CN109938334A - A kind of compound tabletting prescription of deer whip and preparation method thereof - Google Patents
A kind of compound tabletting prescription of deer whip and preparation method thereof Download PDFInfo
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- CN109938334A CN109938334A CN201910264523.XA CN201910264523A CN109938334A CN 109938334 A CN109938334 A CN 109938334A CN 201910264523 A CN201910264523 A CN 201910264523A CN 109938334 A CN109938334 A CN 109938334A
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Abstract
The present invention relates to compound tabletting prescriptions of a kind of deer whip and preparation method thereof.The compound tabletting prescription of deer whip includes the raw material of following parts by weight: 35~45 parts of Penis et testis cervi extract, 25~35 parts of pizzle, 20~30 parts of mulberries, 20~30 parts of fructus lycii, 15~25 parts of dateplum persimmon, 20~30 parts of cortex cinnamomi, 20~30 parts of oyster, 25~35 parts of raspberry, 35~45 parts of sweet potato, 35~45 parts of Gorgon fruit and 20~30 parts of rhizoma polygonati.The compound tabletting prescription each component material combination science of the deer whip, acts on mutually collaboration, and tonifying kidney and strengthening yang while can also improve the complication such as frequent micturition, hair be few, and absorb rapid.The preparation method only needs dry, granulation, tabletting after mixing each raw material, and simple process, controllability is strong, is conducive to large-scale production.
Description
Technical field
The invention belongs to field of health care products, and in particular to a kind of compound tabletting prescription of deer whip and preparation method thereof.
Background technique
With the increase of modern life pressure, often there are the symptoms such as the soreness of waist, backache, tinnitus, body sleepiness in middle-aged male, right
The harmony of family inevitably causes unstable.
The patent of invention of Publication No. CN103284138A discloses a kind of formula for making deer whip cream, the group of affiliated formula
Point and each component weight percent are as follows: deer whip 0.3~0.8%, pilose antler 0.2~0.4%, deer's sinew 8~15%, deer bone 20~
30%, the water of deerskin 7~14%, sugar 0.4~0.8% and remaining content.The deer whip cream, which has, significantly to be kept fit and healthy, nourishes
The effect of kidney yang.However, type of feed used in preparation deer whip cream is single, deer itself is only derived from, it is incomplete in effect
Still there is limitation in face.
Summary of the invention
Of the existing technology in order to solve the problems, such as, the present invention provides a kind of compound tabletting prescription of deer whip and its preparation sides
Method.The compound tabletting prescription each component material combination science of the deer whip, acts on mutually collaboration, and tonifying kidney and strengthening yang while can also improve
Frequent micturition sends out the complication such as few, and absorbs rapid.The preparation method only needs drying after mixing each raw material, granulation, tabletting i.e.
Can, simple process, controllability is strong, is conducive to large-scale production.
The solution of the present invention is to provide a kind of compound tabletting prescription of deer whip, the raw material including following parts by weight: deer whip extracts
35~45 parts of object, 25~35 parts of pizzle, 20~30 parts of mulberries, 20~30 parts of fructus lycii, 15~25 parts of dateplum persimmon, cortex cinnamomi 20~30
Part, 20~30 parts of oyster, 25~35 parts of raspberry, 35~45 parts of sweet potato, 35~45 parts of Gorgon fruit and 20~30 parts of rhizoma polygonati.
Preferably, the compound tabletting prescription of the deer whip includes the raw material of following parts by weight: 40 parts of Penis et testis cervi extract, pizzle 30
Part, 25 parts of mulberries, 25 parts of fructus lycii, 20 parts of dateplum persimmon, 25 parts of cortex cinnamomi, 25 parts of oyster, 30 parts of raspberry, 40 parts of sweet potato, Gorgon fruit 40
Part and 25 parts of rhizoma polygonati.
Preferably, the preparation method of the Penis et testis cervi extract includes the following steps:
(1) it is added to the water together after crushing deer whip with neutral proteinase, adjusts pH and temperature, carries out enzyme digestion reaction, it is complete
A filter residue and first-time filtrate are filtered to obtain after finishing；
(2) filter residue obtained by step (1) is mixed to progress refluxing extraction with isopropanol, after filter to obtain secondary filter residue
With secondary filtrate；
(3) secondary filter residue obtained by step (2) mix into progress refluxing extraction with acetic acid aqueous solution, after obtain filter residue three times
Filtrate three times；
(4) merge first-time filtrate, secondary filtrate and filtrate obtains amalgamation liquid three times, obtain deer whip after amalgamation liquid is concentrated, is evaporated
Extract.
Preferably, in step (1), the weight ratio of the deer whip, neutral proteinase and water is 1:0.01~0.03:6~10.
Preferably, in step (1), the pH of the adjusting is 6.8~7.0, and temperature is 45~50 DEG C；The enzyme digestion reaction time 4
~6h.
Preferably, in step (2), the weight ratio of a filter residue and isopropanol is 1:3~5；The refluxing extraction
Temperature is 78~80 DEG C, and the time of refluxing extraction is 2~3h.
Preferably, in step (3), the acetic acid aqueous solution concentration is 60~70%；The secondary filter residue and acetic acid are water-soluble
The weight ratio of liquid is 1:5~7；The temperature of the refluxing extraction is 92~96 DEG C, and the time of refluxing extraction is 1~2h.
Preferably, described to be concentrated into the 20~30% of amalgamation liquid volume in step (4).
Preferably, in step (4), the evaporated temperature is 40~60 DEG C.
The present invention also provides a kind of preparation methods of the compound tabletting prescription of deer whip, in 60~80 DEG C of conditions after raw material is mixed
Lower drying, then through wet granulation, rotary tablet press is to get the compound tabletting of deer whip.In preparation process can also according to demand,
Candy taste is made in tabletting, to improve mouthfeel.
It is of the invention for ease of understanding, raw materials used effect is illustrated:
Deer whip: it is sweet in flavor, salty, it is warm-natured；Return liver, kidney, bladder meridian；There is the effect of kidney tonifying essence, shape kidney yang, strengthening the essence, strong waist and knee.
Pizzle: taste is salty, warm-natured；Return kidney channel；Has effects that tonifying kidney and strengthening yang.
Mulberries: sweet in flavor, sour, cold in nature, return heart, liver and kidney channel；Have effects that liver-kidney tonifying, fluid dryness, UFA eyesight.
Fructus lycii: it is sweet in flavor, it is mild-natured；Return liver and kidney channel；Have effects that nourshing kidney, moistening lung, tonifying liver, improving eyesight.
Dateplum persimmon: it is sweet in flavor, puckery, it is cool in nature；Return heart, lung, stomach meridian have effects that tonifying middle-Jiao and Qi, nourishing stomach and spleen, the strong mind of blood-nourishing.
Cortex cinnamomi: acrid flavour, sweet, extremely hot in nature；Return kidney, spleen, the heart, Liver Channel；With mends fire supporing yang, guiding fire to origin, eliminating cold to stop pain, temperature
The effect of qualcomm meridian.
Oyster: taste is salty, cool in nature；Return liver and kidney channel；Function with calming the liver, transquilization with heavy material, resolving hard lump, astringency inducing
Effect.
Raspberry: it is sweet in flavor, sour, it is warm-natured；Return liver, kidney, bladder meridian；With supplementing the kidney to control the nocturnal reducing urination, the effect of nourishing the liver to improve visual acuity.
Sweet potato: it is sweet in flavor, it is mild-natured；Returns spleen, stomach, large intestine channel；With tonifying spleen benefit stomach, defaecation, nourishing generate fluid, moistening lung laxation function
Effect.
Gorgon fruit: it is sweet in flavor, puckery, it is mild-natured；Returns spleen, kidney channel；Have effects that supplementing the kidney to control the nocturnal, tonifying spleen and stopping diarrhea, eliminating dampness and arresting leucorrhea.
Rhizoma polygonati: it is sweet in flavor, it is mild-natured；Returns spleen, lung, kidney channel；Have effects that boosting qi and nourishing yin, invigorating the spleen, moistening lung, kidney-nourishing.
The invention has the benefit that
1, the compound tabletting prescription of deer whip of the present invention, contains plurality of active ingredients, in which: according to " mending shape with shape "
Thought takes and is formulated based on deer whip and pizzle, fundamentally solves the problems, such as function of male deficiency；Chinese medicine thinks " kidney " for this
Source, then be equipped with can supplementing the kidney to control the nocturnal, the fructus lycii of tonifying kidney and strengthening yang, cortex cinnamomi, oyster and Gorgon fruit, can in medical treatment treat soreness and weakness of waist and knees, hold
The symptoms such as long power difference, it is self-confident to regenerate male；Situations such as in view of kidney deficiency gas weak person frequent micturition that may be present, hair less, spy's addition tool
There are astringent sperm contracting urine, the raspberry of blackening and generating hair effect and mulberries, the symptom that enuresis nocturna is various, dried and withered hair is dark yellow can be improved；It is last auxiliary
With can nourishing the stomach, the dateplum persimmon of invigorating the spleen, sweet potato and rhizoma polygonati, the absorption of effective component can be promoted.In conclusion each component raw material is matched
5 science, act on mutually collaboration, and tonifying kidney and strengthening yang while can also improve the complication such as frequent micturition, hair be few, and absorb rapid.
2, the preparation method of the compound tabletting prescription of deer whip of the present invention, it is only necessary to dry after mixing each raw material, granulation,
Tabletting, simple process, controllability is strong, is conducive to large-scale production.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, technical solution of the present invention will be carried out below
Detailed description.Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Base
Embodiment in the present invention, those of ordinary skill in the art are obtained all without making creative work
Other embodiment belongs to the range that the present invention is protected.
Embodiment 1
The present embodiment provides a kind of preparation methods of the compound tabletting prescription of deer whip, include the following steps:
(I) Penis et testis cervi extract is prepared, is included the following steps:
(1) will deer whip crush after be added to the water together with serine protease, the deer whip, serine protease and water
Weight ratio is 1:0.01:10, adjust pH to 6.8, temperature to 50 DEG C, carry out enzyme digestion reaction 4h, after filter to obtain a filter residue
And first-time filtrate；
(2) filter residue obtained by step (1) is mixed with isopropanol by the weight ratio of 1:3, is returned under the conditions of 78 DEG C
Stream extract 3h, after filter to obtain secondary filter residue and secondary filtrate；
(3) secondary filter residue obtained by step (2) is mixed with 60% acetic acid aqueous solution by the weight ratio of 1:7, in 92 DEG C of conditions
Lower progress refluxing extraction 2h, after filter residue and three times filtrate three times；
(4) merge first-time filtrate, secondary filtrate and filtrate obtains amalgamation liquid three times, amalgamation liquid is concentrated into original volume
20%, and be slowly evaporated under the conditions of 40 DEG C to get Penis et testis cervi extract.
(II) the compound tabletting of deer whip, method are prepared are as follows:
By Penis et testis cervi extract, 35g pizzle obtained by 35g step (I), 20g mulberries, 20g fructus lycii, 15g dateplum persimmon, 30g cortex cinnamomi,
It is dry under the conditions of 60 DEG C after 20g oyster, 35g raspberry, 35g sweet potato, 45g Gorgon fruit and the mixing of 20g rhizoma polygonati, then through wet process system
Grain, rotary tablet press is to get the compound tabletting of deer whip.
Embodiment 2
The present embodiment provides a kind of preparation methods of the compound tabletting prescription of deer whip, include the following steps:
(I) Penis et testis cervi extract is prepared, is included the following steps:
(1) will deer whip crush after be added to the water together with aspartic protease, the deer whip, aspartic protease and
The weight ratio of water be 1:0.03:6, adjust pH to 7.0, temperature to 45 DEG C, carry out enzyme digestion reaction 6h, after filter once to filter
Slag and first-time filtrate；
(2) filter residue obtained by step (1) is mixed with isopropanol by the weight ratio of 1:5, is returned under the conditions of 80 DEG C
Stream extract 2h, after filter to obtain secondary filter residue and secondary filtrate；
(3) secondary filter residue obtained by step (2) is mixed with 70% acetic acid aqueous solution by the weight ratio of 1:5, in 96 DEG C of conditions
Lower progress refluxing extraction 1h, after filter residue and three times filtrate three times；
(4) merge first-time filtrate, secondary filtrate and filtrate obtains amalgamation liquid three times, amalgamation liquid is concentrated into original volume
30%, and be slowly evaporated under the conditions of 60 DEG C to get Penis et testis cervi extract.
(II) the compound tabletting of deer whip, method are prepared are as follows:
By Penis et testis cervi extract, 25g pizzle obtained by 45g step (I), 30g mulberries, 20g fructus lycii, 25g dateplum persimmon, 20g cortex cinnamomi,
It is dry under the conditions of 80 DEG C after 30g oyster, 25g raspberry, 45g sweet potato, 35g Gorgon fruit and the mixing of 30g rhizoma polygonati, then through wet process system
Grain, rotary tablet press is to get the compound tabletting of deer whip.
Embodiment 3
The present embodiment provides a kind of preparation methods of the compound tabletting prescription of deer whip, include the following steps:
(I) Penis et testis cervi extract is prepared, is included the following steps:
(1) will deer whip crush after be added to the water together with serine protease, the deer whip, serine protease and water
Weight ratio is 1:0.02:8, adjusts pH to 6.9, and temperature carries out enzyme digestion reaction 5h to 48 DEG C, after filter filter residue and
First-time filtrate；
(2) filter residue obtained by step (1) is mixed with isopropanol by the weight ratio of 1:4, is returned under the conditions of 79 DEG C
Stream extract 2.5h, after filter to obtain secondary filter residue and secondary filtrate；
(3) secondary filter residue obtained by step (2) is mixed with 65% acetic acid aqueous solution by the weight ratio of 1:6, in 94 DEG C of conditions
Lower progress refluxing extraction 1.5h, after filter residue and three times filtrate three times；
(4) merge first-time filtrate, secondary filtrate and filtrate obtains amalgamation liquid three times, amalgamation liquid is concentrated into original volume
25%, and be slowly evaporated under the conditions of 50 DEG C to get Penis et testis cervi extract.
(II) the compound tabletting of deer whip, method are prepared are as follows:
By Penis et testis cervi extract, 30g pizzle obtained by 40g step (I), 25g mulberries, 25g fructus lycii, 20g dateplum persimmon, 25g cortex cinnamomi,
It is dry under the conditions of 70 DEG C after 25g oyster, 30g raspberry, 40g sweet potato, 40g Gorgon fruit and the mixing of 25g rhizoma polygonati, then through wet process system
Grain, rotary tablet press is to get the compound tabletting of deer whip.
For the effect for showing the compound tabletting prescription of deer whip of the present invention, following typical case is chosen to illustrate:
Case 1:
Lee, male, 37 years old；Previously the normal soreness of waist, backache, even companion's tinnitus, function of male decline Mr. Li, no erection phenomenon；
The compound tabletting of deer whip described in the embodiment of the present invention 3 is taken afterwards, is taken before sleeping daily once, every time 4~6g, after 3 months, Li Xian
Life is had a pain in the back and tinnitus symptom substantially eliminates, and love life restores harmonious, and follow-up half a year, Li Xiansheng symptom does not recur.
Case 2:
Sun, male, 45 years old；Mr. Sun gets up in the night to urinate number 3~4 times at previous night, it is serious to lead to insomnia, and private prosecution tooth slightly has
It loosens；The compound tabletting of deer whip described in the embodiment of the present invention 1 is taken afterwards, is taken before sleeping daily once, every time 4~6g, 2 months
Afterwards, Sun Xiansheng number of getting up in the night to urinate is reduced to 1 time, and sleep quality greatly improves, and after 4 months, tooth mobility phenomenon is also obviously improved.
Case 3
Zhang, male, 27 years old；Mr. Zhang is due to great work intensity, and in poor health, night wakes up finds to have night sweat existing often
As personal bedding all wet is saturating when serious；The compound tabletting of deer whip described in the embodiment of the present invention 2 is taken afterwards, takes one before sleeping daily
Secondary, 3~5g every time, 1 after half a month, and Mr. Zhang's night sweat phenomenon is obviously improved, and does not recur after follow-up 2 months.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any
Those familiar with the art in the technical scope disclosed by the present invention, can easily think of the change or the replacement, and should all contain
Lid is within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.
Claims (10)
1. a kind of compound tabletting prescription of deer whip, which is characterized in that the raw material including following parts by weight: Penis et testis cervi extract 35~45
Part, 25~35 parts of pizzle, 20~30 parts of mulberries, 20~30 parts of fructus lycii, 15~25 parts of dateplum persimmon, 20~30 parts of cortex cinnamomi, oyster 20
~30 parts, 25~35 parts of raspberry, 35~45 parts of sweet potato, 35~45 parts of Gorgon fruit and 20~30 parts of rhizoma polygonati.
2. the compound tabletting prescription of deer whip according to claim 1, which is characterized in that the raw material including following parts by weight: deer
40 parts of whip extract, 30 parts of pizzle, 25 parts of mulberries, 25 parts of fructus lycii, 20 parts of dateplum persimmon, 25 parts of cortex cinnamomi, 25 parts of oyster, raspberry 30
Part, 40 parts of sweet potato, 40 parts of Gorgon fruit and 25 parts of rhizoma polygonati.
3. the compound tabletting prescription of deer whip according to claim 1 or 2, which is characterized in that the preparation of the Penis et testis cervi extract
Method includes the following steps:
(1) it is added to the water together after crushing deer whip with neutral proteinase, adjusts pH and temperature, carries out enzyme digestion reaction, after
Filter to obtain a filter residue and first-time filtrate；
(2) filter residue obtained by step (1) is mixed to progress refluxing extraction with isopropanol, after filter to obtain secondary filter residue and two
Secondary filtrate；
(3) secondary filter residue obtained by step (2) mix into progress refluxing extraction with acetic acid aqueous solution, after obtain filter residue and three three times
Secondary filtrate；
(4) merge first-time filtrate, secondary filtrate and filtrate obtains amalgamation liquid three times, obtain deer whip after amalgamation liquid is concentrated, is evaporated and extract
Object.
4. the compound tabletting prescription of deer whip according to claim 3, which is characterized in that in step (1), the deer whip, neutrality
The weight ratio of protease and water is 1:0.01~0.03:6~10.
5. the compound tabletting prescription of deer whip according to claim 3, which is characterized in that in step (1), the pH of the adjusting is
6.8~7.0, temperature is 45~50 DEG C；4~6h of enzyme digestion reaction time.
6. the compound tabletting prescription of deer whip according to claim 3, which is characterized in that in step (2), a filter residue with
The weight ratio of isopropanol is 1:3~5；The temperature of the refluxing extraction is 78~80 DEG C, and the time of refluxing extraction is 2~3h.
7. the compound tabletting prescription of deer whip according to claim 3, which is characterized in that in step (3), the acetic acid aqueous solution
Concentration is 60~70%；The weight ratio of the secondary filter residue and acetic acid aqueous solution is 1:5~7；The temperature of the refluxing extraction is
92~96 DEG C, the time of refluxing extraction is 1~2h.
8. the compound tabletting prescription of deer whip according to claim 3, which is characterized in that described to be concentrated into merging in step (4)
The 20~30% of liquid product.
9. the compound tabletting prescription of deer whip according to claim 3, which is characterized in that in step (4), the evaporated temperature is
40~60 DEG C.
10. the preparation method of any one of the claim 1~9 compound tabletting prescription of deer whip, which is characterized in that mix raw material
Dry afterwards, granulation, tabletting to obtain the final product.
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| CN201910264523.XA CN109938334A (en) | 2019-04-03 | 2019-04-03 | A kind of compound tabletting prescription of deer whip and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111012857A (en) * | 2019-12-17 | 2020-04-17 | 抚州市东乡区志方梅花鹿养殖有限公司 | Deer penis cream and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111012857A (en) * | 2019-12-17 | 2020-04-17 | 抚州市东乡区志方梅花鹿养殖有限公司 | Deer penis cream and preparation method thereof |
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Application publication date: 20190628 |