CN110037335A - A kind of processing method and its application of dendrobium candidum - Google Patents
A kind of processing method and its application of dendrobium candidum Download PDFInfo
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- CN110037335A CN110037335A CN201910216203.7A CN201910216203A CN110037335A CN 110037335 A CN110037335 A CN 110037335A CN 201910216203 A CN201910216203 A CN 201910216203A CN 110037335 A CN110037335 A CN 110037335A
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- product
- processing method
- dendrobium candidum
- cigarette
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
Abstract
The invention belongs to plant product processed and applied field more particularly to the processing methods and its application of a kind of dendrobium candidum.The present invention provides a kind of processing methods of dendrobium candidum, and the present invention also provides a kind of products that above-mentioned processing method obtains in cigarette products, electronic cigarette cartridge or the application for brewing drink product field.In technical solution provided by the invention, cigarette or electronic cigarette cartridge is made in dendrobium candidum converted products, as the substitute of cigarette, dendrobium candidum processed goods is in burning, the benefit materials such as the polysaccharide being rich in dendrobium candidum can both play the role of the refreshing health-care to smoker, have the effect of promoting the production of body fluid, is hypoglycemic and improve immunity of organisms, at the same time it can also the substitute as the smoking cessation stage.The processing method and its application of a kind of dendrobium candidum provided by the invention solve the technological deficiency for lacking a kind of effective cigarette substitute in the prior art.
Description
Technical field
The invention belongs to the processing method of plant product processed and applied field more particularly to a kind of dendrobium candidum and its answer
With.
Background technique
Cigarette made of traditional pipe tobacco has the history of more than one thousand years, there is vast smoker basis in worldwide.Mesh
Before, cigarette product on the market can release the substances such as nicotine, tar, benzene, to smoker and people around when burning suction
Group brings great security risk.
For the consumption demand for cigarette for meeting smoker, meanwhile, reduce a series of suction health of traditional cigarette bring
Problem has developed a series of cigarette for being mixed with dendrobium candidum extracting solution or dendrobium candidum silk, still on the market at present
Such product can not fundamentally reduce health hazard of the cigarette for smoker and periphery secondhand smoke crowd, for smoking people
The cigarette substitute products exploitation of group is imperative.
Therefore, the processing method and its application of a kind of dendrobium candidum are developed, lacks one kind in the prior art for solving
The technological deficiency of effective cigarette substitute, becomes those skilled in the art's urgent problem to be solved.
Summary of the invention
In view of this, the present invention provides a kind of processing method of dendrobium candidum and its applications, for solving the prior art
In, lack a kind of technological deficiency of effective cigarette substitute.
The present invention provides a kind of processing method of dendrobium candidum, the processing method are as follows:
Step 1: pulverizing and sieving after dendrobium candidum freeze-drying, the first product is obtained；
Step 2: dendrobium candidum ungrease treatment, obtains the second product；
Step 3: after second product is mixed with organic solvent, refluxing extraction collects extracting solution and obtains third product；
Step 4: the third product is concentrated after purification, the 4th product is obtained；
Step 5: the 4th product is sprayed at the surface of first product, and it is dry after throwing, obtain product.
Preferably, in step 1, the partial size of first product is 200~300 mesh.
Preferably, in step 1, the temperature of the freeze-drying is -30~-20 DEG C, and the time of the freeze-drying is 90
~120min.
Preferably, in step 2, the method for the ungrease treatment are as follows: after dendrobium candidum is mixed with petroleum ether, 120~
150 DEG C of 2~3h of refluxing extraction collect extracting solution and obtain the second product.
Preferably, in step 3, the organic solvent is selected from: any one in methylene chloride, ether and ethyl acetate
Kind is a variety of.
Preferably, in step 3, the temperature of the refluxing extraction is 70~90 DEG C, the time of the refluxing extraction is 3~
4h。
Preferably, in step 4, the method for the purifying are as follows: washed after flowing through macroporous resin purification.
Preferably, in step 4, the temperature of the concentration is 60~80 DEG C, and the time of the concentration is 40~60min.
Preferably, in step 5, the feed ratio of the 4th product and first product is (1.5~2.5): 1ml/
Kg。
Preferably, in step 5, the water content of the product is 5~15%；
In step 5, the width of the product is 0.5~2.3mm.
The present invention also provides a kind of product obtained including processing method described in any of the above one cigarette products,
Electronic cigarette cartridge or the application for brewing drink product field.
In conclusion the present invention provides a kind of processing method of dendrobium candidum, are as follows: it is crushed after dendrobium candidum freeze-drying
Sieving, obtains the first product；Dendrobium candidum ungrease treatment obtains the second product；After second product is mixed with organic solvent, reflux
It extracts, collects extracting solution and obtain third product；The third product is concentrated after purification, obtains the 4th product；The 4th product sprinkling
It is dry after throwing on the surface of first product, obtain product.The present invention also provides a kind of productions that above-mentioned processing method obtains
Product are in cigarette products, electronic cigarette cartridge or the application for brewing drink product field.In technical solution provided by the invention, by iron sheet
Cigarette or electronic cigarette cartridge is made in dendrobium nobile converted products, and as the substitute of cigarette, dendrobium candidum processed goods is in burning, iron sheet
The benefit materials such as the polysaccharide being rich in dendrobium nobile can both play the role of the refreshing health-care to smoker, have promote the production of body fluid, it is hypoglycemic and
The effect of immunity of organisms is improved, at the same time it can also the substitute as the smoking cessation stage.A kind of dendrobium candidum provided by the invention
Processing method and its application, solve the technological deficiency for lacking a kind of effective cigarette substitute in the prior art.
Specific embodiment
The embodiment of the invention provides a kind of processing method of dendrobium candidum and its applications, for solving in the prior art,
Lack a kind of technological deficiency of effective cigarette substitute.
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common
Technical staff's every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
In order to which the present invention is described in more detail, below with reference to embodiment to a kind of processing side of dendrobium candidum provided by the invention
Method and its application, are specifically described.
Embodiment 1
The present embodiment is the specific embodiment for preparing product 1.
Removal of impurities, the dendrobium candidum cleaned, sterilized under vacuum conditions, crush after -22 DEG C of freeze-drying 90min, cross 200
~300 meshes obtain the first product 1.
After dendrobium candidum 1 is dissolved in the petroleum ether of 10 times of volumes, ungrease treatment is carried out in 120 DEG C of refluxing extraction 2.5h,
It collects extracting solution and obtains the second product 1.
After second product 1 is mixed with organic solvent 1, in 90 DEG C of refluxing extraction 3.6h, collects extracting solution and obtain third product 1；
In the present embodiment, organic solvent 1 is methylene chloride.
Third product 1 washes purifying after flowing through macroreticular resin again, in 70 DEG C of concentration 40min, obtains the 4th product 1.
4th product 1 is sprayed at the surface of the first product 1, dry after throwing, obtains product 1；Wherein, the 4th product 1 and
The feed ratio of one product is 1.8:1ml/Kg.The water content of obtained product 1 be the width of 5~15% products be 0.5~
2.3mm。
Embodiment 2
The present embodiment is the specific embodiment for preparing product 2.
Removal of impurities, the dendrobium candidum cleaned, sterilized under vacuum conditions, crush, mistake after -30 DEG C of freeze-drying 105min
200~300 meshes obtain the first product 2.
After dendrobium candidum 2 is dissolved in the petroleum ether of 10 times of volumes, ungrease treatment is carried out in 130 DEG C of refluxing extraction 2h, is received
Collection extracting solution obtains the second product 2.
After second product 2 is mixed with organic solvent 2, in 70 DEG C of refluxing extraction 4h, collects extracting solution and obtain third product 2；This
In embodiment, organic solvent 2 is ether.
Third product 2 washes purifying after flowing through macroreticular resin again, in 60 DEG C of concentration 60min, obtains the 4th product 2.
4th product 2 is sprayed at the surface of the first product 2, dry after throwing, obtains product 2；Wherein, the 4th product 2 and
The feed ratio of one product is 2.5:1ml/Kg.The water content of obtained product 2 be the width of 5~15% products be 0.5~
2.3mm。
Embodiment 3
The present embodiment is the specific embodiment for preparing product 3.
Removal of impurities, the dendrobium candidum cleaned, sterilized under vacuum conditions, crush, mistake after -20 DEG C of freeze-drying 120min
200~300 meshes obtain the first product 3.
After dendrobium candidum 3 is dissolved in the petroleum ether of 10 times of volumes, ungrease treatment is carried out in 150 DEG C of refluxing extraction 3h, is received
Collection extracting solution obtains the second product 3.
After second product 3 is mixed with organic solvent 3, in 85 DEG C of refluxing extraction 3h, collects extracting solution and obtain third product 3；This
In embodiment, organic solvent 3 is ethyl acetate.
Third product 3 washes purifying after flowing through macroreticular resin again, in 80 DEG C of concentration 50min, obtains the 4th product 3.
4th product 3 is sprayed at the surface of the first product 3, dry after throwing, obtains product 3；Wherein, the 4th product 3 and
The feed ratio of one product is 1.5:1ml/Kg.The water content of obtained product 3 be the width of 5~15% products be 0.5~
2.3mm。
Embodiment 4
The present embodiment is that the present embodiment is the specific of 1~3 panelist of product marking assessment made from measurement Examples 1 to 3
Product 1~3 made from Examples 1 to 3 is rolled into cigarette products 1~3 and smoke grenade product 1~3 by embodiment；In the present embodiment, institute
The reference substance used is commercial cigarettes product or commercially available smoke grenade product.
Five panelists carry out measurement of smokeing panel test, and carry out blind suction in continuous mode, i.e., panelist smoke panel test give a mark when and do not know
The number of road sample to be tested.Panelist suction when, from cigarette flavor, mouthfeel, effect of refreshing oneself and comprehensive score four dimensions into
Row marking, scoring is 1~5 point, and 5 points are optimal.The scoring for measuring cigarette products 1~3, smoke grenade product 1~3 and reference substance is average
Point, acquired results please refer to table 1.
Table 1
As can be drawn from Table 1, compared with cigarette/smoke grenade, dendrobium candidum made from technical solution provided by the invention adds
Work product, fragrance and mouthfeel are slightly better than commercially available traditional cigarette/smoke grenade, and effect of refreshing oneself and comprehensive score are better than reference substance, show
Product has good market acceptance.
From above-described embodiment, it can be concluded that, technical solution provided by the invention is had the advantage that
1, the present invention provides a kind of Pure dendrobium officinale kimura et migo converted products thinks instead of the processing of traditional cigarette/electronic cigarette cartridge
Road, the substitute products that can be used as cigarette use, and reduce the cigarette intake of smoker, while can also avoid non-smoker's secondhand smoke
The problem of intake；
2, dendrobium candidum product during processing, can release the benefit materials such as polysaccharide, and the present invention is used for a long time
Dendrobium candidum tobacco product made from technical solution will not only damage health, there is health care, have and promote the production of body fluid, drop blood
Sugar and the effect for improving immunity of organisms；
3, product produced by the present invention, not only can be as novel cigarette products, can also be with traditional dendrobium candidum
Teas is seemingly brewed and is drunk, and is stewed, is had wide range of applications at the same time it can also the tonic as Baoshang, easy to carry；
4, processing method provided by the invention, using the control of procedural style, atomization degree is high, needs not rely upon skill
The experience of art personnel, stable product quality, defect rate is low, effectively reduces processing cost.
In conclusion the present invention provides a kind of processing method of dendrobium candidum, are as follows: it is crushed after dendrobium candidum freeze-drying
Sieving, obtains the first product；Dendrobium candidum ungrease treatment obtains the second product；After second product is mixed with organic solvent, reflux
It extracts, collects extracting solution and obtain third product；The third product is concentrated after purification, obtains the 4th product；The 4th product sprinkling
It is dry after throwing on the surface of first product, obtain product.The present invention also provides a kind of productions that above-mentioned processing method obtains
Product are in cigarette products, electronic cigarette cartridge or the application for brewing drink product field.In technical solution provided by the invention, by iron sheet
Cigarette or electronic cigarette cartridge is made in dendrobium nobile converted products, and as the substitute of cigarette, dendrobium candidum processed goods is in burning, iron sheet
The benefit materials such as the polysaccharide being rich in dendrobium nobile can both play the role of the refreshing health-care to smoker, have promote the production of body fluid, it is hypoglycemic and
The effect of immunity of organisms is improved, at the same time it can also the substitute as the smoking cessation stage.A kind of dendrobium candidum provided by the invention
Processing method and its application, solve the technological deficiency for lacking a kind of effective cigarette substitute in the prior art.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also answered
It is considered as protection scope of the present invention.
Claims (10)
1. a kind of processing method of dendrobium candidum, which is characterized in that the processing method are as follows:
Step 1: pulverizing and sieving after dendrobium candidum freeze-drying, the first product is obtained；
Step 2: dendrobium candidum ungrease treatment, obtains the second product；
Step 3: after second product is mixed with organic solvent, refluxing extraction collects extracting solution and obtains third product；
Step 4: the third product is concentrated after purification, the 4th product is obtained；
Step 5: the 4th product is sprayed at the surface of first product, and it is dry after throwing, obtain product.
2. processing method according to claim 1, which is characterized in that in step 1, the partial size of first product is 200
~300 mesh.
3. processing method according to claim 1, which is characterized in that in step 1, the temperature of the freeze-drying is -30
~-20 DEG C, the time of the freeze-drying is 90~120min.
4. processing method according to claim 1, which is characterized in that in step 2, the method for the ungrease treatment are as follows: iron
After skin dendrobium nobile is mixed with petroleum ether, in 120~150 DEG C of 2~3h of refluxing extraction, collects extracting solution and obtain the second product.
5. processing method according to claim 1, which is characterized in that in step 3, the organic solvent is selected from: dichloromethane
Any one or more in alkane, ether and ethyl acetate；
In step 3, the temperature of the refluxing extraction is 70~90 DEG C, and the time of the refluxing extraction is 3~4h.
6. processing method according to claim 1, which is characterized in that in step 4, the method for the purifying are as follows: flow through big
It is washed after the purifying resin of hole.
7. processing method according to claim 1, which is characterized in that in step 4, the temperature of the concentration is 60~80
DEG C, the time of the concentration is 40~60min.
8. processing method according to claim 1, which is characterized in that in step 5, the 4th product and described first
The feed ratio of product is (1.5~2.5): 1ml/Kg.
9. processing method according to claim 1, which is characterized in that in step 5, the water content of the product is 5~
15%；
In step 5, the width of the product is 0.5~2.3mm.
10. a kind of product obtained including processing method described in claim 1 to 9 any one is in cigarette products, electronic cigarette
Smoke grenade or the application for brewing drink product field.
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| CN201910216203.7A CN110037335A (en) | 2019-03-20 | 2019-03-20 | A kind of processing method and its application of dendrobium candidum |
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| CN201910216203.7A CN110037335A (en) | 2019-03-20 | 2019-03-20 | A kind of processing method and its application of dendrobium candidum |
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