CN110016387A - Edible vegetable oil degumming agent and preparation method thereof and refined oil method - Google Patents

Edible vegetable oil degumming agent and preparation method thereof and refined oil method Download PDF

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Publication number
CN110016387A
CN110016387A CN201910382509.XA CN201910382509A CN110016387A CN 110016387 A CN110016387 A CN 110016387A CN 201910382509 A CN201910382509 A CN 201910382509A CN 110016387 A CN110016387 A CN 110016387A
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CN
China
Prior art keywords
oil
parts
degumming agent
degumming
diatomite
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910382509.XA
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Chinese (zh)
Inventor
姚英政
熊伟
宣朴
梁强
曾诗琴
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Saas Agro-Food Science & Technology Research Institute
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Saas Agro-Food Science & Technology Research Institute
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Saas Agro-Food Science & Technology Research Institute filed Critical Saas Agro-Food Science & Technology Research Institute
Priority to CN201910382509.XA priority Critical patent/CN110016387A/en
Publication of CN110016387A publication Critical patent/CN110016387A/en
Priority to PCT/CN2020/071071 priority patent/WO2020224293A1/en
Priority to AU2020239775A priority patent/AU2020239775B2/en
Pending legal-status Critical Current

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Classifications

    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
    • A23D9/04—Working-up
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/10—Refining fats or fatty oils by adsorption

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Fats And Perfumes (AREA)
  • Edible Oils And Fats (AREA)

Abstract

The invention discloses a kind of edible vegetable oil degumming agent and preparation method thereof and using the refined oil method of the edible vegetable oil degumming agent；The degumming agent includes: silica, diatomite and oil cake；The method of refining includes: in parts by weight, 100 parts of crude oils and 0.5~10 part of degumming agent to be mixed, are stirred, and filtering obtains refined oil；The method of refining degumming effect is good, improves grease color, retains vegetable oil fragrance, can reduce cost and time-consuming can consume, and waste water handling problem is not present.

Description

Edible vegetable oil degumming agent and preparation method thereof and refined oil method
Technical field
The present invention relates to edible oil processing technique fields, and in particular to edible vegetable oil degumming agent and preparation method thereof and food With vegetable oil fine smelting method.
Background technique
Edible vegetable oil usually passes through degumming raw oil, removing impurities, depickling, precipitation, drying, decoloration, deodorization and winterisation etc. Full refining process is processed, and the triglycerides of high-purity is obtained, and also has lost active constituent while removing harmful substance With vegetable oil peculiar taste, the unnecessary energy and the consumption of materials are caused, and is taken a long time, also will increase sewage discharge can It can property.
The technique that phosphatide is removed in oil and fat refining process is referred to as degumming.Existing degumming tech includes water to current line in the industry Degumming and enzymatic degumming.Phosphatide can be divided into hydrated phospholipid and non-hydratable phospholipid, and the defect of water degumming be not removing it is non-aqueous Change phosphatide, phosphatide removal rate is lower；The removal effect of enzymatic degumming is good, but defect is the on the high side of enzyme, opposite to be produced into This height.
Summary of the invention
In view of this, the application provides edible vegetable oil degumming agent and preparation method thereof and refined oil method； The refined oil method is economic, practical, and degumming effect is good, improves grease color, retains vegetable oil fragrance, can reduce Cost and the time-consuming consumption of energy, and waste water handling problem is not present.
In order to solve the above technical problems, technical solution provided by the present application is a kind of edible vegetable oil degumming agent, with weight Part meter, the degumming agent includes: silica 1~7 part, 1~7 part of diatomite and 2~18 parts of oil cake.
Preferably, in parts by weight, the degumming agent is by silica 1~7 part, 1~7 part of diatomite and oil cake 2~18 Part composition.
Preferably, in parts by weight, the degumming agent includes: 2 parts of silica, 1 part of diatomite and 7 parts of oil cake.
The present invention provides the preparation methods of above-mentioned edible vegetable oil degumming agent, in parts by weight, by silica 1~7 Part, 1~7 part of diatomite and 2~18 parts of oil cake mixing, both.
The present invention also provides a kind of refined oil methods characterized by comprising in parts by weight, by 100 Part crude oil and 0.5~10 part of degumming agent mixing, are stirred, filtering obtains refined oil；The degumming agent includes: silica, diatom Soil and oil cake.
Preferably, the crude oil is selected to the tea-seed oil of degumming process, rapeseed oil, peanut oil, maize germ oil, beans Any one in oil, autumn seed oil of sunflower, walnut oil, idesia oil and linseed oil.
Preferably, the temperature condition of the whipping process is 20~50 DEG C.
Preferably, the mixing speed of the whipping process is 30~120r/min.
Preferably, the mixing time of the whipping process is 5~30min.
Preferably, the filter process is secondary filtration.
Preferably, the secondary filtration specifically includes:
First order filtering: plate-frame filtering；
Second level filtering: vacuum filter.
Compared with prior art, detailed description are as follows by the application: the present invention provides edible vegetable oil degumming agent and its Preparation method, edible vegetable oil degumming agent use silica, diatomite and oil cake for raw material, and cost of material is low, reduce and use The refined oil method cost of edible vegetable oil degumming agent of the present invention, and then reduce edible vegetable oil production cost.
Edible vegetable oil degumming agent preparation method provided by the invention is simple, easy to use, de- using the edible vegetable oil Jelly adsorption capacity is strong, using the refined oil method that it is carried out, carries out degumming, degumming effect by physical adsorption way Fruit is good, and phosphatide removal rate has decolorizing effect, can improve grease color, and can retain plant incense oil up to 85% or more Gas.Further, it using the method for refining of edible vegetable oil degumming agent provided by the invention, without additional depickling, precipitation, does Dry, decoloration, deodorising step, edible vegetable oil degumming agent of the present invention and refined oil method of the present invention, it is economic, practical.
Edible vegetable oil degumming agent is mixed crude oil and degumming agent in refined oil method of the present invention, stirring is Realize degumming, decoloration, simple process, degumming effect is good, and phosphatide removal rate is up to 85% or more.Whipping process temperature condition is 20 ~50 DEG C, mixing time is 5~30min, is not necessarily to high temperature, and mixing time is short, and reducing degumming can time-consuming consumption.It was only needed after stirring The problem of filter, there is no wastewater treatments.
The present invention uses filter process for secondary filtration, sufficiently filters out degumming agent and adsorbate, promotes Vegetable Oil Quality.
Specific embodiment
It is right combined with specific embodiments below in order to make those skilled in the art more fully understand technical solution of the present invention The present invention is described in further detail.
Embodiment 1
Edible vegetable oil degumming agent component and proportion are shown in Table 1, wherein silica, diatomite and oil cake are commercially available production Product, part is in gram.
Table 1
The preparation method of above-mentioned edible vegetable oil degumming agent is mixed silica, diatomite and oil cake by the proportion of table 1, Both.
Embodiment 4
Refined oil method, comprising: degumming agent in crude oil and Examples 1 to 3 is mixed, is stirred, filtering obtains Refined oil；
Wherein,
The crude oil and degumming agent dosage are shown in Table 2, and part is in gram；
The whipping process, temperature condition be 20~50 DEG C, mixing speed be 30~120r/min, mixing time be 5~ 30min。
The filter process is secondary filtration, specifically: plate-frame filtering first order filtering: is carried out using flame filter press； Second level filtering: vacuum filter is carried out under the conditions of vacuum degree 0.05-0.09MPa.
Above-mentioned method of refining crude oil is commercial product, and through detecting, phosphorus content, color are shown in Table 2；The refining being prepared Oil, phosphorus content, color, smell, flavour are shown in Table 2；Above-mentioned method of refining phosphatide removal rate is shown in Table 2.
Table 2
The mode of applying is not construed as limitation of the present invention, and protection scope of the present invention should be with model defined by claim Subject to enclosing.For those skilled in the art, without departing from the spirit and scope of the present invention, it can also do Several improvements and modifications out, these modifications and embellishments should also be considered as the scope of protection of the present invention.

Claims (10)

1. a kind of edible vegetable oil degumming agent, which is characterized in that in parts by weight, the degumming agent includes: silica 1~7 Part, 1~7 part of diatomite and 2~18 parts of oil cake.
2. degumming agent according to claim 1, which is characterized in that in parts by weight, the degumming agent includes: silica 2 parts, 1 part of diatomite and 7 parts of oil cake.
3. the preparation method of any one of the claim 1~2 edible vegetable oil degumming agent, which is characterized in that in parts by weight, By silica 1~7 part, 1~7 part of diatomite and 2~18 parts of oil cake mixing, both.
4. a kind of refined oil method characterized by comprising in parts by weight, by 100 parts of crude oils and 0.5~10 Part degumming agent mixing, is stirred, and filtering obtains refined oil；The degumming agent includes: silica, diatomite and oil cake.
5. method of refining according to claim 4, which is characterized in that in parts by weight, the degumming agent includes: titanium dioxide 2 parts of silicon, 1 part of diatomite and 7 parts of oil cake.
6. method of refining according to claim 4, which is characterized in that the crude oil is selected from the tea seed to degumming process Any one in oil, rapeseed oil, peanut oil, maize germ oil, soya-bean oil, autumn seed oil of sunflower, walnut oil, idesia oil and linseed oil.
7. method of refining according to claim 4, which is characterized in that the temperature condition of the whipping process is 20~50 ℃。
8. method of refining according to claim 4, which is characterized in that the mixing speed of the whipping process be 30~ 120r/min。
9. method of refining according to claim 4, which is characterized in that the mixing time of the whipping process be 5~ 30min。
10. method of refining according to claim 4, which is characterized in that the filter process is secondary filtration.
Preferably, the secondary filtration specifically includes:
First order filtering: plate-frame filtering；
Second level filtering: vacuum filter.
CN201910382509.XA 2019-05-09 2019-05-09 Edible vegetable oil degumming agent and preparation method thereof and refined oil method Pending CN110016387A (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
CN201910382509.XA CN110016387A (en) 2019-05-09 2019-05-09 Edible vegetable oil degumming agent and preparation method thereof and refined oil method
PCT/CN2020/071071 WO2020224293A1 (en) 2019-05-09 2020-01-09 Edible vegetable oil degumming agent and preparation method therefor, and method for refining edible vegetable oil
AU2020239775A AU2020239775B2 (en) 2019-05-09 2020-01-09 Edible vegetable oil degumming agent and preparation method thereof and refining method of edible vegetable oil

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WO (1) WO2020224293A1 (en)

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CN110548480A (en) * 2019-10-14 2019-12-10 广汉市迈德乐食品有限公司 Degumming adsorbent for hot pot beef tallow and application thereof
CN110616113A (en) * 2019-10-14 2019-12-27 广汉市迈德乐食品有限公司 Non-foaming degumming process for beef tallow for chafing dish
WO2020224293A1 (en) * 2019-05-09 2020-11-12 四川省农业科学院农产品加工研究所 Edible vegetable oil degumming agent and preparation method therefor, and method for refining edible vegetable oil
CN115678674A (en) * 2022-10-31 2023-02-03 武汉轻工大学 Degumming rice bran crude oil and degumming method for refining rice bran oil by using adsorbent and composite phospholipase

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CN113088374A (en) * 2021-04-06 2021-07-09 四川省川海晨洋食品有限责任公司 Sesame oil extraction process with high oil yield and sesame oil prepared by same
CN113308296B (en) * 2021-06-08 2023-11-21 长沙中战茶油集团有限公司 Preparation method of direct drinking tea oil and tea oil

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WO2020224293A1 (en) * 2019-05-09 2020-11-12 四川省农业科学院农产品加工研究所 Edible vegetable oil degumming agent and preparation method therefor, and method for refining edible vegetable oil
CN110548480A (en) * 2019-10-14 2019-12-10 广汉市迈德乐食品有限公司 Degumming adsorbent for hot pot beef tallow and application thereof
CN110616113A (en) * 2019-10-14 2019-12-27 广汉市迈德乐食品有限公司 Non-foaming degumming process for beef tallow for chafing dish
CN115678674A (en) * 2022-10-31 2023-02-03 武汉轻工大学 Degumming rice bran crude oil and degumming method for refining rice bran oil by using adsorbent and composite phospholipase

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WO2020224293A1 (en) 2020-11-12
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