CN109811539A - A kind of antibacterial uvioresistant traffic police subdues the preparation method of Reflection fabric - Google Patents
A kind of antibacterial uvioresistant traffic police subdues the preparation method of Reflection fabric Download PDFInfo
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- CN109811539A CN109811539A CN201910071182.4A CN201910071182A CN109811539A CN 109811539 A CN109811539 A CN 109811539A CN 201910071182 A CN201910071182 A CN 201910071182A CN 109811539 A CN109811539 A CN 109811539A
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Abstract
The invention discloses the preparation methods that a kind of antibacterial uvioresistant traffic police subdues Reflection fabric, specific preparation step are as follows: (1) coating is carried out to the synthetic fiber fabric containing anti-bacterial fibre using inorganic uvioresistant finishing agent, obtain uvioresistant fabrics after dry out solvent；(2) coating is carried out to uvioresistant fabrics after being uniformly mixed reflective resin, strontium aluminate, butyl acetate and curing agent；(3) glass microballoon is pre-processed, is added in the aqueous solution of dodecyl sodium sulfate, dispersing agent after dry, the suspension of coated glass microballon is made after continuously stirring；(4) fabric prepared by step (2) is immersed in the suspension of coated glass microballon, adhesive is added, taken out and roll after immersion, then step is dried in two times, obtains uvioresistant Reflection fabric.Fabric reflecting effect prepared by the present invention is good, it is strong to absorb UV resistance, is provided simultaneously with certain biocidal property.
Description
Technical field
The present invention relates to the preparation methods that a kind of antibacterial uvioresistant traffic police subdues Reflection fabric, and it is reflective to belong to traffic police's uniform
Technical field of material.
Background technique
Reflectorized material, also referred to as retroreflecting material or reflecting material, including reflective membrane, reflective ink, reflector marking
Paint, reflective fabric, reflective leather, reflective fabric and reflection safety sex pilus fabric etc..Its principle is introduced on corresponding material surface
A kind of glass microballoon or the micro- lattice structure of prism of high refractive index, are widely used in traffic mark, License Plate, clothing shoes
Cap, fire-fighting, railway, water transport, mining area etc..Reflective cloth is relatively conventional one of reflectorized material, is mainly used for various reflecting clothes
The production of object, such as the production for traffic police's uniform.
Consider that traffic police's work causes skin injury and sweat that bacterium is easily caused to grow vulnerable to ultraviolet radiation under hot environment
It is raw, and reflective cloth reflective function used in existing traffic police uniform is low and does not usually have biocidal property and uviolresistance, because
This provides the antibacterial uvioresistant traffic police uniform that a kind of reflecting effect is good, absorption UV resistance is provided simultaneously with by force certain biocidal property
Reflection fabric.
Summary of the invention
In view of the above existing problems in the prior art, the present invention provides a kind of antibacterial uvioresistant traffic police to subdue Reflection fabric
Preparation method, prepared fabric reflecting effect is good, it is strong to absorb UV resistance, is provided simultaneously with certain biocidal property.
To achieve the above object, the present invention adopts the following technical scheme:
(1) synthetic fiber fabric containing 20~30wt% anti-bacterial fibre is carried out using inorganic uvioresistant finishing agent
Coating, after dry out solvent uvioresistant fabrics；
(2) step (1) preparation is resisted after being uniformly mixed reflective resin, strontium aluminate, butyl acetate and curing agent
Ultraviolet light fabric carries out coating；
(3) glass microballoon that parts by weight are 0.5~0.8 times of the reflective resin is pre-processed, is added to after dry and accounts for institute
State reflective 10% mass fraction of weight resin be 60~75% sodium dodecyl sulfate aqueous solution, account for the reflective weight resin
In the aqueous dispersant that 8% mass fraction is 10~20%, 3~5h is then continuously stirred, the outstanding of coated glass microballon is made
Supernatant liquid；
(4) fabric prepared by step (2) is immersed in the suspension of coated glass microballon, addition accounts for the reflective resin
The adhesive of weight 12% takes out and rolls after impregnating 1~2d, and then step is dried in two times, and it is anti-to obtain uvioresistant
Smooth surface material.
As the further improvement of invention, the synthetic fiber fabric is polyester fabric.
As the further improvement of invention, the anti-bacterial fibre is copper modified polyester fiber.
As the further improvement of invention, the inorganic uvioresistant finishing agent includes the raw material of following parts by weight:
21.5~26.5 parts of nanometer Zinc oxide powders, 21.5~26.5 parts of nano-titanium dioxide powders, 65~80 parts of distilled water, 55~65
Part dehydrated alcohol.
As the further improvement of invention, the coating layer thickness in the step (1), step (2) is 150~250 μm.
As the further improvement of invention, step (4) described drying steps specifically: fabric is first placed in ventilation nature
Sunning to water content is 50~60%, then with drying removal residual moisture at 60 DEG C of dryer.
As the further improvement of invention, each weight of material part in step (2) are as follows: 45~55 parts of reflective resins, 2.7~
3.3 parts of strontium aluminates, 3.6~4.4 parts of butyl acetates, 4.5~5.5 parts of curing agent.
As the further improvement of invention, the reflective resin is acrylic resin；The curing agent is solid for amino resins
Agent.
As the further improvement of invention, step (3) described preprocessing process are as follows: by weight be the reflective resin 0.5
~0.8 times of glass microballoon is successively in 0.5% sodium hydrate aqueous solution, 1.0% ammonium persulfate aqueous solution, 2.0% stannous chloride
With 1~2h is continuously stirred in 6.0% mixed in hydrochloric acid aqueous solution, and be all washed with distilled water twice in every step.
As the further improvement of invention, 3~4 parts by weight mass fractions are also added into aqueous solution described in step (3)
For 1.0~2.0% aqueous isopropanol.
The present invention has the advantage that compared with prior art
1, the present invention is using the stronger polyester fabric of ultraviolet-resistent property itself as cloth base, while having both wearability and comfort；It washs
The copper modified polyester fiber added in synthetic fibre fabric has stronger redox property, and copper ion penetrating cell film enters intracellular
It when portion, can react with protein group, destroy the activity of cell synzyme, make cell loss schizogamy ability and dead
It dies, to reach restraining and sterilizing bacteria purpose.
2, the present invention uses inorganic uvioresistant finishing agent, nontoxic, environmentally protective, while inorganic uvioresistant
Finishing agent is mainly by forming the stronger nanometer Zinc oxide powder of ultraviolet absorption ability and nano-titanium dioxide powder, Ke Yiqiang
Change the anti-ultraviolet property of fabric.
3, the present invention first by acrylic resin and strontium aluminate etc. with reflection action by curing agent to antibacterial fabric into
Row coating, resin transparency after solidification is good, brightness is high, heat-resist, keeps the Reflection fabric reflective of preparation more preferable.
4, the present invention first carries out coating film treatment to glass microballoon before planting glass microballoon onto polyester fabric, and is plating
Alkali cleaning, roughening, sensitized treatment first are carried out to glass microballoon before film, effectively enhance coating effects；Simultaneously by by terylene face
Material is immersed in the coated glass microballon suspension containing adhesive, makes coated glass microballon that can effectively be implanted to polyester fabric
On, it is reliable that method is simple, being capable of save the cost.
5, the mode that the present invention takes first natural drying to Tumble Dry again after impregnating polyester fabric removes internal water
Part, enable adhesive that first glass microballoon to be bonded on polyester fabric during natural drying, then in drying machine drying
It is fixed in the process, temperature is higher when avoiding directly drying causes adhesive declines.
6, antibacterial uvioresistant traffic police prepared by the present invention subdues Reflection fabric, has preferable reflecting effect, absorbs purple
Outside line ability, and have certain biocidal property, while can also make the function of Reflection fabric by the way that hydrophobing agent is added during the preparation process
Property it is unaffected after continuous washing, therefore have preferable market application prospect.
Specific embodiment
Below with reference to embodiment, the present invention will be described in detail, it is to be understood that protection scope of the present invention is not had
The limitation of body embodiment.
Embodiment 1
A kind of antibacterial uvioresistant traffic police subdues the preparation method of Reflection fabric, specific preparation step are as follows:
(1) use by 25 parts by weight nanometer Zinc oxide powders, 25 parts by weight nano-titanium dioxide powders, 80 parts of distilled water,
The inorganic uvioresistant finishing agent of 65 parts of dehydrated alcohols composition to containing 30wt% from Huzhou pearl excitability rice material scientific and technological development
The polyester fabric for the copper modified polyester fiber that the specification of Co., Ltd's purchase is 1.5D × 38mm carries out coating, and coating layer thickness is
200 μm, uvioresistant fabrics are obtained after dry out solvent；
(2) by 50 parts by weight propylene acid resins, 3 parts by weight strontium aluminates, 4 parts by weight acetic acid butyl esters and 5 parts by weight amino trees
Rouge curing agent carries out coating to the uvioresistant fabrics of step (1) preparation after being uniformly mixed, and coating layer thickness is 200 μm；
(3) by parts by weight be 0.8 times of the reflective resin glass microballoon successively 0.5% sodium hydrate aqueous solution,
2h is continuously stirred in 1.0% ammonium persulfate aqueous solution, 2.0% stannous chloride and 6.0% mixed in hydrochloric acid aqueous solution, and in every step
It is all washed with distilled water twice, it is water-soluble that the dodecyl sodium sulfate that 5 parts by weight mass fractions are 60~75% is added to after dry
The isopropanol water that the aqueous dispersant and 4 parts by weight mass fractions that liquid, 4 parts by weight mass fractions are 10~20% are 2.0%
In solution, 5h is then continuously stirred, the suspension of coated glass microballon is made；
(4) fabric prepared by step (2) is immersed in the suspension of coated glass microballon, 6 parts by weight of binder is added,
It takes out and rolls after immersion 2d, it is 50~60% that fabric is first placed in ventilation natural drying to water content, then uses dryer 60
Drying removal residual moisture, obtains uvioresistant Reflection fabric at DEG C.
Embodiment 2
A kind of antibacterial uvioresistant traffic police subdues the preparation method of Reflection fabric, specific preparation step are as follows:
(1) use by 25 parts by weight nanometer Zinc oxide powders, 25 parts by weight nano-titanium dioxide powders, 80 parts of distilled water,
The inorganic uvioresistant finishing agent of 65 parts of dehydrated alcohols composition to containing 30wt% from Huzhou pearl excitability rice material scientific and technological development
The polyester fabric for the copper modified polyester fiber that the specification of Co., Ltd's purchase is 1.5D × 38mm carries out coating, and coating layer thickness is
200 μm, uvioresistant fabrics are obtained after dry out solvent；
(2) by 50 parts by weight propylene acid resins, 3 parts by weight strontium aluminates, 4 parts by weight acetic acid butyl esters and 5 parts by weight amino trees
Rouge curing agent carries out coating to the uvioresistant fabrics of step (1) preparation after being uniformly mixed, and coating layer thickness is 200 μm；
(3) by parts by weight be 0.8 times of the reflective resin glass microballoon successively 0.5% sodium hydrate aqueous solution,
2h is continuously stirred in 1.0% ammonium persulfate aqueous solution, 2.0% stannous chloride and 6.0% mixed in hydrochloric acid aqueous solution, and in every step
It is all washed with distilled water twice, it is water-soluble that the dodecyl sodium sulfate that 5 parts by weight mass fractions are 60~75% is added to after dry
In the aqueous dispersant that liquid and 4 parts by weight mass fractions are 10~20%, 5h is then continuously stirred, coated glass microballon is made
Suspension；
(4) fabric prepared by step (2) is immersed in the suspension of coated glass microballon, 6 parts by weight of binder is added,
It takes out and rolls after immersion 2d, it is 50~60% that fabric is first placed in ventilation natural drying to water content, then uses dryer 60
Drying removal residual moisture, obtains uvioresistant Reflection fabric at DEG C.
Embodiment 3
A kind of antibacterial uvioresistant traffic police subdues the preparation method of Reflection fabric, specific preparation step are as follows:
(1) use by 22 parts by weight nanometer Zinc oxide powders, 22 parts by weight nano-titanium dioxide powders, 65 parts of distilled water,
The inorganic uvioresistant finishing agent of 55 parts of dehydrated alcohols composition to containing 20wt% from Huzhou pearl excitability rice material scientific and technological development
The polyester fabric for the copper modified polyester fiber that the specification of Co., Ltd's purchase is 1.5D × 38mm carries out coating, and coating layer thickness is
200 μm, uvioresistant fabrics are obtained after dry out solvent；
(2) by 45 parts by weight propylene acid resins, 2.7 parts by weight strontium aluminates, 3.6 parts by weight acetic acid butyl esters and 4.5 parts by weight
Amino resin curing agents carry out coating, coating layer thickness 200 to the uvioresistant fabrics of step (1) preparation after being uniformly mixed
μm；
(3) by parts by weight be 0.6 times of the reflective resin glass microballoon successively 0.5% sodium hydrate aqueous solution,
2h is continuously stirred in 1.0% ammonium persulfate aqueous solution, 2.0% stannous chloride and 6.0% mixed in hydrochloric acid aqueous solution, and in every step
It is all washed with distilled water twice, the dodecyl sodium sulfate water that 4.5 parts by weight mass fractions are 60~75% is added to after dry
The isopropyl that the aqueous dispersant and 4 parts by weight mass fractions that solution, 3.6 parts by weight mass fractions are 10~20% are 2.0%
In alcohol solution, 5h is then continuously stirred, the suspension of coated glass microballon is made；
(4) fabric prepared by step (2) is immersed in the suspension of coated glass microballon, the bonding of 5.4 parts by weight is added
Agent is taken out and is rolled after impregnating 2d, and it is 50~60% that fabric is first placed in ventilation natural drying to water content, then uses dryer
Drying removal residual moisture, obtains uvioresistant Reflection fabric at 60 DEG C.
Antibacterial uvioresistant traffic police prepared by Example 1 to 3 subdues Reflection fabric sample 5cm × 5cm piece sample, presses respectively
According to the standard of AATCC183, GB/T20944.3-2008, GB/T3979-2008, to print ultraviolet ray transmissivity, reflectivity and suppression
Bacterium rate is tested, and has anti-bacterial fibre and untreated terylene print does control group with unmixed, while according to identical
Standard and method test washing 20 times prints, as a result as shown in Table 1 and Table 2 respectively.
Print performance before table 1 is washed
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Control group | |
| Average UV line transmitance (%) | 0.85 | 0.86 | 0.89 | 6.8 |
| Reflectivity (%) | 98.5 | 98 | 98.5 | 0 |
| Escherichia coli bacteriostasis rate (%) | 76.5 | 76.4 | 76.4 | 60 |
| Candida albicans bacteriostasis rate (%) | 88 | 88.2 | 84.5 | 54 |
Print performance after table 2 is washed 20 times
| Embodiment 1 | Embodiment 2 | Embodiment 3 | |
| Average UV line transmitance (%) | 0.85 | 1.08 | 0.89 |
| Reflectivity (%) | 98.4 | 97.4 | 98.5 |
| Escherichia coli bacteriostasis rate (%) | 76.5 | 76.3 | 76.5 |
| Candida albicans bacteriostasis rate (%) | 88 | 87.6 | 84.3 |
According to the result of table 1 as can be seen that antibacterial uvioresistant traffic police prepared by embodiment 1 to 3 subdues Reflection fabric tool
Have it is preferable absorb UV resistance and reflectivity, referring concurrently to the evaluation criterion of GB/T20944.3-2008, (sample is to large intestine
Bacteriostasis rate >=70% of bacillus, sample have antibiotic property effect；Sample has bacteriostasis rate >=60% of Candida albicans, sample
Antibiotic property effect；), there are also preferable antibiotic properties for embodiment.In addition, the result of comparison Tables 1 and 2 can be seen that washing 20 times
The fabric that afterwards prepared by embodiment 1 and embodiment 3 absorbs UV resistance, reflectivity and anti-microbial property and is substantially unaffected, and real
The properties for applying example 2 are affected to some extent compared to embodiment 1 and embodiment 3, it is seen that hydrophobing agent is added and is conducive to raising face
Material keeps functional stabilization.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit and essential characteristics of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.In addition, it should be understood that although this specification is described in terms of embodiments, but it is not each
Embodiment only contains an independent technical solution, this narrating mode of specification only for clarity, this field skill
Art personnel should consider the specification as a whole, and the technical solutions in the various embodiments may also be suitably combined, form ability
The other embodiments that field technique personnel are understood that.
Claims (10)
1. the preparation method that a kind of antibacterial uvioresistant traffic police subdues Reflection fabric, which is characterized in that specific preparation step are as follows:
(1) synthetic fiber fabric containing 20~30wt% anti-bacterial fibre is applied using inorganic uvioresistant finishing agent
Layer, uvioresistant fabrics are obtained after dry out solvent；
(2) to the uvioresistant of step (1) preparation after reflective resin, strontium aluminate, butyl acetate and curing agent being uniformly mixed
Line fabric carries out coating；
(3) glass microballoon that parts by weight are 0.5~0.8 times of the reflective resin is pre-processed, be added to after dry account for it is described anti-
10% mass fraction of photopolymer resin weight be 60~75% sodium dodecyl sulfate aqueous solution, account for the reflective weight resin 8%
In the aqueous dispersant that mass fraction is 10~20%, 3~5h is then continuously stirred, the suspension of coated glass microballon is made
Liquid；
(4) fabric prepared by step (2) is immersed in the suspension of coated glass microballon, addition accounts for the reflective weight resin
12% adhesive takes out and rolls after impregnating 1~2d, and then step is dried in two times, obtains uvioresistant reflective surface
Material.
2. a kind of antibacterial uvioresistant traffic police according to claim 1 subdues the preparation method of Reflection fabric, feature exists
In the synthetic fiber fabric is polyester fabric.
3. a kind of antibacterial uvioresistant traffic police according to claim 1 subdues the preparation method of Reflection fabric, feature exists
In the anti-bacterial fibre is copper modified polyester fiber.
4. a kind of antibacterial uvioresistant traffic police according to claim 1 subdues the preparation method of Reflection fabric, feature exists
In the inorganic uvioresistant finishing agent includes the raw material of following parts by weight: 21.5~26.5 parts of nanometer Zinc oxide powders,
21.5~26.5 parts of nano-titanium dioxide powders, 65~80 parts of distilled water, 55~65 parts of dehydrated alcohols.
5. a kind of antibacterial uvioresistant traffic police according to claim 1 subdues the preparation method of Reflection fabric, feature exists
In the coating layer thickness in the step (1), step (2) is 150~250 μm.
6. a kind of antibacterial uvioresistant traffic police according to claim 1 subdues the preparation method of Reflection fabric, feature exists
In step (4) described drying steps specifically: it is 50~60% that fabric, which is first placed in ventilation natural drying to water content, so
Afterwards with drying removal residual moisture at 60 DEG C of dryer.
7. a kind of antibacterial uvioresistant traffic police according to claim 1 subdues the preparation method of Reflection fabric, feature exists
In each weight of material part in step (2) are as follows: 45~55 parts of reflective resins, 2.7~3.3 parts of strontium aluminates, 3.6~4.4 parts of acetic acid fourths
Ester, 4.5~5.5 parts of curing agent.
8. a kind of antibacterial uvioresistant traffic police according to claim 7 subdues the preparation method of Reflection fabric, feature exists
In the reflective resin is acrylic resin；The curing agent is amino resin curing agents.
9. a kind of antibacterial uvioresistant traffic police according to claim 1 subdues the preparation method of Reflection fabric, feature exists
In step (3) described preprocessing process are as follows: the glass microballoon that weight is 0.5~0.8 times of the reflective resin successively exists
In 0.5% sodium hydrate aqueous solution, 1.0% ammonium persulfate aqueous solution, 2.0% stannous chloride and 6.0% mixed in hydrochloric acid aqueous solution
1~2h is continuously stirred, and is all washed with distilled water twice in every step.
10. a kind of antibacterial uvioresistant traffic police according to claim 1 subdues the preparation method of Reflection fabric, feature exists
In, be also added into aqueous solution described in step (3) 3~4 parts by weight mass fractions be 1.0~2.0% aqueous isopropanol.
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