CN109825083A - A kind of Multifunctional plastic additive and preparation method thereof - Google Patents
A kind of Multifunctional plastic additive and preparation method thereof Download PDFInfo
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- CN109825083A CN109825083A CN201810190244.9A CN201810190244A CN109825083A CN 109825083 A CN109825083 A CN 109825083A CN 201810190244 A CN201810190244 A CN 201810190244A CN 109825083 A CN109825083 A CN 109825083A
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Abstract
The invention discloses a kind of Multifunctional plastic additives and preparation method thereof, it include: 8-13 parts of glass powder, 15-20 parts of dibutyl phthalate, vegetable esters 10-15 parts of synthesis, 8-10 parts of dioctyl phthalate, 10-12 parts of phosphite, 8-10 parts of sulfydryl acid esters, 5-8 parts of mica powder, 4-7 parts of carbon dust, three 2-4 parts of monooctyl esters, 10-15 parts of benzotriazole, 20-25 parts of salicylate, 4-10 parts of aluminium hydroxide, 2-5 parts of inorganic nano material, 12-15 parts of ethoxylated alkyl polyamines, 15-20 parts of alkyl trimethyl quaternary ammonium, 5-10 parts of antistatic agent, 1-3 parts of silane coupling agent, 2-6 parts of methyl-silicone oil, 0.1-0.2 parts and toughener 0.5-1 parts of antibacterial agent.The present invention adopts with anti-oxidant, antistatic, sterilization and can be improved intensity again convenient for plasticity, also has the function of facilitating preservation.
Description
Technical field
The present invention relates to a kind of Multifunctional plastic additive processing technical field, especially a kind of Multifunctional plastic additive and
Preparation method.
Background technique
With social development and scientific and technological progress, plastics have become people production and life in necessary new material it
One.Plastics are mainly made of synthetic resin and various additives, therefore synthesis, processing and the application of additive are always that plastics are ground
Study carefully one of direction most popular in field.It is inorganic fill out that usage amount is maximum and most popular in plastic additive
Material, such as calcium carbonate, talcum powder, glass powder, carbon black.The dispersion and processing performance of these inorganic fillers in the polymer
It is the hot spot that plastic material research worker pays special attention to.But it solves inorganic filler dispersity in the polymer, improve
The interface of inorganic filler and polymeric matrix, the processing for improving plastic composite and application performance improve plastic composite
Performance/price ratio the problems such as, require special processing aid to solve.Mainly have point for the plastic additive of inorganic filler
The processing aids such as powder, coupling agent, lubricant.There are many type of these auxiliary agents, and performance is relatively simple, give plastic processing row
Industry brings the complexity of processing technology and the non-green of processing environment, so developing the multifunctionality for inorganic filler
It is more and more important in the plastic additive of one, it is the epoch needs of plastic new material processing and application, but current auxiliary agent function
Can be single, reach requirement, it is therefore desirable to improve.
Summary of the invention
There is provided the purpose of the present invention is to solve above-mentioned the deficiencies in the prior art a kind of Multifunctional plastic additive and its
Preparation method.
To achieve the goals above, a kind of Multifunctional plastic additive designed by the present invention, including by following parts by weight
The raw material of proportion is made: 8-13 parts of glass powder, 15-20 parts of dibutyl phthalate, vegetable esters 10-15 parts of synthesis, adjacent benzene
8-10 parts of diformazan dioctyl phthalate, 10-12 parts of phosphite, 8-10 parts of sulfydryl acid esters, 5-8 parts of mica powder, 4-7 parts of carbon dust, three
2-4 parts of monooctyl ester, 10-15 parts of benzotriazole, 20-25 parts of salicylate, 4-10 parts of aluminium hydroxide, 2-5 parts of inorganic nano material,
12-15 parts of ethoxylated alkyl polyamines, 15-20 parts of alkyl trimethyl quaternary ammonium, 5-10 parts of antistatic agent, 1-3 parts of silane coupling agent,
2-6 parts of methyl-silicone oil, 0.1-0.2 parts of antibacterial agent, 0.5-1 parts 1-2 parts of toughener.
Further, the raw material including being matched according to following number: 10-13 parts of glass powder, dibutyl phthalate 18-
20 parts, synthesis vegetable esters 12-15 parts, 9-10 parts of dioctyl phthalate, 11-12 parts of phosphite, 9-10 parts of sulfydryl acid esters,
6-7 parts of mica powder, 5-7 parts of carbon dust, 3-4 parts of three monooctyl ester, 12-15 parts of benzotriazole, 22-25 parts of salicylate, aluminium hydroxide
8-10 parts, 3-5 parts of inorganic nano material, 13-15 parts of ethoxylated alkyl polyamines, 16-20 parts of alkyl trimethyl quaternary ammonium, resist it is quiet
Electric agent 8-10 parts, 2-3 parts of silane coupling agent, 3-5 parts of methyl-silicone oil, 0.15-0.18 parts of antibacterial agent, 0.6-0.8 parts of toughener
1.5-1.8 part.
Further, the inorganic nano material is nano-titanium dioxide, nano silicon-based oxide, graphene-based inorganic nano
Material, nano aluminum base oxide receive one of aluminium rice calcium carbonate or a variety of compoundings, simple particle size range 20-80nm.
Further, the antibacterial agent is the antibacterial agent prepared by inorganic solvent.
The invention also discloses a kind of preparation methods of Multifunctional plastic additive, which is characterized in that specific step is as follows:
S1, raw material is weighed according to formula, by inorganic nano material grinding distribution；
S2, raw material is weighed according to formula, by glass powder, dioctyl phthalate, synthesis vegetable esters, phthalic acid
Dibutyl ester, phosphite, sulfydryl acid esters, mica powder, carbon dust, three monooctyl esters and benzotriazole are put into reaction kettle, spare；
Reaction kettle heating temperature in S3, regulating step S2 is 120-125 DEG C, mixing speed 2500-2800r/min,
Reaction time is 20-25 minutes, adds benzotriazole, salicylate, aluminium hydroxide, inorganic nano material, ethoxylation alkane
Quito amine, alkyl trimethyl quaternary ammonium, antistatic agent, silane coupling agent, methyl-silicone oil, antibacterial agent, toughener, and it is warming up to 135-
140 DEG C, reaction 10-20 minutes is stirred at low speed, discharging obtains Multifunctional plastic additive finished product.
Further, inorganic nano material selects nano-titanium dioxide, nano silicon-based oxide, graphene-based in step sl
Inorganic nano material, nano aluminum base oxide receive one of aluminium rice calcium carbonate or a variety of compoundings, simple particle size range 20-
80nm。
A kind of Multifunctional plastic additive and preparation method thereof that the present invention obtains, using adding anti-oxidant original in inorganic filler
Material, antistatic raw material, raw bactericidal material make manufactured plastic additive have anti-oxidant, antistatic, sterilization and be convenient for plasticity again
It can be improved intensity, also have the function of facilitating preservation.
Specific embodiment
Innovation and creation are described further below with reference to embodiment.
Embodiment 1:
A kind of Multifunctional plastic additive provided in this embodiment, the raw material including being matched by following parts by weight are made: glass
8-13 parts of glass powder, 15-20 parts of dibutyl phthalate, synthesis vegetable esters 10-15 parts, dioctyl phthalate 8-10
Part, 10-12 parts of phosphite, 8-10 parts of sulfydryl acid esters, 5-8 parts of mica powder, 4-7 parts of carbon dust, 2-4 parts of three monooctyl ester, benzo three
10-15 parts of azoles, 20-25 parts of salicylate, 4-10 parts of aluminium hydroxide, 2-5 parts of inorganic nano material, ethoxylated alkyl polyamines
12-15 parts, 15-20 parts of alkyl trimethyl quaternary ammonium, 5-10 parts of antistatic agent, 1-3 parts of silane coupling agent, 2-6 parts of methyl-silicone oil,
0.1-0.2 parts of antibacterial agent, 0.5-1 parts of toughener.
The Multifunctional plastic additive in the present embodiment, the raw material including being matched by following parts by weight are made: glass powder
8 parts of end, 15 parts of dibutyl phthalate, synthesis 10 parts of vegetable esters, 8 parts of dioctyl phthalate, 11 parts of phosphite, mercapto
8 parts of base acid esters, 5 parts of mica powder, 4 parts of carbon dust, 2 parts of three monooctyl ester, 10 parts of benzotriazole, 20 parts of salicylate, aluminium hydroxide 4
Part, 2 parts of inorganic nano material, 12 parts of ethoxylated alkyl polyamines, 15 parts of alkyl trimethyl quaternary ammonium, 5 parts of antistatic agent, silane
1 part of coupling agent, 2 parts of methyl-silicone oil, 0.1 part of antibacterial agent, 0.5 part of toughener.
Further, the inorganic nano material is nano-titanium dioxide, nano silicon-based oxide, graphene-based inorganic nano
Material, nano aluminum base oxide receive one of aluminium rice calcium carbonate or a variety of compoundings, simple particle size range 20-80nm.In this reality
Applying inorganic nano material described in example is nano-titanium dioxide, simple particle size range 20nm.
Further, the antibacterial agent is the antibacterial agent prepared by inorganic solvent.
The present embodiment also discloses a kind of preparation method of Multifunctional plastic additive, which is characterized in that specific step is as follows:
S1, raw material is weighed according to formula, by inorganic nano material grinding distribution；
S2, raw material is weighed according to formula, by glass powder, dioctyl phthalate, synthesis vegetable esters, phthalic acid
Dibutyl ester, phosphite, sulfydryl acid esters, mica powder, carbon dust, three monooctyl esters and benzotriazole are put into reaction kettle, spare；
Reaction kettle heating temperature in S3, regulating step S2 is 120 DEG C, mixing speed 2500r/min, and the reaction time is
20 minutes, add benzotriazole, salicylate, aluminium hydroxide, inorganic nano material, ethoxylated alkyl polyamines, alkyl three
Methyl quaternary ammonium, antistatic agent, silane coupling agent, methyl-silicone oil, antibacterial agent, toughener, and 135 DEG C are warming up to, it stirs at low speed anti-
It answers 10 minutes, discharging obtains Multifunctional plastic additive finished product.
Embodiment 2:
A kind of Multifunctional plastic additive provided in this embodiment, the raw material including being matched by following parts by weight are made: glass
13 parts of glass powder, 20 parts of dibutyl phthalate, synthesis 15 parts of vegetable esters, 10 parts of dioctyl phthalate, phosphite
12 parts, 10 parts of sulfydryl acid esters, 8 parts of mica powder, 7 parts of carbon dust, 4 parts of three monooctyl ester, 15 parts of benzotriazole, 25 parts of salicylate, hydrogen
10 parts of aluminium oxide, 5 parts of inorganic nano material, 15 parts of ethoxylated alkyl polyamines, 20 parts of alkyl trimethyl quaternary ammonium, antistatic agent 10
Part, 3 parts of silane coupling agent, 6 parts of methyl-silicone oil, 0.2 part of antibacterial agent, 1 part of toughener.
Further, the inorganic nano material is the compounding of nano-titanium dioxide, nano silicon-based oxide, simple partial size
Range 30nm.
Further, the antibacterial agent is the antibacterial agent prepared by inorganic solvent.
The present embodiment also discloses a kind of preparation method of Multifunctional plastic additive, which is characterized in that specific step is as follows:
S1, raw material is weighed according to formula, by inorganic nano material grinding distribution；
S2, raw material is weighed according to formula, by glass powder, dioctyl phthalate, synthesis vegetable esters, phthalic acid
Dibutyl ester, phosphite, sulfydryl acid esters, mica powder, carbon dust, three monooctyl esters and benzotriazole are put into reaction kettle, spare；
Reaction kettle heating temperature in S3, regulating step S2 is 121 DEG C, mixing speed 2600r/min, and the reaction time is
22 minutes, add benzotriazole, salicylate, aluminium hydroxide, inorganic nano material, ethoxylated alkyl polyamines, alkyl three
Methyl quaternary ammonium, antistatic agent, silane coupling agent, methyl-silicone oil, antibacterial agent, toughener, and 136 DEG C are warming up to, it stirs at low speed anti-
It answers 15 minutes, discharging obtains Multifunctional plastic additive finished product.
Embodiment 3:
A kind of Multifunctional plastic additive provided in this embodiment, the raw material including being matched by following parts by weight are made: glass
10 parts of glass powder, 18 parts of dibutyl phthalate, synthesis 13 parts of vegetable esters, 9 parts of dioctyl phthalate, phosphite 11
Part, 9 parts of sulfydryl acid esters, 6 parts of mica powder, 5 parts of carbon dust, 3 parts of three monooctyl ester, 13 parts of benzotriazole, 23 parts of salicylate, hydroxide
6 parts of aluminium, 3 parts of inorganic nano material, 13 parts of ethoxylated alkyl polyamines, 16 parts of alkyl trimethyl quaternary ammonium, 8 parts of antistatic agent, silicon
2 parts of alkane coupling agent, 5 parts of methyl-silicone oil, 0.15 part of antibacterial agent, 0.6 part of toughener.
Further, the inorganic nano material is nano-titanium dioxide, nano silicon-based oxide, graphene-based inorganic nano
The compounding of material, simple particle size range 50nm.
Further, the antibacterial agent is the antibacterial agent prepared by inorganic solvent.
The present embodiment also discloses a kind of preparation method of Multifunctional plastic additive, which is characterized in that specific step is as follows:
S1, raw material is weighed according to formula, by inorganic nano material grinding distribution；
S2, raw material is weighed according to formula, by glass powder, dioctyl phthalate, synthesis vegetable esters, phthalic acid
Dibutyl ester, phosphite, sulfydryl acid esters, mica powder, carbon dust, three monooctyl esters and benzotriazole are put into reaction kettle, spare；
Reaction kettle heating temperature in S3, regulating step S2 is 124 DEG C, mixing speed 2700r/min, and the reaction time is
23 minutes, add benzotriazole, salicylate, aluminium hydroxide, inorganic nano material, ethoxylated alkyl polyamines, alkyl three
Methyl quaternary ammonium, antistatic agent, silane coupling agent, methyl-silicone oil, antibacterial agent, toughener, and 138 DEG C are warming up to, it stirs at low speed anti-
It answers 15 minutes, discharging obtains Multifunctional plastic additive finished product.
Embodiment 4:
A kind of Multifunctional plastic additive provided in this embodiment, including the raw material matched according to following number: glass powder
10-13 parts, 18-20 parts of dibutyl phthalate, synthesis vegetable esters 12-15 parts, 9-10 parts of dioctyl phthalate, phosphorous
11-12 parts of hydrochlorate, 9-10 parts of sulfydryl acid esters, 6-7 parts of mica powder, 5-7 parts of carbon dust, 3-4 parts of three monooctyl ester, benzotriazole 12-15
Part, 22-25 parts of salicylate, 8-10 parts of aluminium hydroxide, 3-5 parts of inorganic nano material, 13-15 parts of ethoxylated alkyl polyamines,
16-20 parts of alkyl trimethyl quaternary ammonium, 8-10 parts of antistatic agent, 2-3 parts of silane coupling agent, 3-5 parts of methyl-silicone oil, antibacterial agent
0.15-0.18 parts, 0.6-0.8 parts of toughener.The Multifunctional plastic additive in the present embodiment, including match according to following number
The raw material of ratio: 10 parts of glass powder, 18 parts of dibutyl phthalate, synthesis 12 parts of vegetable esters, dioctyl phthalate 9
Part, 11 parts of phosphite, 9-10 parts of sulfydryl acid esters, 6 parts of mica powder, 5 parts of carbon dust, 3 parts of three monooctyl ester, 12 parts of benzotriazole, water
22-25 parts of poplar acid esters, 8 parts of aluminium hydroxide, 3 parts of inorganic nano material, 13-15 parts of ethoxylated alkyl polyamines, alkyl trimethyl
16 parts of quaternary ammonium, 8 parts of antistatic agent, 2-3 parts of silane coupling agent, 3 parts of methyl-silicone oil, 0.15 part of antibacterial agent, 0.6 part of toughener.
Further, the inorganic nano material is nano-titanium dioxide, nano silicon-based oxide, graphene-based inorganic nano
Material, nano aluminum base oxide, the compounding of aluminium rice calcium carbonate received, simple particle size range 50nm.
Further, the antibacterial agent is the antibacterial agent prepared by inorganic solvent.
The present embodiment also discloses a kind of preparation method of Multifunctional plastic additive, which is characterized in that specific step is as follows:
S1, raw material is weighed according to formula, by inorganic nano material grinding distribution；
S2, raw material is weighed according to formula, by glass powder, dioctyl phthalate, synthesis vegetable esters, phthalic acid
Dibutyl ester, phosphite, sulfydryl acid esters, mica powder, carbon dust, three monooctyl esters and benzotriazole are put into reaction kettle, spare；
Reaction kettle heating temperature in S3, regulating step S2 is 125 DEG C, mixing speed 2800r/min, and the reaction time is
25 minutes, add benzotriazole, salicylate, aluminium hydroxide, inorganic nano material, ethoxylated alkyl polyamines, alkyl three
Methyl quaternary ammonium, antistatic agent, silane coupling agent, methyl-silicone oil, antibacterial agent, toughener, and 140 DEG C are warming up to, it stirs at low speed anti-
It answers 20 minutes, discharging obtains Multifunctional plastic additive finished product.
Embodiment 5:
A kind of Multifunctional plastic additive provided in this embodiment, including the raw material matched according to following number: glass powder
13 parts, 20 parts of dibutyl phthalate, synthesis 15 parts of vegetable esters, 10 parts of dioctyl phthalate, 12 parts of phosphite, mercapto
9.8 parts of base acid esters, 7 parts of mica powder, 7 parts of carbon dust, 4 parts of three monooctyl ester, 15 parts of benzotriazole, 25 parts of salicylate, aluminium hydroxide
10 parts, 3-5 parts of inorganic nano material, 15 parts of ethoxylated alkyl polyamines, 20 parts of alkyl trimethyl quaternary ammonium, 9 parts of antistatic agent,
3 parts of silane coupling agent, 5 parts of methyl-silicone oil, 0.18 part of antibacterial agent, 0.8 part of toughener.
Further, the inorganic nano material is graphene-based inorganic nano material, nano aluminum base oxide, aluminium rice carbonic acid of receiving
The compounding of calcium, simple particle size range 70nm.
Further, the antibacterial agent is the antibacterial agent prepared by inorganic solvent.
The present embodiment also discloses a kind of preparation method of Multifunctional plastic additive, which is characterized in that specific step is as follows:
S1, raw material is weighed according to formula, by inorganic nano material grinding distribution；
S2, raw material is weighed according to formula, by dioctyl phthalate, synthesis vegetable esters, dibutyl phthalate, Asia
Phosphate, sulfydryl acid esters, mica powder, glass powder, carbon dust, three monooctyl esters and benzotriazole are put into reaction kettle, spare；
Reaction kettle heating temperature in S3, regulating step S2 is 124 DEG C, mixing speed 2650r/min, and the reaction time is
24 minutes, add benzotriazole, salicylate, aluminium hydroxide, inorganic nano material, ethoxylated alkyl polyamines, alkyl three
Methyl quaternary ammonium, antistatic agent, silane coupling agent, methyl-silicone oil, antibacterial agent, toughener, and 138 DEG C are warming up to, it stirs at low speed anti-
It answers 18 minutes, discharging obtains Multifunctional plastic additive finished product.
Verified, above-described embodiment is due to using addition antioxidant material, antistatic raw material, raw bactericidal material in inorganic filler
So that manufactured plastic additive has anti-oxidant, antistatic, sterilization and can be improved intensity again convenient for plasticity, it is convenient also to have
The function of preservation.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention, for this field skill
For art personnel, it is clear that invention is not limited to the details of the above exemplary embodiments, and without departing substantially from spirit of the invention or
In the case where essential characteristic, the present invention can be realized in other specific forms.Therefore, in all respects, should all incite somebody to action
Embodiment regards exemplary as, and is non-limiting, the scope of the present invention by appended claims rather than on state
Bright restriction, it is intended that including all changes that fall within the meaning and scope of the equivalent elements of the claims in the present invention
It is interior.Any label in claim should not be construed as limiting the claims involved.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (7)
1. a kind of Multifunctional plastic additive, which is characterized in that the raw material including being matched by following parts by weight is made: glass powder
8-13 parts, 15-20 parts of dibutyl phthalate, synthesis vegetable esters 10-15 parts, 8-10 parts of dioctyl phthalate, phosphorous
10-12 parts of hydrochlorate, 8-10 parts of sulfydryl acid esters, 5-8 parts of mica powder, 4-7 parts of carbon dust, 2-4 parts of three monooctyl ester, benzotriazole 10-15
Part, 20-25 parts of salicylate, 4-10 parts of aluminium hydroxide, 2-5 parts of inorganic nano material, 12-15 parts of ethoxylated alkyl polyamines,
15-20 parts of alkyl trimethyl quaternary ammonium, 5-10 parts of antistatic agent, 1-3 parts of silane coupling agent, 2-6 parts of methyl-silicone oil, antibacterial agent 0.1-
0.2 part and toughener 0.5-1 parts.
2. a kind of Multifunctional plastic additive according to claim 1, which is characterized in that including what is matched according to following number
Raw material: 10-13 parts of glass powder, 18-20 parts of dibutyl phthalate, vegetable esters 12-15 parts of synthesis, phthalic acid two are pungent
9-10 parts of ester, 11-12 parts of phosphite, 9-10 parts of sulfydryl acid esters, 6-7 parts of mica powder, 5-7 parts of carbon dust, 3-4 parts of three monooctyl ester,
12-15 parts of benzotriazole, 22-25 parts of salicylate, 8-10 parts of aluminium hydroxide, 3-5 parts of inorganic nano material, ethoxylated alkyl
13-15 parts of polyamines, 16-20 parts of alkyl trimethyl quaternary ammonium, 8-10 parts of antistatic agent, 2-3 parts of silane coupling agent, methyl-silicone oil 3-5
Part, 0.15-0.18 parts of antibacterial agent and 0.6-0.8 parts of toughener.
3. a kind of Multifunctional plastic additive according to claim 1 or 2, which is characterized in that the inorganic nano material is
Nano-titanium dioxide, graphene-based inorganic nano material, nano aluminum base oxide, is received in aluminium rice calcium carbonate nano silicon-based oxide
One or more compoundings, simple particle size range 20-80nm.
4. a kind of Multifunctional plastic additive according to claim 1 or 2, which is characterized in that the antibacterial agent is by inorganic
The antibacterial agent of solvent preparation.
5. a kind of Multifunctional plastic additive according to claim 3, which is characterized in that the antibacterial agent is by inorganic solvent
The antibacterial agent of preparation.
6. a kind of preparation method of Multifunctional plastic additive, which is characterized in that specific step is as follows:
S1, raw material is weighed according to formula, by inorganic nano material grinding distribution；
S2, raw material is weighed according to formula, by glass powder, dioctyl phthalate, synthesis vegetable esters, two fourth of phthalic acid
Ester, phosphite, sulfydryl acid esters, mica powder, carbon dust, three monooctyl esters and benzotriazole are put into reaction kettle, spare；
Reaction kettle heating temperature in S3, regulating step S2 is 120-125 DEG C, mixing speed 2500-2800r/min, reaction
Time is 20-25 minutes, and it is more to add benzotriazole, salicylate, aluminium hydroxide, inorganic nano material, ethoxylated alkyl
Amine, alkyl trimethyl quaternary ammonium, antistatic agent, silane coupling agent, methyl-silicone oil, antibacterial agent, toughener, and it is warming up to 135-140
DEG C, reaction 10-20 minutes is stirred at low speed, discharging obtains Multifunctional plastic additive finished product.
7. a kind of preparation method of Multifunctional plastic additive according to claim 6, which is characterized in that in step sl without
Machine nano material select nano-titanium dioxide, nano silicon-based oxide, graphene-based inorganic nano material, nano aluminum base oxide,
Receive one of aluminium rice calcium carbonate or a variety of compoundings, simple particle size range 20-80nm.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112300623A (en) * | 2020-11-06 | 2021-02-02 | 南京同溧晶体材料研究院有限公司 | Coating additive and preparation method thereof |
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| CN105440221A (en) * | 2015-11-24 | 2016-03-30 | 安徽世林照明股份有限公司 | Plastic additive and preparation method thereof |
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Application publication date: 20190531 |