CN110117159B - 一种人造芙蓉晶及其制备方法 - Google Patents
一种人造芙蓉晶及其制备方法 Download PDFInfo
- Publication number
- CN110117159B CN110117159B CN201910564694.4A CN201910564694A CN110117159B CN 110117159 B CN110117159 B CN 110117159B CN 201910564694 A CN201910564694 A CN 201910564694A CN 110117159 B CN110117159 B CN 110117159B
- Authority
- CN
- China
- Prior art keywords
- hibiscus
- crystal
- artificial
- cooling
- raw materials
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000013078 crystal Substances 0.000 title claims abstract description 64
- 235000005206 Hibiscus Nutrition 0.000 title claims abstract description 38
- 235000007185 Hibiscus lunariifolius Nutrition 0.000 title claims abstract description 38
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 241001075721 Hibiscus trionum Species 0.000 title 1
- 241000218033 Hibiscus Species 0.000 claims abstract description 37
- 238000001816 cooling Methods 0.000 claims abstract description 28
- 239000002994 raw material Substances 0.000 claims abstract description 20
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000011651 chromium Substances 0.000 claims abstract description 12
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229910052804 chromium Inorganic materials 0.000 claims abstract description 11
- 238000000034 method Methods 0.000 claims abstract description 11
- 238000002156 mixing Methods 0.000 claims abstract description 9
- 230000008569 process Effects 0.000 claims abstract description 9
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229910052814 silicon oxide Inorganic materials 0.000 claims abstract description 8
- 238000000137 annealing Methods 0.000 claims abstract description 7
- 229910052810 boron oxide Inorganic materials 0.000 claims abstract description 6
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 claims abstract description 6
- 229910021380 Manganese Chloride Inorganic materials 0.000 claims abstract description 4
- GLFNIEUTAYBVOC-UHFFFAOYSA-L Manganese chloride Chemical compound Cl[Mn]Cl GLFNIEUTAYBVOC-UHFFFAOYSA-L 0.000 claims abstract description 4
- 239000011565 manganese chloride Substances 0.000 claims abstract description 4
- 235000002867 manganese chloride Nutrition 0.000 claims abstract description 4
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 3
- ORUIBWPALBXDOA-UHFFFAOYSA-L magnesium fluoride Chemical compound [F-].[F-].[Mg+2] ORUIBWPALBXDOA-UHFFFAOYSA-L 0.000 claims abstract 2
- 229910001635 magnesium fluoride Inorganic materials 0.000 claims abstract 2
- PHFQLYPOURZARY-UHFFFAOYSA-N chromium trinitrate Chemical compound [Cr+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O PHFQLYPOURZARY-UHFFFAOYSA-N 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 10
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims description 7
- 239000000843 powder Substances 0.000 claims description 7
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims description 6
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 6
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims description 3
- 239000000292 calcium oxide Substances 0.000 claims description 3
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims description 3
- 238000007598 dipping method Methods 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 3
- CHWRSCGUEQEHOH-UHFFFAOYSA-N potassium oxide Chemical compound [O-2].[K+].[K+] CHWRSCGUEQEHOH-UHFFFAOYSA-N 0.000 claims description 3
- 229910001950 potassium oxide Inorganic materials 0.000 claims description 3
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims description 3
- 229910001948 sodium oxide Inorganic materials 0.000 claims description 3
- 230000004907 flux Effects 0.000 claims description 2
- -1 manganese sulfate Neodymium sulfate Chemical compound 0.000 claims 1
- 238000005562 fading Methods 0.000 abstract description 4
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titanium dioxide Inorganic materials O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 abstract description 4
- 238000009776 industrial production Methods 0.000 abstract description 3
- 229940099596 manganese sulfate Drugs 0.000 abstract description 3
- 239000011702 manganese sulphate Substances 0.000 abstract description 3
- 235000007079 manganese sulphate Nutrition 0.000 abstract description 3
- SQQMAOCOWKFBNP-UHFFFAOYSA-L manganese(II) sulfate Chemical compound [Mn+2].[O-]S([O-])(=O)=O SQQMAOCOWKFBNP-UHFFFAOYSA-L 0.000 abstract description 3
- RHVPCSSKNPYQDU-UHFFFAOYSA-H neodymium(3+);trisulfate;hydrate Chemical compound O.[Nd+3].[Nd+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O RHVPCSSKNPYQDU-UHFFFAOYSA-H 0.000 abstract description 3
- 230000000638 stimulation Effects 0.000 abstract description 3
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 abstract 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 3
- 230000007547 defect Effects 0.000 description 3
- 239000004519 grease Substances 0.000 description 3
- 239000002932 luster Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 229910021645 metal ion Inorganic materials 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 230000005274 electronic transitions Effects 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B19/00—Other methods of shaping glass
- C03B19/02—Other methods of shaping glass by casting molten glass, e.g. injection moulding
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B25/00—Annealing glass products
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B5/00—Melting in furnaces; Furnaces so far as specially adapted for glass manufacture
- C03B5/16—Special features of the melting process; Auxiliary means specially adapted for glass-melting furnaces
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/062—Glass compositions containing silica with less than 40% silica by weight
- C03C3/064—Glass compositions containing silica with less than 40% silica by weight containing boron
- C03C3/068—Glass compositions containing silica with less than 40% silica by weight containing boron containing rare earths
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/11—Glass compositions containing silica with 40% to 90% silica, by weight containing halogen or nitrogen
- C03C3/112—Glass compositions containing silica with 40% to 90% silica, by weight containing halogen or nitrogen containing fluorine
- C03C3/115—Glass compositions containing silica with 40% to 90% silica, by weight containing halogen or nitrogen containing fluorine containing boron
- C03C3/118—Glass compositions containing silica with 40% to 90% silica, by weight containing halogen or nitrogen containing fluorine containing boron containing aluminium
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Manufacturing & Machinery (AREA)
- Glass Compositions (AREA)
Abstract
Description
莫氏硬度 | 比重 | 折光率 | 色泽 | |
实施例1 | 7.5 | 2.66 | 1.548 | 粉红透亮 |
实施例2 | 7.5 | 2.73 | 1.550 | 粉红透亮 |
实施例3 | 8 | 2.86 | 1.551 | 粉红透亮 |
实施例4 | 8 | 2.94 | 1.553 | 粉红透亮 |
实施例5 | 8.5 | 3.08 | 1.552 | 粉红透亮 |
Claims (4)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201910564694.4A CN110117159B (zh) | 2019-06-27 | 2019-06-27 | 一种人造芙蓉晶及其制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201910564694.4A CN110117159B (zh) | 2019-06-27 | 2019-06-27 | 一种人造芙蓉晶及其制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN110117159A CN110117159A (zh) | 2019-08-13 |
CN110117159B true CN110117159B (zh) | 2020-07-03 |
Family
ID=67524565
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201910564694.4A Expired - Fee Related CN110117159B (zh) | 2019-06-27 | 2019-06-27 | 一种人造芙蓉晶及其制备方法 |
Country Status (1)
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CN (1) | CN110117159B (zh) |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100588630C (zh) * | 2008-08-04 | 2010-02-10 | 江苏拜富色釉料有限公司 | 一种玻璃无铅颜料及其制备方法 |
CN101597138B (zh) * | 2009-07-23 | 2012-07-04 | 中国计量学院 | 一种析出LiAl5O8纳米晶的微晶玻璃及其制备方法 |
CN102198396A (zh) * | 2011-03-17 | 2011-09-28 | 大连理工大学 | 一种含铬轻烃燃烧催化剂及制备方法 |
CN102442816B (zh) * | 2011-10-17 | 2013-12-18 | 王蕴渔 | 一种合成青白玉及其制造方法 |
CN103030292B (zh) * | 2012-12-05 | 2016-04-06 | 毛庆云 | 一种含有改性玻璃体粉末的微晶玻璃及其制备方法 |
CN103409806A (zh) * | 2013-08-13 | 2013-11-27 | 安徽环巢光电科技有限公司 | 一种掺钕、铈和铬的钇铝石榴石晶体的退火方法 |
CN107265847A (zh) * | 2017-08-01 | 2017-10-20 | 合肥利裕泰玻璃制品有限公司 | 一种无铅环保水晶玻璃及其制备方法 |
CN108559501B (zh) * | 2018-01-05 | 2021-03-30 | 电子科技大学 | 一种铬掺杂氧化铝光致发光材料的水热制备方法 |
CN108706713A (zh) * | 2018-05-16 | 2018-10-26 | 芜湖市艾德森自动化设备有限公司 | 一种畜禽养殖废水降解净化剂的制备方法 |
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2019
- 2019-06-27 CN CN201910564694.4A patent/CN110117159B/zh not_active Expired - Fee Related
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CN110117159A (zh) | 2019-08-13 |
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Effective date of registration: 20211227 Address after: 257000 No. 112-2, urban empowerment center, No. 817, Bingsheng Road, economic development zone, Guangrao County, Dongying City, Shandong Province Patentee after: Dongying zhuanxin Technology Service Co.,Ltd. Address before: 322200 No. 15, Zhenye Road, Huangzhai Town, Pujiang County, Jinhua City, Zhejiang Province Patentee before: Pujiang Hengkai Crystal Co.,Ltd. |
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Effective date of registration: 20220801 Address after: 226000 room 402, building 1, Huahui Zhigu Science Industrial Park, No. 17, Yuanyuan Road, Guanyinshan street, Chongchuan District, Nantong City, Jiangsu Province Patentee after: Jiangsu zhuanxin Intellectual Property Operation Co.,Ltd. Address before: 257000 No. 112-2, urban empowerment center, No. 817, Bingsheng Road, Guangrao Economic Development Zone, Guangrao County, Dongying City, Shandong Province Patentee before: Dongying zhuanxin Technology Service Co.,Ltd. |
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Effective date of registration: 20221220 Address after: 224005 Room 102, Building A-19, Big Data Industrial Park, Kecheng Street, Yannan Hi tech Zone, Yancheng City, Jiangsu Province Patentee after: Yancheng Jiayu Shichuang Surveying and Mapping Technology Co.,Ltd. Address before: 226000 room 402, building 1, Huahui Zhigu Science Industrial Park, No. 17, Yuanyuan Road, Guanyinshan street, Chongchuan District, Nantong City, Jiangsu Province Patentee before: Jiangsu zhuanxin Intellectual Property Operation Co.,Ltd. |
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CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20200703 |