CN110025512A - A kind of black mud oil control and acne removal whitening mask and preparation method thereof - Google Patents

A kind of black mud oil control and acne removal whitening mask and preparation method thereof Download PDF

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Publication number
CN110025512A
CN110025512A CN201910315548.8A CN201910315548A CN110025512A CN 110025512 A CN110025512 A CN 110025512A CN 201910315548 A CN201910315548 A CN 201910315548A CN 110025512 A CN110025512 A CN 110025512A
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alginic acid
black mud
mask
oil control
acne removal
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CN110025512B (en
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王从相
朱信德
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GUANGDONG BEIHAO BIOTECHNOLOGY Co.,Ltd.
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Wenzhou Guangli Biomedical Technology Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0212Face masks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/676Ascorbic acid, i.e. vitamin C
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/731Cellulose; Quaternized cellulose derivatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/00Cosmetics or similar toiletry preparations
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    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/965Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
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    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P17/00Drugs for dermatological disorders
    • A61P17/10Anti-acne agents
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/008Preparations for oily skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin

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Abstract

The invention belongs to cosmetic fields, specifically, the present invention relates to a kind of black mud oil control and acne removal whitening mask and preparation method thereof.A kind of black mud oil control and acne removal whitening mask, the facial mask is made of substrate and mask composition ingredient, the mask composition is coated uniformly on substrate, the mask composition includes component below by mass percentage: black mud powder 5 ~ 20%, chamomile extract 1.0 ~ 5.0%, Baical Skullcap root P.E 1.0 ~ 5.0%, tranexamic acid 1.0 ~ 5.0%, 3-o- ethylascorbyl 0.1 ~ 0.5%, octyl phenol polyoxyethylene ether 0.1 ~ 1.0%, glycerol 5.0 ~ 10%, propylene glycol 5.0 ~ 10%, hydroxyethyl cellulose 0.1 ~ 0.5%, Sodium Hyaluronate 0.5 ~ 3.0%, deionized water 40 ~ 60%.The facial mask has absorption grease using black mud powder, and combines chamomile extract, Baical Skullcap root P.E, tranexamic acid and Sodium Hyaluronate, carries out pox-eliminating whitening effect, has reached safely and effectively oil control and acne removal whitening purpose.

Description

A kind of black mud oil control and acne removal whitening mask and preparation method thereof
Technical field
The invention belongs to cosmetic fields, specifically, the present invention relates to a kind of black mud oil control and acne removal whitening mask and its Preparation method.
Background technique
Acne is commonly called as whelk, acne, dark sore, and Chinese medicine ancient times are called face sore, acne.Acne is dermatology common disease, It is a kind of chronic inflammatory skin disease for betiding hair follicle and sebaceous glands, is mainly in the sebums such as Head And Face, neck, shirtfront back Suffered from different degrees of acne there are about 85% people in puberty according to statistics in gland position abundant.The scar that acne generates, meeting The appearance of patient is seriously affected, adverse effect further is generated to its psychology.The clinical manifestation of acne from physiological acne to Inflammatory papules, warts, tubercle, tumour, serious person also easily form scar, facial melanin deposition.Acne not only influences people's Beauty, mood and mental health to people also generate certain influence down to behavior.Modern medicine thinks the cause of disease of acne It is more complicated, be caused by many reasons, such as: male sex hormone adjusts the exception of sebum secretion, keratinization is abnormal, microorganism Infection, inflammatory reaction, immune response etc., wherein the infection and inflammatory reaction of microorganism are an important spies of acne Property.
As the improvement of people's living standards, requirement of the people for beauty also increasingly improves.Facial mask becomes people's beauty Maintenance is preferred.Facial mask is a classification in skin care item, and its most basic and most important purpose is to make up makeup removing and wash one's face still Right insufficient cleaning cooperates other essential ingredients to realize other maintenance functions, such as replenishing water and preserving moisture, beauty on this basis White, anti-aging, Sage Extract etc..
Instantly facial mask has become the category that beauty market increasingly occupies the initiative position, and facial mask application method is simple, both saves Nursing time, and can easily enjoy the nursing of beauty parlor's formula.The principle of facial mask is that the of short duration time of face is covered on using it, It is temporarily isolating extraneous air and pollution by Face film towel, expands the pore of skin, promotes the secretion and metabolism of sweat gland, The oxygen content of skin is risen, and skin is promoted to exclude the product of the metabolism of epidermal cell and the grease type object of accumulation Matter is rapidly soaked into highly condensed nutritious ingredient in facial mask liquid in the cuticula of skin epidermis, to realize quickly having for skin The effects of effect is nursed, and replenishing water and preserving moisture, whitening and anti-aging, Sage Extract, Eradicates acne are played, thus have by numerous people seeking beauties' Like.
Facial mask core is that the liquid containing various effective components is carried with face mask substrate material spreads on face to extend effective component Performance of keeping humidity with the time of skin contact, therefore face mask substrate material is the basis of facial mask effect, in addition, the wet strength of facial mask, wet Toughness and certain gas permeability are also facial mask and skin is in close contact and the basis of comfortable wearing.Current facial masks most on the market Substrate is using raw materials such as chitosan, carboxymethyl cellulose, azelon, gelatin, alginic acid, polyester fiber, viscose fibers The blended non-woven fabrics of preparation.The non-woven fabrics moisture-retaining capacity and wet toughness of the preparation of the chemical materials such as terylene etc. are not ideal enough, and And due to bio-compatible sexual stimulus problem more need to make using anti-irritant or anti-sensitive composition such as bisabol, dipotassium glycyrrhizinate etc. Cause mask product ingredient organoleptic impression bad with chemical products;Natural fiber non-woven fabrics has good biocompatibility more, But wet strength is often insufficient, and moisture-retaining capacity is also different multifarious with formula, it is difficult to realize ideal balance with other performances.
Alginic acid is the natural macromolecular material extracted from brown algae plant, and good thickening property, can drop at film forming Solution property and pro-skin characteristic make it have a wide range of applications in fields such as facial mask, medical dressing, but alginic acid fibre is wet strong There are biggish deficiencies in terms of degree, wet toughness, even if being modified the effect for being still difficult to reach satisfied using chitosan, gelatin etc. Fruit, and often will affect its performance of keeping humidity.
For this purpose, applicant has applied for that Chinese invention patent (application number: 2019101806906) provides a kind of natural component Non-woven fabrics face mask substrate material and preparation method thereof, the natural component non-woven fabrics face mask substrate material by chitin modified alginic acid fibre and Chitin fiber is made, and is pre-processed using sodium acetate to it before alginic acid fibre is modified, can effectively improve alginic acid The mechanical performance of sodium non-woven fabrics face mask substrate material product, while also having very great help to the moisture-retaining capacity of facial mask.
Summary of the invention
The purpose of the application provides a kind of black mud oil control and acne removal whitening mask, which has absorption using black mud powder Grease, and chamomile extract, Baical Skullcap root P.E, tranexamic acid and Sodium Hyaluronate are combined, pox-eliminating whitening effect is carried out, is reached Reach safely and effectively oil control and acne removal whitening purpose.Further, the substrate of the application by chitin modified alginic acid fibre with And chitin fiber is made, and is pre-processed using sodium acetate to it before alginic acid fibre is modified, effectively improves alginic acid The mechanical performance of sodium non-woven fabrics face mask substrate material product, while also having very great help to the moisture-retaining capacity of facial mask.
In order to achieve the above purpose, present invention employs technical solutions below:
A kind of black mud oil control and acne removal whitening mask, the facial mask are made of substrate and mask composition ingredient, the mask composition Object is coated uniformly on substrate, and the mask composition includes component below by mass percentage: black mud powder 5 ~ 20%, Chamomile extract 1.0 ~ 5.0%, Baical Skullcap root P.E 1.0 ~ 5.0%, tranexamic acid 1.0 ~ 5.0%, 3-o- ethylascorbyl 0.1 ~ 0.5%, octyl phenol polyoxyethylene ether 0.1 ~ 1.0%, glycerol 5.0 ~ 10%, propylene glycol 5.0 ~ 10%, hydroxyethyl cellulose 0.1 ~ 0.5%, Sodium Hyaluronate 0.5 ~ 3.0%, deionized water 40 ~ 60%.
Preferably, the mask composition includes component below by mass percentage: black mud powder 8 ~ 15%, spring Yellow chrysanthemum extract 2.0 ~ 4.0%, Baical Skullcap root P.E 2.0 ~ 4.0%, tranexamic acid 2.0 ~ 4.0%, 3-o- ethylascorbyl 0.2 ~ 0.4%, octyl phenol polyoxyethylene ether 0.2 ~ 0.8%, glycerol 6.0 ~ 10%, propylene glycol 8.0 ~ 10%, hydroxyethyl cellulose 0.2 ~ 0.4%, Sodium Hyaluronate 1.0 ~ 2.5%, deionized water 45 ~ 55%.
As most preferably, the mask composition includes component below by mass percentage: black mud powder 15.2%, Chamomile extract 2.5%, Baical Skullcap root P.E 3.2%, tranexamic acid 3.5%, 3-o- ethylascorbyl 0.3%, octyl phenol polyoxy Vinethene 0.5%, glycerol 10.6%, propylene glycol 8.2%, hydroxyethyl cellulose 0.4%, Sodium Hyaluronate 1.2%, deionized water 51.2%。
Preferably, the composition further includes one of anti-inflammatory agent, chelating agent, preservative and essence or a variety of.
As further preferably, anti-inflammatory agent is dipotassium glycyrrhizinate;Chelating agent is EDTA disodium;Preservative selects oxazolidinyl urea, second Interior uride, one of isothiazolinone and parabens or a variety of.
Inventor has found in face mask substrate material experimental formula, the low concentration highly basic that alginic acid fibre uses more before modified at present Pre-swollen processing is broken in the method for fiber surface molecules align, and highly basic is breaking fiber surface molecules align convenient for subsequent crosslinking While, destruction also is produced to the main body of alginic acid fibre.It is found by the applicant that being manufactured using the sodium acetate of higher concentration opposite Mild alkaline condition pre-processes the machine that can effectively improve sodium alginate non-woven fabrics face mask substrate material product to sodium alginate Tool performance, while also having very great help to the moisture-retaining capacity of facial mask.
For this purpose, further, the substrate is made of chitin modified alginic acid fibre and chitin fiber, chitosan The mass ratio of modified alginic acid fibre and chitin fiber is 4:1 ~ 2:1;The preparation of the chitin modified alginic acid fibre Method is as follows: 1) when preparing chitin modified alginic acid fibre, using alkaline solution to it before alginic acid fibre is modified Pre-processed, 2) slough lye after, be added alginic acid fibre dry mass 2% ~ 10%;Chitosan solution changes at 35 ~ 45 degrees Celsius Property 30 ~ 60 minutes, take off liquid, drying, shredding.
Further, molten using sodium acetate before alginic acid fibre is modified when preparing chitin modified alginic acid fibre Liquid pre-processes it.
Further, preprocessing process specifically: use the sodium acetate solution of 10 times of 80g/L of alginic acid fibre dry mass Pretreatment alginic acid fibre 30 minutes.
Further, modifying process specifically: the sodium acetate solution using 10 times of 80g/L of alginic acid fibre dry mass is pre- After sloughing lye, the chitosan solution of 5 times of alginic acid fibre dry mass of concentration 1.5% is added in processing alginic acid fibre 30 minutes 40 degrees Celsius modification 45 minutes, take off liquid, drying, shredding.
The present invention also provides a kind of method for preparing the oil control and acne removal whitening mask, this method is by mask composition Then the mask composition is coated on substrate, radiation treatment, segmentation packaging by uniformly mixing.
Alginic acid and chitosan in the present invention can choose the product in various sources, as kelp, small kelp, thallus laminariae, The alginic acid and chitosan of the preparations such as shrimp shell, crab shell, silkworm chrysalis, can be according to raw material sources, required product performance and preparation process Need the alginic acid for selecting various molecular weight and deacetylation and chitosan to prepare face mask substrate material.
Due to the adoption of the above technical solution, which has absorption grease using black mud powder to the present invention, and combines the spring Yellow chrysanthemum extract, Baical Skullcap root P.E, tranexamic acid and Sodium Hyaluronate carry out pox-eliminating whitening effect, and having reached safety has The oil control and acne removal whitening purpose of effect.Further, the substrate of the application is by chitin modified alginic acid fibre and chitin fiber It is made, it is pre-processed using sodium acetate before alginic acid fibre is modified, effectively improves sodium alginate non-woven fabrics facial mask The mechanical performance of substrate product, while also having very great help to the moisture-retaining capacity of facial mask.
Detailed description of the invention
Fig. 1 alginic acid fibre non-woven fabrics scanning electron microscope image;
The chitin modified alginic acid fibre non-woven fabrics scanning electron microscope image of Fig. 2 NaOH pretreatment;
Fig. 3 sodium acetate pre-processes chitin modified alginic acid fibre non-woven fabrics scanning electron microscope image.
Specific embodiment
Main agents and instrument
Alginic acid fibre and chitin fiber: the production of Qingdao bright moon bio-medical material Co., Ltd;
Chitosan: Jiangsu is emerging to be produced at biological products Co., Ltd, and inventor is from deacetylation about 72.5% is surveyed, and molecular weight is about 1.4x105
Sodium acetate: Tianjin Tian Mao Chemical Co., Ltd. production;
Black mud powder: Beihai Bo Sheng mining industry Co., Ltd provides;
Chamomile extract, Baical Skullcap root P.E: the production of Xi'an Rayleigh Biotechnology Co., Ltd;
Tranexamic acid: Hubei Mao Er irrigates the production of biological medicine Co., Ltd;
3-o- ethylascorbyl, Sodium Hyaluronate, propylene glycol, glycerol, hydroxyethyl cellulose: Shantou City's merit promise chemical science and technology has Limit company provides;
Double screw extruder: XF, the Zhangjiagang rising sun send out mechanical Science and Technology Ltd.'s production;
Spun-bonded non-woven fabrics Weaving-machine: RH-PC-4/750, the production of Wenzhou Rong Hui Machinery Manufacturing Co., Ltd.;
JSM-840 scanning electron microscope: Tokyo Electronics Inc.'s production
Other reagents and instrument and equipment are conventional homemade goods (tensile property and performance of keeping humidity detection commission quality testing department research It is carried out, examination criteria is only provided, specific equipment is unknown).
The preparation of the chitin modified alginic acid fibre of embodiment 1
According to mechanical performance and performance of keeping humidity carry out orthogonal experiment choose suitable concentration of lye, the processing time, chitosan concentration, Modification time, dosage parameter prepare chitin modified alginic acid fibre with two optimal embodiments.
Chitin modified alginic acid fibre 1:
It is pre-processed alginic acid fibre 30 minutes using the sodium acetate solution of 10 times of 80g/L of alginic acid fibre dry mass, sloughs alkali After liquid, 40 degrees Celsius of the chitosan solution modification 45 minutes of 5 times of alginic acid fibre dry mass of concentration 1.5% is added, takes off liquid, do Dry, shredding.
Chitin modified alginic acid fibre 2:
It is pre-processed alginic acid fibre 10 minutes, is taken off using the sodium hydroxide solution of 10 times of 30g/L of alginic acid fibre dry mass After removing lye, 50 degrees Celsius of the chitosan solution modification 30 minutes of the concentration 1% of 5 times of alginic acid fibre dry mass of addition, de- liquid, Dry, shredding.
The preparation of 2 non-woven fabrics face mask substrate material of embodiment
Orthogonal experiment is carried out according to mechanical performance and performance of keeping humidity and chooses suitable chitin fiber dosage and processing parameter, with most It is in order to which closing to reality mask product as far as possible is in reality that softening agent, which is added, in ten times of non-woven fabrics face mask substrate material 1-3(of good embodiment Apply in example 4 more accurately test performance;It is since a variety of softening agents are to Electronic Speculum that softening agent, which is not used, in mask product in embodiment 3 Observation has interference;60Coradiation processing carries out in oxygen/nitrogen atmosphere, away from radiation center 1m, amount of radiation amount about 2.4kGy).
Non-woven fabrics face mask substrate material 1:
It takes in 1 30 parts of chitin modified alginic acid fibre and 10 parts of loading batch mixers of chitin fiber and is blended 10-20 minutes, lead to Cross double screw extruder heating melting 30 minutes, be drawn into silk, be laid with networking, it is hot-forming, coating pure water (dissolved with 3% it is sweet Oily ether quaternary ammonium salt softening agent), drying, radiation treatment (Co 60), segmentation packaging.
Non-woven fabrics face mask substrate material 2:
It takes in 2 30 parts of chitin modified alginic acid fibre and 10 parts of loading batch mixers of chitin fiber and is blended 10-20 minutes, lead to Cross double screw extruder heating melting 30 minutes, be drawn into silk, be laid with networking, it is hot-forming, coating pure water (dissolved with 3% it is sweet Oily ether quaternary ammonium salt softening agent), drying, radiation treatment (Co 60), segmentation packaging.
Non-woven fabrics face mask substrate material 3:
It takes in 30 parts of unmodified alginic acid fibre and 10 parts of loading batch mixers of chitin fiber and is blended 10-20 minutes, pass through double spiral shells Bar extruder heating melting 30 minutes is drawn into silk, is laid with networking, hot-forming, is coated with pure water (dissolved with 3% glycerin ether season Ammonium salt softening agent), drying, radiation treatment (Co 60), segmentation packaging.
The electron microscopic morphology of 3 non-woven fabrics face mask substrate material of embodiment is observed
Facial mask (no softener, other are with embodiment 2) is prepared to the piece of 5 millimeters of square, surface metal spraying 20 minutes, thickness about 10 was micro- Rice, liquid nitrogen frozen fracture, acceleration voltage 20kv observation, the results are shown in attached figure 1-3.
Alginic acid fibre nonwoven surface chitosan and the alginic acid winding of NaOH pretreatment have been cross-linked to form coarse Network, this network may cause the raising of its mechanical performance, but unfavorable to performance of keeping humidity;Sodium acetate is pre- in contrast The cross-linked state of the alginic acid fibre nonwoven surface of processing is finer and close and uniform, not only facilitates raising performance of keeping humidity, Be conducive to the further improvement of mechanical performance.
The mechanical performance and performance of keeping humidity of 4 non-woven fabrics face mask substrate material of embodiment
Tensile property is according to GB/T 3923.1-2013 (textile fabric tensile property part 1 ultimate strength and extension at break The measurement (galley proof method) of rate) measurement mask product tensile property
Performance of keeping humidity detection method is as follows: the film sample of 8 centimeter squares taken, is weighed, at 25 degrees Celsius, 60% relative humidity The film sample of 8 centimeter squares is impregnated 15 minutes in the culture dish equipped with pure water in insulating box, 1 is vacantly placed after taking-up Or so minute drips to without continuous droplet, weighing.By the comparative determination performance of keeping humidity of dry weight and weight in wet base (after water absorption rate=water suction Weight/water suction before weight x100%).
As a result as shown in the table:
By the visible NaOH pretreatment of above-mentioned data alginic acid fibre non-woven fabrics mechanical performance be improved significantly, but inhale It is aqueous to have no progress, or even it is declined slightly (possible reason is referring to embodiment 2).And the pretreated alginic acid fibre of sodium acetate (tensile strength is essentially identical with NaOH pretreatment, and fracture is stretched while realizing marked improvement in mechanical performance for non-woven fabrics Long rate is obviously preferable, is easier to be in close contact skin when sticking), facial mask water suction performance of keeping humidity is also greatly improved, other width Degree is more than 30%.The technique of the pretreated alginic acid fibre of the application sodium acetate effectively increases the performance of mask nonwoven fabric product, And it is expected after improving for being required for clothing, medical dressing etc. to mechanical, water absorbing properties in other formula of non-woven cloth Other purposes.
The preparation of 5 oil control and acne removal whitening mask of embodiment
A kind of black mud oil control and acne removal whitening mask, which is characterized in that the mask composition include by mass percentage with Under component: black mud powder 15.2%, chamomile extract 2.5%, Baical Skullcap root P.E 3.2%, tranexamic acid 3.5%, 3-o- ethyl are anti- Bad hematic acid 0.3%, octyl phenol polyoxyethylene ether 0.5%, glycerol 10.6%, propylene glycol 8.2%, hydroxyethyl cellulose 0.4%, hyalomitome Sour sodium 1.2%, dipotassium glycyrrhizinate 0.1%, EDTA disodium 0.05%, oxazolidinyl urea 0.2%, deionized water 54.05%.
The preparation method is as follows: this method uniformly mixes mask composition, then the mask composition is coated on Non-woven fabrics face mask substrate material 1, radiation treatment, segmentation packaging.
The experiment of 6 oil control and acne removal of embodiment
1, voluntary 160 people of trier (80 people of male, 80 people of women, 18-25 years old age) is chosen, there are papule, useless fellow, acne in face Trace, physical condition is normal, no cosmetic allergic contact dermatitis history.Volunteer is divided into 4 groups, every group of 40 people, male to female ratio is fifty-fifty.First group, 5 product of embodiment on probation;Second group, the mask composition composition formula of embodiment 5 is tried out, common non-woven fabric is aided with;Third group, it is commercially available Pox-eliminating whitening facial mask.
2, application method: volunteer uses a whitening mask every 2 d, and continuous 8 weeks, while deactivating it during test His all whitening class skin care item.By questionnaire form, subjective assessment of the trier to used product, including whitening effect are investigated And the indexs such as product is dry and astringent, excitement.It the results are shown in Table 1.Meanwhile observation improves situation, knot with statistics volunteer's facial skin Fruit is shown in Table 2.
It is effective: face's papule, useless fellow, pockmark recession 60%~90%;
It is effective: face's papule, useless fellow, pockmark recession 20%~60%;
It is invalid: face's papule, useless fellow, pockmark recession < 20%.
3, experimental result
1 trier of table is to product evaluation application form
2 product anti-acne effect evaluation table of the embodiment of the present invention of table
Above-mentioned two table is trier to the evaluation table of Evaluation product, the results show that first group, second group and third of the invention in table Set product has preferable anti-acne and whitening function.Wherein, table 1 the result shows that, first group of the present invention, the whitening of the second set product Effect is obvious, and trier is substantially better than commercially available pox-eliminating whitening frost to the evaluation of whitening effect, wherein the whitening of the first set product is imitated Fruit is best;Table 2 is the results show that first group of the present invention, the second set product can significantly improve the shape of tested volunteer's facial skin State, the symptoms such as papule, useless fellow, pockmark be improved significantly, it is efficient 85.0% or more, it is bright to illustrate that product of the present invention has Aobvious anti-acne effect, wherein the effect of the first set product is the most obvious, and effective percentage reaches 95.0%, is better than the second set product, Also it is significantly better than commercially available pox-eliminating whitening frost.In addition, the application product is without allergy and excitement, Product Safety is high.

Claims (10)

1. a kind of black mud oil control and acne removal whitening mask, the facial mask are made of substrate and mask composition ingredient, the facial mask group It closes object to be coated uniformly on substrate, which is characterized in that the mask composition includes component below by mass percentage: Black mud powder 5 ~ 20%, chamomile extract 1.0 ~ 5.0%, Baical Skullcap root P.E 1.0 ~ 5.0%, tranexamic acid 1.0 ~ 5.0%, 3-o- ethyl Ascorbic acid 0.1 ~ 0.5%, octyl phenol polyoxyethylene ether 0.1 ~ 1.0%, glycerol 5.0 ~ 10%, propylene glycol 5.0 ~ 10%, ethoxy Cellulose 0.1 ~ 0.5%, Sodium Hyaluronate 0.5 ~ 3.0%, deionized water 40 ~ 60%.
2. a kind of black mud oil control and acne removal whitening mask according to claim 1, which is characterized in that the mask composition By mass percentage including component below: black mud powder 8 ~ 15%, chamomile extract 2.0 ~ 4.0%, Baical Skullcap root P.E 2.0 ~ 4.0%, tranexamic acid 2.0 ~ 4.0%, 3-o- ethylascorbyl 0.2 ~ 0.4%, octyl phenol polyoxyethylene ether 0.2 ~ 0.8% is sweet Oil 6.0 ~ 10%, propylene glycol 8.0 ~ 10%, hydroxyethyl cellulose 0.2 ~ 0.4%, Sodium Hyaluronate 1.0 ~ 2.5%, deionized water 45 ~ 55%。
3. a kind of black mud oil control and acne removal whitening mask according to claim 1, which is characterized in that the mask composition It by mass percentage include component below: black mud powder 15.2%, chamomile extract 2.5%, Baical Skullcap root P.E 3.2%, ammonia first Naphthenic acid 3.5%, 3-o- ethylascorbyl 0.3%, octyl phenol polyoxyethylene ether 0.5%, glycerol 10.6%, propylene glycol 8.2%, hydroxyl second Base cellulose 0.4%, Sodium Hyaluronate 1.2%, deionized water 54.2%.
4. a kind of black mud oil control and acne removal whitening mask according to claim 1, which is characterized in that it is characterized in that, the group Closing object further includes one of anti-inflammatory agent, chelating agent, preservative and essence or a variety of.
5. a kind of black mud oil control and acne removal whitening mask according to claim 1, which is characterized in that it is characterized in that, anti-inflammatory Agent is dipotassium glycyrrhizinate;Chelating agent is EDTA disodium;Preservative selects oxazolidinyl urea, hydantoins, isothiazolinone and Ni Bo One of golden esters are a variety of.
6. a kind of black mud oil control and acne removal whitening mask according to claim 1, which is characterized in that the substrate is gathered by shell The modified alginic acid fibre of sugar and chitin fiber are made, and the mass ratio of chitin modified alginic acid fibre and chitin fiber is 4:1 ~ 2:1;The chitin modified alginic acid fibre the preparation method is as follows: 1) preparing chitin modified alginic acid fibre When, it is pre-processed using alkaline solution before alginic acid fibre is modified, 2) slough lye after, alginic acid fibre is added 2% ~ 10% chitosan solution of dry mass is 30 ~ 60 minutes modified at 35 ~ 45 degrees Celsius, takes off liquid, drying, shredding.
7. a kind of black mud oil control and acne removal whitening mask according to claim 6, which is characterized in that prepare chitin modified sea When alginate fibre, it is pre-processed using sodium acetate solution before alginic acid fibre is modified.
8. a kind of black mud oil control and acne removal whitening mask according to claim 7, which is characterized in that dry using alginic acid fibre The sodium acetate solution for the 80g/L that 10 times of quality pre-processes alginic acid fibre 30 minutes.
9. a kind of black mud oil control and acne removal whitening mask according to claim 7, which is characterized in that dry using alginic acid fibre The sodium acetate solution for the 80g/L that 10 times of quality pre-processes alginic acid fibre 30 minutes, and after sloughing lye, it is dry that alginic acid fibre is added 40 degrees Celsius of the chitosan solution modification 45 minutes for the concentration 1.5% that 5 times of quality takes off liquid, drying, shredding.
10. a kind of method for preparing oil control and acne removal whitening mask described in claim 1 ~ 9 any one claim, feature It is, this method uniformly mixes mask composition, and the mask composition is then coated on substrate, and radiation treatment is divided Steamed sandwich dress.
CN201910315548.8A 2019-04-19 2019-04-19 Black mud oil-control acne-removing whitening mask and preparation method thereof Active CN110025512B (en)

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