CN109796843A - A kind of fire proofing material preparation method - Google Patents

A kind of fire proofing material preparation method Download PDF

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Publication number
CN109796843A
CN109796843A CN201910017658.6A CN201910017658A CN109796843A CN 109796843 A CN109796843 A CN 109796843A CN 201910017658 A CN201910017658 A CN 201910017658A CN 109796843 A CN109796843 A CN 109796843A
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CN
China
Prior art keywords
fire proofing
polypropylene
proofing material
propylene glycol
aluminate
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Pending
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CN201910017658.6A
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Chinese (zh)
Inventor
董孝宇
赵建章
史云晶
杨长德
李玉梅
管述哲
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Individual
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Individual
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Priority to CN201910017658.6A priority Critical patent/CN109796843A/en
Publication of CN109796843A publication Critical patent/CN109796843A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a kind of fire proofing material preparation methods, it is made of epoxy resin, iron oxide, ethyl acetate, propandiol butyl ether, graphene, titanium dioxide, aluminate, strontium chromate, ammonium metaborate, carbon fiber, dibutyl phthalate, propylene glycol monomethyl ether, aluminium powder, ceramic powder, polypropylene and asbestos, experiments verify that, material of the invention can not melt at 400 degrees Celsius or less, 400 degrees Celsius or more melt, but it can not burn, effectively play fireproofing function.Compared with prior art, a variety of such as plates can be made in fire proofing material of the invention, can high temperature resistant, prevent from burning, effectively play fireproofing function, have the value of popularization and application.

Description

A kind of fire proofing material preparation method
Technical field
The present invention relates to field of material technology more particularly to a kind of fire proofing material preparation methods.
Background technique
Fire proofing material be with prevent or retard flame sprawling performance material.For preventing fires.There is incombustible material and fire retardant Two class of material.Incombustible material will not burn.Though nonflammable material incendivity has anti-flammability, i.e., difficult charing on fire, difficult, in fire source Removing after-combustion can stop, therefore also known as fire proofing.In nonflammable material, in addition to minority itself has flame retarding function, more Number occasion is all to be carried out prepared by flame retardant treatment using fire retardant, fire prevention impregnating agent or fireproof coating etc. to combustible material.From Fire safety sets out, and combustible material should be replaced using fire proofing material as far as possible in civil construction, to reduce fire load and reduction Spreading velocity of fire.Its fire protecting performance is assert according to different requirements by corresponding combustion test.
Summary of the invention
The object of the invention is that providing a kind of fire proofing material preparation method to solve the above-mentioned problems.
The present invention through the following technical solutions to achieve the above objectives:
The present invention includes epoxy resin, iron oxide, ethyl acetate, propandiol butyl ether, graphene, titanium dioxide, aluminate, chromium Sour strontium, ammonium metaborate, carbon fiber, dibutyl phthalate, propylene glycol monomethyl ether, aluminium powder, ceramic powder, polypropylene and asbestos, system Preparation Method the following steps are included:
(1) ceramic powder, aluminium powder, iron oxide, titanium dioxide are ground up, sieved;
(2) epoxy resin, ethyl acetate, dibutyl phthalate, polypropylene are put into vessel in heating and melt mixing;
(3) propandiol butyl ether, graphene are added in step (2), are uniformly mixed under keeping warm mode;
(4) aluminate, strontium chromate, ammonium metaborate, carbon fiber, propylene glycol monomethyl ether, polypropylene and stone will be added in step (3) It is uniformly mixed under cotton keeping warm mode, and size keeps the temperature 10 minutes;
(5) pulvis of step (1) preparation is added in step (4) and is uniformly mixed, stop heating, it is cooling fixed in mold to pour into Type is up to fire proofing material.
Preferably, by weight, every part containing the epoxy resin 15%, the iron oxide 5%, the ethyl acetate 8%, The propandiol butyl ether 1%, the graphene 3%, the titanium dioxide 3%, the aluminate 1%, the strontium chromate 0.5%, The ammonium metaborate 0.5%, the carbon fiber 5%, the dibutyl phthalate 2%, the propylene glycol monomethyl ether 2%, institute State aluminium powder 5%, the ceramic powder 25%, the polypropylene 5%, the asbestos 19%.
The beneficial effects of the present invention are:
The present invention is a kind of fire proofing material preparation method, and compared with prior art, fire proofing material of the invention can be made A variety of such as plates, can high temperature resistant, prevent from burning, effectively play fireproofing function, have the value of popularization and application.
Specific embodiment
The invention will be further described below:
The present invention includes epoxy resin, iron oxide, ethyl acetate, propandiol butyl ether, graphene, titanium dioxide, aluminate, chromium Sour strontium, ammonium metaborate, carbon fiber, dibutyl phthalate, propylene glycol monomethyl ether, aluminium powder, ceramic powder, polypropylene and asbestos, system Preparation Method the following steps are included:
(1) ceramic powder, aluminium powder, iron oxide, titanium dioxide are ground up, sieved;
(2) epoxy resin, ethyl acetate, dibutyl phthalate, polypropylene are put into vessel in heating and melt mixing;
(3) propandiol butyl ether, graphene are added in step (2), are uniformly mixed under keeping warm mode;
(4) aluminate, strontium chromate, ammonium metaborate, carbon fiber, propylene glycol monomethyl ether, polypropylene and stone will be added in step (3) It is uniformly mixed under cotton keeping warm mode, and size keeps the temperature 10 minutes;
(5) pulvis of step (1) preparation is added in step (4) and is uniformly mixed, stop heating, it is cooling fixed in mold to pour into Type is up to fire proofing material.
Preferably, by weight, every part containing the epoxy resin 15%, the iron oxide 5%, the ethyl acetate 8%, The propandiol butyl ether 1%, the graphene 3%, the titanium dioxide 3%, the aluminate 1%, the strontium chromate 0.5%, The ammonium metaborate 0.5%, the carbon fiber 5%, the dibutyl phthalate 2%, the propylene glycol monomethyl ether 2%, institute State aluminium powder 5%, the ceramic powder 25%, the polypropylene 5%, the asbestos 19%.
Experiments verify that material of the invention can not melt at 400 degrees Celsius or less, 400 degrees Celsius or more melt, but It can not burn, effectively play fireproofing function.
Basic principles and main features and advantages of the present invention of the invention have been shown and described above.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its Equivalent thereof.

Claims (2)

1. a kind of fire proofing material preparation method, it is characterised in that: including epoxy resin, iron oxide, ethyl acetate, propylene glycol fourth Ether, graphene, titanium dioxide, aluminate, strontium chromate, ammonium metaborate, carbon fiber, dibutyl phthalate, propylene glycol monomethyl ether, aluminium Powder, ceramic powder, polypropylene and asbestos, preparation method the following steps are included:
(1) ceramic powder, aluminium powder, iron oxide, titanium dioxide are ground up, sieved;
(2) epoxy resin, ethyl acetate, dibutyl phthalate, polypropylene are put into vessel in heating and melt mixing;
(3) propandiol butyl ether, graphene are added in step (2), are uniformly mixed under keeping warm mode;
(4) aluminate, strontium chromate, ammonium metaborate, carbon fiber, propylene glycol monomethyl ether, polypropylene and asbestos will be added in step (3) to protect It is uniformly mixed under temperature state, and size keeps the temperature 10 minutes;
(5) pulvis of step (1) preparation is added in step (4) and is uniformly mixed, stopped heating, pour into mold cooling and shaping i.e. Obtain fire proofing material.
2. fire proofing material preparation method according to claim 1, it is characterised in that: by weight, every part contains the epoxy Resin 15%, the iron oxide 5%, the ethyl acetate 8%, the propandiol butyl ether 1%, the graphene 3%, the titanium White powder 3%, the aluminate 1%, the strontium chromate 0.5%, the ammonium metaborate 0.5%, the carbon fiber 5%, the neighbour Dibatyl phithalate 2%, the propylene glycol monomethyl ether 2%, the aluminium powder 5%, the ceramic powder 25%, the polypropylene 5%, The asbestos 19%.
CN201910017658.6A 2019-01-07 2019-01-07 A kind of fire proofing material preparation method Pending CN109796843A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910017658.6A CN109796843A (en) 2019-01-07 2019-01-07 A kind of fire proofing material preparation method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910017658.6A CN109796843A (en) 2019-01-07 2019-01-07 A kind of fire proofing material preparation method

Publications (1)

Publication Number Publication Date
CN109796843A true CN109796843A (en) 2019-05-24

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Citations (12)

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CN102827401A (en) * 2012-10-08 2012-12-19 西华大学 Flame-retardant composite material and preparation method thereof
CN103131166A (en) * 2011-12-01 2013-06-05 合肥杰事杰新材料股份有限公司 Low coefficient of thermal expansion thermoplastic resin composition, preparation method and application thereof
CN103525055A (en) * 2013-10-17 2014-01-22 西华大学 Flame retardant composite material with double polymer components and preparation method thereof
CN103881291A (en) * 2014-02-26 2014-06-25 黄忠娟 Enhanced flame retardant plastic
CN105017641A (en) * 2015-05-08 2015-11-04 镇江荣诚管业有限公司 Light fire retardant board and processing method thereof
CN105368009A (en) * 2015-12-30 2016-03-02 青岛宇星智能科技开发有限公司 Fireproof and flame-retardant polymer material
CN105860680A (en) * 2016-06-14 2016-08-17 烟台民望机电技术有限公司 High-temperature-resistant metal rustproof paint
CN106084477A (en) * 2016-07-11 2016-11-09 安徽海纳川塑业科技有限公司 A kind of composite resin sill and preparation method thereof
CN106750891A (en) * 2016-11-15 2017-05-31 墨宝股份有限公司 A kind of nano fire-retarding composite material and preparation method thereof
CN107141590A (en) * 2017-06-07 2017-09-08 太仓市龙华塑胶有限公司 A kind of flame retardant plastics particle
CN108530669A (en) * 2018-05-16 2018-09-14 鸿纳(东莞)新材料科技有限公司 A kind of graphene-based fireproofing plastic board and preparation method thereof

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103131166A (en) * 2011-12-01 2013-06-05 合肥杰事杰新材料股份有限公司 Low coefficient of thermal expansion thermoplastic resin composition, preparation method and application thereof
CN102746560A (en) * 2012-07-27 2012-10-24 深圳市飞荣达科技股份有限公司 Heat-conducting plastic and preparation method thereof
CN102827401A (en) * 2012-10-08 2012-12-19 西华大学 Flame-retardant composite material and preparation method thereof
CN103525055A (en) * 2013-10-17 2014-01-22 西华大学 Flame retardant composite material with double polymer components and preparation method thereof
CN103881291A (en) * 2014-02-26 2014-06-25 黄忠娟 Enhanced flame retardant plastic
CN105017641A (en) * 2015-05-08 2015-11-04 镇江荣诚管业有限公司 Light fire retardant board and processing method thereof
CN105368009A (en) * 2015-12-30 2016-03-02 青岛宇星智能科技开发有限公司 Fireproof and flame-retardant polymer material
CN105860680A (en) * 2016-06-14 2016-08-17 烟台民望机电技术有限公司 High-temperature-resistant metal rustproof paint
CN106084477A (en) * 2016-07-11 2016-11-09 安徽海纳川塑业科技有限公司 A kind of composite resin sill and preparation method thereof
CN106750891A (en) * 2016-11-15 2017-05-31 墨宝股份有限公司 A kind of nano fire-retarding composite material and preparation method thereof
CN107141590A (en) * 2017-06-07 2017-09-08 太仓市龙华塑胶有限公司 A kind of flame retardant plastics particle
CN108530669A (en) * 2018-05-16 2018-09-14 鸿纳(东莞)新材料科技有限公司 A kind of graphene-based fireproofing plastic board and preparation method thereof

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Application publication date: 20190524

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