CN109988545A - A kind of electrolytic cell seal grease and its encapsulating method - Google Patents
A kind of electrolytic cell seal grease and its encapsulating method Download PDFInfo
- Publication number
- CN109988545A CN109988545A CN201910291126.1A CN201910291126A CN109988545A CN 109988545 A CN109988545 A CN 109988545A CN 201910291126 A CN201910291126 A CN 201910291126A CN 109988545 A CN109988545 A CN 109988545A
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- CN
- China
- Prior art keywords
- electrolytic cell
- grease
- vaseline
- vacuum grease
- current vacuum
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J191/00—Adhesives based on oils, fats or waxes; Adhesives based on derivatives thereof
- C09J191/06—Waxes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
- C09K3/10—Materials in mouldable or extrudable form for sealing or packing joints or covers
- C09K3/1006—Materials in mouldable or extrudable form for sealing or packing joints or covers characterised by the chemical nature of one of its constituents
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Sealing Material Composition (AREA)
Abstract
The invention discloses a kind of methods that trace moisture analyzer electrolytic cell is sealed with vacuum grease, belong to electrolytic cell field of sealing technology, which is mixed by current vacuum grease and vaseline according to the mass ratio of 5:1 with sealant.The electrolytic cell is mixed with seal grease by current vacuum grease and vaseline, current vacuum grease can be effectively prevented from, the status that failure is hardened occurs after a period of use, there is a situation where electrolytic cells and yin, yang electrode, dry column adhesion to take out when efficiently avoiding replacement electrolyte, keeps the replacement of electrolyte more convenient.
Description
Technical field
The invention belongs to electrolytic cell technical field of sealing technology, and in particular to a kind of electrolytic cell seal grease and its sealing side
Method.
Background technique
Micro-water analyzer is otherwise known as karl Fischer moisture teller, similar to have moisture teller, Moisture Meter, water
Divide meter, moisture detector, drimeter, moisture analyser.The electrolytic cell of trace water analyzer and two electrodes, two it is dry
Dry column junction is needed to be sealed using sealant fixed and prevents moisture content in air from entering.
Since Cattell electrolyte has a certain amount of trace acidic in the process of test in the electrolytic cell of micro-water analyzer
Gas generates, cause used in vacuum grease for a period of time after, can fail and harden, make yin, yang electrode, dry column and electrolytic cell
Adhesion is dead, can not take out, and the Cattell of failure can not be just also electrolysed to fluid exchange and the desiccant of dry column is replaced.
Summary of the invention
The purpose of the present invention is to provide a kind of electrolytic cell vacuum grease and its encapsulating methods, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the invention provides the following technical scheme:
A kind of electrolytic cell sealant, the vacuum grease are made of current sealant and vaseline.
Preferably, the preparation mass ratio of the current vacuum grease and vaseline is 5:1.
A kind of encapsulating method of electrolytic cell vacuum grease, including using vacuum grease as claimed in claim 2 to electrolysis
Pond is sealed, which is characterized in that this method comprises the following steps:
Deployed vacuum grease is set according to the current vacuum grease and vaseline of mass ratio 5:1 selection corresponding mass
Enter in agitating device and is uniformly mixed；
Uniformly mixed current sealant and vaseline are applied to the junction of electrode and dry column and electrolytic cell；
A circle is rotated after installation slightly, is uniformly distributed sealant in junction.
Preferably, the revolving speed of the agitating device is 120r/min-180r/min, and incorporation time is 5-10 minutes, temperature
It is 40-50 DEG C.
Compared with prior art, the beneficial effects of the present invention are:
The electrolytic cell is mixed with sealant by current sealant and vaseline, and it is dry can be effectively prevented from current sealant
It is dry to harden, efficiently avoid the feelings for electrolytic cell occurring when replacement electrolyte and yin, yang electrode, dry column adhesion can not take out
Condition keeps the replacement of electrolyte more convenient.
Specific embodiment
Below with reference to embodiment, the present invention will be further described.
The following examples are intended to illustrate the invention, but cannot be used to limit the scope of the invention.Item in embodiment
Part can be adjusted according to actual conditions are further, under concept thereof of the invention all to method simple modifications of the invention
Belong to the scope of protection of present invention.
Embodiment 1
A kind of electrolytic cell sealant, the sealant are made of current vacuum grease and vaseline；The current vacuum oil
The preparation mass ratio of rouge and vaseline is 5:1.
A kind of encapsulating method of electrolytic cell sealant, including using vacuum grease described in the present embodiment to electrolytic cell
It is sealed, this method comprises the following steps:
It, will according to the current vacuum grease and vaseline of mass ratio 5:1 selection corresponding mass, and at a temperature of 40-50 DEG C
Current vacuum grease and vaseline the merging revolving speed selected divides to mix 5-10 in the agitating device of 120r/min-180r/min
Clock is uniformly mixed current vacuum grease and vaseline；
Uniformly mixed current seal grease is applied to the junction of electrode and dry column and electrolytic cell；
A circle is rotated after installation slightly, is uniformly distributed deployed seal grease in junction.
Embodiment 2
A kind of electrolytic cell sealant, the sealant are made of current vacuum grease and vaseline；The current vacuum oil
The preparation mass ratio of rouge and vaseline is 5:1.
A kind of encapsulating method of electrolytic cell sealant, including using vacuum grease described in the present embodiment to electrolytic cell
It is sealed, this method comprises the following steps:
According to the current vacuum grease and vaseline of mass ratio 5:1 selection corresponding mass, and at 50 °C, will select
Current vacuum grease and vaseline merging revolving speed be 120r/min agitating device in mix 10 minutes, make current vacuum grease
It is uniformly mixed with vaseline；
Uniformly mixed current seal grease is applied to the junction of electrode and dry column and electrolytic cell；
A circle is rotated after installation slightly, is uniformly distributed deployed seal grease in junction.
Embodiment 3
A kind of electrolytic cell sealant, the sealant are made of current vacuum grease and vaseline；The current vacuum oil
The preparation mass ratio of rouge and vaseline is 5:1.
A kind of encapsulating method of electrolytic cell sealant, including using vacuum grease described in the present embodiment to electrolytic cell
It is sealed, this method comprises the following steps:
According to the current vacuum grease and vaseline of mass ratio 5:1 selection corresponding mass, and at a temperature of 40 DEG C, will select
Current vacuum grease and vaseline merging revolving speed be 180r/min agitating device in mix 5 minutes, make current vacuum grease
It is uniformly mixed with vaseline；
Uniformly mixed current seal grease is applied to the junction of electrode and dry column and electrolytic cell；
A circle is rotated after installation slightly, is uniformly distributed deployed seal grease in junction.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (4)
1. a kind of electrolytic cell seal grease, which is characterized in that the vacuum grease is made of current vacuum grease and vaseline.
2. sealant according to claim 1, which is characterized in that the preparation quality of the current vacuum grease and vaseline
Than for 5:1.
3. a kind of encapsulating method of electrolytic cell seal grease, including use sealant as claimed in claim 2 to electrolytic cell into
Row sealing, which is characterized in that this method comprises the following steps:
According to the current vacuum grease and vaseline of mass ratio 5:1 selection corresponding mass, it is placed into agitating device and is uniformly mixed；
Uniformly mixed current vacuum grease and vaseline are applied to the junction of electrode and dry column and electrolytic cell；
A circle is rotated after installation slightly, is uniformly distributed deployed vacuum grease in junction.
4. encapsulating method according to claim 3, which is characterized in that the revolving speed of the agitating device is 120r/min-
180r/min, incorporation time are 5-10 minutes, and temperature is 40-50 degree.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910291126.1A CN109988545B (en) | 2019-04-11 | 2019-04-11 | Sealing grease for electrolytic cell and sealing method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910291126.1A CN109988545B (en) | 2019-04-11 | 2019-04-11 | Sealing grease for electrolytic cell and sealing method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109988545A true CN109988545A (en) | 2019-07-09 |
| CN109988545B CN109988545B (en) | 2022-03-15 |
Family
ID=67133257
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910291126.1A Active CN109988545B (en) | 2019-04-11 | 2019-04-11 | Sealing grease for electrolytic cell and sealing method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN109988545B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112283348A (en) * | 2020-10-22 | 2021-01-29 | 陕西省计量科学研究院 | Standard conductivity solution sealing method for preventing carbon dioxide from dissolving in water |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL111782C (en) * | 1955-08-08 | |||
| DE3017297A1 (en) * | 1980-05-06 | 1981-11-12 | Dynamit Nobel Ag, 5210 Troisdorf | Barbed cap pushed on explosive cord end - with intermediate grease prevents water entering |
| CN105647466A (en) * | 2016-02-29 | 2016-06-08 | 中国石油化工股份有限公司 | Carbon battery sealing agent and preparation method thereof |
-
2019
- 2019-04-11 CN CN201910291126.1A patent/CN109988545B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL111782C (en) * | 1955-08-08 | |||
| DE3017297A1 (en) * | 1980-05-06 | 1981-11-12 | Dynamit Nobel Ag, 5210 Troisdorf | Barbed cap pushed on explosive cord end - with intermediate grease prevents water entering |
| CN105647466A (en) * | 2016-02-29 | 2016-06-08 | 中国石油化工股份有限公司 | Carbon battery sealing agent and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 许苗军，等: "《有机化学实验》", 31 July 2017, 中国农业大学出版社 * |
| 高清泽: "卡尔费休双通道微量水分测定仪构建技术研究", 《中国优秀博硕士学位论文全文数据库(硕士) 工程科技Ⅱ辑》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112283348A (en) * | 2020-10-22 | 2021-01-29 | 陕西省计量科学研究院 | Standard conductivity solution sealing method for preventing carbon dioxide from dissolving in water |
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| Publication number | Publication date |
|---|---|
| CN109988545B (en) | 2022-03-15 |
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