CN109880410A - The manufacture craft and its formula of a kind of entirety immersion type waterproof material through walls - Google Patents
The manufacture craft and its formula of a kind of entirety immersion type waterproof material through walls Download PDFInfo
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- CN109880410A CN109880410A CN201910197761.3A CN201910197761A CN109880410A CN 109880410 A CN109880410 A CN 109880410A CN 201910197761 A CN201910197761 A CN 201910197761A CN 109880410 A CN109880410 A CN 109880410A
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Abstract
The invention discloses the manufacture crafts and its formula of a kind of whole immersion type waterproof material through walls, raw material including following weight proportion: 0.02-0.04 parts of alkyl benzene sulphonate, 0.02-0.05 parts of nonylphenol polyoxyethylene ether, 15-20 parts of sodium silicate aqueous solution, 4-7 parts of potassium methyl silicate, 2.2-2.8 parts of tartaric acid, 1.8-2.2 parts of sodium carbonate, 0.1-0.2 parts of isopropanol, 68-75 parts of deionized water, and provide a kind of manufacture craft of whole immersion type waterproof material through walls, waterproof material through walls made from formula of the invention is without organic volatile, it is nontoxic, it is non-ignitable, there is no corrosivity, belong to safety, ep-type material, upstream face back side can be done, resistance to compression is impervious, inside concrete can be penetrated into, there is penetration capacity, it can be used for the construction of conventional waterproof material Secondary repairing after failure, can be used for house ornamentation such as toilet warterproof, and effect is higher than market and exempts to pound brick, slip casting AB solidification glue, structural strength that is easy to operate and will not destroying wall, and waterproof effect is more long.
Description
Technical field
The present invention relates to waterproof material technical field more particularly to a kind of production works of whole immersion type waterproof material through walls
Skill and its formula.
Background technique
Architectural waterproof material is the important component of functional materials for building, and in construction, waterproof material is being built
The surface of object forms integral waterproofing layer, and to reach waterproof or enhance the ability of anti-leakage, therefore, quality and application effect are direct
Be related to the effect structure and service life of architectural engineering, therefore, develop waterproof material solve seepage in buildings at
For current problem to be solved.
On the market existing waterproofing agent of organosilicon, exempt to pound the purposes of the waterproofing agents such as brick, forever lime set all than wide, can be used for
Exempt from the waterproofs such as waterproof, external wall waterproof, roof waterproof, underground project waterproof, basement tunnel water proofing, garage waterproof of laying bricks in toilet
Engineering, and be applied to all kinds of waterproofing agents of buildings waterproof at present and more or less all exist with base adhesive intensity difference, penetration performance is poor,
The problems such as environmental-protecting performance is bad, therefore, waterproof material in the prior art are not ideal, are not still able to satisfy wanting of using
It asks, proposes the manufacture craft and its formula of a kind of whole immersion type waterproof material through walls thus.
Summary of the invention
The purpose of the present invention is to solve prior art waterproofing agent and base adhesive intensity difference, penetration performance is poor, ring
The disadvantages of guaranteed cost is bad, and the manufacture craft and its formula of a kind of whole immersion type waterproof material through walls proposed.
To achieve the goals above, present invention employs following technical solutions:
The manufacture craft and its formula for designing a kind of whole immersion type waterproof material through walls, by the raw material of following weight proportion
It is made: 0.02-0.04 parts of alkyl benzene sulphonate, 0.02-0.05 parts of nonylphenol polyoxyethylene ether, 15-20 parts of sodium silicate aqueous solution, first
4-7 parts of base potassium silicate, 2.2-2.8 parts of tartaric acid, 1.8-2.2 parts of sodium carbonate, 0.1-0.2 parts of isopropanol, deionized water 68-75
Part.
Preferably, it is made of the raw material of following weight proportion: 0.02 part of alkyl benzene sulphonate, nonylphenol polyoxyethylene ether 0.02
Part, 15 parts of sodium silicate aqueous solution, 4 parts of potassium methyl silicate, 2.2 parts of tartaric acid, 1.8 parts of sodium carbonate, 0.1 part of isopropanol, deionization
68 parts of water.
Preferably, it is made of the raw material of following weight proportion: 0.04 part of alkyl benzene sulphonate, nonylphenol polyoxyethylene ether 0.05
Part, 20 parts of sodium silicate aqueous solution, 7 parts of potassium methyl silicate, 2.8 parts of tartaric acid, 2.2 parts of sodium carbonate, 0.2 part of isopropanol, deionization
75 parts of water.
Preferably, it is made: being made of the raw material of following weight proportion: alkyl benzene sulphonate of the raw material of following weight proportion
0.03 part, 0.035 part of nonylphenol polyoxyethylene ether, 17.5 parts of sodium silicate aqueous solution, 5.5 parts of potassium methyl silicate, tartaric acid 2.5
Part, 2 parts of sodium carbonate, 0.15 part of isopropanol, 71.5 parts of deionized water.
The present invention also provides a kind of manufacture crafts of whole immersion type waterproof material through walls, include the following steps:
1) it weighs a certain amount of deionized water according to formula ratio to be added in reaction kettle, under the mixing speed of 150-200r/min
It is slowly added to nonylphenol polyoxyethylene ether and persistently stirs 5-10min, be then slowly added into alkyl benzene sulphonate and at the uniform velocity stir 10-
15min, is then slowly added into isopropanol and to stir 10-15min under the mixing speed of 50-100r/min, after being cooled to room temperature,
Stand for standby use；
2) it weighs a certain amount of deionized water according to formula ratio to be added in reaction kettle, under the mixing speed of 150-200r/min
It is slowly added to sodium silicate aqueous solution and persistently stirs 10-15min, then, solution made from step 1 is added and with 50-100r/
10-15min is stirred under the mixing speed of min, mixed solution is made；
3) it weighs a certain amount of deionized water according to formula ratio to be added in reaction kettle, under the mixing speed of 500-600r/min
Equivalent is alternately added tartaric acid and sodium carbonate in two times, is kept stirring 10-15min after being added every time, and step 2) system is then added
Mixed solution and to stir 10-15min under the mixing speed of 50-100r/min, finally, be added potassium methyl silicate stirring
10-15min stands 1h.
Preferably, the step 1), 2) mass ratio with 3) addition deionized water are 3:1:2.
The manufacture craft and its formula of a kind of whole immersion type proposed by the present invention waterproof material through walls, beneficial effect exist
In:
1. waterproof material through walls made from formula of the invention, no organic volatile is nontoxic, non-ignitable, without corrosivity, belongs to
In safe and environment-friendly profile material, upstream face back side can be done, and resistance to compression is impervious, can penetrate into inside concrete, there is penetration capacity,
Secondary repairing after can be used for the construction failure of conventional waterproof material, in addition, can be used for house ornamentation such as toilet warterproof, effect is higher than city
Field exempts to pound brick, slip casting AB solidification glue, and will not destroy the structural strength of wall, and waterproof maintains effect up to 20 years or so.
2. the manufacture craft in the present invention, organic active medium solution is first made, then with sodium silicate aqueous solution is added
Deionized water solution is mixed to prepare mixed solution, finally, by the deionized water solution that tartaric acid and sodium carbonate is added with mix it is molten
Liquid is stirring evenly and then adding into potassium methyl silicate and stirs evenly, and is conducive to that component uniformly waterproof material through walls is made, wherein silicic acid
Sodium and tartaric acid constitute active constituent, penetrate into concrete structure internal void, the silicate with inside concrete
It learns reaction and forms crystalline solid not soluble in water, potassium methyl silicate forms one layer of hydrophobic film in concrete surface after curing and reaches anti-
Water effect.
Specific embodiment
It is clearly and completely described below in conjunction with the technical solution in the embodiment of the present invention, it is clear that described reality
Applying example is only a part of the embodiment of the present invention, instead of all the embodiments.
Embodiment 1
A kind of formula of entirety immersion type waterproof material through walls, is made: alkyl benzene sulphonate of the raw material of following weight proportion
0.02 part, 0.02 part of nonylphenol polyoxyethylene ether, 15 parts of sodium silicate aqueous solution, 4 parts of potassium methyl silicate, 2.2 parts of tartaric acid, carbonic acid
1.8 parts of sodium, 0.1 part of isopropanol, 68 parts of deionized water.
A kind of manufacture craft of entirety immersion type waterproof material through walls, includes the following steps:
1) it weighs a certain amount of deionized water according to formula ratio to be added in reaction kettle, under the mixing speed of 150r/min slowly
Nonylphenol polyoxyethylene ether is added and persistently stirs 5min, is then slowly added into alkyl benzene sulphonate and at the uniform velocity stirs 10min, then slowly
Isopropanol and to stir 10min under the mixing speed of 50r/min, after being cooled to room temperature, stand for standby use is added；
2) it weighs a certain amount of deionized water according to formula ratio to be added in reaction kettle, under the mixing speed of 150r/min slowly
Sodium silicate aqueous solution is added and persistently stirs 10min, then, solution made from step 1 is added and with the stirring of 50r/min speed
Degree is lower to stir 10min, and mixed solution is made；
3) a certain amount of deionized water is weighed according to formula ratio to be added in reaction kettle, be divided to two under the mixing speed of 500r/min
Secondary equivalent is alternately added tartaric acid and sodium carbonate, is kept stirring 10min after being added every time, and step 2) mixing obtained is then added
Solution and to stir 10min under the mixing speed of 50r/min stands 1h finally, potassium methyl silicate, which is added, stirs 10min.
Wherein, step 1), 2) mass ratio with 3) addition deionized water are 3:1:2.
Embodiment 2
A kind of formula of entirety immersion type waterproof material through walls, is made: alkyl benzene sulphonate of the raw material of following weight proportion
0.04 part, 0.05 part of nonylphenol polyoxyethylene ether, 20 parts of sodium silicate aqueous solution, 7 parts of potassium methyl silicate, 2.8 parts of tartaric acid, carbonic acid
2.2 parts of sodium, 0.2 part of isopropanol, 75 parts of deionized water.
A kind of manufacture craft of entirety immersion type waterproof material through walls, includes the following steps:
1) it weighs a certain amount of deionized water according to formula ratio to be added in reaction kettle, under the mixing speed of 150r/min slowly
Nonylphenol polyoxyethylene ether is added and persistently stirs 5min, is then slowly added into alkyl benzene sulphonate and at the uniform velocity stirs 10min, then slowly
Isopropanol and to stir 10min under the mixing speed of 50r/min, after being cooled to room temperature, stand for standby use is added；
2) it weighs a certain amount of deionized water according to formula ratio to be added in reaction kettle, under the mixing speed of 150r/min slowly
Sodium silicate aqueous solution is added and persistently stirs 10min, then, solution made from step 1 is added and with the stirring of 50r/min speed
Degree is lower to stir 10min, and mixed solution is made；
3) a certain amount of deionized water is weighed according to formula ratio to be added in reaction kettle, be divided to two under the mixing speed of 500r/min
Secondary equivalent is alternately added tartaric acid and sodium carbonate, is kept stirring 10min after being added every time, and step 2) mixing obtained is then added
Solution and to stir 10min under the mixing speed of 50r/min stands 1h finally, potassium methyl silicate, which is added, stirs 10min.
Wherein, step 1), 2) mass ratio with 3) addition deionized water are 3:1:2.
Embodiment 3
A kind of formula of entirety immersion type waterproof material through walls, is made: alkyl benzene sulphonate of the raw material of following weight proportion
0.03 part, 0.035 part of nonylphenol polyoxyethylene ether, 17.5 parts of sodium silicate aqueous solution, 5.5 parts of potassium methyl silicate, tartaric acid 2.5
Part, 2 parts of sodium carbonate, 0.15 part of isopropanol, 71.5 parts of deionized water.
A kind of manufacture craft of entirety immersion type waterproof material through walls, includes the following steps:
1) it weighs a certain amount of deionized water according to formula ratio to be added in reaction kettle, under the mixing speed of 200r/min slowly
Nonylphenol polyoxyethylene ether is added and persistently stirs 10min, is then slowly added into alkyl benzene sulphonate and at the uniform velocity stirs 15min, then delay
It is slow isopropanol to be added and to stir 15min under the mixing speed of 100r/min, after being cooled to room temperature, stand for standby use；
2) it weighs a certain amount of deionized water according to formula ratio to be added in reaction kettle, under the mixing speed of 200r/min slowly
Sodium silicate aqueous solution is added and persistently stirs 15min, then, solution made from step 1 is added and with the stirring of 100r/min speed
Degree is lower to stir 15min, and mixed solution is made；
3) a certain amount of deionized water is weighed according to formula ratio to be added in reaction kettle, be divided to two under the mixing speed of 600r/min
Secondary equivalent is alternately added tartaric acid and sodium carbonate, is kept stirring 15min after being added every time, and step 2) mixing obtained is then added
Solution and to stir 15min under the mixing speed of 100r/min, finally, potassium methyl silicate, which is added, stirs 15min, standing 1h is
It can.
Wherein, step 1), 2) mass ratio with 3) addition deionized water are 3:1:2.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (6)
1. a kind of formula of entirety immersion type waterproof material through walls, it is characterised in that: the entirety immersion type waterproof material through walls by
The raw material of following weight proportion is made: 0.02-0.04 parts of alkyl benzene sulphonate, 0.02-0.05 parts of nonylphenol polyoxyethylene ether, silicic acid
15-20 parts of sodium water solution, 4-7 parts of potassium methyl silicate, 2.2-2.8 parts of tartaric acid, 1.8-2.2 parts of sodium carbonate, isopropanol 0.1-0.2
Part, 68-75 parts of deionized water.
2. a kind of formula of whole immersion type according to claim 1 waterproof material through walls, it is characterised in that: by weighing as follows
The raw material of amount proportion is made: 0.02 part of alkyl benzene sulphonate, 0.02 part of nonylphenol polyoxyethylene ether, 15 parts of sodium silicate aqueous solution, first
4 parts of base potassium silicate, 2.2 parts of tartaric acid, 1.8 parts of sodium carbonate, 0.1 part of isopropanol, 68 parts of deionized water.
3. a kind of formula of whole immersion type according to claim 1 waterproof material through walls, it is characterised in that: by weighing as follows
The raw material of amount proportion is made: 0.04 part of alkyl benzene sulphonate, 0.05 part of nonylphenol polyoxyethylene ether, 20 parts of sodium silicate aqueous solution, first
7 parts of base potassium silicate, 2.8 parts of tartaric acid, 2.2 parts of sodium carbonate, 0.2 part of isopropanol, 75 parts of deionized water.
4. a kind of formula of whole immersion type according to claim 1 waterproof material through walls, it is characterised in that: by weighing as follows
Amount proportion raw material be made: 0.03 part of alkyl benzene sulphonate, 0.035 part of nonylphenol polyoxyethylene ether, 17.5 parts of sodium silicate aqueous solution,
5.5 parts of potassium methyl silicate, 2.5 parts of tartaric acid, 2 parts of sodium carbonate, 0.15 part of isopropanol, 71.5 parts of deionized water.
5. a kind of manufacture craft of entirety immersion type waterproof material through walls, characterized by the following steps:
1) it weighs a certain amount of deionized water according to formula ratio to be added in reaction kettle, under the mixing speed of 150-200r/min slowly
Nonylphenol polyoxyethylene ether is added and persistently stirs 5-10min, is then slowly added into alkyl benzene sulphonate and at the uniform velocity stirs 10-15min, so
It is slowly added to isopropanol and afterwards to stir 10-15min under the mixing speed of 50-100r/min, after being cooled to room temperature, stands standby
With；
2) it weighs a certain amount of deionized water according to formula ratio to be added in reaction kettle, under the mixing speed of 150-200r/min slowly
Sodium silicate aqueous solution is added and persistently stirs 10-15min, then, solution made from step 1 is added and with 50-100r/min's
10-15min is stirred under mixing speed, mixed solution is made；
3) a certain amount of deionized water is weighed according to formula ratio to be added in reaction kettle, be divided to two under the mixing speed of 500-600r/min
Secondary equivalent is alternately added tartaric acid and sodium carbonate, is kept stirring 10-15min after being added every time, and it is obtained that step 2) is then added
Mixed solution and to stir 10-15min under the mixing speed of 50-100r/min, finally, potassium methyl silicate, which is added, stirs 10-
15min stands 1h.
6. a kind of manufacture craft of whole immersion type according to claim 5 waterproof material through walls, it is characterised in that: described
Step 1), 2) mass ratio with 3) addition deionized water are 3:1:2.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910197761.3A CN109880410A (en) | 2019-03-15 | 2019-03-15 | The manufacture craft and its formula of a kind of entirety immersion type waterproof material through walls |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910197761.3A CN109880410A (en) | 2019-03-15 | 2019-03-15 | The manufacture craft and its formula of a kind of entirety immersion type waterproof material through walls |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101671154A (en) * | 2009-10-15 | 2010-03-17 | 上海交通大学 | Water-borne permeable crystalline waterproofing material and preparation method thereof |
| CN102557726A (en) * | 2011-12-27 | 2012-07-11 | 华南理工大学 | High-permeability multi-effect concrete water-proofing agent and preparation method thereof |
| KR101337376B1 (en) * | 2012-04-17 | 2013-12-05 | 주식회사 제이에스기술 | The penetrating waterproof agent and manufacturing method thereof |
| CN104130605A (en) * | 2013-12-12 | 2014-11-05 | 中国建筑第四工程局有限公司 | Hydrophobic capillary crystalline waterproof agent and preparation method thereof |
-
2019
- 2019-03-15 CN CN201910197761.3A patent/CN109880410A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101671154A (en) * | 2009-10-15 | 2010-03-17 | 上海交通大学 | Water-borne permeable crystalline waterproofing material and preparation method thereof |
| CN102557726A (en) * | 2011-12-27 | 2012-07-11 | 华南理工大学 | High-permeability multi-effect concrete water-proofing agent and preparation method thereof |
| KR101337376B1 (en) * | 2012-04-17 | 2013-12-05 | 주식회사 제이에스기술 | The penetrating waterproof agent and manufacturing method thereof |
| CN104130605A (en) * | 2013-12-12 | 2014-11-05 | 中国建筑第四工程局有限公司 | Hydrophobic capillary crystalline waterproof agent and preparation method thereof |
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Application publication date: 20190614 |