CN110041828A - The formula and production method of liquid waterproof coiled material coating - Google Patents
The formula and production method of liquid waterproof coiled material coating Download PDFInfo
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- CN110041828A CN110041828A CN201910416210.1A CN201910416210A CN110041828A CN 110041828 A CN110041828 A CN 110041828A CN 201910416210 A CN201910416210 A CN 201910416210A CN 110041828 A CN110041828 A CN 110041828A
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- parts
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- coiled material
- material coating
- waterproof coiled
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
- C08J3/03—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D195/00—Coating compositions based on bituminous materials, e.g. asphalt, tar, pitch
- C09D195/005—Aqueous compositions, e.g. emulsions
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2395/00—Bituminous materials, e.g. asphalt, tar or pitch
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Inorganic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses the formula and production method of liquid waterproof coiled material coating, the raw material including following parts by weight: 30-50 parts of asphalt emulsion, 28-40 parts of pitch, 20-30 parts of filler, 4-6 parts of dispersing agent, 3-5 parts of defoaming agent, 2-3 parts of fungicide, 3-5 parts of thickener.The formula and production method of liquid waterproof coiled material coating proposed by the present invention, formula science, proportion is rigorous, its product has the characteristics that high tenacity, with preferable ductility, the caused crack of the slight vibration of building can be effectively resisted, high temperature resistant, water resistance are good, guarantee the waterproof performance of product, it is with good economic efficiency.
Description
Technical field
The present invention relates to the formulas of architectural waterproof material technical field more particularly to liquid waterproof coiled material coating and production side
Method.
Background technique
Liquid waterproof coiled material coating is a one-component water-based environment-friendly products, and product contains high molecular polymer and Gao Pin
High polymer and pitch are merged one by special modified technique by matter emulsified asphalt completely, and solid content is high, and rate of drying is fast, with
Concrete base layer adhesive force is strong, and high resiliency, shiny black waterproof coating are formed after solid, and waterproof coating has the effect of rubber like coiled material
Fruit, and there is excellent low temperature flexibility and high temperature sag resistance.It is connected as ne-leakage between engineering foundation and building, is
The first barrier of entire engineering waterproofing, plays a crucial role entire engineering.
The toughness of current liquid waterproof coiled material coating is low, and under the action of extraneous tensile stress, easy fracture is impaired, loses anti-
Water effect, and high temperature resistant, water resistance are poor, the application not being able to satisfy under various scenes, are based on above statement, the present invention proposes
The formula and production method of liquid waterproof coiled material coating.
Summary of the invention
The purpose of the present invention is to solve disadvantages existing in the prior art, and the liquid waterproof coiled material coating proposed
Formula and production method.
The formula of liquid waterproof coiled material coating, the raw material including following parts by weight: 30-50 parts of asphalt emulsion, pitch 28-40
Part, 20-30 parts of filler, 4-6 parts of dispersing agent, 3-5 parts of defoaming agent, 2-3 parts of fungicide, 3-5 parts of thickener.
Preferably, the raw material including following parts by weight: 40 parts of asphalt emulsion, 34 parts of pitch, 25 parts of filler, 5 parts of dispersing agent,
4 parts of defoaming agent, 2.5 parts of fungicide, 4 parts of thickener.
Preferably, the asphalt emulsion is prepared by the following method:
The pitch that parts by weight are 90 parts is weighed, constant temperature 50-60 minutes in 150 ° ± 0.5 ° of insulating box；Weigh parts by weight
For 1-2 parts of emulsifier, be dissolved in 40-45 parts of deionized water and be configured to soap lye, 65 ° water bath with thermostatic control 15-20 minutes；By constant temperature
Good pitch is added to as early as possible in soap lye, and starting high-shearing dispersion emulsifying machine is dispersed with stirring 10-15 minutes, and asphalt emulsion is made.
Preferably, the emulsifier uses cetyl trimethylammonium bromide or octadecyltrimethylammonium chloride.
Preferably, the revolving speed of the high-shearing dispersion emulsifying machine is 10000 rap/min.
Preferably, the pitch uses commercially available Period In Maoming 70# asphalt.
Preferably, the filler uses the wollastonite in powder of 400 mesh.
Preferably, the dispersing agent is commercially available ancient cooking vessel and DH-504, and the defoaming agent is commercially available ancient cooking vessel and DH-202, the sterilization
Agent is commercially available ancient cooking vessel and DH-LXF, and the thickener is commercially available ancient cooking vessel and DH-935.
The production method of liquid waterproof coiled material coating includes the following steps: to delay asphalt emulsion and pitch in a manner of thread
It is slow to be added in vacuum dispersator, filler is added after stirring evenly into mixing kettle, adds dispersing agent after mixing evenly, disappear
Infusion, fungicide allow the blade of high-speed mixer that mixture to be uniformly dispersed, and stir 30mim, add thickener stirring
30min, mixture in kettle to be mixed after viscous liquid in shutting down；With finished product after the filtering of 80 mesh gauze filters.
The formula and production method of liquid waterproof coiled material coating proposed by the present invention, proportion science, proportion is rigorous, product
Have the characteristics that high tenacity, there is preferable ductility, can effectively resist the caused crack of the slight vibration of building, it is resistance to
High temperature, water resistance are good, guarantee the waterproof performance of product, with good economic efficiency.
Specific embodiment
Combined with specific embodiments below the present invention is made further to explain.
Embodiment one
The formula of liquid waterproof coiled material coating, the raw material including following parts by weight: 30 parts of asphalt emulsion, 28 parts of pitch, filler 20
Part, 4 parts of dispersing agent, 3 parts of defoaming agent, 2 parts of fungicide, 3 parts of thickener.
The asphalt emulsion is prepared by the following method: the pitch that parts by weight are 90 parts is weighed, in 150 ° ± 0.5 ° of perseverance
Constant temperature 50 minutes in incubator；The emulsifier that parts by weight are 1 part is weighed, is dissolved in 40 parts of deionized water and is configured to soap lye, 65 °
Water bath with thermostatic control 15 minutes；The good pitch of constant temperature is added in soap lye as early as possible, starting high-shearing dispersion emulsifying machine is dispersed with stirring 10
Minute, asphalt emulsion is made；The emulsifier uses cetyl trimethylammonium bromide or octadecyltrimethylammonium chloride；Institute
The revolving speed for stating high-shearing dispersion emulsifying machine is 10000 rap/min.
The pitch uses commercially available Period In Maoming 70# asphalt；The filler uses the wollastonite in powder of 400 mesh；It is described
Dispersing agent be commercially available ancient cooking vessel and DH-504, the defoaming agent be commercially available ancient cooking vessel and DH-202, the fungicide be commercially available ancient cooking vessel and DH-LXF,
The thickener is commercially available ancient cooking vessel and DH-935.
Asphalt emulsion and pitch are slowly added into vacuum dispersator by the technique in a manner of thread, are stirred evenly backward
Filler is added in mixing kettle, adds dispersing agent, defoaming agent, fungicide after mixing evenly, the blade of high-speed mixer will be mixed
It closes object to be uniformly dispersed, stirs 30mim, add thickener stirring 30min, the mixture in kettle to be mixed is in after viscous liquid
It shuts down；With finished product after the filtering of 80 mesh gauze filters.
Embodiment two
The formula of liquid waterproof coiled material coating, the raw material including following parts by weight: 40 parts of asphalt emulsion, 34 parts of pitch, filler 25
Part, 5 parts of dispersing agent, 4 parts of defoaming agent, 2.5 parts of fungicide, 4 parts of thickener.
The asphalt emulsion is prepared by the following method: the pitch that parts by weight are 60 parts is weighed, in 150 ° ± 0.5 ° of perseverance
Constant temperature 55 minutes in incubator；The emulsifier that parts by weight are 1.5 parts is weighed, is dissolved in 42.5 parts of deionized water and is configured to soap
Liquid, 65 ° water bath with thermostatic control 17.5 minutes；The good pitch of constant temperature is added in soap lye as early as possible, starting high-shearing dispersion emulsifying machine stirs
Dispersion 12.5 minutes is mixed, asphalt emulsion is made；The emulsifier uses cetyl trimethylammonium bromide or octadecyl front three
Ammonium chloride；The revolving speed of the high-shearing dispersion emulsifying machine is 10000 rap/min.
The pitch uses commercially available Period In Maoming 70# asphalt；The filler uses the wollastonite in powder of 400 mesh；It is described
Dispersing agent be commercially available ancient cooking vessel and DH-504, the defoaming agent be commercially available ancient cooking vessel and DH-202, the fungicide be commercially available ancient cooking vessel and DH-LXF,
The thickener is commercially available ancient cooking vessel and DH-935.
Asphalt emulsion and pitch are slowly added into vacuum dispersator by the technique in a manner of thread, are stirred evenly backward
Filler is added in mixing kettle, adds dispersing agent, defoaming agent, fungicide after mixing evenly, the blade of high-speed mixer will be mixed
It closes object to be uniformly dispersed, stirs 30mim, add thickener stirring 30min, the mixture in kettle to be mixed is in after viscous liquid
It shuts down；With finished product after the filtering of 80 mesh gauze filters.
Embodiment three
The formula of liquid waterproof coiled material coating, the raw material including following parts by weight: 50 parts of asphalt emulsion, 40 parts of pitch, filler 30
Part, 6 parts of dispersing agent, 5 parts of defoaming agent, 3 parts of fungicide, 5 parts of thickener.
The asphalt emulsion is prepared by the following method: the pitch that parts by weight are 90 parts is weighed, in 150 ° ± 0.5 ° of perseverance
Constant temperature 60 minutes in incubator；The emulsifier that parts by weight are 2 parts is weighed, is dissolved in 45 parts of deionized water and is configured to soap lye, 65 °
Water bath with thermostatic control 20 minutes；The good pitch of constant temperature is added in soap lye as early as possible, starting high-shearing dispersion emulsifying machine is dispersed with stirring 15
Minute, asphalt emulsion is made；The emulsifier uses cetyl trimethylammonium bromide or octadecyltrimethylammonium chloride；Institute
The revolving speed for stating high-shearing dispersion emulsifying machine is 10000 rap/min.
The pitch uses commercially available Period In Maoming 70# asphalt；The filler uses the wollastonite in powder of 400 mesh；It is described
Dispersing agent be commercially available ancient cooking vessel and DH-504, the defoaming agent be commercially available ancient cooking vessel and DH-202, the fungicide be commercially available ancient cooking vessel and DH-LXF,
The thickener is commercially available ancient cooking vessel and DH-935.
Asphalt emulsion and pitch are slowly added into vacuum dispersator by the technique in a manner of thread, are stirred evenly backward
Filler is added in mixing kettle, adds dispersing agent, defoaming agent, fungicide after mixing evenly, the blade of high-speed mixer will be mixed
It closes object to be uniformly dispersed, stirs 30mim, add thickener stirring 30min, the mixture in kettle to be mixed is in after viscous liquid
It shuts down；With finished product after the filtering of 80 mesh gauze filters.
Through detecting, the product of technique production 5h under 80 DEG C of hot conditions, product is without trickling, crackle, peeling, blistering etc.
Phenomenon；Detect 4h respectively in the environment of 40 DEG C, -18 DEG C of minimum temperature of maximum temperature, 30 circulations are without product anomalous variation；?
Irradiate 400h under the weather-proof instrument of 6KW xenon lamp, product without trickling, blistering, elephant skin, fall off phenomena such as.
The formula and production method of liquid waterproof coiled material coating proposed by the present invention, proportion science, proportion is rigorous, product
Have the characteristics that high tenacity, there is preferable ductility, can effectively resist the caused crack of the slight vibration of building, it is resistance to
High temperature, water resistance are good, guarantee the waterproof performance of product, with good economic efficiency.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (9)
1. the formula of liquid waterproof coiled material coating, which is characterized in that the raw material including following parts by weight: 30-50 parts of asphalt emulsion,
28-40 parts of pitch, 20-30 parts of filler, 4-6 parts of dispersing agent, 3-5 parts of defoaming agent, 2-3 parts of fungicide, 3-5 parts of thickener.
2. the formula of liquid waterproof coiled material coating according to claim 1, which is characterized in that the original including following parts by weight
Material: 40 parts of asphalt emulsion, 34 parts of pitch, 25 parts of filler, 5 parts of dispersing agent, 4 parts of defoaming agent, 2.5 parts of fungicide, 4 parts of thickener.
3. the formula of liquid waterproof coiled material coating according to claim 1, which is characterized in that the asphalt emulsion is by as follows
Method preparation:
The pitch that parts by weight are 90 parts is weighed, constant temperature 50-60 minutes in 150 ° ± 0.5 ° of insulating box；Weigh parts by weight
For 1-2 parts of emulsifier, be dissolved in 40-45 parts of deionized water and be configured to soap lye, 65 ° water bath with thermostatic control 15-20 minutes；By constant temperature
Good pitch is added to as early as possible in soap lye, and starting high-shearing dispersion emulsifying machine is dispersed with stirring 10-15 minutes, and asphalt emulsion is made.
4. the formula of liquid waterproof coiled material coating according to claim 3, which is characterized in that the emulsifier uses 16
Alkyl trimethyl ammonium bromide or octadecyltrimethylammonium chloride.
5. the formula of liquid waterproof coiled material coating according to claim 3, which is characterized in that the high cut disperse emulsification
The revolving speed of machine is 10000 rap/min.
6. according to claim 1 with the formula of liquid waterproof coiled material coating described in 3, which is characterized in that the pitch use city
Sell Period In Maoming 70# asphalt.
7. the formula of liquid waterproof coiled material coating according to claim 1, which is characterized in that the filler uses 400 mesh
Wollastonite in powder.
8. the formula of liquid waterproof coiled material coating according to claim 1, which is characterized in that the dispersing agent is commercially available ancient cooking vessel
And DH-504, the defoaming agent are commercially available ancient cooking vessel and DH-202, the fungicide is commercially available ancient cooking vessel and DH-LXF, and the thickener is city
Sell ancient cooking vessel and DH-935.
9. the production method of liquid waterproof coiled material coating, which comprises the steps of: by asphalt emulsion and pitch with thin
Stream mode is slowly added into vacuum dispersator, and filler is added after stirring evenly into mixing kettle, adds after mixing evenly
Dispersing agent, defoaming agent, fungicide allow the blade of high-speed mixer that mixture to be uniformly dispersed, and stir 30mim, add thickening
30min is stirred in agent, and the mixture in kettle to be mixed after viscous liquid in shutting down；It is made into after being filtered with 80 mesh gauze filters
Product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910416210.1A CN110041828A (en) | 2019-05-20 | 2019-05-20 | The formula and production method of liquid waterproof coiled material coating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910416210.1A CN110041828A (en) | 2019-05-20 | 2019-05-20 | The formula and production method of liquid waterproof coiled material coating |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110041828A true CN110041828A (en) | 2019-07-23 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910416210.1A Pending CN110041828A (en) | 2019-05-20 | 2019-05-20 | The formula and production method of liquid waterproof coiled material coating |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111875974A (en) * | 2020-07-17 | 2020-11-03 | 徐鑫 | High-elasticity liquid waterproof coiled material and preparation method thereof |
| CN114874669A (en) * | 2021-12-31 | 2022-08-09 | 东方雨虹民用建材有限责任公司 | Energy-saving heat-preserving polymer modified asphalt waterproof coating and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105295730A (en) * | 2015-11-03 | 2016-02-03 | 景晓丽 | Asphalt waterproof coating and preparation method thereof |
| CN105694494A (en) * | 2016-03-30 | 2016-06-22 | 徐州卧牛山新型防水材料有限公司 | Emulsified asphalt and preparation method thereof, and water-based substrate treating agent for asphalt waterproof coiled materials and preparation method thereof |
-
2019
- 2019-05-20 CN CN201910416210.1A patent/CN110041828A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105295730A (en) * | 2015-11-03 | 2016-02-03 | 景晓丽 | Asphalt waterproof coating and preparation method thereof |
| CN105694494A (en) * | 2016-03-30 | 2016-06-22 | 徐州卧牛山新型防水材料有限公司 | Emulsified asphalt and preparation method thereof, and water-based substrate treating agent for asphalt waterproof coiled materials and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 姜晨光: "《土木工程材料学》", 31 July 2017, 中国建材工业出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111875974A (en) * | 2020-07-17 | 2020-11-03 | 徐鑫 | High-elasticity liquid waterproof coiled material and preparation method thereof |
| CN114874669A (en) * | 2021-12-31 | 2022-08-09 | 东方雨虹民用建材有限责任公司 | Energy-saving heat-preserving polymer modified asphalt waterproof coating and preparation method thereof |
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Application publication date: 20190723 |