CN110106012A - A kind of long-acting water-based antirust agent - Google Patents

A kind of long-acting water-based antirust agent Download PDF

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Publication number
CN110106012A
CN110106012A CN201910508301.8A CN201910508301A CN110106012A CN 110106012 A CN110106012 A CN 110106012A CN 201910508301 A CN201910508301 A CN 201910508301A CN 110106012 A CN110106012 A CN 110106012A
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CN
China
Prior art keywords
parts
water
antirust
long
hld
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910508301.8A
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Chinese (zh)
Inventor
冯栋
冯斌
熊金平
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HENGLIDA CHEMICAL CO Ltd LAIZHOU CITY
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HENGLIDA CHEMICAL CO Ltd LAIZHOU CITY
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Priority to CN201910508301.8A priority Critical patent/CN110106012A/en
Publication of CN110106012A publication Critical patent/CN110106012A/en
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04—Mixtures of base-materials and additives
    • C10M169/048—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution, non-macromolecular and macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M173/00—Lubricating compositions containing more than 10% water
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02—Hydroxy compounds
    • C10M2207/021—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02—Hydroxy compounds
    • C10M2207/023—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings
    • C10M2207/026—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings with tertiary alkyl groups
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28—Esters
    • C10M2207/287—Partial esters
    • C10M2207/289—Partial esters containing free hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/40—Fatty vegetable or animal oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C10M2209/104—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing two carbon atoms only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C10M2209/108—Polyethers, i.e. containing di- or higher polyoxyalkylene groups etherified
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/08—Amides
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/40—Low content or no content compositions
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/56—Boundary lubrication or thin film lubrication
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/64—Environmental friendly compositions
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/48—Slushing oils

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Preventing Corrosion Or Incrustation Of Metals (AREA)
  • Lubricants (AREA)

Abstract

The invention discloses a kind of long-acting water-based antirust agent, be by parts by weight be 500-800 parts of industrial alcohol, 15-25 parts of HLD-1 antirust dispersing agents, 100-140 parts of base oils, 1.5-2 part 2.6- di-tert-butyl p-cresol, 15-25 parts of dinonyl naphthalene sulfonate bariums, 40-70 parts of water, 15-25 parts of anhydrous sorbitol list olein compositions, it is that above-mentioned material is added in 2T reaction kettle to fuse stirring, 60 DEG C are heated to after 2 hours, stop heating, add deionized water, when temperature is down to 30 DEG C or less, finished product is released, the present invention has damage of the aromatic hydrocarbons gas to human body thoroughly solved in solvent, reduce the inflammable and explosive dangerous and destruction to environment, in the case of meeting special parts and oil-free must there are the characteristics that.

Description

A kind of long-acting water-based antirust agent
Technical field
The invention belongs to antirust agent technical fields, cast the parts isometric phase mainly for ferrous metal more particularly, to one kind The long-acting water-based antirust agent of preservation and packaging.
Background technique
Aqueous rustproof is to perplex domestic and international manufacturing a great problem, the antirust of most of water-based antirust always for many years Phase at three months or so, be unable to satisfy at all product antirust require and alkalinity it is extremely strong (be main with sodium oxide molybdena and sodium hydroxide Material increases alkalinity), pollute environment, it is difficult to which processing and discharge, most of product is also with poisonous and hazardous sodium nitrite chemistry Ingredient is as antirust agent, and surface of the work after antirust treatment is matt, remaining surface jaundice easy to whiten, seriously affects parts Product quality, and long-term storage, it is more difficult to go abroad and export to foreign countries.Most enterprises can only high price import, such as U.S.'s product WD -40 etc., but the product is still toxic, inflammable.Even if there are individual formulas using other compositions, accomplish environment-friendly type, but antirust as far as possible Phase is unable to reach the requirement of 1 year or more rust-proof life at all generally within half a year.
Summary of the invention
A kind of aromatic hydrocarbons gas thoroughly solved in solvent is provided it is an object of the invention to improve the deficiency of prior art Damage to human body, reduce it is inflammable and explosive dangerous and to the destruction of environment, meet special parts must be in the case of oil-free presence The long-acting water-based antirust agent that long-term rust prevention requires.
The object of the present invention is achieved like this, a kind of long-acting water-based antirust agent, it is characterized in that being 500-800 by parts by weight Part industrial alcohol, 15-25 parts of HLD-1 antirust dispersing agents, 100-140 parts of base oils, 1.5-2 parts of 2.6- di-tert-butyl p-cresol, 15-25 parts of dinonyl naphthalene sulfonate bariums, 40-70 parts of water, 15-25 parts of anhydrous sorbitol list olein compositions, are to add above-mentioned material Enter and fused in batches in 2T reaction kettle, is sufficiently stirred, while being heated to 60 DEG C after 2 hours, stops after completely dissolution in various raw material It only heats, adds deionized water, when temperature is down to 30 DEG C hereinafter, finished product is released.
Compared with the prior art the present invention has following distinguishing feature and a good effect: the present invention without silicon, kerosene, it is cured, Graphite, chlorofluorocarbons (CFC) or any known carcinogenic medium, pH value 6-7, the waste water based anti-rusting agent under replacing can be used for work Parts short-term rust prevention between sequence solves the problems such as emission treatment and pollution environment.
The present invention is because of organic materials such as spirituosity, base oils, so penetration is strong, has extremely strong permeability and metal watch Face affinity, but it absolutely not damages the materials such as the paint, fiber, plastic nylon of metal surface.It is stronger affine by its Power and penetration effectively exclude the moisture inside metal surface and pore so as to penetrate into inside metal pore And moisture, the dense protective layer of one layer of only 0.003-0.005mm is formed, reaches ideal rust-proof effect, and surface brightness is high, water Divide fast drying, general 1-1.5 minutes forms dry face.And successfully reached preservation and packaging rust-proof life 1 year or more effect with Requirement.
The present invention, which is free of, has carcinogenic chemical ingredient: sodium nitrite to human body.It is long with rust-proof life, salt spray test: ironcasting Up to 12 hours or more, steel part was up to 15-20 hours；Preservation and packaging was up to 1 year or more.This formula has without any pair of human body Evil chemical components, meet environment protection requirement, and simple process is easy to use, and highly-safe, raw material are easily purchased, and cost is lower than oil Base antirust oil, use, production, transport, storage safe coefficient are high.
Specific embodiment
Embodiment 1, it is 500-800 parts of industrial alcohol, 15-25 parts of HLD-1 that a kind of long-acting water-based antirust agent, which is by parts by weight, Antirust dispersing agent, 100-140 part base oil, 1.5-2 parts of 2.6- di-tert-butyl p-cresol, 15-25 parts of dinonyl naphthalene sulfonate bariums, 40-70 parts of water, 15-25 parts of anhydrous sorbitol list olein compositions, HLD-1 antirust dispersing agent is by lanolin magnesium soap, N- oleoyl Amino acid ammonium salt, NP-9 are formed by weight 3:2:1 ratio, are that above-mentioned material is added in 2T reaction kettle to fuse in batches, are sufficiently stirred It mixes, while being heated to 60 DEG C after 2 hours, stop heating after completely dissolution in various raw material, add deionized water, work as temperature 30 DEG C are down to hereinafter, finished product is released.
The present embodiment is using 500kg industrial alcohol, 25kgHLD-1 antirust dispersing agent, 100kg base oil, 2kg2.6- bis- Butylated Hydroxytoluene, 15kg dinonyl naphthalene sulfonate barium, 70kg water, 15kg anhydrous sorbitol list olein composition.
Embodiment 2, a kind of long-acting water-based antirust agent, be using 800 kg industrial alcohol, 15kgHLD-1 antirust dispersing agent, 140kg base oil, 1.5 antioxidant, 25kg dinonyl naphthalene sulfonate barium, 40kg water, 25kg anhydrous sorbitol list olein composition, He is identical with embodiment 1.
Embodiment 3, a kind of long-acting water-based antirust agent, be using 650 kg industrial alcohol, 20kgHLD-1 antirust dispersing agent, 120kg base oil, 1.8kg antioxidant, 20kg dinonyl naphthalene sulfonate barium, 55kg water, 20kg anhydrous sorbitol list olein composition, Other are identical with embodiment 1.
The long-acting water-based antirust agent of the present invention, suitable for cast iron, cast steel, metallic sintered products long-term rust prevention, especially suitable for Shipping and the antirust for storing metalwork, apply also for precise electronic instrument, radar and gear, automatic weapon, hardware tool, machinery The long-term rust prevention of the products such as accessory.

Claims (1)

1. a kind of long-acting water-based antirust agent, it is characterized in that being 500-800 parts of industrial alcohol, 15-25 parts of HLD-1 antirusts by parts by weight Dispersing agent, 100-140 part base oil, 1.5-2 parts of 2.6- di-tert-butyl p-cresol, 15-25 parts of dinonyl naphthalene sulfonate bariums, 40-70 Part water, 15-25 parts of anhydrous sorbitol list oleins compositions, HLD-1 antirust dispersing agent is by lanolin magnesium soap, N- oleoyl amino acid ammonium Salt, NP-9 are formed by weight 3:2:1 ratio；It is that above-mentioned material is added in 2T reaction kettle to fuse in batches, is sufficiently stirred, simultaneously 60 DEG C are heated to after 2 hours, stops heating after completely dissolution in various raw material, adds deionized water, when temperature is down to 30 DEG C hereinafter, finished product is released.
CN201910508301.8A 2019-06-13 2019-06-13 A kind of long-acting water-based antirust agent Pending CN110106012A (en)

Priority Applications (1)

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CN201910508301.8A CN110106012A (en) 2019-06-13 2019-06-13 A kind of long-acting water-based antirust agent

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CN110106012A true CN110106012A (en) 2019-08-09

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103695915A (en) * 2013-11-29 2014-04-02 明光市留香泵业有限公司 Emulsion-type antirust liquid and preparation method thereof
WO2014151185A1 (en) * 2013-03-14 2014-09-25 Buckman Laboratories International, Inc. Method to control corrosion of a metal surface using alkyl sulfamic acids or salts thereof
CN106675744A (en) * 2016-12-27 2017-05-17 长沙艾森设备维护技术有限公司 Water-based metal rust inhibitor
CN109135896A (en) * 2018-10-10 2019-01-04 华阳-恩赛有限公司 A kind of dehydration-type antirust agent, Preparation method and use

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014151185A1 (en) * 2013-03-14 2014-09-25 Buckman Laboratories International, Inc. Method to control corrosion of a metal surface using alkyl sulfamic acids or salts thereof
CN103695915A (en) * 2013-11-29 2014-04-02 明光市留香泵业有限公司 Emulsion-type antirust liquid and preparation method thereof
CN106675744A (en) * 2016-12-27 2017-05-17 长沙艾森设备维护技术有限公司 Water-based metal rust inhibitor
CN109135896A (en) * 2018-10-10 2019-01-04 华阳-恩赛有限公司 A kind of dehydration-type antirust agent, Preparation method and use

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
国务院学位委员会办公室: "《第五届博士生学术年会论文集 下》", 30 June 2008, 中国科学技术出版社 *
王建清: "《"十二五"普通高等教育本科国家级规划教材 包装材料学 第2版》", 28 February 2017, 中国轻工业出版社 *

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Application publication date: 20190809