CN110180009A

CN110180009A - A kind of pet cat and dog disinfection deodorizer and preparation method thereof

Info

Publication number: CN110180009A
Application number: CN201910420051.2A
Authority: CN
Inventors: 陈巧玲; 胡衎; 刘玲玲; 乔丽君; 刘�文; 王思蒙; 赵学成
Original assignee: Anhui Kai Wei Biological Technology Co Ltd
Current assignee: Anhui Kai Wei Biological Technology Co Ltd
Priority date: 2019-05-20
Filing date: 2019-05-20
Publication date: 2019-08-30

Abstract

The present invention provides a kind of pet cat and dog disinfection deodorizers, including following parts by weight material: 0.005-0.1% lemon peel oil, 0.005-0.1% lavender oil, 0.1-2% Radix Notoginseng root extract, 0.1-2% radix stemonae tuberosae root extract, 0.1-2% Radix et Caulis Opuntiae Dillenii extract, 0.1-2% leaf of Mentha piperita extract and 0.15-0.20% chlorocarbon base dimethyl-benzyl amine and 1-3%PEG-7 olive oil carboxylic acid sodium.A kind of pet cat and dog disinfection deodorizer that the present invention prepares, the defects such as overcome essence excessive concentration present in existing pet deodorising product, formula addition alcohol, deodorizing rate low, one kind is provided without artificial synthetic essence, the deodorant products of foul odour after Pet excrement collecting can be effectively eliminated.Pet cat and dog disinfection deodorizer of the present invention is all larger than 99.999% to the killing rate of Escherichia coli and staphylococcus aureus effect 3min, inhibits the breeding and diffusion of bacterium at Pet excrement collecting；Pet cat and dog disinfection deodorizer of the present invention not easy volatile solvents such as spirituosity, can lick and lick, not stimulate respiratory tract, on materials such as floor, carpets without influence, have good environmental safety.

Description

A kind of pet cat and dog disinfection deodorizer and preparation method thereof

Technical field

The present invention relates to field of deodorization, and in particular to a kind of pet cat and dog disinfection deodorizer and preparation method thereof.

Background technique

Iowa State University is attached using headspace solid-phase microextraction (SPME) method measurement Texas beef cattle feeding field The field mephitic air in nearly lower air port, determines vaccary feed place using multidimensional gas chromatographic-olfactometry (MDGC-O) Or near-field signature odor compound is hydrogen sulfide, organic sulfur compound and volatile fatty acid, such as isoamyl with body odor, musty Acid, butyric acid (Wright D W, Eaton D K, Nielsen L T, the et al.Multidimensional of vomitus smell gas chromatography-olfactometry for identification and prioritization of malodors from confined animal feeding operations[C]//American Society ofAgricultural andBiological Engineers.2004:8663-8672.)。

Patent document US9358191B2 is disclosed to various odor pollutants (including methyl mercaptan, hydrogen sulfide, dimethyl sulphide, fourth Acid, isovaleric acid) show the composition of excellent deodorizing effect.Composition includes: (1) polyphenols, is selected from chlorogenic acid, catechu Element, protocatechuic acid, catechol, otoginsenoside, quinhydrones, Quercetin, gallic acid, tannic acid, green coffee extract (polyphenol Content 45%), green-tea extract (polyphenol content 30%), apple extract (polyphenol content 60%), Rosmarinus officinalis extract (polyphenol content 50%), mint extract (polyphenol content 32%), spearmint extract (polyphenol content 33%), grape fruit One of bark extract (polyphenol content 90%) and grape seed extract (polyphenol content 40%)；(2) alkaline matter is selected from Sodium carbonate, potassium carbonate, sodium bicarbonate, ammonium carbonate, borate such as potassium borate and Boratex, silicate such as potassium silicate, sodium metasilicate, original Sodium metasilicate and sodium metasilicate, disodium-hydrogen, sodium sulfite, sodium hydroxide, calcium hydroxide, potassium hydroxide, magnesium hydroxide, hydrogen-oxygen Change one of ammonium, sodium pyrophosphate and potassium pyrophosphate；(3) amino acid be selected from glycine, alanine, glutamic acid, aspartic acid, rely Propylhomoserin, arginine, histidine, serine, cystine, methionine, cysteine, sodium glutamate, NaAsp, tyrosine One of.Polyphenol and amino acid preferred molar ratio are 3:1-1:3.The preferred 8-13 of the pH value of composition reaction system.Select gas Physical examination test tube (Gastech corporation) measures residual odors gas concentration after deodorization.

The patent US20180027843A1 that South Korea's bioscience and biotechnology research institute were delivered in 2018 declare containing The composition of oleoresin Turmeric P.E, licorice and salmon fish-skin extract can reduce in animal excrements cause it is smelly The aminated compounds of taste.

The patent US7056948B2 of George Preti company discloses a kind of combination of stench for reducing animal excrements Object includes chlorophyllin-copper complex, bismuth compound (bismuth salicylate, bismuth subgallate, bismuth citrate) and aluminium polychloride (PAC).It is reported that the chemical substance of animal wastes and urinary odor is made of organic acid and sulphur compound and indoles, the research Select common quantizer scale (General Labeled Magnitude Scale, gLMS) sensory evaluation method.

Wuhan Chopper Lvya Biotechnology Co., Ltd. discloses a kind of edible taste of dispelling for pet living environment Disinfectant (CN105251030A), composition include 0.1-0.8% coco-nut oil fatty acid disinfectant, 0.1-1% aromatic, 0.5- 8% surfactant, 1-12% edible alcohol, 82-98% pure water.The composition can quickly be eliminated in housing pets environment Bad smell kills the microorganism in environment.It is sprayed directly on to the place of pet life, such as kennel can play sterilization and improve empty The effect of makings amount.

Shanghai Shen Asia animal health-care product Fuyang Co., Ltd discloses a kind of pet sterilizing deodorizing agent (CN105724439A), comprising dioctadecyl dimethyl ammonium chloride 0.1-0.4 parts, 0.5-1 parts of double-track suspended self-propelled conveyor, 15-25 parts of benzalkonium bromide, 0.1-0.3 parts of glutaraldehyde, 15-25 parts of pure plant extracting solution, plants essential oil 0.05-0.15, distilled water In right amount.Product of the invention uses after tap water dilution can be used, and is sprayed on Pet cage, urine, at excrement, or need to sterilize Deodorization and sterilization it is aerial, can play the role of disinfection and sterilization, eliminate peculiar smell.

In order to solve the offensive odour discharged after Pet excrement collecting and then pet living environment peculiar smell be caused to disturb people, Pet, which licks, to be licked and more dynamic characteristics cause to urinate and defecate place, bacterial reproduction and diffusion problem at environment of playing, and the present invention can effectively eliminate Foul odour after Pet excrement collecting, inhibit Pet excrement collecting after bacterium breeding and diffusion, meet pet and its owner's living environment without Peculiar smell demand provides pet deodorization and disinfection solution for consumer.

Summary of the invention

The object of the present invention is to provide a kind of pet cat and dog disinfection deodorizers and preparation method thereof, can effectively solve the problem that raising Pet family, feeding dog, pet clinic keep with fresh air and disinfecting problem in pet living environment.

The present invention solves above-mentioned technical problem using following technical scheme:

A kind of pet cat and dog disinfection deodorizer, including following parts by weight material:

0.005-0.1% lemon peel oil, 0.005-0.1% lavender oil, 0.1-2% Radix Notoginseng root extract, 0.1-2% Radix stemonae tuberosae root extract, 0.1-2% Radix et Caulis Opuntiae Dillenii extract, 0.1-2% leaf of Mentha piperita extract and 0.15-0.20% chlorocarbon base Dimethyl-benzyl amine and 1-3%PEG-7 olive oil carboxylic acid sodium.

Further, the deodorant includes the preservative of 0.3-1.0% parts by weight.

Further, the preservative is one or both of Phenoxyethanol and Sensiva SC50.

Further, the deodorant includes the solubilizer of 0.03-0.15% parts by weight and the deionized water of surplus.

Further, the solubilizer includes Cremophor RH40.

The preparation method of this deodorant, mainly comprises the steps that

(1) lemon peel oil, lavender oil and solubilizer are uniformly mixed under stirring conditions, it is molten obtains clear viscous Liquid；

(2) deionized water stirring is added until being completely dissolved in mixed solution in step (1) under stirring conditions, according to Secondary addition Radix Notoginseng root extract, radix stemonae tuberosae root extract, Radix et Caulis Opuntiae Dillenii extract, leaf of Mentha piperita extract, chlorocarbon base dimethyl Benzene methanamine and PEG-7 olive oil carboxylic acid sodium are sufficiently stirred up to being completely dissolved, are eventually adding preservative and are stirred continuously until completely Dissolution；

(3) pH adjusting agent is added into the mixed solution of step (2) under stirring conditions, adjusts the pH of solution system Value obtains pet cat dog disinfection deodorizer after the completion of preparing.

Further, the mixing speed is 300-500rpm.

Further, the pH adjusting agent is sodium citrate.

Further, the pH value of the system is 6.0-8.0.

The present invention has the advantages that

1, the problem of being solved of the invention is to overcome existing pet deodorising product there are essence excessive concentration, add wine Essence, the defects such as deodorizing rate is low, provide a kind of without artificial synthesized natural flavor, can effectively eliminate foul gas after Pet excrement collecting Deodorant products, meet the needs of pet and its owner's living environment free from extraneous odour, inhibit bacterial reproduction and expansion at Pet excrement collecting It dissipates, provides pet deodorization and disinfection solution for consumer；

2, the present invention provides a kind of pet cat and dog disinfection deodorizer, after cat dung cat urine mixture effect 1-3min, deodorization Rate is up to 78%；After acting on 1-3min to dog urine, deodorizing rate is up to 81%, and suitable for solving the family of raising pet, pet clinic is protected It holds with fresh air in living environment；

3, natural plant essential oils, natural plant extracts and fungicide are made jointly in pet cat and dog disinfection deodorizer of the present invention With the killing rate for acting on 3min to Escherichia coli and staphylococcus aureus is all larger than 99.999%, inhibits thin at Pet excrement collecting The breeding and diffusion of bacterium reduce bacterial metabolism organic matter at pet living environment and generate foul gas；

4, the pH=6.0-8.0 of pet cat and dog disinfection deodorizer of the present invention, close to neutrality, close to pet body surface environment pH, Can be sprayed directly on be drained object pollution floor or carpet, cat litter box, cage tool, pet clothing, at environment of playing；Pet of the present invention Cat and dog disinfection deodorizer not easy volatile solvents such as spirituosity, can lick and lick, not stimulate respiratory tract, to materials such as floor, carpets without shadow It rings, there is good environmental safety.

Detailed description of the invention

Fig. 1 shows different samples to stench intensity map after the urine mixture deodorization of cat dung cat；

Fig. 2 indicates different samples to deodorizing rate figure after the urine mixture deodorization of cat dung cat；

Fig. 3 indicates different samples to stench intensity map after dog urine deodorization；

Fig. 4 indicates different samples to deodorizing rate figure after dog urine deodorization；

Fig. 5 is E. coli clones number result figure after the sterilization of 1 sample amounts of the embodiment of the present invention；

Fig. 6 is S. aureus colonies number result figure after the sterilization of 1 sample amounts of the embodiment of the present invention；

Fig. 7 is diagram of 1 sample effect of the embodiment of the present invention in Chinese rural area dog cage tool；

Fig. 8 is 1 sample effect of the embodiment of the present invention to play the diagram of environment in safe enlightening dog；

Fig. 9 is diagram of 1 sample effect of the embodiment of the present invention in Chinese leopard cat spotted cat cage；

Figure 10 is to the diaper for 1 sample effect of the embodiment of the present invention other one Chinese leopard cat spotted cat by figure at urine pollution Show；

Figure 11 is 1 sample effect of the embodiment of the present invention contaminated pallet diagram below collie cage；

Figure 12 is 1 sample effect of the embodiment of the present invention contaminated pallet diagram below PEMBROKE WELSH CORGI cage.

Specific embodiment

The present invention will be further described with reference to the accompanying drawings and detailed description, and following embodiment is intended to illustrate hair Bright rather than limitation of the invention further.

The conventional means that technological means used in following embodiment is well known to those skilled in the art, all raw materials are equal For versatile material.

The present invention is a kind of pet cat and dog disinfection deodorizer, including following parts by weight material:

0.005-0.1% lemon peel oil, 0.005-0.1% lavender oil, 0.1-2% Radix Notoginseng root extract, 0.1-2% Radix stemonae tuberosae root extract, 0.1-2% Radix et Caulis Opuntiae Dillenii extract, 0.1-2% leaf of Mentha piperita extract and 0.15-0.20% chlorocarbon base Dimethyl-benzyl amine, 1-3%PEG-7 olive oil carboxylic acid sodium, the preservative of 0.3-1.0% parts by weight, 0.03-0.15% parts by weight Solubilizer and surplus deionized water.

Further, the preservative is one or both of Phenoxyethanol and Sensiva SC50, the solubilizer For Cremophor RH40.

It is illustrated so that aqueous solution is made by spraying in deodorant as an example.

The weight ratio of the raw material of embodiment 1-3 and comparative example 1-2 is as shown in table 1 below:

1 embodiment 1-3 of table and comparative example 1-2 formula composition

Embodiment 1

The preparation method of pet cat and dog disinfection deodorizer in embodiment 1, comprising the following steps:

(1) lemon peel oil, lavender oil and Cremophor RH40 are uniformly mixed under stirring conditions, are obtained The solution of clear viscous；

(2) deionized water is added to being completely dissolved to the mixed solution of step (1) under conditions of 400rpm is stirred.Successively Radix Notoginseng root extract, radix stemonae tuberosae root extract, Radix et Caulis Opuntiae Dillenii extract, leaf of Mentha piperita extract, chlorocarbon base dimethyl benzene is added Methylamine, PEG-7 olive oil carboxylic acid sodium, Phenoxyethanol are continued stirring until and are completely dissolved；

(3) sodium citrate pH adjusting agent, system is added into the mixed solution of step (2) under conditions of 400rpm is stirred PH value be adjusted to 7.3, pet cat dog disinfection deodorizer is obtained after the completion of preparing.

Embodiment 2

Unlike the first embodiment, the mixing speed in embodiment 2 is 500rpm；In addition, being not added with lemon in embodiment 2 Lemon peel oil, lavender oil and Cremophor RH40.

Embodiment 3

Unlike the first embodiment, mixing speed is 300rpm, PEG-7 olive oil carboxylic acid in step (2) in embodiment 3 Na concn is improved to 2.5%.

Comparative example 1

Unlike embodiment, be not added in 1 step of comparative example (2) Radix Notoginseng root extract, radix stemonae tuberosae root extract, Radix et Caulis Opuntiae Dillenii extract, leaf of Mentha piperita extract, chlorocarbon base dimethyl-benzyl amine and PEG-7 olive oil carboxylic acid sodium.

Comparative example 2

Unlike the first embodiment, PEG-7 olive oil carboxylic acid sodium is not added in comparative example 2 in step (2).

It is as follows that deodorization test is carried out for product preparation-obtained in embodiment and comparative example:

Cat dung cat urinates the foundation of mixture deodorization evaluating in vitro model and deodouring effect verification method:

(1) smelly source is collected: Hefei City, Anhui Province Fu You pet clinic provides this and studies smelly source used.Collect fresh cat excrement Just it with the blend sample of urine, is sealed in 100mL plastic bottle for experimental study of the present invention；

(2) the fresh cat excrement of 0.01g and urine mixture are accurately weighed in 500mL beaker；

(3) different deodorization samples are contained in the plastic mist spray bottle (material: poly terephthalic acid class PET, rule of same size Lattice: 120mL) in, pressing 5 times (every time pressing spray amount of composition about 0.31g), with Sprayable act on entire beaker and Cat excrement and urine mixture surface；Entire external model is urinated and defecated close to cat locates environment.

Cat excrement and the smelly source of urine mixture are not dealt with and are set as blank control, is carried out with the water of deodorant equivalent Processing be set as negative control, embodiment 1-3, comparative example 1-2 and existing product be respectively acting on to smelly source 1min, 3min, After 10min, 30min, 3h, according to 6 grades of representations (as shown in table 2) of stench intensity, sense organ is selected for condition with osmatic Assessment experts, each 5 people of men and women carry out sensory evaluation to stench intensity after deodorization.

Existing product, which includes: that natural miracle dog cat is shared, cleans the dirty deodorization spray agent (NATURE'S that dispels ORIGINAL STAINAND ODOR REMOVER, the place of production: the U.S.), the precious easypro pet decontamination eliminating smell agent (SIMPLE of parentSTAIN&ODOR REMOVER, the place of production: the U.S.), lion king LION pet peculiar smell deodorizing agent (dog use) after an action of the bowels (place of production: Japan), it is small dote on disinfecting, deodorizing curing fluid (place of production: Wuhan), enzyme adds net polyphenol powde pet eliminating smell agent (Wuhan, China), cat It is spraying (potent formula) (dog use) (place of production: Britain) with spraying (place of production: Guangzhou), Glenn bodyguard treasured environment in Taro cat peculiar smell. Deodorizing rate %=(stench average strength after 5- deodorization)/5*100；

Table 2 stench intensity, 6 grades of representations

Stench intensity rank	Reaction of the smell to foul smell
		0	Odorless
1	Stink (detection threshold value) can be felt reluctantly
		2	It is easy to feel less malodor (cognition threshold value)
3	Obviously feel stink
		4	Strong odor
5	Intolerable extremely strong stink

Stench intensity is as shown in table 3 after sample urinates mixture deodorization to cat dung cat, according to data draw to obtain Fig. 1 and Fig. 2.

3 deodorant of table is sprayed stench intensity after deodorization to cat dung cat urine mixture

Fig. 1 shows different samples to stench intensity after the urine mixture deodorization of cat dung cat, and every group of histogram is from left to right While respectively indicating the stench intensity after deodorization 1min, 3min, 10min, 30min and 3h；

Fig. 2 indicates different samples to deodorizing rate after the urine mixture deodorization of cat dung cat, according to data in figure:

Blank control group is that untreated cat dung cat urinates mixture, generates strong offending smell, deodorizing rate 0.

Water process of the negative control group with deodorant equivalent, water can not eliminate the strong unhappy gas that cat dung cat urine generates Taste, deodorizing rate 0.

Enzyme can experience stink after adding net sample deodorization 1min, 3min reluctantly, and stench intensity is respectively 1.1,1.5；It removes Smelly 10min, 30min, 3h are easy to feel less malodor, and stench intensity is respectively 1.8,2.5,2.3, deodorizing rate 63%.

It is small dote on sample deodorization 1min, 3min after can experience stink reluctantly, stench intensity is respectively 1.0,1.0；Deodorization Stink is obviously felt after 10min, 30min, 3h, stench intensity is respectively 1.9,2.5,2.7；Deodorizing rate is 63%.

It is easy to feel stink, stench intensity point after SIMPLE SOLUTION sample deodorization 1min, 3min, 10min, 30min It Wei 1.4,1.5,1.9 and 1.7；It is easy to feel less malodor after deodorization 3h, stench intensity is 2.3, deodorizing rate 65%.

Glenn bodyguard treasured sample deodorization 1min, 3min can experience stink reluctantly, and stench intensity is respectively 1.1,1.1, is removed Smelly 10min, 30min, 3h are easy to feel less malodor, and stench intensity is respectively 1.9,1.9,1.6；Deodorizing rate is 70%.

Stink, stench intensity difference can be experienced after cat Taro sample deodorization 1min, 3min, 10min, 30min reluctantly It is 1.2,1.2,1.5,1.4；Deodorization 3h is easy to feel less malodor, and stench intensity is 1.7；Deodorizing rate is 72%.

Essence excessive concentration in NATURE'S MIEACLE sample formulations, essence can obviously cover cat dung cat urine effluvium Taste, the sucking that evaluator feeds back product odour keep bronchia mucosal uncomfortable, and without obvious smell after deodorization 1min, 3min, stench is strong Degree is respectively 0.8,0.8；Stink can be felt after deodorization 10min, 30min reluctantly, stench intensity is 1.1,1.1；After deodorization 3h, The volatilization of essence smell disperses, and stench intensity is 2.1, is easy to feel less malodor；Deodorizing rate is 76%.

Stink can be experienced reluctantly after lion king's sample deodorization 1min, 3min, 10min, 30min, and stench intensity is respectively 0.9,0.9,1.0,1.2；Deodorization 3h is easy to feel less malodor, and stench intensity is 1.9；Deodorizing rate is 76%.

After comparative example 1 deodorization 1min, 3min, 10min, 30min, stench intensity is respectively 3.0,3.0,3.0,4.0；Deodorization Still there is strong odor after 3h, stench intensity is 3.8；Deodorizing rate is 33%.The display of comparative example 1 is not added with Radix Notoginseng root extract, right Leaf tuber of stemona root extract, Radix et Caulis Opuntiae Dillenii extract, leaf of Mentha piperita extract, chlorocarbon base dimethyl-benzyl amine and PEG-7 olive oil carboxylic Sour sodium, composition can not eliminate the fetor smell in cat dung cat urine mixture.

After comparative example 2 deodorization 1min, 3min, 10min, 30min, stench intensity is respectively 3.0,2.5,3.0,3.0；Deodorization Still there is strong odor after 3h, stench intensity is 3.9；Deodorizing rate is 38%.Compared with Example 1, comparative example 2 is not added with PEG-7 Olive oil carboxylic acid sodium, composition can not eliminate unpleasant fetor smell in cat dung cat urine mixture, make without deodorization With.

After embodiment 1 deodorization 1min, 3min, 10min, 30min, 3h, stink, stench intensity difference can be experienced reluctantly It is 1.0,1.0,1.0,1.2,1.3；Deodorizing rate is 78%；1 deodorizing effect of embodiment is substantially better than natural miracle, lion king, cat too Youth, Glenn bodyguard be precious, precious easypro SIMPLE SOLUTION of parent, enzyme add and net, small the commercial product formula such as dote on.The result shows that containing simultaneously 0.02% lemon peel oil, 0.01% lavender oil, 0.5% Radix Notoginseng root extract, 0.5% radix stemonae tuberosae root extract, 0.5% Radix et Caulis Opuntiae Dillenii extract, 0.5% leaf of Mentha piperita extract, 0.20% chlorocarbon base dimethyl-benzyl amine and 2%PEG-7 olive oil carboxylic acid The composition of sodium has deodorizing effect to the strong unhappy smell that cat dung cat urine generates.

After embodiment 2 deodorization 1min, 3min, 10min, stink can be experienced reluctantly, stench intensity is respectively 1.2, 1.0,1.3；It is easy to feel less malodor after deodorization 30min, 3h, stench intensity is respectively 1.2,1.5；Deodorizing rate is 75%.Knot Fruit shows that lavender oil main component is limonene, citral, sinensal, octanal, capraldehyde, linalool；Lemon peel oil, this A little compounds have certain inhibiting effect to cat excrement specific scent volatile compound smell, but cannot effectively eliminate effluvium Taste.Embodiment 2 does not add any essence or odor suppressing agents, only contains 0.5% Radix Notoginseng root extract, 0.5% radix stemonae tuberosae root Extract, 0.5% Radix et Caulis Opuntiae Dillenii extract, 0.5% leaf of Mentha piperita extract, 0.20% chlorocarbon base dimethyl-benzyl amine and 2% PEG-7 olive oil carboxylic acid sodium, composition have certain deodorizing effect to the strong unhappy smell that cat dung cat urine generates.

After embodiment 3 deodorization 1min, 3min, 10min, 30min, 3h, odorless or stink, stench can be experienced reluctantly Intensity is respectively 1.0,0.4,1.2,0.7,1.3；Deodorizing rate is 82%；3 deodorizing effect of embodiment is substantially better than other commercially available productions Product formula.The result shows that the formula deodorizing effect containing 2.5%PEG-7 olive oil carboxylic acid sodium is more excellent.

Dog urinates deodorization evaluating in vitro model and deodouring effect verification method is established:

(1) smelly source is collected: Hefei City, Anhui Province Fu You pet clinic provides this and studies smelly source used.Under dog rearging cage Square placement tray, the dog urine after a period of time in collection tray, is sealed in 100mL plastic bottle.

(2) in accurately weighing 0.3g dog urine sample in 500mL beaker.

(3) different deodorization samples are contained in the plastic mist spray bottle (material: poly terephthalic acid class PET, rule of same size Lattice: 120mL) in, pressing 4 times (every time pressing spray amount of composition about 0.31g), with Sprayable act on entire beaker and Dog urine surface.

Blank control does not deal with the smelly source of dog urine.Negative control is handled with the water with test sample equivalent, is incited somebody to action Embodiment 1-3, comparative example 1-2 and existing product are respectively acting on smelly source.Sensory evaluation expert indicates according to 6 grades of stench intensity Method (as shown in table 2) carries out sensory evaluation to stench intensity after 1min, 3min, 10min, 30min, 3h.Sensory evaluation expert is Osmatic 5 males and 5 women.

Existing product, which includes: that natural miracle dog cat is shared, cleans the dirty deodorization spray agent (NATURE'S that dispels ORIGINAL STAINAND ODOR REMOVER, the place of production: the U.S.), the precious easypro pet decontamination eliminating smell agent (SIMPLE of parentSTAIN&ODOR REMOVER, the place of production: the U.S.), lion king LION pet peculiar smell deodorizing agent (dog use) after an action of the bowels (place of production: Japan), it is small dote on disinfecting, deodorizing curing fluid (place of production: Wuhan), enzyme adds net polyphenol powde pet eliminating smell agent (Wuhan, China), cat It is spraying (potent formula) (dog use) (place of production: Britain) with spraying (place of production: Guangzhou), Glenn bodyguard treasured environment in Taro cat peculiar smell.

Deodorizing rate %=(stench average strength after 5- deodorization)/5*100；

Stench intensity is as shown in table 4 after sample urinates deodorization to dog, draws to obtain Fig. 3 and Fig. 4 according to 4 data of table.

4 deodorant of table is to stench intensity after the spraying deodorization of dog urine

Fig. 3 indicates different samples to stench intensity map after dog urine deodorization, and table is distinguished on side to every group of histogram from left to right Stench intensity after showing deodorization 1min, 3min, 10min, 30min and 3h；Fig. 4 indicates that different samples urinate deodorization to dog Deodorizing rate afterwards, according to data in figure:

Blank control group is untreated dog urine, generates disgusting smell, deodorizing rate 0.

Negative control is handled with the water with deodorant equivalent, and water can not eliminate offensive smell in dog urine, deodorization Rate is 0.

It is easy to feel less malodor, stench intensity difference after SIMPLE SOLUTION sample deodorization 1min, 3min, 10min It is 1.9,1.8,1.5；Stink can be experienced after deodorization 30min, 3h reluctantly, stench intensity is respectively 1.0,1.3；Deodorizing rate is 70%.

Glenn bodyguard treasured sample deodorization 1min can experience stink reluctantly, and stench intensity is 1.1, deodorization 3min, 10min, It is easy to feel less malodor after 30min, 3h, stench intensity is respectively 1.8,1.3,1.3,1.4.Deodorizing rate is 73%.

Essence excessive concentration in NATURE'S MIEACLE formula, essence can obviously cover the offensive gas that dog urine generates Taste, but evaluator feeds back product odour sucking and keeps bronchia mucosal slightly uncomfortable.After deodorization 1min, 3min, 10min, 30min reluctantly Stink can be experienced, stench intensity is respectively 1.4,1.2,0.8,1.2；Stink, stench can be experienced after deodorization 3h reluctantly Intensity is 1.3；Deodorizing rate is 76%.

It can experience stink after lion king's sample deodorization 1min, 3min, 10min reluctantly, stench intensity is respectively 0.9, 1.0,1.3；It is easy to feel less malodor after deodorization 30min, 3h, stench intensity is respectively 1.3,1.4；Deodorizing rate is 76%.

Stink, stench intensity point can be experienced after cat Taro sample deodorization 1min, 3min, 10min, 30min, 3h reluctantly It Wei 1.1,1.5,1.1,1.2,1.3；Deodorizing rate is 76%.

It is small dote on stink can be experienced after sample 1min, 3min, 10min, 30min reluctantly, stench intensity is not 1.0, 1.1, it is easy to feel less malodor after 1.2,1.1, deodorization 3h, stench intensity is 1.6；Deodorizing rate is 76%.

Enzyme can experience stink, stench intensity difference after adding net sample deodorization 1min, 3min, 10min, 30min reluctantly It is 1.1,1.1,1.1,1.0；Deodorization 3h is easy to feel less malodor, and stench intensity is 1.5.Deodorizing rate is 77%.

After comparative example 1 deodorization 1min, 3min, 10min, 30min, stench intensity is respectively 3.0,3.0,3.0,3.5；Deodorization Still there is strong odor after 3h, stench intensity is 4.0；Deodorizing rate is 34%.The extraction of antibacterial agent Roots of Panax Notoginseng is not added in comparative example 1 Object, radix stemonae tuberosae root extract, Radix et Caulis Opuntiae Dillenii extract, leaf of Mentha piperita extract, chlorocarbon base dimethyl-benzyl amine and PEG-7 olive Oily carboxylic acid sodium, comparative example 1 can not eliminate the offensive smell that dog urine generates, without deodorizing effect.

After comparative example 2 deodorization 1min, 3min, 10min, 30min, stench intensity is respectively 3.0,2.5,3.0,3.0；Deodorization Still there is strong odor after 3h, stench intensity is 4.0；Deodorizing rate is 38%.Compared with Example 1, comparative example 2 is not added with PEG-7 Olive oil carboxylic acid sodium.Comparative example 2 can not eliminate disgusting smell in dog urine, without deodorization.

After embodiment 1 deodorization 1min, 3min, 10min, 30min, 3h, odorless or stink, stench can be felt reluctantly Intensity is 1.0,0.9,0.8,1.0 and 1.0, deodorizing rate 81%.1 deodorizing effect of embodiment is substantially better than other commercial product and matches Side.The result shows that containing 0.02% lemon peel oil, 0.01% lavender oil, 0.5% Radix Notoginseng root extract, 0.5% pair simultaneously Leaf tuber of stemona root extract, 0.5% Radix et Caulis Opuntiae Dillenii extract, 0.5% leaf of Mentha piperita extract and 0.20% chlorocarbon Ji Erjiajibenjia Amine, 2%PEG-7 olive oil carboxylic acid sodium composition to dog urine have deodorizing effect.

After embodiment 2 deodorization 1min, 3min, 10min, odorless or stink can be experienced reluctantly, make us detesting in dog urine Bad odor taste is largely eliminated, and stench intensity is respectively 1.0,0.7,1.0.It can be experienced reluctantly after deodorization 30min, 3h smelly Taste, stench intensity are respectively 1.3 and 1.1, deodorizing rate 79%.It is precious, close precious easypro that 2 deodorizing effect of embodiment is substantially better than Glenn bodyguard SIMPLE SOLUTION, 2 deodorizing effect of embodiment and right miracle, lion king, cat Taro, it is small dote on, enzyme adds net phase to work as.The result shows that The aromatic compounds such as lemon peel oil, lavender oil have certain inhibition to make the offensive smell of volatile compound in dog urine With, but foul odour cannot be effectively eliminated.Embodiment 2 does not add any essence or odor suppressing agents, only contains 0.5% Roots of Panax Notoginseng Extract, 0.5% radix stemonae tuberosae root extract, 0.5% Radix et Caulis Opuntiae Dillenii extract, 0.5% leaf of Mentha piperita extract, 0.20% chlorocarbon Base dimethyl-benzyl amine and 2%PEG-7 olive oil carboxylic acid sodium have deodorizing effect to offensive smell in dog urine.

After embodiment 3 deodorization 1min, 3min, 10min, 30min, odorless or stink can be experienced reluctantly, stench is strong Degree is respectively 1.0,0.4,0.5,1.2.Stink can be experienced after deodorization 3h reluctantly, stench intensity is chosen as 1.1, and deodorizing rate is 83%.Deodorizing effect is substantially better than other commercial product formula.The result shows that matching containing 2.5%PEG-7 olive oil carboxylic acid sodium Square deodorizing effect is more excellent.

According to China " disinfection technology standard " (2002 editions), with Escherichia coli ATCC25922, staphylococcus aureus ATCC6538 is indicator strain, is tested using bacteria quantified killing test method, through 3 repetitions experiments have shown that, embodiment 1 99.999% is all larger than to the killing rate of Escherichia coli and staphylococcus aureus effect 3min in suspension.

After Fig. 5 indicates quantitative sterilization, E. coli clones number in figure as a result, show after cultivating in 37 DEG C of incubators for 24 hours Without bacterium colony.After Fig. 6 indicates quantitative sterilization, S. aureus colonies number knot after being to be cultivated for 24 hours in 37 DEG C of incubators in temperature Fruit, display is without bacterium colony in figure.

Pet clinic's scene deodorization test:

It is carried out in " 2017 years Chinese hundred good pet clinics " Chinese economic and technological development zone Fu You pet clinic, Hefei City The live deodorization of present composition embodiment 1 is tested.

Application method: present composition embodiment 2 is contained in plastic mist spray bottle (material: poly terephthalic acid class PET, specification: 450mL) in, pressing sprays amount of composition about 1.0g every time.Distance 20cm, avoid the eye of people and pet, mouth, Nose, alignment needs to sterilize, dispels and the aerial spraying of taste region or directly sprays against cat stool and urine place, nest pad, cage tool, cat litter box etc. It spills.Sufficiently it should be made to parch after sprinkling.Record deodorization object: Pet cage (Fig. 7, Fig. 9), is urinated and defecated at environment of playing (Fig. 8) Locate (Figure 10, Figure 11, Figure 12)；Record pet kind；It records spray number (compression number)；Spraying deodorization 3- After 10min (instant), 2h (long-time), according to 6 grades of representations (as shown in table 2) of stench intensity, to stench intensity before and after deodorization Carry out sensory evaluation；Deodorizing rate %=(stench intensity after 5- deodorization)/5*100；Embodiment 1 is tested in pet clinic's scene deodorization As a result it is listed in table 5.

5 embodiment 1 of table is in pet clinic's scene deodorization test result

We are in " 2017 years Chinese hundred good pet clinics " economic and technological development zone Fu You pet clinic, Chinese Hefei City Carry out the live deodorization test of present composition embodiment 1.

Fig. 7 is the diagram that the embodiment of the present invention 1 acts on Chinese rural area dog cage tool, and stench intensity is after deodorization 3-10min 1.9, it is easy to feel less malodor, deodorizing rate 62%.Stench intensity is 2.1 after deodorization 2h, is easy to feel less malodor, deodorization Rate is 58%.

Fig. 8 is the diagram that the embodiment of the present invention 1 acts on that teddy bear formula Poodle is played at environment, after deodorization 3-10min Stench intensity is 1.3, can experience stink, deodorizing rate 74% reluctantly；Stench intensity is 1.7 after deodorization 2h, is easy to feel Less malodor, deodorizing rate 66%.

Fig. 9 is the diagram that the embodiment of the present invention 1 acts on Chinese leopard cat spotted cat cage, and stench intensity is after deodorization 3-10min 1.5, stink, deodorizing rate 70% can be experienced reluctantly；Stench intensity is 1.8 after deodorization 2h, is easy to feel less malodor, remove Smelly rate is 64%.

Figure 10 is to the diagram for being used in the diaper that one is polluted by Chinese leopard cat spotted cat urine for the embodiment of the present invention 1, deodorization 3- Stench intensity is 1.4 after 10min, can feel stink, deodorizing rate 72% reluctantly；It is sprayed deodorization against diaper, it can be temporary Mitigate the offensive smell of cat urine in cage, reduces diaper replacement frequency；Stench intensity is 3 after deodorization 2h, hence it is evident that feels smelly Taste, deodorizing rate 40%.

Figure 11 is the diagram that the embodiment of the present invention 1 is used in contaminated pallet below collie cage, deodorization 3- Stench intensity is 1.5 after 10min, is easy to feel less malodor, deodorizing rate 70%；Stench intensity is 1.7 after deodorization 2h, is easy Feel less malodor, deodorizing rate 66%.

Figure 12 is the diagram that the embodiment of the present invention 1 is used in contaminated pallet below PEMBROKE WELSH CORGI cage, deodorization 3- Stench intensity is 1.2 after 10min, can experience stink, deodorizing rate 76% reluctantly；Stench intensity is 2.1 after deodorization 2h, is held It is susceptible to arrive less malodor, deodorizing rate 58%.

To the smelly source of pet, (3-10min) average deodorizing rate is 71% to present composition embodiment 1 immediately, and deodorizing effect can To receive, to the smelly source of pet, (2h) average deodorizing rate is 59% for a long time；Since the smelly source generation frequency of pet clinic is higher, when long Between deodorizing effect it is lower.

Finally, it should be noted that above embodiments are only to illustrate the present invention and not limit technology described in the invention Scheme；Those skilled in the art should understand that still can modify to the present invention or equivalent replacement；And all are not It is detached from the technical solution and its improvement of the spirit and scope of the present invention, should all be covered within the scope of the claims of the present invention.

Claims

1. a kind of pet cat and dog disinfection deodorizer, which is characterized in that including following parts by weight material:

0.005-0.1% lemon peel oil, 0.005-0.1% lavender oil, 0.1-2% Radix Notoginseng root extract, 0.1-2% are to leaf Tuber of stemona root extract, 0.1-2% Radix et Caulis Opuntiae Dillenii extract, 0.1-2% leaf of Mentha piperita extract and 0.15-0.20% chlorocarbon base diformazan Base benzene methanamine and 1-3%PEG-7 olive oil carboxylic acid sodium.

2. deodorant according to claim 1, which is characterized in that the deodorant includes the anti-of 0.3-1.0% parts by weight Rotten agent.

3. deodorant according to claim 2, which is characterized in that the preservative is Phenoxyethanol and Sensiva SC50 One or both of.

4. deodorant according to claim 2, which is characterized in that the deodorant includes the increasing of 0.03-0.6% parts by weight The deionized water of solvent and surplus.

5. deodorant according to claim 4, which is characterized in that the solubilizer includes Cremophor RH40.

6. the preparation method of deodorant as claimed in claim 4, which comprises the following steps:

(1) lemon peel oil, lavender oil and solubilizer are uniformly mixed under stirring conditions, obtain clear viscous solution；

(2) deionized water stirring is added until being completely dissolved in mixed solution in step (1) under stirring conditions, successively plus Enter Radix Notoginseng root extract, radix stemonae tuberosae root extract, Radix et Caulis Opuntiae Dillenii extract, leaf of Mentha piperita extract, chlorocarbon Ji Erjiajibenjia Amine and PEG-7 olive oil carboxylic acid sodium are sufficiently stirred until be completely dissolved, be eventually adding preservative be stirred continuously until it is completely molten Solution；

(3) pH adjusting agent is added into the mixed solution of step (2) under stirring conditions, adjusts the pH value of solution, has prepared Pet cat dog disinfection deodorizer is obtained at rear.

7. preparation method according to claim 6, which is characterized in that the mixing speed is 300-500rpm.

8. preparation method according to claim 6, which is characterized in that the pH adjusting agent is sodium citrate.

9. preparation method according to claim 6, which is characterized in that the pH value of the system is 6.0-8.0.