CN110157367A - A kind of disposable sanitary articles mosquito repellent hot melt adhesive and preparation method thereof - Google Patents
A kind of disposable sanitary articles mosquito repellent hot melt adhesive and preparation method thereof Download PDFInfo
- Publication number
- CN110157367A CN110157367A CN201910497152.XA CN201910497152A CN110157367A CN 110157367 A CN110157367 A CN 110157367A CN 201910497152 A CN201910497152 A CN 201910497152A CN 110157367 A CN110157367 A CN 110157367A
- Authority
- CN
- China
- Prior art keywords
- hot melt
- melt adhesive
- mosquito repellent
- disposable sanitary
- sanitary articles
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J153/00—Adhesives based on block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Adhesives based on derivatives of such polymers
- C09J153/02—Vinyl aromatic monomers and conjugated dienes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J157/00—Adhesives based on unspecified polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C09J157/02—Copolymers of mineral oil hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses a kind of disposable sanitary articles mosquito repellent hot melt adhesive and preparation method thereof, the hot melt adhesive is made of main polymer, tackifying resin, White Mineral Oil, culicifuge and antioxidant, preparation method includes the following steps: 1) reaction kettle is added in main polymer, White Mineral Oil and antioxidant, 145~160 DEG C are heated to, stirring is vacuumized and is melted completely to material;2) reaction kettle is added in tackifying resin, constant temperature is stirred to material and melted completely, adds culicifuge, and constant temperature stirs evenly, then stops stirring, and is evacuated to bubble-free in material.Disposable sanitary articles mosquito repellent hot melt adhesive of the invention has apparent expelling mosquito, causes the unresponsive effect of mosquito, and adhesion strength is high, peeling force is big.
Description
Technical field
The present invention relates to a kind of disposable sanitary articles mosquito repellent hot melt adhesive and preparation method thereof.
Background technique
Hot melt adhesive is a kind of adhesive of plasticity, its physical state changes with temperature and changed in certain temperature range
Become, and chemical characteristic is constant, it is non-toxic and tasteless, belong to environmental-protecting chemical product, is widely used in hygienic articles, packaging, book
Nationality bookbinding, clothes, adhesive tape, shoemaking, refrigerator, cable, automobile and other industries.
The state of development in domestic hot melt adhesive market and developed country are widely different, on the developed countries such as America and Europe, Japan and ground
Area, the industry for accounting for 4 before hot melt adhesive market is packaging, hygienic articles, bookbinding, carpenter or assembling respectively, wherein packaging row
Industry accounts for the 30%~40% of market aggregate demand, and domestic hot melt adhesive market account for former industries be respectively hygienic articles, clothes,
Glue stick, books and packaging, wherein hygienic articles are ranked first with glue, and it is sanitary napkin and baby that accounting is maximum in hygienic articles
Both disposable sanitary articles of paper diaper.
Disposable sanitary articles are the market of a high speed development with hot melt adhesive market, and the past 10 years compound growth rates are high
Up to 16%.With the relieving of national two tire policies, the market demand of baby paper diaper is very big, and hot melt adhesive is baby paper diaper
Basic material, therefore have broad application prospects.Along with the fast development and consumption upgrading in market, not only to disposably defending
The quality of raw articles has higher requirement, and to the function of disposable sanitary articles, there has also been some new requirements, such as urinate
Aobvious, sterilization, repelling effect etc..
Therefore, a kind of disposable sanitary articles mosquito repellent hot melt adhesive product is developed for pushing the upgrading of downstream product function
The replacement is of great significance.
Summary of the invention
The purpose of the present invention is to provide a kind of disposable sanitary articles mosquito repellent hot melt adhesive and preparation method thereof.
The technical solution used in the present invention is:
A kind of disposable sanitary articles mosquito repellent hot melt adhesive, consists of the following mass percentage components:
Main polymer: 10%~25%;
Tackifying resin: 40%~55%;
White Mineral Oil: 10%~20%;
Culicifuge: 5%~20%;
Antioxidant: 0.1%~0.5%.
Preferably, a kind of disposable sanitary articles mosquito repellent hot melt adhesive, consists of the following mass percentage components:
Main polymer: 14%~25%;
Tackifying resin: 45%~55%;
White Mineral Oil: 10%~20%;
Culicifuge: 8%~20%;
Antioxidant: 0.1%~0.5%.
Preferably, the main polymer is that Styrene-Butadiene-Styrene Block Copolymer (SBS), styrene-are different
Isoprene-styrene block copolymer (SIS), styrene-ethylene-butylene-styrene block copolymer (SEBS), ethylene-vinegar
At least one of sour ethylene copolymer (EVA).
Preferably, the mass percentage of styrene is less than in the Styrene-Butadiene-Styrene Block Copolymer
30%.
Preferably, the mass percentage of styrene is less than in the styrene-isoprene-styrene block copolymer
30%.
Preferably, the tackifying resin is at least one of Petropols, hydrogenated petroleum resin.
Preferably, the Petropols are at least one of C5 Petropols, C9 Petropols, DCPD Petropols.
Preferably, the hydrogenated petroleum resin is C5 hydrogenated petroleum resin, C9 hydrogenated petroleum resin, DCPD hydrotreated petroleum tree
At least one of rouge.
Preferably, the mass percentage of cycloalkane is greater than 40% in the White Mineral Oil.
Preferably, the culicifuge is at least one of mosquito repellent rouge, Peppermint essential oil, eucalyptus leaf oil.
Preferably, the antioxidant is antioxidant 1010, irgasfos 168, antioxidant CA, at least one in antioxidant BHT
Kind.
The preparation method of above-mentioned disposable sanitary articles mosquito repellent hot melt adhesive the following steps are included:
1) reaction kettle is added in main polymer, White Mineral Oil and antioxidant, is heated to 145~160 DEG C, vacuumize stirring extremely
Material melts completely;
2) reaction kettle is added in tackifying resin, constant temperature is stirred to material and melted completely, adds culicifuge, and constant temperature stirring is equal
It is even,
Stop stirring again, be evacuated to bubble-free in material, obtains disposable sanitary articles mosquito repellent hot melt adhesive.
The beneficial effects of the present invention are: disposable sanitary articles mosquito repellent hot melt adhesive of the invention, which has, significantly drives mosquito
Worm causes the unresponsive effect of mosquito, and adhesion strength is high, peeling force is big.
Detailed description of the invention
Fig. 1 is the infrared spectrogram of the disposable sanitary articles mosquito repellent hot melt adhesive of embodiment 3.
Specific embodiment
The present invention will be further explained combined with specific embodiments below and explanation.
Embodiment 1:
A kind of disposable sanitary articles mosquito repellent hot melt adhesive, raw material composition are as shown in the table:
A kind of raw material of the disposable sanitary articles of table 1 mosquito repellent hot melt adhesive forms table
The preparation method of above-mentioned disposable sanitary articles mosquito repellent hot melt adhesive the following steps are included:
1) reaction kettle, heating is added in Styrene-Butadiene-Styrene Block Copolymer, White Mineral Oil and antioxidant 1010
To 150 DEG C, vacuumizes stirring and melted completely to material;
2) reaction kettle is added in C5 Petropols, constant temperature is stirred to material and melted completely, adds Peppermint essential oil, constant temperature stirs
It mixes uniformly, then stops stirring, be evacuated to bubble-free in material, obtain disposable sanitary articles mosquito repellent hot melt adhesive (infrared light
Spectrogram is as shown in Figure 1).
Above-mentioned disposable sanitary articles are tested for the property with mosquito repellent hot melt adhesive, test result is as follows shown in table:
The performance test results of table 2 disposable sanitary articles mosquito repellent hot melt adhesive
Note:
SUMMIT: spiral glue spraying mode.
Embodiment 2:
A kind of disposable sanitary articles mosquito repellent hot melt adhesive, raw material composition are as shown in the table:
A kind of raw material of the disposable sanitary articles of table 3 mosquito repellent hot melt adhesive forms table
The preparation method of above-mentioned disposable sanitary articles mosquito repellent hot melt adhesive the following steps are included:
1) reaction kettle is added in styrene-ethylene-butylene-styrene block copolymer, White Mineral Oil and antioxidant 1010, added
Heat vacuumizes stirring and melts completely to material to 150 DEG C;
2) reaction kettle is added in C9 hydrogenated petroleum resin, constant temperature is stirred to material and melted completely, adds eucalyptus leaf oil, permanent
Temperature stirs evenly, then stops stirring, and is evacuated to bubble-free in material, obtains disposable sanitary articles mosquito repellent hot melt adhesive.
Above-mentioned disposable sanitary articles are tested for the property with mosquito repellent hot melt adhesive, test result is as follows shown in table:
The performance test results of table 4 disposable sanitary articles mosquito repellent hot melt adhesive
Note:
SUMMIT: spiral glue spraying mode.
Embodiment 3:
A kind of disposable sanitary articles mosquito repellent hot melt adhesive, raw material composition are as shown in the table:
A kind of raw material of the disposable sanitary articles of table 5 mosquito repellent hot melt adhesive forms table
The preparation method of above-mentioned disposable sanitary articles mosquito repellent hot melt adhesive the following steps are included:
1) by Styrene-Butadiene-Styrene Block Copolymer, ethylene-vinyl acetate copolymer, White Mineral Oil and antioxidant
1010 are added reaction kettle, are heated to 160 DEG C, vacuumize stirring and melt completely to material;
2) reaction kettle is added in DCPD Petropols, constant temperature is stirred to material and melted completely, adds mosquito repellent rouge, constant temperature stirs
It mixes uniformly, then stops stirring, be evacuated to bubble-free in material, obtain disposable sanitary articles mosquito repellent hot melt adhesive.
Above-mentioned disposable sanitary articles are tested for the property with mosquito repellent hot melt adhesive, test result is as follows shown in table:
The performance test results of table 6 disposable sanitary articles mosquito repellent hot melt adhesive
Note:
SUMMIT: spiral glue spraying mode.
Embodiment 4:
A kind of disposable sanitary articles mosquito repellent hot melt adhesive, raw material composition are as shown in the table:
A kind of raw material of the disposable sanitary articles of table 7 mosquito repellent hot melt adhesive forms table
The preparation method of above-mentioned disposable sanitary articles mosquito repellent hot melt adhesive the following steps are included:
1) reaction kettle is added in styrene-isoprene-styrene block copolymer, White Mineral Oil and antioxidant 1010, added
Heat vacuumizes stirring and melts completely to material to 155 DEG C;
2) reaction kettle being added in C5 Petropols and C9 hydrogenated petroleum resin, constant temperature is stirred to material and is melted completely, then plus
Enter Peppermint essential oil and eucalyptus leaf oil, constant temperature stirs evenly, then stops stirring, and is evacuated to bubble-free in material, obtains disposable
Amenities mosquito repellent hot melt adhesive.
Above-mentioned disposable sanitary articles are tested for the property with mosquito repellent hot melt adhesive, test result is as follows shown in table:
The performance test results of table 8 disposable sanitary articles mosquito repellent hot melt adhesive
Note:
SUMMIT: spiral glue spraying mode.
Embodiment 5:
A kind of disposable sanitary articles mosquito repellent hot melt adhesive, raw material composition are as shown in the table:
A kind of raw material of the disposable sanitary articles of table 9 mosquito repellent hot melt adhesive forms table
The preparation method of above-mentioned disposable sanitary articles mosquito repellent hot melt adhesive the following steps are included:
1) reaction kettle is added in styrene-isoprene-styrene block copolymer, White Mineral Oil and antioxidant 1010, added
Heat vacuumizes stirring and melts completely to material to 155 DEG C;
2) reaction kettle being added in C5 Petropols and C9 hydrogenated petroleum resin, constant temperature is stirred to material and is melted completely, then plus
Enter dimethyl phthalate and eucalyptus leaf oil, constant temperature stirs evenly, then stops stirring, and is evacuated to bubble-free in material, is disposably defended
Raw articles mosquito repellent hot melt adhesive.
Above-mentioned disposable sanitary articles are tested for the property with mosquito repellent hot melt adhesive, test result is as follows shown in table:
The performance test results of table 10 disposable sanitary articles mosquito repellent hot melt adhesive
Note:
SUMMIT: spiral glue spraying mode.
The above embodiment is a preferred embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment
Limitation, other any changes, modifications, substitutions, combinations, simplifications made without departing from the spirit and principles of the present invention,
It should be equivalent substitute mode, be included within the scope of the present invention.
Claims (10)
1. a kind of disposable sanitary articles mosquito repellent hot melt adhesive, it is characterised in that: consist of the following mass percentage components:
Main polymer: 10%~25%;
Tackifying resin: 40%~55%;
White Mineral Oil: 10%~20%;
Culicifuge: 5%~20%;
Antioxidant: 0.1%~0.5%.
2. disposable sanitary articles according to claim 1 mosquito repellent hot melt adhesive, it is characterised in that: the main polymer
For Styrene-Butadiene-Styrene Block Copolymer, styrene-isoprene-styrene block copolymer, styrene-second
At least one of alkene-butylene-styrene block copolymer, ethylene-vinyl acetate copolymer.
3. disposable sanitary articles according to claim 2 mosquito repellent hot melt adhesive, it is characterised in that: the styrene-fourth
The mass percentage of styrene is less than 30% in styrene block copolymer.
4. disposable sanitary articles according to claim 2 mosquito repellent hot melt adhesive, it is characterised in that: the styrene-is different
The mass percentage of styrene is less than 30% in isoprene-styrene block copolymer.
5. disposable sanitary articles according to claim 1 or 2 mosquito repellent hot melt adhesive, it is characterised in that: the thickening tree
Rouge is at least one of Petropols, hydrogenated petroleum resin.
6. disposable sanitary articles according to claim 5 mosquito repellent hot melt adhesive, it is characterised in that: the Petropols are
At least one of C5 Petropols, C9 Petropols, DCPD Petropols.
7. disposable sanitary articles according to claim 5 mosquito repellent hot melt adhesive, it is characterised in that: the non-hydrogenated petroleum tree
Rouge is at least one of C5 hydrogenated petroleum resin, C9 hydrogenated petroleum resin, DCPD hydrogenated petroleum resin.
8. disposable sanitary articles according to claim 1 or 2 mosquito repellent hot melt adhesive, it is characterised in that: the White Mineral Oil
The mass percentage of middle cycloalkane is greater than 40%.
9. disposable sanitary articles according to claim 1 or 2 mosquito repellent hot melt adhesive, it is characterised in that: the culicifuge
For at least one of mosquito repellent rouge, Peppermint essential oil, eucalyptus leaf oil.
10. the preparation method of mosquito repellent hot melt adhesive of disposable sanitary articles described in any one of claim 1~9, special
Sign is: the following steps are included:
1) reaction kettle is added in main polymer, White Mineral Oil and antioxidant, is heated to 145~160 DEG C, vacuumize stirring to material
Melting completely;
2) reaction kettle being added in tackifying resin, constant temperature is stirred to material and is melted completely, adds culicifuge, and constant temperature stirs evenly,
Stop stirring again, be evacuated to bubble-free in material, obtains disposable sanitary articles mosquito repellent hot melt adhesive.
Priority Applications (1)
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CN201910497152.XA CN110157367A (en) | 2019-06-06 | 2019-06-06 | A kind of disposable sanitary articles mosquito repellent hot melt adhesive and preparation method thereof |
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CN201910497152.XA CN110157367A (en) | 2019-06-06 | 2019-06-06 | A kind of disposable sanitary articles mosquito repellent hot melt adhesive and preparation method thereof |
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CN201910497152.XA Pending CN110157367A (en) | 2019-06-06 | 2019-06-06 | A kind of disposable sanitary articles mosquito repellent hot melt adhesive and preparation method thereof |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111978897A (en) * | 2020-09-04 | 2020-11-24 | 上海路嘉胶粘剂有限公司 | Defluorination pressure-sensitive hot melt adhesive for sanitary towel breathable film back adhesive and preparation method thereof |
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CN1646656A (en) * | 2002-04-17 | 2005-07-27 | 于尔戈实验室 | Novel hydrophilic adhesive compositions |
CN101186794A (en) * | 2007-12-03 | 2008-05-28 | 周飞鹏 | Adhesive tape for mosquito eradication lamp, hot-melt adhesive of the adhesive tap and preparation method of the hot-melt adhesive |
CN102170917A (en) * | 2008-08-06 | 2011-08-31 | 英威达技术有限公司 | Preparation of elastic composite structures useful for components of disposable hygiene products and articles of apparel |
WO2015195613A1 (en) * | 2014-06-16 | 2015-12-23 | Ingevity South Carolina, Llc | Composite polymer materials for modification of adhesive compositions and associated methods of manufacture |
CN106085306A (en) * | 2016-08-24 | 2016-11-09 | 泉州市嘉华卫生用品有限公司 | A kind of diaper PUR and preparation method thereof |
CN106281150A (en) * | 2016-09-07 | 2017-01-04 | 李金平 | A kind of diaper hot melt adhesive |
-
2019
- 2019-06-06 CN CN201910497152.XA patent/CN110157367A/en active Pending
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1646656A (en) * | 2002-04-17 | 2005-07-27 | 于尔戈实验室 | Novel hydrophilic adhesive compositions |
CN101186794A (en) * | 2007-12-03 | 2008-05-28 | 周飞鹏 | Adhesive tape for mosquito eradication lamp, hot-melt adhesive of the adhesive tap and preparation method of the hot-melt adhesive |
CN102170917A (en) * | 2008-08-06 | 2011-08-31 | 英威达技术有限公司 | Preparation of elastic composite structures useful for components of disposable hygiene products and articles of apparel |
WO2015195613A1 (en) * | 2014-06-16 | 2015-12-23 | Ingevity South Carolina, Llc | Composite polymer materials for modification of adhesive compositions and associated methods of manufacture |
CN106085306A (en) * | 2016-08-24 | 2016-11-09 | 泉州市嘉华卫生用品有限公司 | A kind of diaper PUR and preparation method thereof |
CN106281150A (en) * | 2016-09-07 | 2017-01-04 | 李金平 | A kind of diaper hot melt adhesive |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111978897A (en) * | 2020-09-04 | 2020-11-24 | 上海路嘉胶粘剂有限公司 | Defluorination pressure-sensitive hot melt adhesive for sanitary towel breathable film back adhesive and preparation method thereof |
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PB01 | Publication | ||
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Application publication date: 20190823 |