CN109811014A - A method of feed addictive sodium humate is produced using bioactivity zymotechnic - Google Patents
A method of feed addictive sodium humate is produced using bioactivity zymotechnic Download PDFInfo
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- CN109811014A CN109811014A CN201910023997.5A CN201910023997A CN109811014A CN 109811014 A CN109811014 A CN 109811014A CN 201910023997 A CN201910023997 A CN 201910023997A CN 109811014 A CN109811014 A CN 109811014A
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- feed addictive
- bioactivity
- sodium humate
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- enzyme
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Abstract
The present invention relates to sodium humate preparation technical fields, in particular a kind of method using bioactivity zymotechnic production feed addictive sodium humate, the following steps are included: S1, prepare raw material: weathered coal, water, bioactive enzyme, sodium hydroxide, S2, it weighs raw material: using electronic scale respectively, weigh the weathered coal of constant weight respectively according to weight ratio, water, bioactive enzyme, it sodium hydroxide and is respectively put into inside different containers, S3, load weighted weathering enzyme is put into inside pulverizer and is crushed, S4, by smashed weathered coal by belt conveyor make a gift to someone agitating reaction pond and respectively to agitating reaction pond be added water, bioactive enzyme, sodium hydroxide, the regular hour is stirred with certain speed with blender, and guarantee certain temperature, S5, it is heavy that mixture benefit after stirring is piped to Shallow lake pond.For the present invention through design based on environmental type biology enzymatic reaction, sodium humate moisture content of finished products is only 12-15%, greatly improves production efficiency.
Description
Technical field
It is specially a kind of to be added using bioactivity zymotechnic production feed the present invention relates to sodium humate preparation technical field
Add the method for agent sodium humate.
Background technique
Sodium humate is widely used in the animal husbandries such as pig, fowl, plant-eating animal in China, and there is sodium humate convergence to stop
The effect rushing down, promote growth, improving breeding performonce fo animals, in addition sodium humate resource is extensive, cheap, easy to use, effect
Many advantages, such as fruit is obvious and no drug residue, so sodium humate application prospect light is wealthy, sodium humate be with weathered coal, peat and
Lignite is a kind of macromolecular organic monoacid sodium salt with multiple functions that raw material is processed into through special process, and structure compares
It is complicated, it is known that contain phenyl ring, condensed ring and certain heterocycles (such as pyrroles, furans, indoles) in humic acid molecule, between each aromatic rings
There is bridged bond to be connected, there is various functional groups, mainly carboxyl, phenolic group, hydroxyl, methoxyl group, quinonyl etc. on aromatic rings.Sodium humate
Middle humic acid contents on dry basis is more than 75%, is a kind of good veterinary drug and feed addictive for producing green newborn meat and egg production.Tradition
Produce sodium humate technique and raw material composition: 1 ton of raw material, using 1.5-2.2 tons of water, 0.1-0.15 tons of sodium hydroxide, reaction temperature
50-60 DEG C of degree, sedimentation time 24-36 hour, yield rate 55-65%, residue 35-45% out, about 1.4-1.8 tons of wastewater treatment capacity,
PH value 9-10.But traditional production technology, it is impossible to meet the step of the development of today's society, the shortcomings that generation, is wasted
Sewage post-processing energy consumption after raw material production is high, and discharge amount of pollution is larger, and economic benefit is unobvious.
In conclusion the present invention proposes a kind of method using bioactivity zymotechnic production feed addictive sodium humate
To solve problems.
Summary of the invention
The purpose of the present invention is to provide a kind of sides using bioactivity zymotechnic production feed addictive sodium humate
Method, to solve the problems mentioned in the above background technology.
To achieve the above object, the invention provides the following technical scheme:
A method of feed addictive sodium humate is produced using bioactivity zymotechnic, comprising the following steps:
S1 prepares raw material: weathered coal, water, bioactive enzyme, sodium hydroxide；
S2 weighs raw material: using electronic scale respectively, weighs the weathered coal, water, bioactivity of constant weight respectively according to weight ratio
It enzyme, sodium hydroxide and is respectively put into inside different containers；
Load weighted weathering enzyme is put into inside pulverizer and crushes by S3；
S4, by smashed weathered coal by belt conveyor make a gift to someone agitating reaction pond and respectively to agitating reaction pond be added
Water, bioactive enzyme, sodium hydroxide stir the regular hour with blender with certain speed, and guarantee certain temperature；
Mixture benefit after stirring is piped to sedimentation basin by S5, is precipitated a period of time and is utilized alkalinity acidity tester
Detect the pH value of sedimentation basin；
The mixture of sedimentation basin after precipitating, is delivered to scraper drier by delivery pump, obtains feed addictive humic acid by S6
Sodium；
S7, the feed addictive sodium humate after scraper drier is dried weigh process by transmission flood dragon conveying；
Feed addictive sodium humate after weighing is packed into dedicated feed addictive packaging bag, is packaged with baling press by S8
And it is sealed.
Preferably, the S3, pulverizer use vertical-spindle hammer crusher and model PSFL-1000, the pulverizer
Weathered coal size is crushed in 20-30 mesh.
Preferably, the scraper drier uses Rollingscratchboarddrier and model HG-1800A.
Preferably, the S2, electronic scale weigh 1 ton of weight of weathered coal according to weight ratio respectively: 1 ton；Water: 0.8-1 tons；
3-5 kilograms of bioactive enzyme, sodium hydroxide: 15-20 kilograms.
Preferably, the S4, mixing speed is 300r/min and stirs to after being thoroughly mixed, and persistently stirs 1h, temperature:
36-60℃。
Preferably, the S5, the sedimentation time: 20-30 hours, the pH value of the alkalinity acidity tester detection sedimentation basin was 8
Under.
Preferably, the S7, scraper drier are fixed by conduit connection treatment tank and into treatment tank
Portion is added ferrous sulfate and carries out neutralization reaction.
Preferably, DY600*10 meters of the model of the belt conveyor, the model of the blender are as follows: MG-01a is simultaneously
And mounting means is vertical；The model of the delivery pump；500ZLB-7, the model of the transmission flood dragon；hy-006.
Preferably, the vertical-spindle hammer crusher, scraper drier, belt conveyor, blender, delivery pump, transmission flood dragon
Dragon is electrically connected on PLC system control cabinet.
Compared with prior art, the beneficial effects of the present invention are:
1, in the present invention, by design pulverizer using vertical-spindle hammer crusher breaking capacity strong, stable working, operating is reliable,
Noise is small, dust is few, structurally reasonable, and vulnerable part type is few, and operation, maintenance are easy, and compact-sized, occupied area is small.
2, in the present invention, by using Rollingscratchboarddrier material through being pacified in feeding device investment revolving roll
In cylinder mention flitch by material mention top fall, the high speed rotation in cylinder is fallen behind under material, with hot wind contact, take out of
Portion of water moves on to always outlet, is allowed to same hot wind and comes into full contact with, and accelerates drying rate.It is generated simultaneously by direct combustion hot-air furnace
Hot-air enter in cylinder and come into full contact with material, dry material rapidly, then the conveyer discharge through discharge end, to arrive
Up to thermal efficiency height, product aoxidizes and goes bad small, and the scope of application is big, the big feature for the treatment of capacity.
3, in the present invention, by designing based on environmental type biology enzymatic reaction, sodium humate moisture content of finished products is only
12-15%, the yield rate 68-75% of this method, residue 25-32%, and go out this method compared with traditional production technology, corruption is planted
Sour sodium yield rate improves 10-15%, handles waste water raw material saving 95%, and wastewater treatment capacity reduces 45-55%, and product pH value by
Originally 9-10 be reduced to 8 hereinafter, ferrous sulfate usage amount reduce 5%, further to environment while greatly improving production efficiency
It is protected
4, in the present invention, most of high residue high pollution is substituted as catalyst using modern biotechnology organized enzyme by design
Work raw material sodium hydroxide is the beneficial effects are as follows: save raw material；Reduce sewage post-processing energy consumption；Reduce discharge amount of pollution；
It increases economic efficiency；Environment is protected with biotechnology means.
Detailed description of the invention
Fig. 1 is present invention process flowage structure schematic diagram.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments, is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
Referring to Fig. 1, the present invention provides a kind of technical solution:
A method of feed addictive sodium humate is produced using bioactivity zymotechnic, comprising the following steps:
S1 prepares raw material: weathered coal, water, bioactive enzyme, sodium hydroxide；
S2 weighs raw material: using electronic scale respectively, weighs the weathered coal, water, bioactivity of constant weight respectively according to weight ratio
It enzyme, sodium hydroxide and is respectively put into inside different containers；
Load weighted weathering enzyme is put into inside pulverizer and crushes by S3；
S4, by smashed weathered coal by belt conveyor make a gift to someone agitating reaction pond and respectively to agitating reaction pond be added
Water, bioactive enzyme, sodium hydroxide stir the regular hour with blender with certain speed, and guarantee certain temperature；
Mixture benefit after stirring is piped to sedimentation basin by S5, is precipitated a period of time and is utilized alkalinity acidity tester
Detect the pH value of sedimentation basin；
The mixture of sedimentation basin after precipitating, is delivered to scraper drier by delivery pump, obtains feed addictive humic acid by S6
Sodium；
S7, the feed addictive sodium humate after scraper drier is dried weigh process by transmission flood dragon conveying；
Feed addictive sodium humate after weighing is packed into dedicated feed addictive packaging bag, is packaged with baling press by S8
And it is sealed.
The S3, pulverizer crush weathering using vertical-spindle hammer crusher and model PSFL-1000, the pulverizer
Coal size is in 20-30 mesh.
The scraper drier uses Rollingscratchboarddrier and model HG-1800A.
The S2, electronic scale weigh 1 ton of weight of weathered coal according to weight ratio respectively: 1 ton；Water: 0.8-1 tons；Biology is living
Property 3-5 kilograms of enzyme, sodium hydroxide: 15-20 kilograms.
The S4, mixing speed is 300r/min and stirs to after being thoroughly mixed, and persistently stirs 1h, temperature: 36-60 DEG C.
The S5, the sedimentation time: 20-30 hours, the pH value of the alkalinity acidity tester detection sedimentation basin was under 8.
The S7, scraper drier are fixed by conduit connection treatment tank and to sulphur is added inside treatment tank
Sour ferrous progress neutralization reaction.
DY600*10 meters of the model of the belt conveyor, the model of the blender are as follows: MG-01a and the side of installation
Formula is vertical；The model of the delivery pump；500ZLB-7, the model of the transmission flood dragon；hy-006.
The vertical-spindle hammer crusher, scraper drier, belt conveyor, blender, delivery pump, transmission flood dragon are electrical
It is connected on PLC system control cabinet.
Working principle: being powered to PLC system control cabinet, and operation PLC system control cabinet is broken to corresponding vertical shaft hammer
Broken machine, scraper drier, belt conveyor, blender, delivery pump, transmission flood dragon are started, and electronic scale is claimed according to weight
It takes 1 ton to be crushed, when being crushed to size between 20-30 mesh, smashed weathered coal is passed through by skin by belt conveyor
Belt conveyor is made a gift to someone agitating reaction pond and respectively to 0.8-1 ton of water, 3-5 kilograms of biology work are added inside agitating reaction pond
Property enzyme and 15-20 kilograms of sodium hydroxide, while using blender in temperature: between 36-60 DEG C, with 300r/min and stirring extremely
After being thoroughly mixed, 1h is persistently stirred, the mixture benefit after stirring is piped to sedimentation basin, precipitates 20-30 hours and sharp
PH value with alkalinity acidity tester detection sedimentation basin is after precipitating, to be delivered to the mixture of sedimentation basin by delivery pump under 8
Scraper drier obtains feed addictive sodium humate, the feed addictive humic acid after scraper drier is dried
Sodium weighs process by transmission flood dragon conveying, and feed addictive sodium humate is packed into dedicated feed addictive after finally weighing
Packaging bag, remaining waste water air-dried inside scraper drier passes through conduit while be packaged and be sealed with baling press
It connects treatment tank and carries out neutralization reaction to addition ferrous sulfate inside treatment tank, detected with detector,
It is discharged after up to standard, for this Process Design based on environmental type biology enzymatic reaction, sodium humate moisture content of finished products is only 12-
15%, the yield rate 68-75% of this method, residue 25-32%, and go out this method, sodium humate compared with traditional production technology
Yield rate improves 10-15%, handles waste water raw material saving 95%, wastewater treatment capacity reduces 45-55%, and product pH value is by original
9-10 is reduced to 8 hereinafter, the usage amount of ferrous sulfate reduces 5%, further carries out to environment while greatly improving production efficiency
Protection, design is used as catalyst, substitution major part high residue high pollution industrial chemicals hydrogen-oxygen using modern biotechnology organized enzyme
Change sodium the beneficial effects are as follows: saving raw material；Reduce sewage post-processing energy consumption；Reduce discharge amount of pollution；Improve economic effect
Benefit；Environment is protected with biotechnology means.Equipment is put into using Rollingscratchboarddrier material through feeding device rotary simultaneously
In roller, be installed in cylinder mention flitch by material mention top fall, the high speed rotation in cylinder is fallen behind under material, with heat
Wind contact, takes portion of water out of, moves on to outlet always, be allowed to same hot wind and come into full contact with, and accelerates drying rate.Simultaneously by straight
The hot-air that combustion hot-blast stove generates enters in cylinder to be come into full contact with material, dries material rapidly, then through the conveying of discharge end
Machine discharge, to reach thermal efficiency height, product aoxidizes and goes bad small, and the scope of application is big, the big feature for the treatment of capacity and pulverizer
Strong, the stable working using vertical-spindle hammer crusher breaking capacity, operating is reliable, noise is small, dust is few, structurally reasonable, vulnerable part
Type is few, and operation, maintenance are easy, and compact-sized, occupied area is small.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (9)
1. a kind of method using bioactivity zymotechnic production feed addictive sodium humate, which is characterized in that including following
Step:
S1 prepares raw material: weathered coal, water, bioactive enzyme, sodium hydroxide；
S2 weighs raw material: using electronic scale respectively, weighs the weathered coal, water, bioactivity of constant weight respectively according to weight ratio
It enzyme, sodium hydroxide and is respectively put into inside different containers；
Load weighted weathering enzyme is put into inside pulverizer and crushes by S3；
S4, by smashed weathered coal by belt conveyor make a gift to someone agitating reaction pond and respectively to agitating reaction pond be added
Water, bioactive enzyme, sodium hydroxide stir the regular hour with blender with certain speed, and guarantee certain temperature；
Mixture benefit after stirring is piped to sedimentation basin by S5, is precipitated a period of time and is utilized alkalinity acidity tester
Detect the pH value of sedimentation basin；
The mixture of sedimentation basin after precipitating, is delivered to scraper drier by delivery pump, obtains feed addictive humic acid by S6
Sodium；
S7, the feed addictive sodium humate after scraper drier is dried weigh process by transmission flood dragon conveying；
Feed addictive sodium humate after weighing is packed into dedicated feed addictive packaging bag, is packaged with baling press by S8
And it is sealed.
2. a kind of method using bioactivity zymotechnic production feed addictive sodium humate according to claim 1,
It is characterized in that, the S3, pulverizer is crushed using vertical-spindle hammer crusher and model PSFL-1000, the pulverizer
Weathered coal size is in 20-30 mesh.
3. a kind of method using bioactivity zymotechnic production feed addictive sodium humate according to claim 1,
It is characterized in that, the scraper drier uses Rollingscratchboarddrier and model HG-1800A.
4. a kind of method using bioactivity zymotechnic production feed addictive sodium humate according to claim 1,
It is characterized in that, the S2, electronic scale weighs weight weathered coal according to weight ratio respectively: 1 ton；Water: 0.8-1 tons；Bioactivity
3-5 kilograms of enzyme, sodium hydroxide: 15-20 kilograms.
5. a kind of method using bioactivity zymotechnic production feed addictive sodium humate according to claim 1,
It is characterized in that, the S4, mixing speed is 300r/min and stirs to after being thoroughly mixed, and persistently stirs 1h, temperature: 36-60
℃。
6. a kind of method using bioactivity zymotechnic production feed addictive sodium humate according to claim 1,
It is characterized in that, the S5, the sedimentation time: 20-30 hours, the pH value of the alkalinity acidity tester detection sedimentation basin was under 8.
7. a kind of method using bioactivity zymotechnic production feed addictive sodium humate according to claim 1,
It is characterized in that, the S7, scraper drier is fixed by conduit to connect treatment tank and to adding inside treatment tank
Enter ferrous sulfate and carries out neutralization reaction.
8. a kind of method using bioactivity zymotechnic production feed addictive sodium humate according to claim 1,
It is characterized in that, DY600*10 meters of the model of the belt conveyor, the model of the blender are as follows: MG-01a and pacify
Dress mode is vertical；The model of the delivery pump；500ZLB-7, the model of the transmission flood dragon；hy-006.
9. a kind of method using bioactivity zymotechnic production feed addictive sodium humate according to claim 1,
It is characterized in that, the vertical-spindle hammer crusher, scraper drier, belt conveyor, blender, delivery pump, transmission flood dragon are equal
It is electrically connected on PLC system control cabinet.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113180151A (en) * | 2021-05-25 | 2021-07-30 | 北京博思汇科生物技术有限公司 | Method for producing organic trace zinc humate as feed additive |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105967769A (en) * | 2016-05-05 | 2016-09-28 | 耿春斌 | Zymolytic humic acid for agriculture and production method thereof |
| CN108576398A (en) * | 2018-05-15 | 2018-09-28 | 齐鲁工业大学 | Modified humic acid sodium product and preparation method and application |
| CN109007257A (en) * | 2018-08-02 | 2018-12-18 | 北京首钢朗泽新能源科技有限公司 | A kind of animal feeding-stuff containing somatic protein, production technology and its application |
| CN109081924A (en) * | 2018-10-23 | 2018-12-25 | 宁夏天鑫源生物科技有限公司 | A kind of feeding sodium humate and its preparation method and application |
-
2019
- 2019-01-10 CN CN201910023997.5A patent/CN109811014A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105967769A (en) * | 2016-05-05 | 2016-09-28 | 耿春斌 | Zymolytic humic acid for agriculture and production method thereof |
| CN108576398A (en) * | 2018-05-15 | 2018-09-28 | 齐鲁工业大学 | Modified humic acid sodium product and preparation method and application |
| CN109007257A (en) * | 2018-08-02 | 2018-12-18 | 北京首钢朗泽新能源科技有限公司 | A kind of animal feeding-stuff containing somatic protein, production technology and its application |
| CN109081924A (en) * | 2018-10-23 | 2018-12-25 | 宁夏天鑫源生物科技有限公司 | A kind of feeding sodium humate and its preparation method and application |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113180151A (en) * | 2021-05-25 | 2021-07-30 | 北京博思汇科生物技术有限公司 | Method for producing organic trace zinc humate as feed additive |
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Application publication date: 20190528 |