CN109820002A - It is a kind of for controlling the insecticide composition of grain storage pest population - Google Patents

It is a kind of for controlling the insecticide composition of grain storage pest population Download PDF

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Publication number
CN109820002A
CN109820002A CN201910217063.5A CN201910217063A CN109820002A CN 109820002 A CN109820002 A CN 109820002A CN 201910217063 A CN201910217063 A CN 201910217063A CN 109820002 A CN109820002 A CN 109820002A
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grain storage
methoprene
decis
controlling
composition
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CN201910217063.5A
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Chinese (zh)
Inventor
邓业成
邓志勇
骆海玉
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Guangxi Normal University
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Guangxi Normal University
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Abstract

The invention discloses a kind of for controlling the insecticide composition of grain storage pest population, it contains active constituent star anise oil, decis and methoprene, the mass ratio of the star anise oil, decis and methoprene is 1:1-4:4-20, and amount of application of the star anise oil in grain storage is >=0.25mg/kg, amount of application of the decis in grain storage is 0.25-1mg/kg, and amount of application of the methoprene in grain storage is 1-5mg/kg.Insecticide composition of the invention is based on three kinds of methoprene, decis and star anise oil medicaments the characteristics of preventing and treating in terms of grain storage pest, the advantages of making full use of three kinds of medicaments, overcome its deficiency, three is scientifically and rationally combined, has the function of synergy, for grain storage pest controlling, especially to the Population Control of the coleopteras such as red flour beetle and Lepidoptera grain storage pest, existing good quick-acting, it can achieve the purpose that control pest damage for a long time again, safety nuisance free has important application and popularization value.

Description

It is a kind of for controlling the insecticide composition of grain storage pest population
Technical field
The present invention relates to technical field of pesticide compounding more particularly to a kind of for controlling the insecticide group of grain storage pest population Close object.
Background technique
Methoprene (methoprene) is a kind of juvenile hormone class insect growth tune developed by the U.S. the 1970s Save agent.As a kind of insecticide registered with biochemical pesticide, methoprene can control the growth and development of pest, cause pest development different It is often dead.Methoprene insecticidal spectrum is wide, to including that the various insects such as Lepidoptera, Diptera, coleoptera, Homoptera are effective, can use In the prevention and treatment of the pests such as stored product insect, sanitary insect pest, animal body surface pest, it may also be used for silkworm improves it and produces silk amount.Alkene worm Ester belongs to green non-pollution insecticide, less toxic or nontoxic to higher mammal, is evaluated as by FAO (Food and Agriculture Organization of the United Nation) and the World Trade Organization The insecticide harmless to public health, the U.S. also provide to detect it from residue limits when for grain storage pest controlling.Beauty State started to be applied to grain storage pest controlling in 1988, was then used widely in terms of grain storage pest controlling.The medicine When agent is used for grain storage pest controlling, since it has superior control effect to pest offspring flocks quantity, so as to greatly prolong Long drug effect phase, longer term control harm of the pest to grain storage.
Decis is a kind of pyrethroid insecticides, and insecticidal spectrum is wide, and effect is fast, and efficiently, residual toxicity is low.From 20 After the advent of century 70, be widely used in agricultural, health and grain storage pest prevention and treatment, on grain storage pest controlling have compared with Long applicating history has good control efficiency to Lepidoptera and coleoptera grain storage pest, is that a kind of excellent grain storage pest is anti- Control medicament.Decis mainly plays insecticidal action and tagging with stomach toxicity, can rapidly kill pest after application, controls worm Evil loss.
Star anise oil is that a kind of plants essential oil obtained is extracted from Illicillm Verum Fruit, research shows that the essential oil pair A variety of grain storage pests have very strong contact and fumigating insect killing action.The essential oil is safe and non-toxic, and has volatility, wears in grain storage Saturating ability is strong, can enter polypide by insect body wall and tracheal system and play insecticidal action, desinsection is thorough.These features show The essential oil has potential application on grain storage pest controlling.
Although methoprene, decis and star anise oil have many advantages, such as in terms of preventing and treating grain storage pest, in list It also shows when solely using compared with big limitation.Although methoprene can control the next-generation population quantity of pest, drug effect phase well It is long, but there is no control effect to contemporary larva, thus cause serious harm of the contemporary larva to grain storage.Decis and octagonal fennel It is poor to next-generation pest population quantity control effect although essential oil has good control action to contemporary larva, thus make At the big generation of pest of lower generation, final result is that the drug effect phase is short, needs repeatedly to be administered the harm that just can be effectively controlled pest.
Currently, also not about by decis and methoprene combined application, or by star anise oil, decis With the report of methoprene combined application.
Summary of the invention
It is an object of the invention to: in view of the above problems, a kind of existing good quick-acting is provided, and can be long-term Control pest damage, safety nuisance free, the insecticide for being used to control grain storage pest population with important application and popularization value Composition.
In order to achieve the above-mentioned object of the invention, The technical solution adopted by the invention is as follows:
It is a kind of for controlling the insecticide composition of grain storage pest population, containing active constituent decis and methoprene, The mass ratio of the decis and methoprene is 1-4:4-20.
Preferably, it is a kind of for controlling the insecticide composition of grain storage pest population, contain active constituent Chinese anise essence Oil, decis and methoprene, the mass ratio of the star anise oil, decis and methoprene are 1:1-4:4-20.
Preferably, the mass percentage that the decis and methoprene account for composition altogether is 1-85%.
Preferably, the mass percentage that the decis and methoprene account for composition altogether is 10-50%.
Preferably, the mass percentage that the star anise oil, decis and methoprene account for composition altogether is 1- 85%.
Preferably, the mass percentage that the star anise oil, decis and methoprene account for composition altogether is 10- 50%.
Preferably, amount of application of the star anise oil in grain storage is >=0.25mg/kg, decis is in grain storage Amount of application be 0.25-1mg/kg, amount of application of the methoprene in grain storage be 1-5mg/kg.
Insecticide composition of the invention can be used directly, be made using dosage form or as use form prepared therefrom With preferably, formulation of insecticides is preferably spray in the present invention, the solvent of spray can be ethyl alcohol and/or acetone.
Preferably, the insecticide composition is in the application for preventing or controlling grain storage pest population.
Preferably, the grain storage pest population is coleoptera and/or Lepidoptera class pest population.
In conclusion by adopting the above-described technical solution, the beneficial effects of the present invention are:
Insecticide composition of the invention is based on methoprene, three kinds of medicaments of decis and star anise oil are stored up in prevention and treatment The characteristics of in terms of grain pest, overcomes its deficiency, scientifically and rationally combines three one the advantages of making full use of three kinds of medicaments It rises, has the function of synergy, be used for grain storage pest controlling, especially to the coleopteras such as red flour beetle and Lepidoptera grain storage evil The Population Control of worm, existing good quick-acting, and can achieve the purpose that control pest damage for a long time, safety nuisance free has Important application and popularization value.
Specific embodiment
To make the objectives, technical solutions, and advantages of the present invention more comprehensible, preferred embodiment is enumerated below, to this hair Bright further description.However, it is necessary to illustrate, many details listed in specification are used for the purpose of making reader to this The one or more aspects of invention have a thorough explanation, also may be implemented even without these specific details of the invention These aspects.
One, embodiment is prepared
Embodiment 1
It is a kind of for controlling the insecticide composition of grain storage pest population, contain decis 4%, methoprene 80% and third Ketone 16% is prepared into spray after mixing.
Embodiment 2
It is a kind of for controlling the insecticide composition of grain storage pest population, containing decis 0.3%, methoprene 0.7%, Ethyl alcohol 15% and acetone 84%, are prepared into spray after mixing.
Embodiment 3
It is a kind of for controlling the insecticide composition of grain storage pest population, contain decis 4%, methoprene 6% and second Alcohol 90% is prepared into spray after mixing.
Embodiment 4
It is a kind of for controlling the insecticide composition of grain storage pest population, containing decis 10%, methoprene 40% and Acetone 50% is prepared into spray after mixing.
Embodiment 5
It is a kind of for controlling the insecticide composition of grain storage pest population, star anise oil 1%, decis 1%, alkene Worm ester 8% and acetone 90%, are prepared into spray after mixing.
Embodiment 6
It is a kind of for controlling the insecticide composition of grain storage pest population, star anise oil 5%, decis 20%, Methoprene 25% and ethyl alcohol 50%, are prepared into spray after mixing.
Embodiment 7
It is a kind of for controlling the insecticide composition of grain storage pest population, star anise oil 0.1%, decis 0.3%, methoprene 0.6%, ethyl alcohol 15% and acetone 84%, are prepared into spray after mixing.
Embodiment 8
It is a kind of for controlling the insecticide composition of grain storage pest population, star anise oil 1%, decis 4%, alkene Worm ester 80% and ethyl alcohol 15%, are prepared into spray after mixing.
Two, controlling experiment
1 methoprene, decis and star anise oil composition is tested to test the inhibiting effect of granary pest
1, test method
(1) medicament: 92% methoprene crude oil, 98% decis original powder
(2) test worm: red flour beetle adult
(3) 1 setting of test:
Methoprene 1mg/kg+ decis (0.25,0.5,1) mg/kg;
Methoprene 2.5mg/kg+ decis (0.25,0.5,1) mg/kg;
Methoprene 5mg/kg+ decis (0.25,0.5,1) mg/kg.
Methoprene 1mg/kg herein, refers to: dosage of the methoprene in 1kg grain storage is 1mg, other are similar.
2 setting of test: star anise oil 0.25mg/kg+ decis (0.25,0.5) mg/kg+ methoprene (1,2.5, 5)mg/kg。
(4) processing method: weighing 20g wholemeal and be fitted into 250mL triangular flask, and 1mL acetone medical fluid (control acetone is added Instead of), it mixes.It is followed by adult 30 into emergence one week or so completely to solvent volatilization.Adult worms producting eggs remove after 10 days, to children Worm counts high instar larvae number when being developed to advanced age;F1 generation adult quantity is counted after next-generation adult eclosion.Raising temperature 30 ± 1 DEG C, RH75%.Every processing is repeated 3 times.Population inhibiting rate is calculated as follows:
Population inhibiting rate (%)=(control F1 generation is at borer population-processing F1 generation at borer population) ÷ control F1 generation is at borer population × 100
2, test results and analysis
2.1 methoprenes and decis composition are to granary pest inhibiting effect (being shown in Table 1)
1 methoprene of table is with decis composition to the inhibiting effect of granary pest
As shown in Table 1, when decis+methoprene=(0.5-2)+(1-5) mg/kg, composition is to granary pest Inhibiting rate reach 68.76-100%, high instar larvae decline rate reaches 67.50-100%, has to high instar larvae and lower generation population Good control action.When decis+methoprene=0.25+ (2.5-5) mg/kg, although reaching to population inhibiting rate 93.98-100% has good control action to population of lower generation, but because contemporary larva quantity (handles high instar larvae quantity greatly For 120.7-122 head, compareing high instar larvae quantity is 173.3.Handle high instar larvae decline rate and there was only 29.60-30.35%), It will cause the heavy losses to grain storage.
2.2 methoprenes, decis and star anise oil composition are to granary pest inhibiting effect (being shown in Table 2)
The inhibiting effect of 2 methoprene of table, decis and star anise oil composition to granary pest
Note: A- star anise oil, B- decis, C- methoprene.
Table 2 the result shows that, the third active constituent Chinese anise essence is added in the composition of two kinds of active components composition After oil, it is significantly improved to the control action of contemporary high instar larvae and lower generation population.As decis+methoprene=(0.25- 0.5) when mg/kg+ (1-5) mg/kg, high instar larvae decline rate is 25.39-73.56%, is 17.47- to population inhibiting rate 100%;And work as star anise oil+decis+methoprene=0.25mg/kg+ (0.25-0.5) mg/kg+ (1-5) mg/kg When, high instar larvae decline rate is increased to 94.57-100%, is increased to 97.63-100% to population inhibiting rate.Illustrate said combination Object has splendid control effect to contemporary high instar larvae and lower generation population.
Therefore in order to guarantee not only there is good control action to contemporary larva, but also it can control the quantity of population of lower generation, in reality Border must assure that concentration of the star anise oil in grain storage reaches 0.25mg/kg or more when applying, and decis is in grain storage Concentration reach 0.25mg/kg or more, concentration of the methoprene in grain storage reaches 1mg/kg or more.Considering cost etc. because Element is respectively >=0.25mg/kg, 0.25-1mg/kg with the concentration of star anise oil, decis and methoprene in grain storage It is more reasonable with 1-5mg/kg.
The Population breeding feelings that 2.3 methoprenes and decis composition normally raise F1 generation adult after red flour beetle adult Condition (is shown in Table 3)
As can be known from Table 3, decis+methoprene composition also has control well to make to red flour beetle F2 for adult With, the F1 generation adult after decis+methoprene=0.5+1mg/kg processing red flour beetle adult is normally raised, to F2 generation at The population inhibiting rate of worm reaches 96.77%.After explanation is handled with the composition, even if next-generation each worm state no longer contacts composition Medicament still has good control effect to granary pest, to achieve the purpose that the long period controls pest damage.
The kind that F1 generation adult is normally raised after 3 decis of table+methoprene=0.5+1mg/kg processing red flour beetle adult Group's breeding situation
In addition, various compositions to red flour beetle adult without killing effect, can speculate that its makees the control of contemporary larva With mainly since star anise oil and decis have caused by direct killing effect red flour beetle ovum or larva.Cause For through the invention the study found that methoprene to red flour beetle ovum or larva without killing effect, mainly by interference larva It pupates or pupa sprouts wings and controls population quantity of lower generation.
2 methoprenes, decis and star anise oil composition are tested to 3 kinds of coleoptera grain storage pest simulation prevention and treatment examinations It tests
1, test method
(1) test worm: red flour beetle adult, lesser grain borer adult, saw-toothed grain beetle adult.
(2) handle: high, medium and low 3 dosage groups and 1 control group is arranged in test, in which:
High dose group: star anise oil+decis+methoprene=0.5mg/kg+1mg/kg+5mg/kg;
Median dose group: star anise oil+decis+methoprene=0.25mg/kg+0.5mg/kg+2.5mg/kg;
Low dose group: star anise oil+decis+methoprene=0.1mg/kg+0.25mg/kg+1mg/kg.
Control group: the solvent acetone of equivalent.
(3) method
0.5kg wheat berry and 0.5kg wholemeal are mixed, is placed in ceramic whiteware disk and shakeouts.With hand-held miniaturised nebuliser by medicine Liquid is uniformly sprayed on mix surface, and then mixture is placed in mixed grain machine, mixes 10min under the revolving speed of 90r/s, makes medicine Agent is mixed well with mixture.It pours out to be placed in ceramic whiteware disk to shakeout again and allows acetone volatilization dry (volatilization about 6h to no acetone smell is Only), it is then charged into 1000mL beaker.Red flour beetle adult, lesser grain borer adult and the saw of access emergence one week or so in beaker It ostomatid adult each 30, is sealed with gauze, is placed under the conditions of 30 ± 1 DEG C of temperature and RH75% and raises.Every processing is repeated 3 times.To Checked respectively for after next-generation adult eclosion 3 kinds of pests at borer population, and calculate population inhibiting rate.
Population inhibiting rate (%)=(control F1 generation is at borer population-processing F1 generation at borer population) ÷ control F1 generation is at borer population × 100
2, test results and analysis
Composition is shown in Table 4 to the inhibiting effect of 3 kinds of pest populations.
The inhibiting effect of 4 methoprene of table, decis and star anise oil composition to 3 kinds of pest populations
As shown in Table 4, high dose group (star anise oil+decis+methoprene=0.5mg/kg+1mg/kg+5mg/ Kg) and median dose group (star anise oil+decis+methoprene=0.25mg/kg+0.5mg/kg+2.5mg/kg) is right Red flour beetle, lesser grain borer and the population of saw-toothed grain beetle inhibiting rate are up to 100%, low dose group (star anise oil+decis+alkene Worm ester=0.1mg/kg+0.25mg/kg+1mg/kg) be respectively to red flour beetle, lesser grain borer and the population of saw-toothed grain beetle inhibiting rate 98.57%, 99.66% and 100%.Illustrate that composition has good control efficiency to 3 kinds of grain storage pests.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art For member, without departing from the principle of the present invention, it can also make several improvements and retouch, these improvements and modifications are also answered It is considered as protection scope of the present invention.

Claims (10)

1. a kind of for controlling the insecticide composition of grain storage pest population, it is characterised in that: contain active constituent decis And methoprene, the mass ratio of the decis and methoprene are 1-4:4-20.
2. according to claim 1 for controlling the insecticide composition of grain storage pest population, it is characterised in that: contain work Property ingredient star anise oil, decis and methoprene, the mass ratio of the star anise oil, decis and methoprene For 1:1-4:4-20.
3. according to claim 1 for controlling the insecticide composition of grain storage pest population, it is characterised in that: the bromine The mass percentage that Cyano chrysanthemate and methoprene account for composition altogether is 1-85%.
4. according to claim 1 for controlling the insecticide composition of grain storage pest population, it is characterised in that: the bromine The mass percentage that Cyano chrysanthemate and methoprene account for composition altogether is 10-50%.
5. according to claim 2 for controlling the insecticide composition of grain storage pest population, it is characterised in that: described eight The mass percentage that erect hypecoum essential oil, decis and methoprene account for composition altogether is 1-85%.
6. according to claim 2 for controlling the insecticide composition of grain storage pest population, it is characterised in that: described eight The mass percentage that erect hypecoum essential oil, decis and methoprene account for composition altogether is 10-50%.
7. according to claim 2 for controlling the insecticide composition of grain storage pest population, it is characterised in that: described eight Amount of application of the erect hypecoum essential oil in grain storage is >=0.25mg/kg, and amount of application of the decis in grain storage is 0.25-1mg/ Kg, amount of application of the methoprene in grain storage are 1-5mg/kg.
8. according to claim 1 or 2 for controlling the insecticide composition of grain storage pest population, it is characterised in that: institute The insecticide that dosage form is spray can be prepared by stating insecticide composition.
9. according to claim 1 or 2 for controlling the insecticide composition of grain storage pest population, it is characterised in that: institute Insecticide composition is stated in the application for preventing or controlling grain storage pest population.
10. according to claim 9 for controlling the insecticide composition of grain storage pest population, it is characterised in that: described Grain storage pest population is coleoptera and/or Lepidoptera class pest population.
CN201910217063.5A 2019-03-21 2019-03-21 It is a kind of for controlling the insecticide composition of grain storage pest population Pending CN109820002A (en)

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CN115226715A (en) * 2022-07-22 2022-10-25 中国人民解放军海军特色医学中心 Application of attractant composition in insecticide and insecticide

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Application publication date: 20190531