface layer oxide film, is improved The subsequent processing performance of plate;Sheet billet continuous casting and rolling technique belongs to productive technology of short flow, due to cold in aluminum water process of setting But speed is up to 100~1000 DEG C/s, belongs to typical Sub realizable fuzzy matrix, has alloying element super saturated solid solution, microstructure The advantages such as homogeneous fine grain and chemical component are uniform.The homogeneous fine grain feature of tissue have heredity, can be improved product strength and Processability.Meanwhile saving the processes such as semi-continuous casting, milling face, homogenization heat treatment, hot roughing, intermediate annealing, production technology Period shortened to current 0.5 day by original 20 days, and lumber recovery is increased to current 90% or more less than 70% by original, Energy consumption reduces by 50% or more, and production cost reduces by 30% or more, reduces 50% or more the pollutant emissions such as carbon/sulfide, meets Energy-saving and emission-reduction, the requirement for improving stock utilization, generate huge economic benefit and social benefit.
Detailed description of the invention
Fig. 1 is the industrialization producing line arrangement schematic diagram of present device;
Fig. 2 is sheet billet continuous casting and rolling of the present invention-concurrent heating samming-hot continuous rolling production technological process;
Fig. 3 is that the made-up belt microstructure by traditional casting-rolling method continuous casting and rolling process production of 1100 aluminum alloy thin slabs is shone Piece;
Fig. 4 is the microstructure photo of the sheet billet by the preparation of 2 method of embodiment of 1100 aluminum alloy thin slabs;
Fig. 5 is the made-up belt microstructure photograph that 3003 aluminum alloy thin slabs press traditional casting-rolling method continuous casting and rolling process production Piece;
Fig. 6 is microstructure photo of the 3003 aluminum alloy thin slabs by the sheet billet of 3 method of embodiment preparation;
Fig. 7 is that the made-up belt microstructure by traditional casting-rolling method continuous casting and rolling process production of 5182 aluminum alloy thin slabs is shone Piece;
Fig. 8 is the microstructure photo for the sheet billet of 5182 aluminum alloy thin slabs prepared as described in Example 4;
Fig. 9 is that the made-up belt microstructure for the continuous casting and rolling process production that 6022 aluminum alloy thin slabs press traditional casting-rolling method is shone Piece;
Figure 10 is the microstructure photo for the sheet billet that 6022 aluminum alloy thin slabs are prepared as described in Example 5;
Figure 11 is the made-up belt microstructure for the continuous casting and rolling process production that 7075 aluminum alloy thin slabs press traditional casting-rolling method Photo;
Figure 12 is the microstructure photo for the sheet billet that 7075 aluminum alloy thin slabs are prepared as described in Example 6.
Specific embodiment
In order to preferably explain the present invention, in order to understand, with reference to the accompanying drawing, by specific embodiment, to this hair It is bright to be described in detail.
Embodiment 1
A kind of industrialization producing line arrangement of sheet billet continuous casting and rolling production high-performance aluminium alloy Strip, as shown in Figure 1: Smelting furnace stands holding furnace-filter device-depassing unit-chute-continuous casting & rolling line-pinch roller-shearing machine-crimping machine-aluminium volume - three rack continuous hot-rolling mill of rapid transit system-continuous tunnel furnace-uncoiler-cutter-crimping machine, configures, continuous casting and rolling according to production capacity Producing line can be a plurality of;It is as shown in Figure 2 that it corresponds to device structure schematic diagram, comprising: and aluminum alloy smelting furnace 1 stands holding furnace 2, Rose Box 3, degasification tank 4, chute 5, continuous casting & rolling line 6, pinch roller 7, the first shearing machine 8, first pair of coiling machine 9 quickly transport Roller-way 10, continuous tunnel furnace 11, double uncoilers 12, three rack continuous hot-rolling mills 13, the second shearing machine 14, second pair of coiling machine 15.Wherein, After Rose Box and degasification tank are arranged in exquisite holding furnace, Rose Box uses ceramic wafer filter device;Depassing unit uses SNIF stone Black rotor rotary impreller degassing;The bast mouth of silicic acid aluminium material is arranged in the inlet of casting and rolling machine, and bast mouth center line is equal to or omits Lower than the center line of two rolls, for being input to aluminium alloy melt in the roll casting zone being made of roll and bast mouth;Casting Roller It is two, vertical symmetry arrangement is divided into Casting Roller and lower Casting Roller, and Casting Roller includes roller core and roller covers two parts, on roller core It is provided with groove, the logical cooling water in inside;Pinch roller is arranged in after casting and rolling machine, carries out hot-leveling to the high temperature slab that casting goes out, to After the casting volume of coiling machine curling reaches certain size, cutter cuts slab, carries out the curling of next casting volume;In order to Production efficiency with casting and rolling machine and three rack hot continuous rollings is provided with tunnel type holding furnace before entering hot continuous rolling, more to meet Concurrent heating and samming while rolling up casting volume;Casting volume after concurrent heating is carried out multi-pass by three rack continuous hot-rolling mills, continuous to depress, and is obtained There must be certain thickness aluminum alloy hot rolling to roll up;In order to mitigate the center-line segregation defect of aluminium alloy casting, it is arranged between Casting Roller Minimum roll gap >=15mm, to following process process reduction ratio with higher, preferably, roll gap is set as 15- 100mm。
The method for preparing aluminum alloy sheets and strips using above equipment is carried out using following steps:
(1) melting, refining:
According to the standard analysis ingredient for casting 1100,3003,5182,6022,7075 line aluminium alloy sheet billets, it is put into melting Melting is carried out in furnace, first by after fine aluminium ingot all fusing, sequentially adds required intermediate alloy, aluminum water is then transferred to heat preservation Stewing process is carried out in standing furnace, when the aluminum water temperature in standing furnace is 710~750 DEG C, carries out cleaning molten processing, it is described Cleaning molten processing refer specifically to can be significantly reduced using SNIF rotary impreller degassing processing+ceramic wafer filtering and removing slag processing The content that the formation of stomata and large scale are mingled in cast-rolled block improves the quality of slab, and the stable essence of temperature is obtained after cooling Aluminium metallurgy alloy melt;
(2) continuous casting and rolling sheet billet is prepared:
There are the water-cooled casting rolls of nano-graphite coating lubrication etc. to carry out double-roll type sheet billet to refining aluminum water using surface continuous Casting.Roller diameter is 500~1200mm of Φ, and roller set is with a thickness of 20~40mm, the in order to prevent generation of scale, roll Inlet water 25 DEG C~35 DEG C of temperature, suitable 30~35 DEG C of the temperature of roll exit water, cooling water pressure is set as 0.2Mpa~0.4Mpa.Essence The pouring temperature of aluminium metallurgy water is 650~730 DEG C, and roll casting speed is 0.3~35m/min, is obtained with a thickness of the continuous of 15~100mm Casting sheet billet, for vertical plate success and the surface quality of strip, preferred melt cast temperature is 675~720 DEG C, casting Speed is 0.3~1.5m/min, if melt temperature is lower than 675 DEG C or roll casting speed is lower than 0.3m/min, melt heat dissipation is too fast, Melt solidifies in advance in bast mouth, causes bast mouth blocking or strip deflection excessive, while it is serious to split defect;If melt temperature is high It is greater than 1.5m/min in 720 DEG C or speed, melt has little time to solidify in roll casting zone, causes to run soup, vertical plate failure or strip There is tropical defect in surface, reduces the surface quality of strip.
(3) hot-leveling:
A pair of pinch roller with hot-leveling function can be set in the exit of casting and rolling machine, to obtained casting sheet billet Hot-leveling is carried out, 200~600 DEG C of smooth temperature, preferably 300~500 DEG C, smooth drafts is up to 3%~20%, preferably It is 5%~10%, obtains the good sheet billet casting volume of plate shape, thickness, enter in continuous tunnel furnace or holding furnace after batching and mended Hot samming, wherein the maximum effect of pinch roller is to can reduce the crackle tendency of made-up belt, improves the surface smoothness and table of strip Face precision.
(4) continuous tunnel furnace concurrent heating samming:
Sheet billet casting volume is subjected to the processing of concurrent heating samming in continuous tunnel furnace, 300 DEG C~600 DEG C of holding temperature, temperature control is smart ± 3~5 DEG C of degree, storage volume quantity >=5 volume, preferably volume 10~20, effective length >=15m, preferably 30~40mm are realized simultaneously The decomposition of the recrystallized structure regulation and coarse primary crystallization phase of sheet billet.There is the concurrent heating of holding furnace to handle, does not need to cast It rolls speed and multi-frame hot continuous rolling speed carries out stringent matching, improve the processing efficiency and rate of strip.
(5) hot continuous rolling:
It is configured according to production capacity, sheet billet casting volume soaking time range in continuous tunnel furnace is 10-30h, and uncoiling carries out heat essence It rolls.In order to obtain complete recrystallized structure, the rolling load of hot-rolling mill is reduced, the rolling stress of hot-rolled product, open rolling are eliminated Preferably minimum 350 DEG C, preferably 350 DEG C~420 DEG C of temperature;Minimum 200 DEG C of finishing temperature, preferably 225 DEG C~275 DEG C; Hot rolling deformation amount 70%~90%, percentage pass reduction are up to 50%, obtain with a thickness of 2~10mm, preferably 3~6mm at Product/semi-finished product hot rolled coil provide enough deformation rates for the subsequent cold rolling of product.
Embodiment 2
Be in the present embodiment to 1100 aluminum alloy thin slabs, continuous casting and rolling combination hot continuous rolling produce aluminum alloy plate materials technique and The device in embodiment 1 is utilized in method, the specific steps are as follows:
(1) melting, refining:
According to 1100 aluminium alloy standard analysis ingredients, by weight percentage (wt%) (Si+Fe): 0.95, Cu:0.05~ 0.20, Zn:0.10, Mn:0.035, Al: surplus.The intermediate alloys equal proportions such as commercial-purity aluminium, aluminium silicon, aluminum bronze are weighed, are put into molten Melting is carried out in furnace.First by after technical pure aluminium ingot all fusing, above-mentioned intermediate alloy is sequentially added, aluminum water is transferred to guarantor It is stood in warm standing furnace, when the aluminum water temperature in standing furnace is 710 DEG C, carries out cleaning molten processing, the melt Purified treatment refers specifically to that Casting Rolled Sheet can be significantly reduced using SNIF rotary impreller degassing processing+ceramic wafer filtering and removing slag processing The content that the formation of stomata and large scale are mingled in base, improves the quality of slab, is then cooled to 700 DEG C and stands 1 hour again, obtains Obtain the stable refining aluminum water of temperature;
(2) melt conveying:
Melt is delivered to continuous casting & rolling line by chute, by melt temperature control at 685 DEG C ± 2 DEG C, liquid level in chute Height control is 110mm;Roll casting speed is 1.2m/min;
(3) continuous casting and rolling sheet billet is prepared:
The double-roll type sheet billet continuous casting and rolling device for thering is nano-graphite coating to lubricate using surface;Roller set uses gun-steel material Matter, giving casting roll gap up and down is 15mm, and mouth fan opening degree is 40mm to bast mouth up and down, and casting roller diameter is Φ 860mm, and roll surface is wide Spend 1000mm;Roll casting speed is 1.2m/min, in order to prevent the generation of scale, and cooling water pressure is set as 0.4Mpa, roll into About 25 DEG C~35 DEG C of saliva temperature, suitable 30~35 DEG C of roll exit water temperature;After vertical plate success, by the edge for observing cast-rolled block Quality finely tunes roll casting speed, determines so that slab edge is bright, flawless, stablizes roll casting speed, start continuous production.
(4) hot-leveling:
In the exit of casting and rolling machine, a pair of pinch roller with hot-leveling function of setting, carries out obtained casting sheet billet Hot-leveling, about 400 DEG C of smooth temperature, smooth drafts is about 8%, obtains the good sheet billet casting volume of plate shape, thickness;
(5) continuous tunnel furnace:
The progress concurrent heating samming processing in continuous tunnel furnace by sheet billet casting volume, 420 DEG C of holding temperature range, while realizing thin The regulation of the coarse primary crystallization phase such as slab recrystallized structure and Al-Fe-Si.The heat preservation concurrent heating of continuous tunnel furnace is handled, woth no need to Roll casting speed and multi-frame hot continuous rolling speed are subjected to stringent matching, improve the processing efficiency and rate of strip.
(6) hot continuous rolling
After sheet billet casting volume keeps the temperature a period of time in batch-type furnace, uncoiling carries out hot finishing, three rack hot continuous rolling passages Reduction ratio is respectively 30%, 40%, 50%, and controlling hot finishing temperature is 225 ± 5 DEG C, obtain the finished product with a thickness of 3mm/half at Product hot rolled coil, compare conventional casting methods, and using aluminum alloy slab produced by the invention, production cost reduces by 2000 yuan/ton More than, cost reduces by 30% or more (data source Yunnan metallurgy group).
It is illustrated in figure 3 the made-up belt microstructure photo that 1100 aluminum alloy thin slabs use conventional method to prepare, such as Fig. 4 show the made-up belt microstructure photo of the sheet billet of the present embodiment method preparation;As a result illustrate the plate of conventional method preparation The characteristic that material is symmetrically solidified due to it, there are apparent center segregation or distributed segregations, are closed using aluminium produced by the invention Golden plate material improves the subsequent deep drawability energy of plate without apparent banded segregation defect, and the cracking for reducing fault location is several Rate.
Embodiment 3
The present embodiment is to carry out continuous casting and rolling combination hot continuous rolling for 3003 aluminum alloy thin slabs and produce aluminum alloy plate materials work The device in embodiment 1 is utilized in skill, the specific steps are as follows:
(1) melting, refining:
According to 3003 aluminium alloy standard analysis ingredient (wt%) Si:0.6, Cu:0.1, Zn:0.1, Mn:1.2, Fe:0.7, Al: the intermediate alloys equal proportions such as commercial-purity aluminium, aluminium silicon, aluminum bronze are weighed, are put into smelting furnace and carry out melting, to aluminium ingot by surplus All after fusing, above-mentioned intermediate alloy is sequentially added, aluminum water is transferred in heat preservation standing furnace and is stood, when in standing furnace When aluminum water temperature is 710~750 DEG C, cleaning molten processing is carried out, the cleaning molten processing refers specifically to rotate using SNIF It is blown degassing processing+ceramic wafer filtering and removing slag processing, the formation of stomata and large scale in cast-rolled block can be significantly reduced and be mingled with Content, improve the quality of slab, be then cooled to 700 DEG C and stand 1 hour again, obtain the stable refining aluminum water of temperature;
(2) melt conveying:
Melt is delivered to continuous casting & rolling line by chute, by melt temperature control at 690 DEG C ± 2 DEG C, liquid level in chute Height 110mm;Roll casting speed is 1.0m/min;
(3) continuous casting and rolling sheet billet is prepared:
The double-roll type sheet billet continuous casting and rolling device for thering is nano-graphite coating to lubricate using surface;Roller set uses gun-steel material Matter, giving casting roll gap up and down is 40mm, and mouth fan opening degree is 110mm to bast mouth up and down, and casting roller diameter is Φ 860mm;Casting Speed is 1.0m/min, in order to prevent the generation of scale, and cooling water pressure is set as 0.4Mpa, about 25 DEG C of roll inlet water temperature, Suitable 33 DEG C of roll exit water temperature;After vertical plate success, roll casting speed is finely tuned by observing the quality of edges of cast-rolled block, is determined So that slab edge is bright, after the roll casting speed of flawless, continuous production is carried out;
(4) hot-leveling:
In the exit of casting and rolling machine, a pair of pinch roller with hot-leveling function of setting, carries out obtained casting sheet billet Hot-leveling, about 450 DEG C of smooth temperature, smooth drafts is about 5%, obtains plate shape, the good casting sheet billet of thickness;
(5) continuous tunnel furnace:
Sheet billet casting volume is subjected to the processing of concurrent heating samming in continuous tunnel furnace, 570 DEG C~580 DEG C of holding temperature, is eliminated brilliant Interior segregation and MnAl6The form of one para-crystal is irregular.There is the concurrent heating samming of continuous tunnel furnace to handle, reduces plate in deep-draw Cracking probability improves the quality of strip.
(6) hot continuous rolling
After sheet billet casting volume keeps the temperature a period of time in batch-type furnace, uncoiling carries out hot finishing, three rack hot continuous rolling passages Reduction ratio is respectively 30%, 40%, 50%, controls hot finishing temperature greater than 200 DEG C, obtains finished product/semi-finished product with a thickness of 6mm Hot rolled coil.Present invention eliminates the casting of traditional method for producing aluminum alloy plate, Homogenization Treatments, cutting head, milling face, hot roughing etc. Process, the production cycle was by original 20 days.Shorten to current 12h, 92% or more lumber recovery.
It is illustrated in figure 5 the microstructure photo of the slab of traditional casting-rolling method preparation;If Fig. 6 is the present embodiment method system The microstructure photo of standby sheet billet;The result shows that using in continuous casting and rolling device of the present invention and the aluminium alloy of method preparation Heavy slab, compared with common cast-rolled block, the deflection of plate is obviously increased, and without apparent banded segregation, even tissue is tiny.
Embodiment 4
The present embodiment is to carry out continuous casting and rolling combination hot continuous rolling production aluminum alloy plate materials for 5182 aluminum alloy thin slabs The device in embodiment 1 is utilized in method, the specific steps are as follows:
(1) melting, refining:
According to 5182 aluminium alloy standard analysis ingredient (wt%) Mg:4.5, Si:0.20, Cu:0.15, Zn:0.25, Mn: 0.35, Cr:0.10, Fe:0.35, Ti:0.10, Al: surplus claims the intermediate alloys equal proportions such as commercial-purity aluminium, aluminium silicon, aluminum bronze Weight, is put into smelting furnace and carries out melting, after aluminium ingot all fusing, sequentially adds above-mentioned intermediate alloy, aluminum water is transferred to guarantor It is stood in warm standing furnace, when the aluminum water temperature in standing furnace is 710 DEG C, carries out cleaning molten processing, the melt Purified treatment refers specifically to that Casting Rolled Sheet can be significantly reduced using SNIF rotary impreller degassing processing+ceramic wafer filtering and removing slag processing The content that the formation of stomata and large scale are mingled in base improves the quality of slab,.Then 700 DEG C are cooled to and stands 1 hour again, Cooling obtains the stable refining aluminum water of temperature;
(2) melt conveying:
Melt is delivered to continuous casting & rolling line by chute, melt temperature is controlled at 695 DEG C ± 2 DEG C;
(3) continuous casting and rolling sheet billet is prepared:
The double-roll type sheet billet continuous casting and rolling device for thering is nano-graphite coating to lubricate using surface;Roller set uses high-strength highly-conductive Cu-Cr alloy material, giving casting roll gap up and down is 20mm, and mouth fan opening degree is 90mm to bast mouth up and down, and casting roller diameter is Φ 860mm;Roll casting speed is 0.6m/min, in order to prevent the generation of scale, and cooling water pressure is set as 0.4Mpa, roll Inlet water About 25 DEG C, suitable 30~35 DEG C of roll exit water temperature of temperature;After vertical plate success, finely tuned by observing the quality of edges of cast-rolled block Roll casting speed determines so that carrying out continuous production after the roll casting speed of slab edge light, flawless;
(4) hot-leveling:
In the exit of casting and rolling machine, a pair of pinch roller with hot-leveling function of setting, carries out obtained casting sheet billet Hot-leveling, about 400 DEG C of smooth temperature, smooth drafts is about 5%, plate shape, the good casting sheet billet of thickness is obtained, after batching Into progress concurrent heating samming in holding furnace.
(5) continuous tunnel furnace:
The progress concurrent heating samming processing in continuous tunnel furnace by sheet billet casting volume, 460 DEG C of holding temperature, while realizing sheet billet Recrystallized structure regulation.There is the concurrent heating of continuous tunnel furnace to handle, does not need to carry out roll casting speed and multi-frame hot continuous rolling speed Stringent matching improves the processing efficiency and rate of strip.
(6) hot continuous rolling
After sheet billet casting volume keeps the temperature a period of time in batch-type furnace, uncoiling carries out hot finishing, three rack hot continuous rolling passages Reduction ratio is respectively 30%, 40%, 40%, and controlling hot finishing temperature is 250 ± 5 DEG C, obtain the finished product with a thickness of 5mm/half at Product hot rolled coil.
Such as the microstructure photo that Fig. 7 is slab prepared by traditional casting-rolling method;If Fig. 8 is prepared by 4 method of embodiment The microstructure photo of sheet billet;As a result illustrating the plate of traditional casting-rolling method production, there are apparent segregation defects, using this The aluminum alloy plate materials of inventive technique production, increase the deflection of plate, segregation defects are substantially reduced, and even tissue is tiny.
Embodiment 5
The present embodiment is to carry out continuous casting and rolling combination hot continuous rolling production aluminum alloy plate materials for 6022 aluminum alloy thin slabs The device in embodiment 1 is utilized in method, the specific steps are as follows:
(1) melting, refining:
According to 6022 aluminium alloy standard analysis ingredient (wt%) Si:1.0, Cu:0.10, Zn:0.01, Mn:0.01, Mg: 0.8, Fe:0.1, Al: the intermediate alloys equal proportions such as commercial-purity aluminium, aluminium silicon, aluminum bronze are weighed, aluminium ingot are first put into melting by surplus Melting is carried out in furnace, after aluminium ingot all fusing after, sequentially add above-mentioned intermediate alloy, by aluminum water be transferred to heat preservation standing furnace in into Row is stood, and when the aluminum water temperature in standing furnace is 710 DEG C, carries out cleaning molten processing, the cleaning molten processing is specific Refer to using SNIF rotary impreller degassing processing+ceramic wafer filtering and removing slag processing, the shape of stomata in cast-rolled block can be significantly reduced At and the content that is mingled with of large scale, improve the quality of slab,.Then 700 DEG C are cooled to and stands 1 hour again, temperature is obtained and stablizes Refining aluminum water;
(2) melt conveying:
Melt is delivered to continuous casting & rolling line by chute, by melt temperature control at 685 DEG C ± 2 DEG C, liquid level in chute Height is 110mm;
(3) continuous casting and rolling sheet billet is prepared:
The double-roll type sheet billet continuous casting and rolling device for thering is nano-graphite coating to lubricate using surface;Roller set uses high-strength highly-conductive Cu-Cr alloy material, giving casting roll gap up and down is 25mm, and mouth fan opening degree is 100mm to bast mouth up and down, and casting roller diameter is Φ 860mm;Roll casting speed is 0.6m/min, in order to prevent the generation of scale, and cooling water pressure is set as 0.4Mpa, roll Inlet water About 25 DEG C, suitable 30~35 DEG C of roll exit water temperature of temperature;After vertical plate success, finely tuned by observing the quality of edges of cast-rolled block Roll casting speed determines so that carrying out continuous production after the roll casting speed of slab edge light, flawless;
(4) hot-leveling:
In the exit of casting and rolling machine, a pair of pinch roller with hot-leveling function of setting, carries out obtained casting sheet billet Hot-leveling, about 400 DEG C of smooth temperature, smooth drafts is about 5%, plate shape, the good casting sheet billet of thickness is obtained, after batching Into concurrent heating samming is carried out in continuous tunnel furnace or holding furnace, the maximum effect of pinch roller is to can reduce the crackle tendency of made-up belt, is mentioned The surface smoothness and surface accuracy of high strip.
(5) continuous tunnel furnace:
The progress concurrent heating samming processing in continuous tunnel furnace by sheet billet casting volume, 460 DEG C of holding temperature, while realizing sheet billet Recrystallized structure regulation.There is the concurrent heating of holding furnace to handle, does not need to carry out roll casting speed and multi-frame hot continuous rolling speed Stringent matching improves the processing efficiency and rate of strip.
(6) hot continuous rolling
After sheet billet casting volume keeps the temperature a period of time in batch-type furnace, uncoiling carries out hot finishing, three rack hot continuous rolling passages Reduction ratio is respectively 30%, 40%, 50%, controls 275 ± 5 DEG C of hot finishing temperature, obtains finished product/semi-finished product with a thickness of 5mm Hot rolled coil.
Such as the microstructure photo that Fig. 9 is slab prepared by traditional casting-rolling method;It is prepared by the method if Figure 10 is embodiment 5 Sheet billet microstructure photo;As a result illustrating the plate of traditional casting-rolling method production, there are apparent segregation defects, use The aluminum alloy plate materials of apparatus and method of the present invention production, deflection dramatically increase, and segregation defects are substantially reduced, and even tissue is thin It is small.
Embodiment 6
The present embodiment is to carry out continuous casting and rolling combination hot continuous rolling production aluminum alloy plate materials for 7075 aluminum alloy thin slabs The device in embodiment 1 is utilized in method, the specific steps are as follows:
(1) melting, refining:
According to 7075 aluminium alloy standard analysis ingredient (wt%) Cu:1.64, Zn:5.62, Mg:2.72, Cr:0.24, Fe: 0.1, Si:0.4, Al: the alloys equal proportions such as commercial-purity aluminium, pure magnesium, pure zinc are weighed, are put into smelting furnace and carry out melting by surplus, After aluminium ingot all fusing, above-mentioned intermediate alloy is sequentially added, aluminum water is transferred in heat preservation standing furnace and is stood, standing is worked as When aluminum water temperature in furnace is 710 ± 5 DEG C, cleaning molten processing is carried out, the cleaning molten processing is referred specifically to using SNIF Rotary impreller degassing processing+ceramic wafer filtering and removing slag processing, can be significantly reduced the formation and large scale of stomata in cast-rolled block The content being mingled with improves the quality of slab,.Then 700 DEG C are cooled to and stands 1 hour again, obtains the stable refining aluminum water of temperature;
(2) melt conveying:
Melt is delivered to continuous casting & rolling line by chute, melt temperature is controlled at 675 DEG C ± 2 DEG C;
(3) continuous casting and rolling sheet billet is prepared:
The double-roll type sheet billet continuous casting and rolling device for thering is nano-graphite coating to lubricate using surface;Roller set uses high-strength highly-conductive Cu-Cr alloy material, giving casting roll gap up and down is 20mm, and mouth fan opening degree is 105mm to bast mouth up and down, and casting roller diameter is Φ 860mm;Roll casting speed is 0.4m/min, in order to prevent the generation of scale, and cooling water pressure is set as 0.4Mpa, roll Inlet water About 25 DEG C, suitable 30~35 DEG C of roll exit water temperature of temperature;After vertical plate success, finely tuned by observing the quality of edges of cast-rolled block Roll casting speed determines so that carrying out continuous production after the roll casting speed of slab edge light, flawless;
(4) hot-leveling:
In the exit of casting and rolling machine, a pair of pinch roller with hot-leveling function of setting, carries out obtained casting sheet billet Hot-leveling, about 400 DEG C of smooth temperature, smooth drafts is about 6%, obtains the good sheet billet casting volume of plate shape, thickness, batches Enter afterwards and carries out concurrent heating samming in continuous tunnel furnace
(5) continuous tunnel furnace:
The progress concurrent heating samming processing in continuous tunnel furnace by sheet billet casting volume, 420 DEG C of holding temperature, while realizing sheet billet Recrystallized structure regulation.There is the concurrent heating of holding furnace to handle, does not need to carry out roll casting speed and multi-frame hot continuous rolling speed Stringent matching improves the processing efficiency and rate of strip.
(6) hot continuous rolling
After sheet billet casting volume keeps the temperature a period of time in batch-type furnace, uncoiling carries out hot finishing, three rack hot continuous rolling passages Reduction ratio is respectively 40%, 50%, 50%, controls 275 ± 5 DEG C of hot finishing temperature and obtains the finished product with a thickness of 3mm/semi-finished product heat Roll volume.
It is as shown in figure 11 the microstructure photo of the slab of traditional casting-rolling method preparation;It is as shown in figure 12 the present embodiment The microstructure photo of the sheet billet of 6 method preparation, the results showed that, through the invention prepared by the technological process of production and method Aluminum Alloy Plate base, compared with common cast-rolled block, non-stop layer line is segregated and tissue more refines, uniformly.
The above described is only a preferred embodiment of the present invention, being not the limitation for doing other forms to the present invention, appoint What those skilled in the art can use the equivalence enforcement that technology contents disclosed above were changed or be modified as equivalent variations Example.But without departing from the technical solutions of the present invention, according to the technical essence of the invention to the above embodiments What simple modification, equivalent variations and remodeling, still falls within the protection scope of technical solution of the present invention.

Claims (10)

1. a kind of method of sheet billet continuous casting and rolling production high-performance aluminium alloy Strip, which is characterized in that it includes following step It is rapid:
S1, according to the standard analysis ingredient of institute's cast aluminium alloy sheet billet, first by aluminium ingot all fusing after, sequentially add required centre Aluminum water, is then transferred in heat preservation standing furnace and carries out stewing process by alloy, and the stable refining aluminium alloy of temperature is obtained after cooling Melt;
S2, the water-cooled casting rolls for having nano-graphite coating to lubricate using surface carry out double-roll type thin plate to the refining aluminium alloy melt Base continuous casting and rolling obtains the continuous casting and rolling sheet billet with a thickness of 15~100mm;
S3, the pinch roller in the exit of casting and rolling machine setting a pair with hot-leveling function, to obtained continuous casting and rolling sheet billet Hot-leveling is carried out, the good sheet billet casting volume of plate shape, thickness is obtained;
S4, sheet billet casting volume is subjected to the processing of concurrent heating samming in continuous tunnel furnace or holding furnace,
After S5, sheet billet casting volume are kept the temperature in continuous tunnel furnace, uncoiling carries out hot finishing.
2. the method as described in claim 1, which is characterized in that in step sl, the aluminum alloy thin slab include 1100, 3003,5182,6022,7075 line aluminium alloy sheet billet.
3. the method as described in claim 1, which is characterized in that in step sl, the cleaning molten processing refers specifically to adopt Degassing processing is carried out with SNIF rotary blowing;It is filtered using ceramic wafer except Slag treatment.
4. the method as described in claim 1, which is characterized in that in step sl, it is described heat preservation standing furnace temperature be 710~ 750 DEG C, time of repose is 0.5~1.5h.
5. the method as described in claim 1, which is characterized in that in step s 2, the roller diameter of the water-cooled casting rolls is Φ 500~1200mm, roller set are 25 DEG C~35 DEG C with a thickness of 20~40mm, the temperature of roll Inlet water, the temperature of roll exit water 30~35 DEG C of setting, cooling water pressure are set as 0.2Mpa~0.4Mpa, and the pouring temperature of the refining aluminium alloy melt is 650 ~730 DEG C, the speed of the casting is 0.3~35m/min.
6. the method as described in claim 1, which is characterized in that the pouring temperature of the refining aluminium alloy melt is 675~720 DEG C, the speed of the casting is 0.3~1.5m/min.
7. the method as described in claim 1, which is characterized in that in step s3, the temperature of institute's hot-leveling is 200~600 DEG C, Smooth drafts range is 3%~20%.
8. the method as described in claim 1, which is characterized in that in step s3, the temperature of institute's hot-leveling is 300~500 DEG C, Smooth drafts is up to 5%~10%.
9. the method as described in claim 1, which is characterized in that in step s 4, the holding temperature of the concurrent heating samming processing 300 DEG C~600 DEG C, temperature-controlled precision ± 3~5 DEG C, quantity volume 10~20 of storage volume, 30~35m of effective length.
10. the method as described in claim 1, which is characterized in that in step s 5, the uncoiling carries out the open rolling temperature of hot finishing 340~350 DEG C of degree, 180~200 DEG C of finishing temperature, hot rolling deformation amount 70%~90%, percentage pass reduction is up to 50%, obtains Obtain finished product/semi-finished product hot rolled coil with a thickness of 2~10mm.
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CN112522553A (en) * 2020-12-01 2021-03-19 吉林大学 High-performance Al-Mg-Si alloy and preparation method thereof
CN114107760A (en) * 2020-08-26 2022-03-01 宝山钢铁股份有限公司 Novel particle-reinforced 7XXX aluminum alloy thin strip and preparation method thereof
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CN112355259A (en) * 2020-11-09 2021-02-12 中铝材料应用研究院有限公司 Preparation device and preparation method for liquid continuous solidification forming of aluminum alloy sheet
CN112355259B (en) * 2020-11-09 2022-04-19 中铝材料应用研究院有限公司 Preparation device and preparation method for liquid continuous solidification forming of aluminum alloy sheet
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