CN109862867A - The excellent color make-up cosmetic combination and preparation method thereof of water moisture feeling - Google Patents
The excellent color make-up cosmetic combination and preparation method thereof of water moisture feeling Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0216—Solid or semisolid forms
- A61K8/022—Powders; Compacted Powders
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0241—Containing particulates characterized by their shape and/or structure
- A61K8/025—Explicitly spheroidal or spherical shape
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/60—Particulates further characterized by their structure or composition
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Abstract
The present invention relates to the color make-up cosmetic combinations comprising sericite, synthetic mica and spherical powder.Color make-up cosmetic combination of the invention has excellent water moisture feeling and stickiness for skin simultaneously, and has excellent forming stability and whereabouts stability.Also, color make-up cosmetic combination of the invention is not in coacervation of making up caused by particle aggregation, and skin makeup shows as smooth, so that curved part seems be lofty or to highlight, has excellent cutaneous manifestations power.
Description
Technical field
The present invention relates to color make-up cosmetic combinations, more specifically, are related to improving stretchability to become soft and light
It is sliding, so as to realize smooth skin makeup performance, and the color make-up cosmetic combination with excellent water moisture feeling and its
Manufacturing method.
This application claims excellent based on November 9th, 2016 South Korea patent application submitted the 10-2016-0148985th
It first weighs, all the elements disclosed in the specification and attached drawing by this application are introduced into the application.
Background technique
General cosmetic cosmetic preparation has the foundation cream or solid foundation cream etc. of liquid, and the powder formed using powder as principal component
Cream (compact), economic benefits and social benefits muffin (two way cake), sweet muffin (pressed powder) or compression muffin etc..It is above-mentioned each
The purpose of product is and while assign skin covering power, to be also used to show coloured and dazzling for covering chloasma or flaw etc.
Skin.Above-mentioned cosmetic cosmetic preparation has the use feeling of stretchability, stickiness and water profit, but may occur by particle aggregation
Caused floating powder phenomenon of making up.
From the point of view of nearest makeup trend, cosmetic cosmetic preparation not only has the base of covering power, adhesive force or stretchability etc.
This attribute should also have water moisture feeling.Also, water moisture feeling is also paid much attention to using the consumer of cosmetic cosmetic preparation, therefore this is
Main buying policy index (key buying factor) as product selection criteria.Therefore, in order to improve cosmetic cosmetic preparation
Water moisture feeling and carried out various researchs.However, when in common color make-up cosmetic preparation, especially liquid or solid foundation cream cosmetic preparation
When middle raising water moisture feeling, there are problems that stickiness decline.Also, although can mutually be mentioned with the ratio of water phase by changing oil
High water moisture feeling, but it is cunning to increase skin, and so that skin makeup is rough, and oil or particle aggregation may occur for regional area
Phenomenon.Also, when using the low oil of viscosity and with the oil for the phenyl being bonded with end or branched chain type (branch type),
Reflecting feel and water moisture feeling are improved, but have the shortcomings that stickiness and endurance decline.
Also, in order to using powder as in the cosmetic preparations such as the powder foundation (Powder Foundation) of principal component or powder cream
Improve water moisture feeling, it has been proposed that various methods, the method for such as deploying the ester oil of high-content with oily binder form, with natural
The method on the modified powders such as the wax or synthetic wax in source surface and comprising containing polyalcohol, emulsion, starch or modified starch etc.
Emulsion oil-in-water adhesive dosage form etc., but the above method all includes respective limitation.
That is, when deploying the ester oil of high-content with the oily adhesive as the bonding agent for being used for compression forming, water moisture feeling
It is improved, but there is limitation to allotment content.Also, work as with the coatings such as natural wax or synthetic wax or modified powder table
When face, it is difficult to give full play to effect with less amount, when being coated with larger quantities, greasy and binding force is sticked since wax is distinctive, and
It may can not be taken out there is a phenomenon where the spot phenomenon on surface or when extracting (pick-up) product with powder puff or brush etc..
Also it is possible to the cohesion due to oil or wax etc. occurs and occurs greasing (greasing) phenomenon or agglomeration (caking) phenomenon
Deng.Also, include starch or modified starch and be mixed with polyalcohol and emulsion emulsion oil-in-water dosage form cosmetic preparation use
Sintering process is to improve stability by the moisture in evaporation dosage form, however the pure water of the water phase for assigning water moisture feeling exists
It is burned off in sintering process, so that water moisture feeling cannot be played.Also, although attempt using water dispersion adhesive, water-in-oil type or
There are still limitations by the cosmetic cosmetic preparation dosage form of above-mentioned slug type, but to water moisture feeling is assigned for emulsion oil-in-water adhesive.
Also, the shortcomings that cosmetic preparation of slug type, is, has the phenomenon that Surface hardened layer and cracking, whereabouts stability is low, and color
Expressive force is insufficient.
In cosmetic cosmetic preparation, the use feeling and adhesive force of water profit are essential factors, but especially pulvis
There is limitation to the use feeling for assigning water profit due to formulation characteristics in type.Also, powder-type may occur caking phenomenon or play oil
Greasy phenomenon etc., and may cause makeup coacervation or the floating powder phenomenon of the makeup as caused by particle aggregation in coated product
Deng.As described above, having had attempted to various methods, but reality up to the present to improve the use feeling of the water of cosmetic preparation profit
Border situation is to lack actual effect, and do not play the effect that consumer can experience also.
Therefore, it is necessary to develop use feeling that is a kind of while improving water profit and stickiness and do not cause coacervation of making up
And the color make-up cosmetic combination that smooth skin makeup expressive force is excellent.
Summary of the invention
Technical task
The subject to be solved by the invention is to provide a kind of color make-up cosmetic combination, improve simultaneously water profit use feeling and
Stickiness, cutaneous manifestations are smooth, and floating powder phenomenon of making up is less.
The means to solve the problem
The present invention provides the color make-up cosmetic preparation combination of a kind of sericite comprising wet coating, synthetic mica and spherical powder
Object.Also, above-mentioned composition can further include the talcum being coated with by or mixtures thereof fatty acid, emulsifier.Also, it is above-mentioned
Color make-up cosmetic combination can be preferably powder class color make-up cosmetic combination.
The present inventor is in tradeoff with opposite attribute each other in color make-up cosmetic preparation to improve simultaneously
(trade-off) the water moisture feeling of relationship and stickiness and studied.As a result, the present inventor is moistened to improve water
Use feeling, selected the sericite that can be realized soft use feeling, and with the sericite with specified particle diameter and degree of distribution
For object, the modification on various surfaces has been attempted.In addition, having been used together for soft stretchability with excellent dispersibility
And not wide and sharp (sharp) the spherical powder of the particle distribution of powder.Also, for stickiness, selection has been used by spy
The talcum of material working process is determined as material.The stretchability for the color make-up cosmetic combination that surprising discovery is prepared as described above
While excellent with water moisture feeling, there is excellent skin attachement, smooth dressing effect is showed, so as to complete this hair
It is bright.
In the present invention, surface characteristic can be used in order to improve moistening in sericite of the sericite as wet coating
The sericite for being modified or being coated with.Preferably, above-mentioned sericite can be used by lauroyl glutamate disodium (disodium
Lauroyl glutamate), the thin,tough silk of or mixtures thereof two aluminium myristates (aluminium dimyristate) wet coating
Mica.Above-mentioned lauroyl glutamate disodium has excellent skin as the mild surfactant that can be used for sensitive skin
Compatibility.Moreover, powder surface is coated modification with metallicity fatty acid by above-mentioned two aluminium myristate, to improve powder
With the stickiness of skin, meanwhile, strengthen with the power that be combined with each other of other powders, therefore be a kind of material with excellent mouldability
Material.In the present invention, the solvent used when the above-mentioned sericite of wet coating can be used selected from by pure water, ethyl alcohol and isopropanol
It is more than any one of group of equal compositions, but not limited to this.Also, in addition to the above compounds, by using various paintings
Cloth material is modified sericite, so as to the physical property of the use feeling, stretchability and stability that influence cosmetic preparation etc..
Preferably, relative to the total weight of cosmetic combination, above-mentioned sericite can be by 0.1 to 2 weight %, preferably
The lauroyl glutamate disodium of 0.5 to 1.5 weight % and 0.5 to 5 weight %, two aluminium myristates of preferably 1 to 3 weight % are wet
Formula coating.When cosmetic combination of the invention includes the sericite by the compound wet coating of above-mentioned specified weight ratio,
The use feeling and skin attachement of the water profit of most excellent cosmetic combination can be played.
Also, the oil sucting force of above-mentioned sericite, the preferably sericite of wet coating can be about 0.9~1.3cc/g.It is above-mentioned
Sericite E-CL of the Sericite J or East Hill company of K.S.Pearl company, J&J company can be used in sericite
Sericite FFA etc., but not limited to this.
In the present invention, the average grain diameter of above-mentioned sericite can be 5 to 25 μm, preferably 6 to 20 μm, more preferably 8
To 15 μm.According to the average grain diameter of sericite, the degree of the water profit use feeling of cosmetic combination may be different.When this hair
When bright cosmetic combination includes the sericite with average grain diameter as described above, most excellent water moisture feeling can be played.
In the present invention, relative to the total weight of cosmetic combination, the content of above-mentioned sericite can be 5 to 30 weights
Measure %, preferably 8 to 20 weight %, more preferably 10 to 15 weight %.When the content of above-mentioned sericite is less than 5 weight %,
The effect of water moisture feeling and soft stretchability is unable to give full play or hardly significant.Also, work as the content of above-mentioned sericite
When more than 30 weight %, makeup coacervation may cause, and extract (pick-up) using cosmetic applicators such as powder puff and brushes
A large amount of powder are formed when product and fly powder phenomenon to exist, and there are problems that forming stability decline.
In the present invention, the synthetic mica replaced by iron can be used in above-mentioned synthetic mica.Synthetic mica is to utilize element
Come it is synthesizing rather than by original matter that working process is obtained from ore come using, therefore compared with natural mica, tool
There is whiteness excellent, impurity is few, feature with high purity.In the present invention, above-mentioned synthetic mica is characterized in that, is modified into
Also there is different property in synthetic mica.That is, above-mentioned synthetic mica is as the synthetic mica replaced by iron, specifically, can
It include by replacing part or all of aluminium atom present in the crystalline texture tetrahedron of mica as iron atom (Fe) to use
(Al) color synthesized is the synthetic mica of the powder of rufous.
On the other hand, the color of synthetic mica can realize multiplicity according to the temperature of calcining (calcination) process
Change.Preferably, it is of the invention by iron displacement synthetic mica can be used by reduce iron oxide pigment content come with skin
The synthetic mica that color similarly shows.Synthetic mica by iron displacement of the invention serves not only as extender pigment, may be used also
To play the function of the coloring pigment for showing skin-color.Also, the synthetic mica of the invention replaced by iron, with other conjunctions
It is compared at mica, moistening and smooth sense of touch are more excellent, and also have UV absorbability by iron content.
In the present invention, the average grain diameter of above-mentioned synthetic mica can be 5 to 35 μm, preferably 7 to 20 μm, more preferably
8 to 13 μm.When cosmetic combination of the invention includes the synthetic mica with average grain diameter as described above, can play
Most excellent water moisture feeling.
In the present invention, relative to the total weight of cosmetic combination, the content of above-mentioned synthetic mica can be 1 to 15 weight
Measure %, preferably 2 to 10 weight %, more preferably 3 to 5 weight %.When the content of above-mentioned synthetic mica is less than 1 weight %,
The effect of water moisture feeling and soft stretchability is unable to give full play or hardly significant.Also, when the content of synthetic mica is super
When crossing 15 weight %, makeup coacervation may cause, and extract (pick-up) using cosmetic applicators such as powder puff and brushes and produce
A large amount of powder are formed when product and fly powder phenomenon to exist, and there are problems that forming stability decline.
In the present invention, above-mentioned spherical powder may include polymethyl methacrylate (PMMA).Above-mentioned polymethyl
Sour methyl esters can have about 0.5 to 1.5cc/g oil sucting force, and the spherical phase for the non-porous matter not being surface-treated can be used
(spherical phase) powder.Preferably, the microparticle degree of distribution of above-mentioned polymethyl methacrylate is not wide and uniform and sharp
It is sharp.Preferably, above-mentioned polymethyl methacrylate can be single point be made of the disperse system with evenly sized dispersed phase
Dephasing (mono-dispersed).Also, the spherical shape for eliminating residual monomer can be used in above-mentioned polymethyl methacrylate
Grain.The ArtPearl for example, NEGAMI Chemical Industrial company can be used in above-mentioned polymethyl methacrylate
The GM-0800S etc. of K7P or AICA Kogyo company, but not limited to this.
In the present invention, the average grain diameter of above-mentioned spherical powder can be 5 to 25 μm, preferably 6 to 20 μm, more preferably
8 to 12 μm.When cosmetic combination of the invention includes the spherical powder with average grain diameter as described above, can play
Most excellent stretchability.
In the present invention, relative to the total weight of cosmetic combination, the content of above-mentioned spherical powder can be 0.5 to 7
Weight %, preferably 1 to 5 weight %, more preferably 2 to 4 weight %.When the content of above-mentioned spherical powder is more than 7 weight %,
A large amount of powder are formed when extracting (pick-up) product using cosmetic applicators such as powder puff and brushes to exist and fly powder phenomenon, and
There are problems that forming stability decline.Also, when the content of above-mentioned spherical powder is less than 0.5 weight %, it is coated on skin
When play soft stretchability with being unable to fully.
It in the present invention, can include above-mentioned spherical powder with the weight ratio of 1:0.2 to 1:2 (spherical powder: synthetic mica)
Body and synthetic mica.When weight ratio described above includes above-mentioned spherical powder and synthetic mica, most excellent makeup can be played
The sense of touch of stretchability and the water profit of feed composition.And it is possible to 1:0.2 to 1:3 (spherical powder and synthetic mica: sericite)
Weight ratio include above-mentioned spherical powder and synthetic mica and sericite.When weight ratio described above includes above-mentioned spherical powder and conjunction
When at mica and sericite, cosmetic combination can meet the use feeling and stickiness of water profit simultaneously.
Also, color make-up cosmetic combination of the invention can be further included by or mixtures thereof fatty acid, emulsifier
The talcum of coating is as extender pigment.Preferably, the talcum being coated with by stearoyl-glutamic acid disodium can be used in above-mentioned talcum,
In this case, the stretchability and stickiness of cosmetic combination are excellent, and reduce winged powder phenomenon, also improve mouldability
With whereabouts stability.But, in the present invention, the talcum of above-mentioned coating is not limited to the cunning being coated with by stearoyl-glutamic acid disodium
Stone, and may include by the cunning of the substance coating process of the emulsifier comprising fatty acid and amino acid series or ester oil series etc.
Stone.
In the present invention, powder can refer to the aggregate of the usually solid matter with 1mm granular size below.At this
The powder that can be used in the composition of invention may include selected from by the usually used extender pigment of cosmetic field, coloring face
It is more than any one of group of compositions such as material and white pigment.Preferably, cosmetic combination of the invention may include above-mentioned
Extender pigment.Above-mentioned extender pigment can be used selected from by comprising talcum, mica, kaolin, alumina, barium silicate, muscovite, conjunction
At the inorganic pigment of mica, magnesium carbonate and zeolite etc. and having comprising polyethylene powders, nylon powder, Polystyrene powder etc.
It is more than any one of groups of compositions such as machine pigment.Also, it is not limited to above-mentioned example, it can will be generally known in the art
Extender pigment, such as [modern cosmetics, Wan Goo Cho, Moon Jeong Rang, Duk Hwan Bae are collaborateed, South Korea
Academic information (strain), 2007.02 publish] in the extender pigment etc. recorded as extender pigment in the present composition.
Relative to the total weight of cosmetic combination, the content of above-mentioned extender pigment can be 30 to 50 weight %, preferably
For 32 to 48 weight %, more preferably 35 to 45 weight %.When above-mentioned extender pigment is less than 30 weight %, painting exhibition may be decreased
Property, when more than 50 weight %, it may occur however that powder coacervation.
Preferably, the extender pigment of silicic acid anhydride can be used in above-mentioned extender pigment.Specifically, above-mentioned extender pigment
Surface can be used by selected from by silicone, hydro carbons, fluorine, alkyl hydrogen polysiloxanes, surfactant and natural and synthetic wax
The above extender pigment being modified of any one of the group of equal compositions.Also, above-mentioned white pigment can be used by being selected from
By the above dioxy for being coated processing of any one of the groups formed such as silicone, ester system oil, aluminium hydroxide and stearic acid
Change titanium or zinc oxide etc., but not limited to this.
Cosmetic combination according to the present invention can wrap oil-containing, preferred oil adhesive, to come into conjunction with above-mentioned powder
Type.For above-mentioned oil, there is no limit can be used oil usually used in cosmetic combination to type.Above-mentioned oil can make
With selected from by the hydrocarbon system oil comprising mineral oil (mineral oil) etc.；Include three isostearate of polyglycereol -2
(polyglyceryl-2triisostearate), diisooctadecanol malate (diisostearyl malate), hydrogenation are poly-
Isobutene (hydrogenated polyisobutene), phytosterol/isooctadecanol/cetanol/stearyl alcohol/docosyl alcohol dimerization
Linoleate (phytosteryl/isostearyl/cetyl/stearyl/behenyl dimer dilinoleate), hydrogenation
Methyl abietate (methyl hydrogenated rosinate), caprylic/capric triglyceride (caprylic/capric
Triglyceride), isopropyl myristate (isopropyl myristate), neopentyl glycol dicaprate (neopentyl
Glycol dicaprate) and octyl dodecanol stearyl stearate (octyldodecyl stearoyl stearate)
Deng ester system oil；Vegetable oil comprising olive oil (olive oil) and Australia nut oil (macadamia oil) etc.；And packet
Containing cyclo-methicone (cyclomethicone), phenyl trimethicone (phenyl trimethicone), two
The poly- trimethicone of phenylsilane phenyl (diphenylsiloxy phenyl trimethicone) and poly- diformazan
It is more than any one of group of silicone oil composition of radical siloxane (dimethicone) etc., but not limited to this.
Relative to the total weight of cosmetic combination, the content of above-mentioned oil can be 0.1 to 15 weight %, preferably 3 to
13 weight %, more preferably 5 to 12 weight %.When above-mentioned oil is less than 0.1 weight %, powder may be may not proceed sufficiently
In conjunction with when more than 15 weight %, it may occur however that the powder coacervation as caused by oil.
Color make-up cosmetic combination of the invention in the range of not reducing the effect of composition, in addition to mentioned component it
It outside, can also include to be selected to be made of fragrance, colorant, preservative, oxidation stabilizers, UV blockers and pearl agent etc.
It is more than any one of group.Above-mentioned cosmetic combination can be the item or block agent type of solid phase, be selected from specifically, can be
By sweet muffin, compression muffin (Pressed fact), muffin (powder fact), powder foundation (powder
Foundation), powder solidifying white (foundation fact) and compressing powdered foundation cream (pressed powder
Any one powder-type in the group of compositions such as foundation), but not limited to this.
Also, the present invention provides color make-up cosmetic combination, includes 0.5 to 7 relative to the total weight of cosmetic combination
The polymethyl methacrylate (PMMA) of weight %, 1 to 15 weight % by the synthetic mica of iron displacement, 5 to 30 weight %
The extender pigment and 0.1 to 15 of the sericite, 30 to 50 weight % that are coated with by lauroyl glutamate disodium and two aluminium myristates
The oil of weight %.Preferably, above-mentioned cosmetic combination can further include the talcum being coated with by stearoyl-glutamic acid disodium.Packet
Combined color make-up cosmetic combination containing the ingredient with specified weight ratio as described above improves the sense of touch of water profit, and soft
With and glossily improve stretchability, so as to realize smooth skin makeup performance, and there is excellent stickiness.
Also, the preparation method of present invention offer color make-up cosmetic combination, comprising: (s1) is to the thin,tough silk comprising wet coating
The step of powder portion of mica, synthetic mica and spherical powder is stirred；(s2) the step of Xiang Shangshu powder portion injection oil portion；
And (s3) the step of product of above-mentioned (s2) step is mixed and crushes and filter.It preferably, can in above-mentioned steps (s1)
Additionally further include the talcum being coated with by or mixtures thereof fatty acid, emulsifier, in this case, cosmetic combination
Stretchability, stickiness, mouldability and whereabouts stability can significantly improve.
Invention effect
The sense of touch that there is color make-up cosmetic combination of the invention excellent water to moisten, while having excellent for skin
Stretchability and stickiness, and there is excellent forming stability and whereabouts stability.
In addition, color make-up cosmetic combination of the invention is not in coacervation of making up caused by particle aggregation, skin
Makeup shows as smooth, so that curved part seems be lofty or to highlight, has excellent cutaneous manifestations power.
Specific embodiment
Hereinafter, in order to help to enumerate embodiment etc. for the understanding of the present invention and be described in detail.But according to this
The embodiment of invention can be deformed into various other forms, and the scope of the present invention should not be construed as limited to following implementation
Example.The embodiment of the present invention is provided to be more fully explained the present invention to those skilled in the art.
The preparation of the powder class cosmetic preparation of embodiment 1 to 2 and comparative example 1 to 3
Powder class color make-up cosmetic preparation is prepared for using ingredient shown in the following table 1.In Examples 1 and 2, change by lauroyl
The content of the sericite and the synthetic mica by iron displacement of disodium glutamate and two aluminium myristate coating process, thus to score
Sense of touch, stretchability and the stickiness of the water profit of cosmetic combination are analysed.
[table 1]
Above-described embodiment and comparative example are prepared for according to the content of respective mentioned component composition.Firstly, powder portion is thrown
Entering in Henschel mixer, high speed (800~1200rpm) mixes about 5 minutes, and then low speed (400~600rpm) stirs oil portion,
The injection of sprayer has been carried out simultaneously.Then, after high speed (800~1200rpm) mixes about 3 minutes in a in a henschel mixer,
It is crushed twice using atomizer (Atomizer), is then filtered with 30 mesh (mesh).A series of above-mentioned preparations will be passed through
The semi-finished product of process are in 30~50kgf/cm2Forming under the pressure 1 to 3 second.
Experimental example 1: the use feeling evaluation of cosmetic preparation
The use feeling of the sweet muffin prepared in above-described embodiment 1 to 2 and comparative example 1 to 3 is evaluated.For making
With sense, with the experience of making up at least 2 years or more, and it was unmarried to continue to carry out minimum 20~45 years old to make up more than five times in one week
And the entitled object of panel 38 of married femle has carried out Blind Test.Following table 2 shows use feeling evaluation criterion.
Use feeling evaluation is to have rated use after embodiment or comparative example are smeared respectively by the face of subject women
Sense, especially water moisture feeling, stickiness, stretchability, the use feeling of delicacy, makeup cohesion and floating powder phenomenon and winged powder phenomenon.It will
The score of 38 panel's evaluations carries out statistical disposition by projects, takes it average, following table 3 shows score.
[table 2]
[table 3]
As shown in Table 3 above, at the same include polymethyl methacrylate and by iron displacement synthetic mica embodiment 1 to
2 and comparative example 1 to 3 show soft stretchability and be greatly improved.Moreover, comprising lauroyl glutamate disodium and
The sense of touch and stickiness, the use feeling of delicacy, makeup cohesion that the embodiment 1 to 2 of two aluminium myristates coating sericite is moistened in water
Significantly excellent effect is shown in floating powder phenomenon.In addition, comparative example 1 to 3 is closed using the substitution iron displacement of silicone coated mica
At mica and at the same time polymethyl methacrylate is substituted using silica and nylon powder, to obtain in terms of stretchability
Excellent evaluation, but excessively poor evaluation has been obtained in makeup cohesion and floating powder phenomenon project and winged powder phenomenon.Pass through
These experimental results can confirm, with 1 to 3 phase of comparative example for applying nylon powder and silicone coated mica and silica simultaneously
Than, while including by the synthetic mica and polymethyl methacrylate and lauroyl glutamate disodium of iron displacement and two nutmegs
The embodiment 1 to 2 of sour aluminium coating sericite improve in powder class color make-up cosmetic preparation the sense of touch of unconsummated water profit, stickiness and
Stretchability.
Also, by further testing, have rated the coating according to talc content representative in extender pigment
Stretchability, stickiness and winged powder phenomenon of substrate etc..
[table 4]
[table 5]
| It distinguishes | Embodiment 3 | Comparative example 4 |
| Stretchability | 4.3 | 4.0 |
| Stickiness | 4.5 | 4.1 |
| Fly powder phenomenon | 4.3 | 4.0 |
Such as above-mentioned table 5 as can be seen that being coated with 4 phase of comparative example of talcum with application alkyl silane and dimethyl silicone polymer
Than being obtained in the evaluation of stretchability, stickiness and winged powder phenomenon using the embodiment 3 of stearoyl-glutamic acid disodium coating talcum
Superior evaluation.From the above it has been confirmed that being coated with talcum compared with application silicone in color make-up cosmetic combination, preferably
Talcum is coated with using stearoyl-glutamic acid disodium.
Experimental example 2: the mouldability and estimation of stability of cosmetic preparation
It has rated the hardness of the sweet muffin prepared in above-described embodiment 1 and 3 and comparative example 2 and 3 and falls and stablize
Property, and confirmed that the coacervation bring greasing (greasing) of oil and microparticle etc. and agglomeration (caking) are existing
As.For hardness measurement, the JAL Type (JIS K 6301) of Japanese macromolecule gauge Co., Ltd. is used to invade hardometer,
The following table 6 shows respective average value.Measurement for whereabouts stability makes to complete molding respective embodiment and compare
Example is freely fallen on 3mm rubber slab from 70cm high perpendicular, measures damaged opportunity.Also, occur for product surface
Greasing and caking phenomenon, using cosmetic applicators (powder puff) with practical women using when strength take into molding three
Product has rated the phenomenon that occurring when taking product surface about 100~120 times.
[table 6]
* criterion of acceptability: when the average value of 5 samples is at 3 times or more, whereabouts stability is stablized.
It can be confirmed based on the result shown in above-mentioned table 6, sense of touch, stretchability and the stickiness project that embodiment 1 and 3 is moistened in water
Middle acquisition high score, meanwhile, the qualification that hardness appropriate and the stability that falls are 4 times or more is horizontal.And, it is thus identified that by oil
It is also stable and without exception in greasing caused by agglomerating and caking phenomenon.On the contrary, using silica and nylon powder and silicon
The comparative example 2 and 3 of ketone coated mica, while being formed with soft, it is unqualified in the stability of whereabouts to be confirmed to be product
It is horizontal.
Experimental example 3: the makeup state evaluation of cosmetic preparation
Have rated the makeup for showing the practical smearing of the cosmetic combination of embodiment 3 and comparative example 3 afterwards on the skin
State, i.e., film of uniformly making up, smooth makeup performance and makeup persistence.With the entitled evaluation of women 28 in 20 years old to 45 years old
Object, it is thus identified that the feeling and state when spread product and the persistence after makeup.
◎: feel optimal sense of touch or use feeling.
Zero: can feel almost optimal use feeling, but not be the degree met very much.
△: common.
Ⅹ: bad.
[table 7]
| It distinguishes | Uniform makeup film | Smooth makeup performance | Makeup persistence |
| Embodiment 3 | ◎ | ◎ | ○ |
| Comparative example 3 | △ | △ | ○ |
Based on the result shown in above-mentioned table 7 it has been confirmed that embodiment prepared in accordance with the present invention 3 uniformly makeup film and
Very excellent dressing effect is shown in smooth makeup performance, lasting sexual satisfaction of making up is also high.On the contrary, in comparative example 3
In the case where, O-level is confirmed as in terms of uniformly makeup film and smooth makeup performance.In the case where comparative example 3,
Due to spherical powder content and silicone coated mica content, some are high, and stickiness is poor, thus be difficult to form uniform makeup film,
And it is serious due to flying powder phenomenon, it cannot achieve smooth makeup performance.
Based on the above results it is known that cosmetic combination of the invention includes to have average grain diameter appropriate and granularity
The polymethyl methacrylate that is evenly distributed, iron displacement synthetic mica and by lauroyl glutamate disodium and two aluminium myristates
The sericite of coating, thus improve water profit sense of touch, stickiness and stretchability are excellent, also formed in cutaneous manifestations it is smooth and
Uniform makeup film.Also, cosmetic combination of the invention includes the talcum being coated with by stearoyl-glutamic acid disodium, thus aobvious
It writes and improves mouldability and whereabouts stability.
Claims (15)
1. a kind of color make-up cosmetic combination, it includes the sericite of wet coating, synthetic mica and spherical powders.
2. color make-up cosmetic combination according to claim 1, which is characterized in that the composition is further included by rouge
The talcum of or mixtures thereof fat acid, emulsifier coating.
3. color make-up cosmetic combination according to claim 1, which is characterized in that the sericite is by lauroyl glutamate
Or mixtures thereof disodium, two aluminium myristates wet coating.
4. color make-up cosmetic combination according to claim 3, which is characterized in that the gross weight relative to cosmetic combination
Amount, the sericite are wet by the lauroyl glutamate disodium of 0.1 to 2 weight % and two aluminium myristates of 0.5 to 5 weight %
Formula coating.
5. color make-up cosmetic combination according to claim 1, which is characterized in that the gross weight relative to cosmetic combination
Amount, the sericite is 5 to 30 weight %.
6. color make-up cosmetic combination according to claim 1, which is characterized in that the average grain diameter of the sericite is 5
To 25 μm.
7. color make-up cosmetic combination according to claim 1, which is characterized in that the aluminium atom (Al) of the synthetic mica
It is replaced by iron atom (Fe).
8. color make-up cosmetic combination according to claim 1, which is characterized in that the gross weight relative to cosmetic combination
Amount, the synthetic mica is 1 to 15 weight %.
9. color make-up cosmetic combination according to claim 1, which is characterized in that the spherical powder includes poly- methyl-prop
E pioic acid methyl ester (PMMA).
10. color make-up cosmetic combination according to claim 1, which is characterized in that relative to the total of cosmetic combination
Weight, the spherical powder are 0.5 to 7 weight %.
11. color make-up cosmetic combination according to claim 1, which is characterized in that the spherical powder and synthetic mica
Weight ratio be 1:0.2 to 1:2 (spherical powder: synthetic mica).
12. color make-up cosmetic combination according to claim 1, which is characterized in that the spherical powder and synthetic mica
Weight ratio with sericite is 1:0.2 to 1:3 (spherical powder and synthetic mica: sericite).
13. a kind of color make-up cosmetic combination, wherein relative to the total weight of composition, the poly- first comprising 0.5 to 7 weight %
Base methyl acrylate (PMMA), 1 to 15 weight % by iron displacement synthetic mica, 5 to 30 weight % by lauroyl paddy ammonia
Sericite, the extender pigment of 30 to 50 weight % and the oil of 0.1 to 15 weight % of acid disodium and the coating of two aluminium myristates.
14. a kind of preparation method of color make-up cosmetic combination, comprising:
(s1) the step of powder portion for including the sericite of wet coating, synthetic mica and spherical powder being stirred；
(s2) the step of Xiang Suoshu powder portion injection oil portion；And
(s3) the step of product of (s2) step by described in mixes and crushes and filter.
15. the preparation method of color make-up cosmetic combination according to claim 14, which is characterized in that in (s1) step
The talcum being coated with by or mixtures thereof fatty acid, emulsifier is additionally further included in rapid.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1020160148985A KR101854536B1 (en) | 2016-11-09 | 2016-11-09 | Makeup cosmetic composition with excellent moisturizing and Method of preparing the same |
| KR10-2016-0148985 | 2016-11-09 | ||
| PCT/KR2017/005534 WO2018088656A1 (en) | 2016-11-09 | 2017-05-26 | Color cosmetic composition having excellent moistness and method for preparing same |
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| CN109862867A true CN109862867A (en) | 2019-06-07 |
| CN109862867B CN109862867B (en) | 2022-12-16 |
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| CN201780065816.4A Active CN109862867B (en) | 2016-11-09 | 2017-05-26 | Color cosmetic composition with excellent water-retaining feeling and preparation method thereof |
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|---|---|
| JP (1) | JP6976633B2 (en) |
| KR (1) | KR101854536B1 (en) |
| CN (1) | CN109862867B (en) |
| WO (1) | WO2018088656A1 (en) |
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| KR102338785B1 (en) * | 2021-06-17 | 2021-12-15 | 주식회사 한국화장품제조 | Cosmetic composition containing extender pigment surface-treated with metal salt |
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| JP2002255746A (en) * | 2000-12-27 | 2002-09-11 | Kose Corp | Surface coating power and cosmetic containing the same |
| CN1643037A (en) * | 2002-03-12 | 2005-07-20 | 宝洁公司 | Spherical powder components and solid cosmetic compositions comprising thereof |
| JP2011136917A (en) * | 2009-12-26 | 2011-07-14 | Nippon Menaade Keshohin Kk | Solid powder cosmetic |
| JP2011195485A (en) * | 2010-03-18 | 2011-10-06 | Nippon Menaade Keshohin Kk | Solid powder cosmetic |
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| JP2000290526A (en) | 1999-04-02 | 2000-10-17 | Topy Ind Ltd | Pearly lustrous pigment, paint composition, cosmetic, ink and plastic containing said pigment |
| JP4880047B2 (en) | 2010-02-23 | 2012-02-22 | 三好化成株式会社 | Coated powder and cosmetics using the powder |
| KR20130068118A (en) * | 2011-12-15 | 2013-06-25 | 한국콜마주식회사 | Color tone cosmetic composition comprising coated illite |
| JP6021024B2 (en) * | 2013-08-23 | 2016-11-02 | 住友電工システムソリューション株式会社 | Display method, display device, display system, and computer program |
| KR20160002515A (en) * | 2014-06-30 | 2016-01-08 | 한국콜마주식회사 | Powder coloring cosmetic composition and preparing method thereof |
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2016
- 2016-11-09 KR KR1020160148985A patent/KR101854536B1/en active IP Right Grant
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2017
- 2017-05-26 JP JP2019545210A patent/JP6976633B2/en active Active
- 2017-05-26 WO PCT/KR2017/005534 patent/WO2018088656A1/en active Application Filing
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| JP2002255746A (en) * | 2000-12-27 | 2002-09-11 | Kose Corp | Surface coating power and cosmetic containing the same |
| CN1643037A (en) * | 2002-03-12 | 2005-07-20 | 宝洁公司 | Spherical powder components and solid cosmetic compositions comprising thereof |
| JP2011136917A (en) * | 2009-12-26 | 2011-07-14 | Nippon Menaade Keshohin Kk | Solid powder cosmetic |
| JP2011195485A (en) * | 2010-03-18 | 2011-10-06 | Nippon Menaade Keshohin Kk | Solid powder cosmetic |
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| Publication number | Publication date |
|---|---|
| WO2018088656A1 (en) | 2018-05-17 |
| KR101854536B1 (en) | 2018-05-03 |
| JP6976633B2 (en) | 2021-12-08 |
| JP2019537626A (en) | 2019-12-26 |
| CN109862867B (en) | 2022-12-16 |
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