CN110128015A - A kind of enamel frit makeing method increasing glaze surface evenness - Google Patents
A kind of enamel frit makeing method increasing glaze surface evenness Download PDFInfo
- Publication number
- CN110128015A CN110128015A CN201910341959.4A CN201910341959A CN110128015A CN 110128015 A CN110128015 A CN 110128015A CN 201910341959 A CN201910341959 A CN 201910341959A CN 110128015 A CN110128015 A CN 110128015A
- Authority
- CN
- China
- Prior art keywords
- glaze
- surface evenness
- enamel frit
- frit makeing
- increasing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
Abstract
The invention discloses a kind of enamel frit makeing methods for increasing glaze surface evenness, including step are as follows: (1) weigh glaze quartz, potassium feldspar, kaolin and quick lime, and be added in grinding drum, then water, opacifiers, antibacterial agent and colorant are added into the grinding drum, grinding uniformly obtains glaze;(2) to the glaze material stirring, it is homogenized aging, to be homogenized glaze;(3) by the glaze glazing of homogenizing in porcelain billet, semi-finished product ceramic products are made;(4) the semi-finished product ceramic products are placed in kiln and are sintered, obtain ceramic products.Through the above way, the enamel frit makeing method of increase glaze surface evenness of the invention, temperature change when by choosing suitable glaze component and control sintering, keep sintered ceramic products glaze surface evenness good, glaze will not generate defect, with extraordinary antibacterial effect, increase the aesthetics of ceramic products entirety, the welcome by consumer.
Description
Technical field
The present invention relates to technical field of ceramic production, more particularly to a kind of enamel frit makeing method for increasing glaze surface evenness.
Background technique
Ceramics are the general names of pottery, stoneware and porcelain, with clay fire vessel cry pottery, with china clay firing vessel
Porcelain.It is raw material that ceramics, which are with clay and china clay both clays of different nature, by works such as ingredient, molding, drying, roastings
Implements made of skill process can be ceramics.
Glaze is the colorless or colored glassy thin layer for being covered on ceramic surface, is with raw mineral materials and other raw materials
Cooperation, is made glaze slip by grinding, imposes on billet surface, calcine through certain temperature.Glaze can increase product mechanical strength,
Thermal stability and dielectric strength, there are also beautify implements, convenient for wipe wash, not erosion dirty by dust raw meat the features such as.Existing enamel frit makeing
Journey is unable to control the flatness of glaze layer, and glazing effect is bad.
Summary of the invention
The invention mainly solves the technical problem of providing a kind of enamel frit makeing method for increasing glaze surface evenness, obtained glaze
Ornamental value is high.
In order to solve the above technical problems, one technical scheme adopted by the invention is that: a kind of increase glaze surface evenness is provided
Enamel frit makeing method, including step are as follows: (1) weigh glaze quartz, potassium feldspar, kaolin and quick lime, and be added in grinding drum,
Water, opacifiers, antibacterial agent and colorant is added into the grinding drum again, grinding uniformly obtains glaze;(2) glaze is stirred
It mixes, is homogenized aging, to be homogenized glaze;(3) by the glaze glazing of homogenizing in porcelain billet, semi-finished product ceramic products are made;
(4) the semi-finished product ceramic products are placed in kiln and are sintered, obtain ceramic products.
In a preferred embodiment of the present invention, the content of glaze each component described in step (1) are as follows: in parts by weight,
20-25 parts quartzy, 50-55 parts of potassium feldspar, 9-13 parts of kaolin, 12-16 parts of quick lime, 1-3 parts of opacifiers, antibacterial agent
4-7 parts, 1-3 parts of colorant.
In a preferred embodiment of the present invention, opacifiers described in step (1) is tin oxide, titanium dioxide, titanium dioxide
One of zirconium, phosphate are a variety of.
In a preferred embodiment of the present invention, antibacterial agent described in step (1) be dissolved in water containing zinc ion, copper from
One of son, silver ion or a variety of inorganic salts.
In a preferred embodiment of the present invention, colorant described in step (1) is Cu oxide, ferriferous oxide, cobalt oxide
One of agent is a variety of.
In a preferred embodiment of the present invention, it is 15-20 hours that the aging time is homogenized described in step (2).
In a preferred embodiment of the present invention, it is room temperature that aging temperature is homogenized described in step (2).
In a preferred embodiment of the present invention, enameling method described in step (3) for brushing glazing or pours glaze.
In a preferred embodiment of the present invention, sintering process described in step (4) are as follows: first will be in kiln in 1 hour
700 degrees Celsius are warming up to, keeps the temperature 30-40 minutes, then 1100 degrees Celsius will be warming up in kiln in 1.5 hours, keeps the temperature 30-40
Minute, it is finally cooled to 900 degrees Celsius in 30-40 minutes, keeps the temperature 60-90 minutes.
In a preferred embodiment of the present invention, it is taken out after being sintered described in step (4), natural cooling.
The beneficial effects of the present invention are: the enamel frit makeing method of increase glaze surface evenness of the invention, by choosing suitable glaze
Expect temperature change when component and control sintering, keep sintered ceramic products glaze surface evenness good, glaze will not generate defect, tool
There is extraordinary antibacterial effect, increases the aesthetics of ceramic products entirety, the welcome by consumer.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiments of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common
Technical staff's all other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
Embodiment one:
A kind of enamel frit makeing method increasing glaze surface evenness, including step are provided are as follows:
(1) glaze quartz, potassium feldspar, kaolin and quick lime are weighed, and is added in grinding drum, then is added into the grinding drum
Enter water, opacifiers, antibacterial agent and colorant, grinding uniformly obtains glaze, wherein the content of the glaze each component are as follows: quartz
20 kg, 55 kg of potassium feldspar, 9 kg of kaolin, 16 kg of quick lime, 1 kg of opacifiers, 7 kg of antibacterial agent, colorant 1
Kg, the opacifiers be tin oxide and titanium dioxide mixture, the antibacterial agent be dissolved in water containing zinc ion, copper from
One of son, silver ion or a variety of inorganic salts, the colorant are one of cobalt oxide agent or a variety of, and it is suitable to choose
Component works in coordination between each component, can guarantee the planarization of the glaze in subsequent step (2), (3) and (4);
(2) to the glaze material stirring, it is homogenized aging, to be homogenized glaze, wherein the homogenizing aging time is 15
Hour, the aging temperature of the homogenizing is room temperature, can make preferably to act between each component by being homogenized aging process, entirety is more
Add uniformly, to keep the glaze of finished product smooth;
(3) by the glaze of homogenizing brushing glazing or by way of pouring glaze, in porcelain billet, obtained semi-finished product ceramic products, use is applied for glazing
Glaze method can control the flatness of glaze;
(4) the semi-finished product ceramic products are placed in kiln and are sintered, obtain ceramic products, wherein the sintering process are as follows: is first small 1
When it is interior will be warming up to 700 degrees Celsius in kiln, keep the temperature 35 minutes, then 1100 degrees Celsius will be warming up in kiln in 1.5 hours,
Heat preservation 35 minutes is finally cooled to 900 degrees Celsius in 35 minutes, keeps the temperature 80 minutes, takes out after the sintering, naturally cold
But, use interim heating mode and cooling method step by step, can make semi-finished product ceramic products not crack during the sintering process, no
Generate defect, it is ensured that the flatness of entire glaze.
Embodiment two:
A kind of enamel frit makeing method increasing glaze surface evenness, including step are provided are as follows:
(1) glaze quartz, potassium feldspar, kaolin and quick lime are weighed, and is added in grinding drum, then is added into the grinding drum
Enter water, opacifiers, antibacterial agent and colorant, grinding uniformly obtains glaze, wherein the content of the glaze each component are as follows: quartz
25 kg, 50 kg of potassium feldspar, 13 kg of kaolin, 12 kg of quick lime, 3 kg of opacifiers, 4 kg of antibacterial agent, colorant 3
Kg, the opacifiers be zirconium dioxide and phosphatic mixture, the antibacterial agent be dissolved in water containing zinc ion, copper from
Son, one of silver ion or a variety of inorganic salts, the colorant are ferriferous oxide, choose suitable component, between each component
It works in coordination, can guarantee the planarization of the glaze in subsequent step (2), (3) and (4);
(2) to the glaze material stirring, it is homogenized aging, to be homogenized glaze, wherein the homogenizing aging time is 20
Hour, the aging temperature of the homogenizing is room temperature, can make preferably to act between each component by being homogenized aging process, entirety is more
Add uniformly, to keep the glaze of finished product smooth;
(3) by the glaze of homogenizing, semi-finished product ceramic products, the enameling method of use is made in porcelain billet in glazing by way of pouring glaze
It can control the flatness of glaze;
(4) the semi-finished product ceramic products are placed in kiln and are sintered, obtain ceramic products, wherein the sintering process are as follows: is first small 1
When it is interior will be warming up to 700 degrees Celsius in kiln, keep the temperature 40 minutes, then 1100 degrees Celsius will be warming up in kiln in 1.5 hours,
Heat preservation 40 minutes is finally cooled to 900 degrees Celsius in 40 minutes, keeps the temperature 60 minutes, takes out after the sintering, naturally cold
But, use interim heating mode and cooling method step by step, can make semi-finished product ceramic products not crack during the sintering process, no
Generate defect, it is ensured that the flatness of entire glaze.
Embodiment three:
A kind of enamel frit makeing method increasing glaze surface evenness, including step are provided are as follows:
(1) glaze quartz, potassium feldspar, kaolin and quick lime are weighed, and is added in grinding drum, then is added into the grinding drum
Enter water, opacifiers, antibacterial agent and colorant, grinding uniformly obtains glaze, wherein the content of the glaze each component are as follows: quartz
23 kg, 54 kg of potassium feldspar, 11 kg of kaolin, 14 kg of quick lime, 2 kg of opacifiers, 5 kg of antibacterial agent, colorant
2kg, the opacifiers are zirconium dioxide, the antibacterial agent be dissolved in water containing one of zinc ion, copper ion, silver ion
Or a variety of inorganic salts, the colorant are Cu oxide, choose suitable component, work in coordination between each component, can guarantee
The planarization of glaze in subsequent step (2), (3) and (4);
(2) to the glaze material stirring, it is homogenized aging, to be homogenized glaze, wherein the homogenizing aging time is 17
Hour, the aging temperature of the homogenizing is room temperature, can make preferably to act between each component by being homogenized aging process, entirety is more
Add uniformly, to keep the glaze of finished product smooth;
(3) by the glaze of homogenizing, semi-finished product ceramic products, the enameling method of use is made in porcelain billet in glazing by way of brushing glazing
It can control the flatness of glaze;
(4) the semi-finished product ceramic products are placed in kiln and are sintered, obtain ceramic products, wherein the sintering process are as follows: is first small 1
When it is interior will be warming up to 700 degrees Celsius in kiln, keep the temperature 30 minutes, then 1100 degrees Celsius will be warming up in kiln in 1.5 hours,
Heat preservation 30 minutes is finally cooled to 900 degrees Celsius in 40 minutes, keeps the temperature 90 minutes, takes out after the sintering, naturally cold
But, use interim heating mode and cooling method step by step, can make semi-finished product ceramic products not crack during the sintering process, no
Generate defect, it is ensured that the flatness of entire glaze.
The beneficial effects of the present invention are:
One, the temperature when enamel frit makeing method for increasing glaze surface evenness is by choosing suitable glaze component and control sintering becomes
Change, keeps sintered ceramic products glaze surface evenness good;
Two, the glaze of the enamel frit makeing method for increasing glaze surface evenness will not generate defect, have extraordinary antibacterial effect, increase
The aesthetics for adding ceramic products entirety, the welcome by consumer.
The above description is only an embodiment of the present invention, is not intended to limit the scope of the invention, all to utilize this hair
Equivalent structure or equivalent flow shift made by bright description is applied directly or indirectly in other relevant technology necks
Domain is included within the scope of the present invention.
Claims (10)
1. a kind of enamel frit makeing method for increasing glaze surface evenness, which is characterized in that including step are as follows: (1) it is long to weigh glaze quartz, potassium
Stone, kaolin and quick lime, and be added in grinding drum, then water, opacifiers, antibacterial agent and coloring are added into the grinding drum
Agent, grinding uniformly obtain glaze;(2) to the glaze material stirring, it is homogenized aging, to be homogenized glaze;(3) by homogenizing
Semi-finished product ceramic products are made in porcelain billet in glaze glazing;(4) the semi-finished product ceramic products are placed in kiln and are sintered, obtain porcelain
Product.
2. the enamel frit makeing method according to claim 1 for increasing glaze surface evenness, which is characterized in that glaze described in step (1)
Expect the content of each component are as follows: in parts by weight, 20-25 parts quartzy, 50-55 parts of potassium feldspar, 9-13 parts of kaolin, quick lime
12-16 parts, 1-3 parts of opacifiers, 4-7 parts of antibacterial agent, 1-3 parts of colorant.
3. the enamel frit makeing method according to claim 1 for increasing glaze surface evenness, which is characterized in that cream described in step (1)
Turbid dose is one of tin oxide, titanium dioxide, zirconium dioxide, phosphate or a variety of.
4. the enamel frit makeing method according to claim 1 for increasing glaze surface evenness, which is characterized in that resist described in step (1)
Microbial inoculum be dissolved in water containing one of zinc ion, copper ion, silver ion or a variety of inorganic salts.
5. the enamel frit makeing method according to claim 1 for increasing glaze surface evenness, which is characterized in that described in step (1)
Toner is one of Cu oxide, ferriferous oxide, cobalt oxide agent or a variety of.
6. the enamel frit makeing method according to claim 1 for increasing glaze surface evenness, which is characterized in that described in step (2)
Changing the aging time is 15-20 hours.
7. the enamel frit makeing method according to claim 1 for increasing glaze surface evenness, which is characterized in that described in step (2)
Changing aging temperature is room temperature.
8. the enamel frit makeing method according to claim 1 for increasing glaze surface evenness, which is characterized in that step is applied described in (3)
Glaze method is brushing glazing or pours glaze.
9. the enamel frit makeing method according to claim 1 for increasing glaze surface evenness, which is characterized in that burnt described in step (4)
Knot process are as follows: will first be warming up to 700 degrees Celsius in kiln in 1 hour, keep the temperature 30-40 minutes, then by kiln in 1.5 hours
1100 degrees Celsius are inside warming up to, keeps the temperature 30-40 minutes, 900 degrees Celsius, 60-90 points of heat preservation are finally cooled in 30-40 minutes
Clock.
10. the enamel frit makeing method according to claim 1 for increasing glaze surface evenness, which is characterized in that burnt described in step (4)
It is taken out after knot, natural cooling.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN112430071A (en) * | 2020-11-19 | 2021-03-02 | 萍乡市兄弟瓷业有限公司 | Easy-to-clean household ceramic product and preparation method thereof |
CN112573824A (en) * | 2020-10-15 | 2021-03-30 | 宁国市众鑫陶业有限公司 | Antique foaming glaze and preparation method thereof |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112573824A (en) * | 2020-10-15 | 2021-03-30 | 宁国市众鑫陶业有限公司 | Antique foaming glaze and preparation method thereof |
CN112430071A (en) * | 2020-11-19 | 2021-03-02 | 萍乡市兄弟瓷业有限公司 | Easy-to-clean household ceramic product and preparation method thereof |
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Application publication date: 20190816 |