CN109868187A - A kind of production technology of rose - Google Patents
A kind of production technology of rose Download PDFInfo
- Publication number
- CN109868187A CN109868187A CN201711249688.7A CN201711249688A CN109868187A CN 109868187 A CN109868187 A CN 109868187A CN 201711249688 A CN201711249688 A CN 201711249688A CN 109868187 A CN109868187 A CN 109868187A
- Authority
- CN
- China
- Prior art keywords
- rose
- distillation
- oil
- water
- condensation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Medicines Containing Plant Substances (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention proposes a kind of production technologies of rose, comprising the following steps: the pre-selection of raw material；Pretreatment of raw material: the roseleaf after will be selected, which is put into salt water, to be impregnated, and places 10-30min；Heating distillation: soaked roseleaf is placed into distilling apparatus, under conditions of temperature is 40-50 DEG C, distilling apparatus internal pressure is 400-500MPa, distills 20-30min；Condensation fractionation；Water-oil separating: water-oil separating processing is carried out to distillate, rose will be floated on and separated with the essential oil on its upper layer, primary rose is obtained；Distillation water outlet: it carries out distillation fractionation processing again to primary rose, obtains purification rose.This method uses pure natural processing gimmick, rose purity is high obtained, and other chemical components are not contained, it ensure that the nutrition of rose, it is sterilized in process, ensure that the clean of rose, take the mode of second distillation, rose is purified, rose quality obtained is higher.
Description
Technical field
The invention belongs to rose flower processing technique fields, and in particular to a kind of production technology of rose.
Background technique
Rose is a kind of valuable ingredients of traditional Chinese medicine, sweet and slightly bitter taste, warm-natured.Rose is extracted by rose low temperature drying
It arrives, has effects that regulating the flow of vital energy and dispeling melancholy, promoting blood circulation scattered silt and menstruction regulating and pain relieving.Rose contained energy is lower, is rich in citronellol, flores aurantii
More aroma volatiles such as alcohol, geraniol, benzyl carbinol, Charming fragrance, the consumer group is wide, meets the development of Modern drinks health
Trend.
With being constantly progressive for science and technology, at present when processing rose production rose, often add
Certain additive, to guarantee in process, rose reduces ingredient and volatilizees, the concentration of Lai Tigao rose, but
This processing method can make to guarantee in rose containing other chemical components the concentration of rose simultaneously, but also at
It is point impure, other negative effects can be brought in use.
Summary of the invention
It is an object of the invention to: it can be added during processing rose for the prior art set forth above
The problem of adding agent and then influencing rose purity, the present invention provides a kind of production technology of rose.
The technical solution adopted by the invention is as follows:
A kind of production technology of rose, comprising the following steps:
(1) pre-selection of raw material: at the rose florescence using artificial picking rose, selected full roseleaf；
(2) pretreatment of raw material: the roseleaf after will be selected, which is put into salt water, to be impregnated, and places 10-30min；
(3) heating distillation: soaked roseleaf is placed into distilling apparatus, is 40-50 DEG C, is distilled dress in temperature
Internal pressure is set to distill 20-30min under conditions of 400-500MPa；
(4) condensation fractionation: the mixed gas of rose and steam that distillation is generated carries out condensation process, is distillated
Liquid；
(5) water-oil separating: carrying out water-oil separating processing to distillate, will float on the essential oil point of rose and its upper layer
From obtaining primary rose；
(6) it distillation water outlet: carries out distillation fractionation processing again to primary rose, obtains purification rose.
Further, in the step (2), the concentration of salt water is 0.9%-1.1%.
Further, in the step (4), the temperature setting of condensation process is 10-20 DEG C.
Further, in the step (5), the detailed process of water-oil separating are as follows:
(5.1) distillate is placed into oil water separator, the bottom of oil water separator is equipped with heater, controls heater
Temperature be 30-40 DEG C；
(5.2) while heater, the air conditioner being arranged at oil water separator top delivery port, air conditioner are opened
Temperature setting at 25 DEG C；
(5.3) when there is condensation of oil on liquid liquid level to be distillated, condensation of oil is siphoned away with fuel sucking pipe.
Further, in the step (6), the temperature setting of second distillation at 20-30 DEG C, pressure 500-600MPa,
Distill 10-20min.
In conclusion by adopting the above-described technical solution, the beneficial effects of the present invention are: this method is using pure natural
Gimmick, rose purity is high obtained are processed, and does not contain other chemical components, ensure that the nutrition of rose,
It is sterilized in process, ensure that the clean of rose, the mode of second distillation is taken, to rose
It is purified, rose quality obtained is higher.
Detailed description of the invention
Fig. 1 is process flow diagram of the invention.
Specific embodiment
All features disclosed in this specification or disclosed all methods or in the process the step of, in addition to mutually exclusive
Feature and/or step other than, can combine in any way.
It elaborates below with reference to Fig. 1 to the present invention.
Embodiment 1:
As shown in Figure 1, a kind of production technology of rose, comprising the following steps:
(1) pre-selection of raw material: at the rose florescence using artificial picking rose, selected full roseleaf；
(2) pretreatment of raw material: the roseleaf after will be selected, which is put into salt water, to be impregnated, and places 10min, and the concentration of salt water is
0.9%；
(3) heating distillation: soaked roseleaf is placed into distilling apparatus, is 40 DEG C, distilling apparatus in temperature
Under conditions of internal pressure is 400MPa, 20min is distilled；
(4) condensation fractionation: the mixed gas of rose and steam that distillation is generated carries out condensation process, is distillated
Liquid, the temperature setting of condensation process are 10 DEG C；
(5) water-oil separating: carrying out water-oil separating processing to distillate, will float on the essential oil point of rose and its upper layer
From obtaining primary rose, the detailed process of water-oil separating are as follows:
(5.1) distillate is placed into oil water separator, the bottom of oil water separator is equipped with heater, controls heater
Temperature be 30 DEG C；
(5.2) while heater, the air conditioner being arranged at oil water separator top delivery port, air conditioner are opened
Temperature setting at 25 DEG C；
(5.3) when there is condensation of oil on liquid liquid level to be distillated, condensation of oil is siphoned away with fuel sucking pipe；
(6) distillation water outlet: carrying out distillation fractionation processing to primary rose again, obtains purification rose, secondary
The temperature setting of distillation distills 10min at 20 DEG C, pressure 500MPa.
Embodiment 2:
A kind of production technology of rose, comprising the following steps:
(1) pre-selection of raw material: at the rose florescence using artificial picking rose, selected full roseleaf；
(2) pretreatment of raw material: the roseleaf after will be selected, which is put into salt water, to be impregnated, and places 30min, and the concentration of salt water is
1.1%；
(3) heating distillation: soaked roseleaf is placed into distilling apparatus, is 50 DEG C, distilling apparatus in temperature
Under conditions of internal pressure is 500MPa, 30min is distilled；
(4) condensation fractionation: the mixed gas of rose and steam that distillation is generated carries out condensation process, is distillated
Liquid, the temperature setting of condensation process are 20 DEG C；
(5) water-oil separating: carrying out water-oil separating processing to distillate, will float on the essential oil point of rose and its upper layer
From obtaining primary rose, the detailed process of water-oil separating are as follows:
(5.1) distillate is placed into oil water separator, the bottom of oil water separator is equipped with heater, controls heater
Temperature be 0 DEG C；
(5.2) while heater, the air conditioner being arranged at oil water separator top delivery port, air conditioner are opened
Temperature setting at 25 DEG C；
(5.3) when there is condensation of oil on liquid liquid level to be distillated, condensation of oil is siphoned away with fuel sucking pipe；
(6) distillation water outlet: carrying out distillation fractionation processing to primary rose again, obtains purification rose, secondary
The temperature setting of distillation distills 20min at 30 DEG C, pressure 600MPa.
Embodiment 3:
A kind of production technology of rose, comprising the following steps:
(1) pre-selection of raw material: at the rose florescence using artificial picking rose, selected full roseleaf；
(2) pretreatment of raw material: the roseleaf after will be selected, which is put into salt water, to be impregnated, and places 20min, and the concentration of salt water is
1%；
(3) heating distillation: soaked roseleaf is placed into distilling apparatus, is 45 DEG C, distilling apparatus in temperature
Under conditions of internal pressure is 450MPa, 25min is distilled；
(4) condensation fractionation: the mixed gas of rose and steam that distillation is generated carries out condensation process, is distillated
Liquid, the temperature setting of condensation process are 15 DEG C；
(5) water-oil separating: carrying out water-oil separating processing to distillate, will float on the essential oil point of rose and its upper layer
From obtaining primary rose, the detailed process of water-oil separating are as follows:
(5.1) distillate is placed into oil water separator, the bottom of oil water separator is equipped with heater, controls heater
Temperature be 35 DEG C；
(5.2) while heater, the air conditioner being arranged at oil water separator top delivery port, air conditioner are opened
Temperature setting at 25 DEG C；
(5.3) when there is condensation of oil on liquid liquid level to be distillated, condensation of oil is siphoned away with fuel sucking pipe；
(6) distillation water outlet: carrying out distillation fractionation processing to primary rose again, obtains purification rose, secondary
The temperature setting of distillation distills 15min at 25 DEG C, pressure 550MPa.
Embodiment 4:
A kind of production technology of rose, comprising the following steps:
(1) pre-selection of raw material: at the rose florescence using artificial picking rose, selected full roseleaf；
(2) pretreatment of raw material: the roseleaf after will be selected, which is put into salt water, to be impregnated, and places 10min, and the concentration of salt water is
1.1%；
(3) heating distillation: soaked roseleaf is placed into distilling apparatus, is 50 DEG C, distilling apparatus in temperature
Under conditions of internal pressure is 400MPa, 30min is distilled；
(4) condensation fractionation: the mixed gas of rose and steam that distillation is generated carries out condensation process, is distillated
Liquid, the temperature setting of condensation process are 10 DEG C；
(5) water-oil separating: carrying out water-oil separating processing to distillate, will float on the essential oil point of rose and its upper layer
From obtaining primary rose, the detailed process of water-oil separating are as follows:
(5.1) distillate is placed into oil water separator, the bottom of oil water separator is equipped with heater, controls heater
Temperature be 40 DEG C；
(5.2) while heater, the air conditioner being arranged at oil water separator top delivery port, air conditioner are opened
Temperature setting at 25 DEG C；
(5.3) when there is condensation of oil on liquid liquid level to be distillated, condensation of oil is siphoned away with fuel sucking pipe；
(6) distillation water outlet: carrying out distillation fractionation processing to primary rose again, obtains purification rose, secondary
The temperature setting of distillation distills 10min at 20 DEG C, pressure 600MPa.
The above is only presently preferred embodiments of the present invention, not does limitation in any form to the present invention, it is all according to
According to technical spirit any simple modification to the above embodiments of the invention, equivalent variations, protection of the invention is each fallen within
Within the scope of.
Claims (5)
1. a kind of production technology of rose, which comprises the following steps:
(1) pre-selection of raw material: at the rose florescence using artificial picking rose, selected full roseleaf；
(2) pretreatment of raw material: the roseleaf after will be selected, which is put into salt water, to be impregnated, and places 10-30min；
(3) heating distillation: soaked roseleaf is placed into distilling apparatus, is 40-50 DEG C, in distilling apparatus in temperature
Under conditions of portion's pressure is 400-500MPa, 20-30min is distilled；
(4) condensation fractionation: the mixed gas of rose and steam that distillation is generated carries out condensation process, obtains distillate；
(5) water-oil separating: water-oil separating processing is carried out to distillate, rose will be floated on and separated with the essential oil on its upper layer, obtained
To primary rose；
(6) it distillation water outlet: carries out distillation fractionation processing again to primary rose, obtains purification rose.
2. a kind of production technology of rose according to claim 1, which is characterized in that in the step (2), salt water
Concentration be 0.9%-1.1%.
3. a kind of production technology of rose according to claim 2, which is characterized in that in the step (4), condensation
The temperature setting of processing is 10-20 DEG C.
4. a kind of production technology of rose according to claim 1, which is characterized in that in the step (5), grease
Isolated detailed process are as follows:
(5.1) distillate is placed into oil water separator, the bottom of oil water separator is equipped with heater, controls the temperature of heater
Degree is 30-40 DEG C；
(5.2) while heater, the air conditioner being arranged at oil water separator top delivery port, the temperature of air conditioner are opened
Degree is arranged at 25 DEG C；
(5.3) when there is condensation of oil on liquid liquid level to be distillated, condensation of oil is siphoned away with fuel sucking pipe.
5. a kind of production technology of rose according to claim 1, which is characterized in that secondary in the step (6)
The temperature setting of distillation distills 10-20min at 20-30 DEG C, pressure 500-600MPa.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711249688.7A CN109868187A (en) | 2017-12-01 | 2017-12-01 | A kind of production technology of rose |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711249688.7A CN109868187A (en) | 2017-12-01 | 2017-12-01 | A kind of production technology of rose |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109868187A true CN109868187A (en) | 2019-06-11 |
Family
ID=66913563
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711249688.7A Pending CN109868187A (en) | 2017-12-01 | 2017-12-01 | A kind of production technology of rose |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109868187A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111830145A (en) * | 2020-03-10 | 2020-10-27 | 北京农业生物技术研究中心 | Method for determining feeding ratio and distillation time of black-branch rose hydrosol |
| CN112076106A (en) * | 2020-09-24 | 2020-12-15 | 中山市荼薇文化产业发展有限公司 | Double-petal red rose hydrosol |
| CN112662477A (en) * | 2020-12-30 | 2021-04-16 | 小金县夹金山清多香野生资源开发有限责任公司 | Extraction method of rose essential oil and rose hydrosol |
| CN113234538A (en) * | 2021-05-14 | 2021-08-10 | 东莞檀香缘实业有限公司 | Production process of sandalwood hydrolat |
| CN113288832A (en) * | 2020-09-11 | 2021-08-24 | 广州辰沐生物科技有限公司 | Bletilla striata root rose hydrosol and preparation method thereof |
-
2017
- 2017-12-01 CN CN201711249688.7A patent/CN109868187A/en active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111830145A (en) * | 2020-03-10 | 2020-10-27 | 北京农业生物技术研究中心 | Method for determining feeding ratio and distillation time of black-branch rose hydrosol |
| CN111830145B (en) * | 2020-03-10 | 2022-11-11 | 北京市农林科学院 | Method for determining feeding ratio and distillation time of black-branch rose hydrosol |
| CN113288832A (en) * | 2020-09-11 | 2021-08-24 | 广州辰沐生物科技有限公司 | Bletilla striata root rose hydrosol and preparation method thereof |
| CN112076106A (en) * | 2020-09-24 | 2020-12-15 | 中山市荼薇文化产业发展有限公司 | Double-petal red rose hydrosol |
| CN112662477A (en) * | 2020-12-30 | 2021-04-16 | 小金县夹金山清多香野生资源开发有限责任公司 | Extraction method of rose essential oil and rose hydrosol |
| CN113234538A (en) * | 2021-05-14 | 2021-08-10 | 东莞檀香缘实业有限公司 | Production process of sandalwood hydrolat |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN109868187A (en) | A kind of production technology of rose | |
| CN105754722B (en) | A kind of preparation method and applications of the cigarette perfume object for reconstituted tobacoo | |
| CN103897807B (en) | A kind of extracting method of Flos Rosae Rugosae quintessence oil | |
| CN104293632B (en) | A kind of white wine decompression distillation system and distillating method | |
| CN106929153A (en) | A kind of preparation method and applications of rosemary hydrosol | |
| CN105969528A (en) | Extracting method for rose essential oil | |
| CN109576054A (en) | A kind of extracting method of Rosa Damascana | |
| CN105861256A (en) | Impurity removal and purification system and method for white wine | |
| CN107157861A (en) | Chrysanthemum hydrolat and beauty fluid prepared from same | |
| CN104946396A (en) | Method for preparing aquilaria essential oil | |
| CN203754681U (en) | Rose essential oil refining device | |
| CN107163972A (en) | A kind of preparation method of functional food level pyrolkigneous liquid | |
| CN104232137A (en) | Complete apparatus for refining bamboo vinegar by use of multistage multiple combination distillation method | |
| CN108342287B (en) | Distillation method for reducing fusel oil in white spirit | |
| CN105581926B (en) | Women privates conditioning liquid and preparation method thereof | |
| CN111471569A (en) | Solid-state liquor distillation equipment and distillation method | |
| CN106318641A (en) | Method for refining lemongrass essential oil | |
| CN102068400B (en) | Chimonanthus salicifolius perfume and preparation method thereof | |
| CN105754716A (en) | Low-temperature extracted snake oil and method for deodorizing and de-coloring snake oil | |
| CN107788314A (en) | The preparation method of rose | |
| CN102807471A (en) | Method for separation preparation of high purity natural phytol | |
| CN108186507A (en) | A kind of traditional Chinese medicine freckle-removing facial mask and its processing technology | |
| CN105747271B (en) | A kind of preparation method of low albumen tobacco extract for novel tobacco | |
| CN102488320B (en) | Application of paper mulberry fruit essential oil in cigarette flavoring and material feeding | |
| CN105331501B (en) | A kind of ginseng liquor and its preparation method and application |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20190611 |