CN110102537B - Method for cleaning high-abrasion low-chemical-stability optical glass - Google Patents
Method for cleaning high-abrasion low-chemical-stability optical glass Download PDFInfo
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- CN110102537B CN110102537B CN201910510634.4A CN201910510634A CN110102537B CN 110102537 B CN110102537 B CN 110102537B CN 201910510634 A CN201910510634 A CN 201910510634A CN 110102537 B CN110102537 B CN 110102537B
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- isopropanol
- optical glass
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- 238000004140 cleaning Methods 0.000 title claims abstract description 49
- 238000000034 method Methods 0.000 title claims abstract description 26
- 239000005304 optical glass Substances 0.000 title claims abstract description 16
- 238000005299 abrasion Methods 0.000 title claims abstract description 15
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims abstract description 28
- 239000002904 solvent Substances 0.000 claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 10
- 239000000126 substance Substances 0.000 claims abstract description 10
- 239000008399 tap water Substances 0.000 claims abstract description 10
- 235000020679 tap water Nutrition 0.000 claims abstract description 10
- 238000001035 drying Methods 0.000 claims abstract description 9
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 8
- 230000007547 defect Effects 0.000 claims abstract description 5
- 238000002156 mixing Methods 0.000 claims abstract description 5
- HXKKHQJGJAFBHI-UHFFFAOYSA-N 1-aminopropan-2-ol Chemical compound CC(O)CN HXKKHQJGJAFBHI-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229940102253 isopropanolamine Drugs 0.000 claims abstract description 4
- 229910000029 sodium carbonate Inorganic materials 0.000 claims abstract description 4
- 239000001488 sodium phosphate Substances 0.000 claims abstract description 4
- 229910000162 sodium phosphate Inorganic materials 0.000 claims abstract description 4
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 claims abstract description 4
- 239000013072 incoming material Substances 0.000 claims description 11
- 238000000227 grinding Methods 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 3
- 238000004506 ultrasonic cleaning Methods 0.000 claims description 3
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 claims 1
- 239000000428 dust Substances 0.000 abstract description 3
- 239000004519 grease Substances 0.000 abstract description 3
- 239000007779 soft material Substances 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 2
- 238000002604 ultrasonography Methods 0.000 abstract description 2
- 239000011521 glass Substances 0.000 description 6
- 230000003287 optical effect Effects 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 241000519995 Stachys sylvatica Species 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 238000007689 inspection Methods 0.000 description 2
- 208000032544 Cicatrix Diseases 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 238000012790 confirmation Methods 0.000 description 1
- 239000007799 cork Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- -1 finger print Substances 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 238000003908 quality control method Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 231100000241 scar Toxicity 0.000 description 1
- 230000037387 scars Effects 0.000 description 1
- HOWHQWFXSLOJEF-MGZLOUMQSA-N systemin Chemical compound NCCCC[C@H](N)C(=O)N[C@@H](CCSC)C(=O)N[C@@H](CCC(N)=O)C(=O)N[C@@H]([C@@H](C)O)C(=O)N[C@@H](CC(O)=O)C(=O)OC(=O)[C@@H]1CCCN1C(=O)[C@H]1N(C(=O)[C@H](CC(O)=O)NC(=O)[C@H](CCCN=C(N)N)NC(=O)[C@H](CCCCN)NC(=O)[C@H](CO)NC(=O)[C@H]2N(CCC2)C(=O)[C@H]2N(CCC2)C(=O)[C@H](CCCCN)NC(=O)[C@H](CO)NC(=O)[C@H](CCC(N)=O)NC(=O)[C@@H](NC(=O)[C@H](C)N)C(C)C)CCC1 HOWHQWFXSLOJEF-MGZLOUMQSA-N 0.000 description 1
- 108010050014 systemin Proteins 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
- B08B3/08—Cleaning involving contact with liquid the liquid having chemical or dissolving effect
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B11/00—Cleaning flexible or delicate articles by methods or apparatus specially adapted thereto
- B08B11/04—Cleaning flexible or delicate articles by methods or apparatus specially adapted thereto specially adapted for plate glass, e.g. prior to manufacture of windshields
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
- B08B3/10—Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration
- B08B3/12—Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration by sonic or ultrasonic vibrations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/02—Inorganic compounds
- C11D7/04—Water-soluble compounds
- C11D7/06—Hydroxides
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/02—Inorganic compounds
- C11D7/04—Water-soluble compounds
- C11D7/10—Salts
- C11D7/12—Carbonates bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/02—Inorganic compounds
- C11D7/04—Water-soluble compounds
- C11D7/10—Salts
- C11D7/16—Phosphates including polyphosphates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/32—Organic compounds containing nitrogen
- C11D7/3218—Alkanolamines or alkanolimines
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D2111/00—Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
- C11D2111/10—Objects to be cleaned
- C11D2111/14—Hard surfaces
- C11D2111/18—Glass; Plastics
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Detergent Compositions (AREA)
- Cleaning By Liquid Or Steam (AREA)
Abstract
The invention discloses a method for cleaning high-abrasion low-chemical-stability optical glass, which is characterized by comprising the following steps of cleaning with a solvent, rinsing with tap water, cleaning with pure water, cleaning with isopropanol and drying with isopropanol, wherein the solvent comprises the following substances in percentage by mass: sodium hydroxide: 0.1% -0.5%; isopropanolamine: 0.1% -0.5%; sodium carbonate: 1% -3%; sodium phosphate: 5% -10%; the balance is water, the pH value of the solvent after blending is 8-9, and the method has the advantages that a cleaning process of high-frequency ultrasound and high-activity low-concentration alkalescent solvent is adopted to replace a manual wiping process, so that dirt such as dust, grease, white dots and the like on the surface of a product can be effectively removed on the basis of ensuring that the product does not generate defects; the efficiency is improved, the soft material cleaning beat is 2 min/basket, and the efficiency is improved by 20 times when 40 pieces are washed in each basket on average; the quality is stable, the human influence factor is low, and the quality yield is improved from 50 percent to more than 95 percent.
Description
Technical Field
The invention relates to a method for cleaning optical glass, in particular to a method for cleaning high-abrasion low-chemical-stability optical glass.
Background
In the manufacturing process of optical instruments and mechanical systems, glass materials used in the fields of lenses, prisms, mirrors, windows, and the like are often called optical glass. According to different optical performance requirements, different glasses are generally selected in optical processing production, and comprise colorless optical glass, colored optical glass, radiation-resistant optical glass, radiation-proof glass, optical quartz glass and the like.
Optical systemIn each processing process of glass, cleaning treatment is usually needed due to the conditions of surface dust, grease, white spots and the like. And the optical glass with high abrasion and low chemical stability refers to the condition that any one of the following conditions is satisfied: 1. the abrasion degree is high: relative grinding hardness FA FANot less than 300, relative grinding hardness FAThe abrasion resistance is a numerical value obtained by multiplying the ratio of the abrasion loss of a sample to the abrasion loss (volume) of standard sample K9 glass by 100 under the same conditions, wherein the higher the value is, the worse the abrasion resistance is; 2. the chemical stability is low: stability to Water action DWNot less than 4, stability against acid action DANot less than 4, stability against water action DWAnd stability against acid action DAThe higher the values of both, the worse the environmental resistance.
The cleaning difficulty of the glass with high abrasion degree and low chemical stability is relatively high, the cleaning mode of the product at present mainly depends on ether and ethanol for manual wiping treatment, and the treatment method has the following problems:
1. the efficiency is low, and if the appearance of a common soft material product meets the coating requirement, a skilled worker can only wipe about 1 sheet per minute;
2. the cost is high, and because the wiping efficiency is low, more personnel are needed for corresponding production, so that the labor cost is high;
3. the quality of the treated product is poor, and bright wires, scars and wiping marks are more in the manual wiping process, so that the qualified rate is low, the appearance requirement of a coating film cannot be met, and the cleaning yield is less than 50%;
disclosure of Invention
The invention aims to solve the technical problem of providing a method for cleaning high-abrasion-degree low-chemical-stability optical glass, which has high efficiency, lower cost and better quality of a treated product.
The technical scheme adopted by the invention for solving the technical problems is as follows: a cleaning method of optical glass with high abrasion degree and low chemical stability comprises the steps of solvent cleaning, tap water rinsing, pure water cleaning, isopropanol cleaning and isopropanol drying, wherein the solvent comprises the following substances in percentage by mass: sodium hydroxide: 0.1% -0.5%; isopropanolamine: 0.1% -0.5%; sodium carbonate: 1% -3%; sodium phosphate: 5% -10%; the balance of water, and the pH value of the solvent after blending is 8-9.
Compared with the prior art, the invention has the advantages that the cleaning process of high-frequency ultrasound and high-activity low-concentration alkalescent solvent is adopted to replace the manual wiping process, and the dirt such as dust, grease, white spots and the like on the surface of the product can be effectively removed on the basis of ensuring that the product does not generate badness; the efficiency is improved, the soft material cleaning beat is 2 min/basket, and the efficiency is improved by 20 times when 40 pieces are washed in each basket on average; the quality is stable, the human influence factor is low, and the quality yield (the appearance requirement before plating) is improved from 50 percent to more than 95 percent.
The incoming materials before cleaning are subjected to spot inspection according to the proportion of 10 percent, so that the incoming materials are ensured not to have the defects of abrasive powder, finger print, cork, bright silk and the like, and if the defect number exceeds 2 percent of the total amount of the incoming materials, the incoming materials are returned to the previous working procedure for treatment. Through the quality control of supplied materials, products before cleaning are free from intractable objects such as grinding powder and fingerprints.
The solvent cleaning is to use the prepared weak alkaline solvent to clean for 2min +/-30S in an ultrasonic groove of 120-170KHZ and 900W at the temperature of 40 +/-5 ℃.
The tap water rinsing refers to that disposable tap water overflows to clean for 2min +/-30S in a 120-DEG 170KHZ 900W tap water ultrasonic cleaning tank.
The pure water cleaning adopts two tanks of pure water cleaning, each tank of pure water uses one-time overflow, the ultrasonic wave of the pure water in each tank is 120-170KHZ and 900W, and the cleaning time is 2min +/-30S respectively.
The isopropanol cleaning adopts two-groove isopropanol cleaning, the ultrasonic wave of each groove is 120-170KHZ and 900W, the cleaning time is 2min +/-30S respectively, and the density is controlled to be less than 0.820g/cm 3.
The drying by isopropanol refers to drying by isopropanol vapor for 70 +/-5S.
Detailed Description
The present invention will be described in further detail with reference to examples.
Example (b): a method for cleaning high-abrasion low-chemical stability optical glass comprises the following steps:
1. and (3) material supply confirmation: performing spot inspection on the incoming materials before cleaning according to a proportion of 10% to ensure that the incoming materials have no bad conditions such as grinding powder, finger prints, weight, bright silks and the like, and returning to the previous working procedure for treatment if the number of the bad conditions exceeds 2% of the total amount of the incoming materials; if the bad number is less than 2% of the total amount of the incoming materials, entering a product cleaning stage;
2. cleaning a product:
2-1, washing with a solvent; preparing a solvent by the following substances in percentage by mass: sodium hydroxide: 0.1% -0.5%; isopropanolamine: 0.1% -0.5%; sodium carbonate: 1% -3%; sodium phosphate: 5% -10%; the balance of water, the pH value of the solvent after the blending is 8-9, and then the solvent after the blending is used for cleaning for 2min +/-30S in an ultrasonic groove of 120-170KHZ and 900W at the temperature of 40 +/-5 ℃;
2-2, in a tap water ultrasonic cleaning tank with the temperature of 120-;
2-3, cleaning by adopting two tanks of pure water, wherein each tank of pure water uses one-time overflow, the ultrasonic wave of the pure water in each tank is 120-170KHZ and 900W, and the cleaning time is 2min +/-30S respectively;
2-4, cleaning by adopting isopropanol in two grooves, wherein the ultrasonic wave in each groove is 120-;
2-5, drying by using isopropanol vapor for 70 +/-5S.
Claims (4)
1. A cleaning method of optical glass with high abrasion degree and low chemical stability is provided, the optical glass satisfies any one of the following conditions: 1) relative grinding hardness FANot less than 300; 2) stability to Water action DWNot less than 4, stability against acid action DAThe cleaning method comprises the steps of solvent cleaning, tap water rinsing, pure water cleaning, isopropanol cleaning and isopropanol drying, and is characterized in that the solvent cleaning is to use a prepared solvent and clean the solvent in an ultrasonic wave groove with the temperature of 40 +/-5 ℃ and the ultrasonic wave groove with the volume of 120-: hydrogen hydroxideSodium: 0.1% -0.5%; isopropanolamine: 0.1% -0.5%; sodium carbonate: 1% -3%; sodium phosphate: 5% -10%; the balance of water, the pH value of the solvent after blending is 8-9, the tap water rinsing refers to overflowing with disposable tap water in a 120-DEG 170KHZ 900W tap water ultrasonic cleaning tank, cleaning is carried out for 2min +/-30S, and the isopropanol drying refers to drying with isopropanol steam, and the drying time is 70 +/-5S.
2. The method for cleaning high abrasion and low chemical stability optical glass according to claim 1, wherein the incoming material before cleaning is inspected at a rate of 10% to ensure that the incoming material is free from abrasive powder, finger print, weight and bright silk defects, and if the number of defects exceeds 2% of the total amount of the incoming material, the process is returned to the previous process.
3. The method as claimed in claim 1, wherein the pure water cleaning comprises two tanks, each tank is used with one-time overflow, the ultrasonic wave of each tank is 120-.
4. The method as claimed in claim 1, wherein the two-tank cleaning process is performed with 120-170KHZ 900W ultrasonic waves for 2min + -30S and the density is controlled to be less than 0.820g/cm 3.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910510634.4A CN110102537B (en) | 2019-06-13 | 2019-06-13 | Method for cleaning high-abrasion low-chemical-stability optical glass |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910510634.4A CN110102537B (en) | 2019-06-13 | 2019-06-13 | Method for cleaning high-abrasion low-chemical-stability optical glass |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN110102537A CN110102537A (en) | 2019-08-09 |
| CN110102537B true CN110102537B (en) | 2021-07-06 |
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| CN201910510634.4A Active CN110102537B (en) | 2019-06-13 | 2019-06-13 | Method for cleaning high-abrasion low-chemical-stability optical glass |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111088119A (en) * | 2019-12-18 | 2020-05-01 | 太湖达名欣盖板制造有限公司 | Touch control type glass cleaning agent |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105419972A (en) * | 2015-12-24 | 2016-03-23 | 东莞市安美润滑科技有限公司 | High-cleanliness degree corrosion-resistant water-based optical glass cleaning compound and application method thereof |
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| CN102151670A (en) * | 2010-12-31 | 2011-08-17 | 苏州市东元光电科技有限公司 | Method for cleaning and drying glass sheet |
| JP6419578B2 (en) * | 2012-12-27 | 2018-11-07 | Hoya株式会社 | Manufacturing method of glass substrate for hard disk |
| CN106583322A (en) * | 2016-11-28 | 2017-04-26 | 莱特巴斯光学仪器（镇江）有限公司 | Optical glass surface cleaning method |
| CN107673625A (en) * | 2017-11-07 | 2018-02-09 | 太仓经济开发区蕴源吉光工艺美术品工作室 | Glass etching liquid and glass etching method |
| CN107737766A (en) * | 2017-11-13 | 2018-02-27 | 苏州麦克博斯仪器有限公司 | A kind of optical glass ultrasonic cleaning process |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105419972A (en) * | 2015-12-24 | 2016-03-23 | 东莞市安美润滑科技有限公司 | High-cleanliness degree corrosion-resistant water-based optical glass cleaning compound and application method thereof |
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