CN109967267A - A kind of efficient nano material centrifugal separation equipment - Google Patents
A kind of efficient nano material centrifugal separation equipment Download PDFInfo
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- CN109967267A CN109967267A CN201910307723.9A CN201910307723A CN109967267A CN 109967267 A CN109967267 A CN 109967267A CN 201910307723 A CN201910307723 A CN 201910307723A CN 109967267 A CN109967267 A CN 109967267A
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- fixed
- separating pipe
- fixed disk
- pipe
- corking
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04B—CENTRIFUGES
- B04B11/00—Feeding, charging, or discharging bowls
- B04B11/04—Periodical feeding or discharging; Control arrangements therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04B—CENTRIFUGES
- B04B13/00—Control arrangements specially designed for centrifuges; Programme control of centrifuges
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04B—CENTRIFUGES
- B04B5/00—Other centrifuges
- B04B5/04—Radial chamber apparatus for separating predominantly liquid mixtures, e.g. butyrometers
- B04B5/0407—Radial chamber apparatus for separating predominantly liquid mixtures, e.g. butyrometers for liquids contained in receptacles
- B04B5/0414—Radial chamber apparatus for separating predominantly liquid mixtures, e.g. butyrometers for liquids contained in receptacles comprising test tubes
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Abstract
The invention proposes a kind of efficient nano material centrifugal separation equipment, including apparatus casing, main support shaft is rotatably equipped in apparatus casing, main support shaft is equipped with bearing assembly；Bearing assembly includes upper fixed disk, lower fixed disk and separating pipe, and upper fixed disk is fixed in main support shaft, and uniformly distributed multiple upper mounted plates, upper mounted plate are hingedly fixed in fixed disk at the outer rim of upper fixed disk, and upper mounted plate is equipped with first through hole；Lower fixed disk is fixed on the lower section in main support shaft and being located at upper fixed disk, the open slot equipped with external opening corresponding with first through hole on lower fixed disk；A separating pipe is fixed on each upper mounted plate；Operation of the present invention is convenient, extracts and purification efficiency is high, can quick separating go out waste water and magnetic Nano material.
Description
Technical field
The present invention relates to a kind of separation equipment, in particular to a kind of efficient nano material centrifugal separation equipment.
Background technique
Magnetic Nano material (such as magnetic carbon nano-tube, magnetic graphene) is as a kind of novel adsorbent material, because of it
Unique physicochemical properties have rapidly become the hot spot of current research.Since it is with large specific surface area, adsorption capacity
Greatly, some surface functional groups and the advantages that hydrophobic surface, can the certain heavy metal ion of strong adsorption and organic compound, in recent years
Researchers or directly using magnetic Nano material as adsorbent or as study on the carrier its to useless Organic substance in water and nothing
The absorption of machine object and isolation of purified.
Commonly used in being based on magnetic Nano material to used in useless Organic substance in water and inorganic matter absorption and isolation of purified
Case is known as centrifuge tube.Centrifuge tube is a kind of tubulose sample container, can with closure or gland.Conventional centrifugal separating pipe
Disadvantage is: being suitable for extensive liquid-liquid extraction and matrix solid phase dispersion, does not have specific aim for magnetic material, causes based on magnetic
The extraction advantage of property nano material does not protrude, cumbersome.
Summary of the invention
The present invention proposes a kind of efficient nano material centrifugal separation equipment regarding to the issue above, easy to operate, extracts
With purification efficiency height, can quick separating go out waste water and magnetic Nano material.
Specific technical solution is as follows:
A kind of efficient nano material centrifugal separation equipment, including apparatus casing are rotatably equipped with master in apparatus casing
Support shaft, main support shaft are equipped with bearing assembly；
Bearing assembly includes upper fixed disk, lower fixed disk and separating pipe, and upper fixed disk is fixed in main support shaft, upper fixation
Uniformly distributed multiple upper mounted plates, upper mounted plate are hingedly fixed in fixed disk at the outer rim of disk, and it is logical that upper mounted plate is equipped with first
Hole；Lower fixed disk is fixed in main support shaft and is located at the lower section of upper fixed disk, corresponding with first through hole on lower fixed disk to set
There is the open slot of external opening；
A separating pipe is fixed on each upper mounted plate；Separating pipe includes upper tube body, lower tube body and end cap, and upper tube body is under
It is connected between tube body by fastener, end cap is fixed on upper tube body, and the bottom of lower tube body is equipped with discharge nozzle, discharging
Pipe is equipped with solenoid valve；Upper tube body is equipped with the first limit pressure ring, and separating pipe passes through corresponding one group of first through hole and opening
Slot is fixed by screws in the first limit pressure ring on upper mounted plate, makes separating pipe can be in the hinge point of upper mounted plate
The heart is swung；
What is be connected in end cap with separating pipe is equipped with first passage, and the top of first passage is equipped with second channel, and first is logical
The aperture in road is greater than the aperture of second channel, is equipped with corking component in first passage, and corking component includes lower limit ring and corking,
Lower limit ring is fixed on the inner wall of first passage, uniformly distributed multiple first guiding between lower limit ring and the top of first passage
Bar, corking are segment-shaped structure, corresponding with the first guide rod in corking to be equipped with multiple first connecting rods, first connecting rod can on
Lower movement is set on the first guide rod, and sheathed spring on the first guide rod, spring is pressed on first connecting rod and lower limit
Between ring；
When spring in a free state, corking is pressed on the bottom of second channel, is in close state end cap；
The top of main support shaft passes through apparatus casing and is connected with the output shaft of variable speed electric motors, particularly, and variable speed electric motors, particularly drives carrying group
Part is rotated；
The top of apparatus casing is equipped with feeding assembly, and feeding assembly includes charging support frame, and charging support frame is moveable
The top of apparatus casing is set, feed support frame bottom it is corresponding with separating pipe be equipped with multiple feed pipes, feed pipe into
Material opening is arranged on the side wall of feed pipe, and charging support frame is moved up and down by first hydraulic cylinder promotion；
After first hydraulic cylinder pushes feed pipe insertion second channel, feed pipe pushes corking to move down, thus by liquid
In material injection separating pipe, after the completion of charging, mobile charging support frame is moved up, feed pipe is removed into second channel, corking
It resets under the action of the spring；
The bottom of apparatus casing is equipped with absorbent module, and absorbent module includes the absorption ring of multiple arc-shaped structures, adsorbs ring
Inner sidewall on fitting fix one layer of first permanent magnet, the bottom for adsorbing ring is rotatably fixed on the bottom of apparatus casing, more
A absorption ring is pushed to inward slant setting by second hydraulic cylinder, and the outside that multiple absorption collar are wound on separating pipe forms annulus
Shape structure；It adsorbs and is rotatably equipped with multiple rubber balls on the inner sidewall of ring；
Uniformly distributed multiple fixed brackets of the inside of separating pipe circumferentially shape, inclined fixed third is hydraulic on fixed bracket
Cylinder, the push rod of third hydraulic cylinder are equipped with push plate, and third hydraulic cylinder is correspondingly arranged, for pushing separating pipe holding to incline with separating pipe
Ramp-like state；
Be equipped with a circle collecting tank between absorbent module and fixed bracket, collecting tank be used to collect be discharged in discharge nozzle it is useless
Liquid.
Further, it is hingedly fixed in fixed disk at the top of upper mounted plate, the bottom of upper mounted plate and upper fixed disk
Equipped with one group of second permanent magnet, the contact jaw polarity of the second permanent magnet is opposite.
Further, openable and closable on the side wall of apparatus casing to be equipped with door-plate.
Further, the control method of centrifugal separation equipment is as follows:
(1) upper mounted plate is horizontally disposed, and corresponding one group of second permanent magnet mutually adsorbs, and separating pipe is in vertical shape
State；
(2) charging support frame is moved up and down by first hydraulic cylinder promotion；When first hydraulic cylinder pushes feed pipe to insert
After entering second channel, feed pipe pushes corking to move down, to liquid material be injected in separating pipe, after the completion of charging, upwards
Mobile charging support frame, removes second channel for feed pipe, corking resets under the action of the spring；
(3) variable speed electric motors, particularly drives bearing assembly to be rotated, and separating pipe is made to be inclined outwardly setting；
(4) outside that multiple absorption collar are wound on separating pipe forms cirque structure, i.e., limits to separating pipe, and logical
The first electromagnet is crossed to assist absorption magnetic Nano material；
(5) after the completion of separating, variable speed electric motors, particularly stops operating, separating pipe is made to go to original position, and third Hydraulic Cylinder is corresponding
Separating pipe keeps heeling condition, opens discharge nozzle, waste liquid is drained into collecting tank；
(6) lower tube body is openable, individually handles the magnetic Nano material isolated after taking-up.
The invention has the benefit that
Operation of the present invention is convenient, extracts and purification efficiency is high, can quick separating go out waste water and magnetic Nano material.
Detailed description of the invention
Fig. 1 is feed state cross-sectional view of the present invention.
Fig. 2 is discrete state cross-sectional view of the present invention.
Fig. 3 is part A enlarged drawing in Fig. 1.
Specific embodiment
It is clear to be more clear technical solution of the present invention, below the present invention is described further, any pair of sheet
The technical characteristic of inventive technique scheme carries out the scheme that equivalencing is obtained with conventional reasoning and each falls within the scope of the present invention.
Appended drawing reference
Apparatus casing 1, main support shaft 2, upper fixed disk 3, lower fixed disk 4, separating pipe 5, upper mounted plate 6, first through hole 7,
Open slot 8, upper tube body 9, lower tube body 10, end cap 11, discharge nozzle 12, solenoid valve 13, first limit pressure ring 14, first passage 16,
Second channel 17, lower limit ring 18, corking 19, the first guide rod 20, first connecting rod 21, spring 22, variable speed electric motors, particularly 23, charging
Support frame 24, feed pipe 25, feed openings 26, first hydraulic cylinder 27, absorption ring 28, the first permanent magnet 29, second hydraulic cylinder 30,
Rubber ball 31, fixed bracket 32, third hydraulic cylinder 33, collecting tank 34, the second permanent magnet 35, door-plate 36.
A kind of efficient nano material centrifugal separation equipment as shown in the figure, including apparatus casing 1 can be rotated in apparatus casing
Be equipped with main support shaft 2, main support shaft be equipped with bearing assembly；
Bearing assembly includes upper fixed disk 3, lower fixed disk 4 and separating pipe 5, and upper fixed disk is fixed in main support shaft, on
Uniformly distributed multiple upper mounted plates 6 at the outer rim of fixed disk, upper mounted plate is hingedly fixed in fixed disk, and upper mounted plate is equipped with the
One through-hole 7；Lower fixed disk is fixed in main support shaft and is located at the lower section of upper fixed disk, on lower fixed disk with first through hole pair
The open slot 8 equipped with external opening answered；
A separating pipe is fixed on each upper mounted plate；Separating pipe includes upper tube body 9, lower tube body 10 and end cap 11, upper tube
It is connected between body and lower tube body by fastener, end cap is fixed on upper tube body, and the bottom of lower tube body is equipped with discharging
Pipe 12, discharge nozzle are equipped with solenoid valve 13；Upper tube body is equipped with the first limit pressure ring 14, and separating pipe passes through corresponding one group the
One through-hole and open slot are fixed by screws in the first limit pressure ring on upper mounted plate, make separating pipe can be with upper mounted plate
It is swung centered on hinge point；
What is be connected in end cap with separating pipe is equipped with first passage 16, and the top of first passage is equipped with second channel 17, the
The aperture in one channel is greater than the aperture of second channel, is equipped with corking component in first passage, corking component includes lower limit ring 18
With corking 19, lower limit ring is fixed on the inner wall of first passage, uniformly distributed multiple between lower limit ring and the top of first passage
First guide rod 20, corking are segment-shaped structure, corresponding with the first guide rod in corking to be equipped with multiple first connecting rods 21, the
One connecting rod is moving up and down to be set on the first guide rod, and sheathed spring 22 on the first guide rod, spring is pressed on first
Between connecting rod and lower limit ring；
When spring in a free state, corking is pressed on the bottom of second channel, is in close state end cap；
The top of main support shaft passes through apparatus casing and is connected with the output shaft of variable speed electric motors, particularly 23, and variable speed electric motors, particularly drives carrying
Component is rotated；
The top of apparatus casing is equipped with feeding assembly, and feeding assembly includes the charging support frame 24 of cirque structure, charging
Support frame is movably disposed at the top of apparatus casing, and the bottom for feeding support frame is corresponding with separating pipe equipped with multiple chargings
The feed openings 26 of pipe 25, feed pipe are arranged on the side wall of feed pipe, charging support frame by first hydraulic cylinder 27 push into
Row moves up and down；
After first hydraulic cylinder pushes feed pipe insertion second channel, feed pipe pushes corking to move down, thus by liquid
In material injection separating pipe, after the completion of charging, mobile charging support frame is moved up, feed pipe is removed into second channel, corking
It resets under the action of the spring；
The bottom of apparatus casing is equipped with absorbent module, and absorbent module includes the absorption ring 28 of multiple arc-shaped structures, absorption
One layer of first permanent magnet 29 is fixed in fitting on the inner sidewall of ring, and the bottom for adsorbing ring is rotatably fixed on the bottom of apparatus casing
Portion, multiple absorption rings are pushed to inward slant setting by second hydraulic cylinder 30, and multiple absorption collar are wound on the outside of separating pipe
Form cirque structure；It adsorbs and is rotatably equipped with multiple rubber balls 31 on the inner sidewall of ring；
Uniformly distributed multiple fixed brackets 32 of the inside of separating pipe circumferentially shape, inclined fixed third is hydraulic on fixed bracket
The push rod of cylinder 33, third hydraulic cylinder is equipped with push plate, and third hydraulic cylinder is correspondingly arranged, for pushing separating pipe to keep with separating pipe
Heeling condition；
Be equipped with a circle collecting tank 34 between absorbent module and fixed bracket, collecting tank be used to collect be discharged in discharge nozzle it is useless
Liquid.
Further, it is hingedly fixed in fixed disk at the top of upper mounted plate, the bottom of upper mounted plate and upper fixed disk
Equipped with one group of second permanent magnet 35, the contact jaw polarity of the second permanent magnet is opposite.
Further, openable and closable on the side wall of apparatus casing to be equipped with door-plate 36.
Further, the control method of centrifugal separation equipment is as follows:
(1) upper mounted plate is horizontally disposed, and corresponding one group of second permanent magnet mutually adsorbs, and separating pipe is in vertical shape
State；
(2) charging support frame is moved up and down by first hydraulic cylinder promotion；When first hydraulic cylinder pushes feed pipe to insert
After entering second channel, feed pipe pushes corking to move down, to liquid material be injected in separating pipe, after the completion of charging, upwards
Mobile charging support frame, removes second channel for feed pipe, corking resets under the action of the spring；
(3) variable speed electric motors, particularly drives bearing assembly to be rotated, and separating pipe is made to be inclined outwardly setting；
(4) outside that multiple absorption collar are wound on separating pipe forms cirque structure, i.e., limits to separating pipe, and logical
The first electromagnet is crossed to assist absorption magnetic Nano material；
(5) after the completion of separating, variable speed electric motors, particularly stops operating, separating pipe is made to go to original position, and third Hydraulic Cylinder is corresponding
Separating pipe keeps heeling condition, opens discharge nozzle, waste liquid is drained into collecting tank；
(6) lower tube body is openable, individually handles the magnetic Nano material isolated after taking-up.
Claims (4)
1. a kind of efficient nano material centrifugal separation equipment, it is characterized in that, including apparatus casing is rotatable in apparatus casing
Equipped with main support shaft, main support shaft is equipped with bearing assembly；
Bearing assembly includes upper fixed disk, lower fixed disk and separating pipe, and upper fixed disk is fixed in main support shaft, upper fixed disk
Uniformly distributed multiple upper mounted plates, upper mounted plate are hingedly fixed in fixed disk at outer rim, and upper mounted plate is equipped with first through hole；Under
Fixed disk is fixed in main support shaft and is located at the lower section of upper fixed disk, on lower fixed disk it is corresponding with first through hole be equipped with it is outer
The open slot of portion's opening；
A separating pipe is fixed on each upper mounted plate；Separating pipe includes upper tube body, lower tube body and end cap, upper tube body and lower tube body
Between connected by fastener, end cap is fixed on upper tube body, and the bottom of lower tube body is equipped with discharge nozzle, on discharge nozzle
Equipped with solenoid valve；Upper tube body is equipped with the first limit pressure ring, and separating pipe passes through corresponding one group of first through hole and open slot, makes
First limit pressure ring is fixed by screws on upper mounted plate, carry out separating pipe can centered on the hinge point of upper mounted plate
It swings；
What is be connected in end cap with separating pipe is equipped with first passage, and the top of first passage is equipped with second channel, first passage
Aperture is greater than the aperture of second channel, is equipped with corking component in first passage, corking component includes lower limit ring and corking, lower limit
Position ring is fixed on the inner wall of first passage, uniformly distributed multiple first guide rods, plug between lower limit ring and the top of first passage
Lid is segment-shaped structure, corresponding with the first guide rod in corking to be equipped with multiple first connecting rods, first connecting rod can on move down
Dynamic is set on the first guide rod, sheathed spring on the first guide rod, spring be pressed on first connecting rod and lower limit ring it
Between；
When spring in a free state, corking is pressed on the bottom of second channel, is in close state end cap；
The top of main support shaft pass through apparatus casing be connected with the output shaft of variable speed electric motors, particularly, variable speed electric motors, particularly drive bearing assembly into
Row rotation；
The top of apparatus casing is equipped with feeding assembly, and feeding assembly includes charging support frame, and charging support frame is movably arranged
At the top of apparatus casing, the bottom for feeding support frame is corresponding with separating pipe equipped with multiple feed pipes, and the charging of feed pipe is opened
Mouth is arranged on the side wall of feed pipe, and charging support frame is moved up and down by first hydraulic cylinder promotion；
After first hydraulic cylinder pushes feed pipe insertion second channel, feed pipe pushes corking to move down, so that liquid material be infused
Enter in separating pipe, after the completion of charging, moves up mobile charging support frame, feed pipe is removed into second channel, corking is in bullet
It is resetted under the action of spring；
The bottom of apparatus casing is equipped with absorbent module, and absorbent module includes the absorption ring of multiple arc-shaped structures, adsorbs the interior of ring
One layer of first permanent magnet is fixed in fitting on side wall, and the bottom for adsorbing ring is rotatably fixed on the bottom of apparatus casing, multiple suctions
Follower ring is pushed to inward slant setting by second hydraulic cylinder, and the outside that multiple absorption collar are wound on separating pipe forms circular ring shape knot
Structure；It adsorbs and is rotatably equipped with multiple rubber balls on the inner sidewall of ring；
Uniformly distributed multiple fixed brackets of the inside of separating pipe circumferentially shape, inclined fixed third hydraulic cylinder on fixed bracket, the
The push rod of three hydraulic cylinders is equipped with push plate, and third hydraulic cylinder is correspondingly arranged, for pushing separating pipe to keep skewed with separating pipe
State；
A circle collecting tank is equipped between absorbent module and fixed bracket, collecting tank is for collecting the waste liquid being discharged in discharge nozzle.
2. a kind of efficient nano material centrifugal separation equipment as described in claim 1, it is characterized in that, the top of upper mounted plate
It is hingedly fixed in fixed disk, the bottom of upper mounted plate and upper fixed disk is equipped with one group of second permanent magnet, the second permanent magnet
Contact jaw polarity is opposite.
3. a kind of efficient nano material centrifugal separation equipment as described in claim 1, it is characterized in that, the side wall of apparatus casing
It is upper openable and closable equipped with door-plate.
4. a kind of efficient nano material centrifugal separation equipment as claimed in claim 2, it is characterized in that, centrifugal separation equipment
Control method is as follows:
(1) upper mounted plate is horizontally disposed, and corresponding one group of second permanent magnet mutually adsorbs, and separating pipe is in a vertical state；
(2) charging support frame is moved up and down by first hydraulic cylinder promotion；When first hydraulic cylinder pushes feed pipe insertion the
Behind two channels, feed pipe pushes corking to move down, so that liquid material be injected in separating pipe, after the completion of charging, moves up
Mobile charging support frame, removes second channel for feed pipe, corking resets under the action of the spring；
(3) variable speed electric motors, particularly drives bearing assembly to be rotated, and separating pipe is made to be inclined outwardly setting；
(4) outside that multiple absorption collar are wound on separating pipe forms cirque structures, i.e., limits to separating pipe, further through the
One electromagnet come assist absorption magnetic Nano material；
(5) after the completion of separating, variable speed electric motors, particularly stops operating, separating pipe is made to go to original position, and third Hydraulic Cylinder separates accordingly
Pipe keeps heeling condition, opens discharge nozzle, waste liquid is drained into collecting tank；
(6) lower tube body is openable, individually handles the magnetic Nano material isolated after taking-up.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910307723.9A CN109967267B (en) | 2019-04-17 | 2019-04-17 | Efficient nano-material centrifugal separation equipment |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910307723.9A CN109967267B (en) | 2019-04-17 | 2019-04-17 | Efficient nano-material centrifugal separation equipment |
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| Publication Number | Publication Date |
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| CN109967267A true CN109967267A (en) | 2019-07-05 |
| CN109967267B CN109967267B (en) | 2020-09-25 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114887779A (en) * | 2022-06-21 | 2022-08-12 | 武汉科拜生物科技有限公司 | High-speed centrifugal equipment is used in biochemical purification |
| CN115029226A (en) * | 2022-08-12 | 2022-09-09 | 北京汉氏联合生物技术股份有限公司 | Intelligent device for culturing immune cells on large scale |
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| US4341343A (en) * | 1980-09-22 | 1982-07-27 | Stuart Beckman | Magnetically driven centrifuge system |
| JPS5810653A (en) * | 1981-07-13 | 1983-01-21 | Hitachi Koki Co Ltd | Centrifuge for cleaning blood corpuscle |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114887779A (en) * | 2022-06-21 | 2022-08-12 | 武汉科拜生物科技有限公司 | High-speed centrifugal equipment is used in biochemical purification |
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| CN115029226A (en) * | 2022-08-12 | 2022-09-09 | 北京汉氏联合生物技术股份有限公司 | Intelligent device for culturing immune cells on large scale |
| CN115029226B (en) * | 2022-08-12 | 2022-12-13 | 北京汉氏联合生物技术股份有限公司 | Intelligent culture apparatus of immune cell scale |
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| CN109967267B (en) | 2020-09-25 |
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