CN110007102A - A kind of liquid relief accurate quantification sampling device - Google Patents

A kind of liquid relief accurate quantification sampling device Download PDF

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Publication number
CN110007102A
CN110007102A CN201910261836.XA CN201910261836A CN110007102A CN 110007102 A CN110007102 A CN 110007102A CN 201910261836 A CN201910261836 A CN 201910261836A CN 110007102 A CN110007102 A CN 110007102A
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CN
China
Prior art keywords
intake passage
valve
liquid relief
sample intake
pump
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Pending
Application number
CN201910261836.XA
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Chinese (zh)
Inventor
刘红光
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Shenzhen Zhichuang Environmental Protection Technology Co Ltd
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Shenzhen Zhichuang Environmental Protection Technology Co Ltd
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Application filed by Shenzhen Zhichuang Environmental Protection Technology Co Ltd filed Critical Shenzhen Zhichuang Environmental Protection Technology Co Ltd
Priority to CN201910261836.XA priority Critical patent/CN110007102A/en
Publication of CN110007102A publication Critical patent/CN110007102A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N35/00Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor
    • G01N35/10Devices for transferring samples or any liquids to, in, or from, the analysis apparatus, e.g. suction devices, injection devices
    • G01N35/1009Characterised by arrangements for controlling the aspiration or dispense of liquids

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The invention discloses a kind of liquid relief accurate quantification sampling devices, pipette including having exhaust outlet and leakage fluid dram, the pump of energy positive and negative rotation, it is able to achieve the multichannel valve group of different liquids sample introduction, connect the connecting tube of pipette exhaust outlet and pump, the two-position three-way valve of connection resolution reactor and multichannel valve group, judge photoelectric detector whether drain, control the valve of draining switch, separator tube between pipette and pump, judge the photoelectric detector of exhaust outlet liquid on-off, and the control module of each module associated working of automation control, the convergent point for the multichannel valve group being connected with two-position three-way valve normal-closed end.

Description

A kind of liquid relief accurate quantification sampling device
Technical field
The present invention relates to liquid relief accurate quantification technical field, specially a kind of liquid relief accurate quantification sampling device.
Background technique
It combines, stablize and accurate liquid relief is quantitative in the automation that technique of analytical chemistry and instrument and meter combine Technical method and system, as the extension application of lab analysis, such as in-line analyzer.
Online analyzer does not all take this chemical laboratory pipette that is equal to operate sample introduction currently on the market Liquid relief quantitative sample injection method and system, traditional photoelectric metering are easy to be influenced by water sample turbidity, greasy dirt, crystallization and coloration, together When multiple-way valve be easy by itself dead volume and liquid leakage to be caused reagent contamination and error, Traditional photovoltaic metered rate is time-consuming slowly It is long, so that this input mode brings biggish inconvenience to product.
Summary of the invention
The purpose of the present invention is to provide a kind of liquid relief accurate quantification sampling devices, to solve to propose in above-mentioned background technique Problem.
To achieve the above object, the invention provides the following technical scheme:
A kind of liquid relief accurate quantification sampling device, pump, energy including pipette, energy positive and negative rotation with exhaust outlet and leakage fluid dram are real Multichannel valve group, the connecting tube of connection pipette exhaust outlet and pump, connection resolution reactor and the multi-pass of existing different liquids sample introduction The two-position three-way valve of road valve group, photoelectric detector whether judge drain, control draining switch valve, pipette and pump between Separator tube, judge the control mould of the photoelectric detector of exhaust outlet liquid on-off and automation control each module associated working The convergent point of block, the multichannel valve group being connected with two-position three-way valve normal-closed end.
Preferably, the multichannel valve group be communicated with the first sample intake passage, the second sample intake passage, third sample intake passage, 4th sample intake passage and the 5th sample intake passage.
The control module is connect with pump, detector, photoelectric detector, valve and two-position three-way valve respectively.
The output end of the pump is connect with separator tube.
First sample intake passage, the second sample intake passage, third sample intake passage, the 4th sample intake passage and the 5th sample intake passage It is connect with convergent point.
The input terminal of the output end of the photoelectric detector and detector connects, the output end of the detector and two three The signal end of port valve connects.
The output end of the photoelectric detector and the signal end of valve connect.
This liquid relief accurate quantification sample injection method and system are completed pair as the module or component part of in-line analyzer Water sample, amount mark, zero standard, pure water, reagent liquid relief sample introduction avoid cross contamination for the operation of chemical laboratory pipette, can be into Liquid relief rinse before row liquid relief sample introduction, can also carry out liquid relief cleaning operation, while can pass through water sample, amount mark and pure water or zero standard Different liquid relief number of injections ratios improve the live work of water quality online analyzer to realize to the different extension rates of water sample to be measured Condition adaptability improves the range ability of in-line analyzer.
Detailed description of the invention
Fig. 1 is positive structure schematic of the present invention;
In figure: 1- pipette, 2- pump, the first sample intake passage of 31-, the second sample intake passage of 32-, 33- third sample intake passage, 34- the Four sample intake passages, the 5th sample intake passage of 35-, 4- two-position three-way valve, 5- photoelectric detector, 6- valve, 7- control module, 8- buffering Pipe, 9- detector, 10- convergent point.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.
In the description of the present invention, it is to be understood that, term " on ", "lower", "front", "rear", "left", "right", "top", The orientation or positional relationship of the instructions such as "bottom", "inner", "outside" is to be based on the orientation or positional relationship shown in the drawings, merely to just In description the present invention and simplify description, rather than the device or element of indication or suggestion meaning must have a particular orientation, with Specific orientation construction and operation, therefore be not considered as limiting the invention.
Referring to Fig. 1, the present invention provides a kind of technical solution: a kind of liquid relief accurate quantification sampling device, including with row The pipette 1 of port and leakage fluid dram, the pump 2 of energy positive and negative rotation, the multichannel valve group for being able to achieve different liquids sample introduction, connection pipette The connecting tube of exhaust outlet and pump, the two-position three-way valve 4 of connection resolution reactor and multichannel valve group, photoelectricity whether judge drain Detector 5, the detection for controlling separator tube 8 between the valve 6 of draining switch, pipette and pump, judging exhaust outlet liquid on-off Device 9 and the control module 7 of automation control each module associated working, the multiple valve being connected with 4 normal-closed end of two-position three-way valve The convergent point 10 of group.
Multichannel valve group is communicated with the first sample intake passage 31, the second sample intake passage 32, third sample intake passage 33, the 4th sample introduction Channel 34 and the 5th sample intake passage 36.
Control module 7 is connect with pump 2, detector 9, photoelectric detector 5, valve 6 and two-position three-way valve 4 respectively.
The output end of pump 2 is connect with separator tube 8.
First sample intake passage 31, the second sample intake passage 32, third sample intake passage 33, the 4th sample intake passage 34 and the 5th sample introduction Channel 36 is connect with convergent point 10.
The output end of photoelectric detector 5 is connect with the input terminal of detector 9, the output end and two-position three-way valve 4 of detector 9 Signal end connection.
The output end of photoelectric detector 5 is connect with the signal end of valve 6
A kind of liquid relief rinse process of liquid relief accurate quantification sample injection method and system, liquid relief rinse operation are to extract respectively in two steps Quantitative, extraction drain, extracts and quantitatively passes through 7 control valve of control module by above-mentioned liquid relief accurate quantification sample injection method and system 6 open, and 4 normal-closed end of two-position three-way valve is opened, and close valve 6, and pump 2 rotates clockwise, and liquid will be passed through the by negative pressure absorbing One sample intake passage 31, the second sample intake passage 32, third sample intake passage 33, the 4th sample intake passage 34, the 5th sample intake passage 35, two Triple valve 4, into pipette, liquid flooding goes out pipette and will enter leakage fluid dram by gravity to be detected by photoelectric detector 5, i.e., It completes to extract quantification steps, extracts drain and opened by the way that the closing of multichannel valve group 3a valve is switched to valve 6 immediately, the second sample introduction is logical Road 32 connects air, and liquid continues overflow and goes out pipette and enter separator tube by detector 9, when detector 9 detects liquid After pipeline no liquid, while opening valve 6, pump 2 rotate clockwise, and liquid passes through separator tube 8, detector 9, photoelectric detector 5, valve Door 6 empties, and until detector 9, detector 9 can't detect liquid, stopping pump 2 is completed to extract drain step, realizes liquid relief Rinse operation.
The operation of liquid relief accurate quantification sampling device liquid relief sample introduction is to extract quantitative, liquid relief sample introduction respectively in two steps, and it is fixed to extract Amount controls 4 normal-closed end of two-position three-way valve by control module 7 by above-mentioned liquid relief accurate quantification sample injection method and system and opens, and closes Valve closing door 6, pump 2 rotate clockwise, and liquid will be by negative pressure absorbing by the first sample intake passage 31, the second sample intake passage 32, the Three sample intake passages 33, the 4th sample intake passage 34, the 5th sample intake passage 35, two-position three-way valve 4, into pipette, liquid flooding goes out Pipette will be entered leakage fluid dram by gravity and be detected by photoelectric detector 5, that is, complete to extract quantification steps, liquid relief sample introduction passes through Pump 2 is stopped immediately, while two-position three-way valve 4 is switched to normally open end connection, valve 6 is opened, by gravity by pipette liquid Body enters resolution reaction tank by normally open end to 4 common end of two-position three-way valve by 1 low side of pipette, i.e. completion liquid relief sample introduction step Suddenly, the accurate sample introduction operation of liquid relief is realized.
A kind of liquid relief cleaning process of liquid relief accurate quantification sample injection method and system, three steps of liquid relief cleaning operation point are respectively It extracts quantitative, extraction cleaning, extract drain, extraction quantitatively passes through control by above-mentioned liquid relief accurate quantification sample injection method and system 7 control valve 6(of module such as connects pure water) it opens, 4 normally open end of two-position three-way valve is opened, and valve 6 is closed, and pump 2 rotates clockwise, It extracts cleaning to continue to rotate clockwise by pump 2, photoelectric detector 5 detects, continues certain scavenging period, that is, completes to extract clear Step is washed, liquid continues overflow and goes out pipette and enter by photoelectric detector 5,4 normally open end of two-position three-way valve to common end slow Washing pipe, after photoelectric detector 5 detects liquid line no liquid, pump 2 is rotated counterclockwise, and liquid passes through separator tube 8, two three Port valve 4,1 exhaust outlet of pipette and photoelectric detector 5,1 leakage fluid dram of pipette and photoelectric detector 5, valve 6 empty, Zhi Daoguang Photodetector 5, photoelectric detector 5 can't detect liquid, stop pump 2, that is, complete to extract drain step, realize liquid relief cleaning behaviour Make, the scavenging period can set control.
The cloche of above-mentioned liquid relief accurate quantification sample injection method and the pipette 1 of system includes that exhaust outlet (is arranged on cloche Port passes through photoelectric detector 5), leakage fluid dram (under cloche leakage fluid dram pass through photoelectric detector 5), in vertical direction, drain Mouth is lower than exhaust outlet, and exhaust outlet is lower than the overflow top of pipette 1, and when pumping 2 main story clockwise, liquid overflows from pipette 1 The outflow of stream top will not be encountered at the top of cloche.When pump 2 continues to rotate forward clockwise, flowed out from the overflow top of pipette 1 Liquid due to 6 closing liquid of valve due to gravity fill up leakage fluid dram space can by the exhaust outlet of pipette 1, two-position three-way valve 4, The persistently discharge of separator tube 8, pump 2.When pump reversion counterclockwise, when valve 6 is opened, pass through two-position three-way valve 4 from the liquid of separator tube The overflow top of pipette 1 will not be entered but under process by entering cloche by 1 exhaust outlet of pipette and upper photoelectric detector 5 Photoelectric detector 5 enters leakage fluid dram, valve 6 is discharged.
Leakage fluid dram can also be used to realize discharge in the cleaning of the liquid relief of a kind of above-mentioned liquid relief accurate quantification sample injection method and system Waste liquid is cleaned, liquid relief cleaning operation is also that two steps are completed to be to extract quantitative, extraction drain, i.e., a kind of shifting respectively with liquid relief rinse Liquid accurate quantification sample injection method and the liquid relief cleaning operation of system pass through 7 control valve 6(of control module and such as connect pure water) it opens, 4 normally open end of two-position three-way valve is opened, and valve 6 is closed, and pump 2 rotates clockwise, and into pipette 1, liquid flooding goes out pipette 1 will Enter leakage fluid dram by gravity to be detected by photoelectric detector 5, that is, completes to extract quantification steps, liquid continues overflow and goes out pipette 1, then enter separator tube to common end by the exhaust outlet of pipette 1, by photoelectric detector 5,4 normally open end of two-position three-way valve 8, after photoelectric detector 5 detects liquid line no liquid, 3b valve, opening valve 6 are simultaneously closed off, pump 2 rotates counterclockwise, liquid From separator tube 8, two-position three-way valve 4, the exhaust outlet of pipette 1 and photoelectric detector 5, the leakage fluid dram of pipette 1 and Photoelectric Detection Device 5, valve 6 empty, and until photoelectric detector 5, photoelectric detector 5 can't detect liquid, stopping pump 2 is completed to extract drain Step realizes liquid relief cleaning operation.The liquid relief cleaning operation, which executes number, can set control wash number.
Liquid and valve 6 emptying that a kind of above-mentioned liquid relief accurate quantification sample injection method and the pump 2 of system empty clockwise The combinable collection of liquid and the collection that selectivity is carried out by two-position three-way valve, have reduced the generation for needing harmless treatment waste liquid Amount, the waste liquid that liquid relief rinse and liquid relief are cleaned merge collection part can direct emission environment, by the reagent waste liquid of liquid relief sample introduction Carry out harmless treatment is collected separately.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (7)

1. a kind of liquid relief accurate quantification sampling device, it is characterised in that: including with exhaust outlet and leakage fluid dram pipette (1), It can the pump (2) of positive and negative rotation, the multichannel valve group for being able to achieve different liquids sample introduction, connection pipette (1) exhaust outlet and the company for pumping (2) Adapter tube, the photoelectric detector (5) whether judge drain, is controlled the two-position three-way valve (4) of connection resolution reactor and multichannel valve group Separator tube (8) between the valve (6) of draining switch processed, pipette and pump (2), the detector for judging exhaust outlet liquid on-off (9) and the control module (7) of automation control each module associated working, the multi-pass that is connected with two-position three-way valve (4) normal-closed end The convergent point (10) of road valve group.
2. a kind of liquid relief accurate quantification sampling device according to claim 1, it is characterised in that: the multichannel valve group connects It is connected with the first sample intake passage (31), the second sample intake passage (32), third sample intake passage (33), the 4th sample intake passage (34) and the 5th Sample intake passage (36).
3. a kind of liquid relief accurate quantification sampling device according to claim 1, it is characterised in that: the control module (7) It is connect respectively with pump (2), detector (9), photoelectric detector (5), valve (6) and two-position three-way valve (4).
4. a kind of liquid relief accurate quantification sampling device according to claim 1, it is characterised in that: the output of the pump (2) End is connect with separator tube (8).
5. a kind of liquid relief accurate quantification sampling device according to claim 2, it is characterised in that: first sample intake passage (31), the second sample intake passage (32), third sample intake passage (33), the 4th sample intake passage (34) and the 5th sample intake passage (36) with Convergent point (10) connection.
6. a kind of liquid relief accurate quantification sampling device according to claim 1, it is characterised in that: the photoelectric detector (5) output end is connect with the input terminal of detector (9), the output end of the detector (9) and the signal of two-position three-way valve (4) End connection.
7. a kind of liquid relief accurate quantification sampling device according to claim 1, it is characterised in that: the photoelectric detector (5) output end is connect with the signal end of valve (6).
CN201910261836.XA 2019-04-02 2019-04-02 A kind of liquid relief accurate quantification sampling device Pending CN110007102A (en)

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Application Number Priority Date Filing Date Title
CN201910261836.XA CN110007102A (en) 2019-04-02 2019-04-02 A kind of liquid relief accurate quantification sampling device

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CN110007102A true CN110007102A (en) 2019-07-12

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111579733A (en) * 2020-05-26 2020-08-25 朱闪闪 Liquid transfer device for food detection
CN115427149A (en) * 2020-02-28 2022-12-02 珀金埃尔默健康科学有限公司 Multiplex polymerase chain reaction in a micropipette format

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Publication number Priority date Publication date Assignee Title
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