CN109778528A - A kind of preparation method of environment-friendlyantibiotic antibiotic textile product - Google Patents
A kind of preparation method of environment-friendlyantibiotic antibiotic textile product Download PDFInfo
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- CN109778528A CN109778528A CN201811649082.7A CN201811649082A CN109778528A CN 109778528 A CN109778528 A CN 109778528A CN 201811649082 A CN201811649082 A CN 201811649082A CN 109778528 A CN109778528 A CN 109778528A
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Abstract
The invention discloses a kind of preparation methods of environment-friendlyantibiotic antibiotic textile product, it is obtained by the way that zinc oxide and Argent grain are added on textile fabrics, the following steps are included: step 1: by textile fabrics weight percent solubility be 0.05-0.5% burnett's solution in impregnation 30-90min, the weight and burnett's solution weight ratio of textile fabrics are 1:10-50, and dipping temperature is 40-60 DEG C；Step 2: silver ammino solution is added, then by textile fabrics impregnation 60min, washing is dried or dried, the textile fabrics after being reacted；Step 3: reaction being obtained into textile fabrics and mixes immersion with glucose solution, obtains antibacterial fabric.For the present invention by the way that zinc oxide and Argent grain are added on textile fabrics, so that the textile fabrics washability that the present invention obtains is good, and the method for preparing textile is simple, with short production cycle；Antibacterial fabric of the invention has excellent antibiotic property and wearability, can satisfy the demand of people, be conducive to the use of people.
Description
Technical field
The present invention relates to textile technology field, specially a kind of preparation method of environment-friendlyantibiotic antibiotic textile product.
Background technique
Weaving original meaning is taken from the general name of spinning and woven fabric, but with the continuous hair of textile knowledge system and subject system
Exhibition and perfect, after the technologies such as especially non-woven textile material and three-dimensional be composite braided generate, present weaving has been not only
Traditional hand spinning and woven fabric also includes nonwoven fabric technology, Modern three-dimensional knitting skill, modern electrostatic nano-netting technology etc.
The clothes of production are used, industry is used, decorative textile product, so, modern textile refers to more rulers of a kind of fiber or fiber assembly
Structure processing technology is spent, the weaving of ancient Chinese and printing technology have very long history, ancient early in primitive society period
The artificial variation of acclimatization, has understood and has gathered materials on the spot, using natural resources as the raw material of weaving and printing and dyeing, and manufactured
Simple Handicraft Textile tool, clothes, air bag and curtain carpet in daily life are all weaving and the production of printing technology
Object.
Textile is textile fabric by a kind of product made of processing weaving, is divided into woven fabric and looped fabric two major classes,
Inventionbroadly textile is from spinning-woven fabric-manufactured goods, including yarn, line, natural silk, artificial silk, chemical fibre length silk, elastic filament,
Wire etc., looped fabric, woven fabric, non-woven fabrics, natural fur fabric etc., clothes, Fashion and Accessories, household textiles etc. also wrap
Other textiles are included, the correct stacking method of textile is to be advantageously selected for divulging information, and convenient for fire prevention, full-cotton fabric is preferably placed in logical
The good place of wind, for example from door, the place nearest from window, in actual production and life, people are inevitably contacted
To the microorganisms such as various bacteriums and fungi, these microorganisms have extremely strong fertility under suitable environmental condition
And spread the disease by contact, the health of people is influenced, however, in daily life, textile is that these microorganisms are good
In place of good existence, and with the increasingly raising of the rapid development of industry and living standards of the people, people are to antibacterial fabric
It increasingly pays close attention to, exploitation antibacterial fabric, which just seems, to be even more important.
Since discovery zinc oxide has antibacterial action, because of its cheap price, resource abundant, and have become anti-
The research hotspot of bacterium material, zinc oxide is to play antibacterial action by photocatalysis, so will not be as other antibacterial agents
Like that with the consumption of anti-biotic material and effect slowly declines, so photocatalyst-type anti-biotic agent have lasting anti-microbial property, this
Outside, nano zine oxide has uviolresistance, chemical stability, thermal stability, nontoxicity etc., is widely used in recent years anti-
Ultraviolet materials, field of textiles, still, it is long there are the production cycle that current technique prepares antibacterial fabric, and production is obtained
Antibacterial fabric washability it is poor, Durability of antimicrobial effect is poor, and it is impossible to meet the demands of people, is unfavorable for the use of people.
Summary of the invention
The purpose of the present invention is to provide a kind of preparation methods of environment-friendlyantibiotic antibiotic textile product, have environment-friendly type antibiotic spinning
The advantages of textile fabrics good anti-bacterial effect of the preparation method preparation of fabric products, solves current technique and prepares antibacterial fabric week
Phase is long, and antibacterial fabric washability is poor, the problem of antibiotic property difference.
To achieve the above object, the invention provides the following technical scheme: a kind of preparation side of environment-friendlyantibiotic antibiotic textile product
Method is obtained by the way that zinc oxide and Argent grain are added on textile fabrics, comprising the following steps:
Step 1: by textile fabrics weight percent solubility be 0.05-0.5% burnett's solution in impregnation 30-
90min, the weight and burnett's solution weight ratio of textile fabrics are 1:10-50, and dipping temperature is 40-60 DEG C；
Step 2: silver ammino solution is added, then by textile fabrics impregnation 60min, washing is dried or dried, after being reacted
Textile fabrics；
Step 3: reaction being obtained into textile fabrics and mixes immersion with glucose solution, obtains antibacterial fabric.
Preferably, the preparation method of the environment-friendlyantibiotic antibiotic textile product can be with are as follows:
Step 1: by textile fabrics weight percent solubility be 0.05-0.5% burnett's solution in impregnation 30-
90min, the weight and burnett's solution weight ratio of textile fabrics are 1:10-50, and dipping temperature is 40-60 DEG C；
Step 2: be added aqueous slkali mixing carry out hydrophilicity-imparting treatment, by after hydrophilicity-imparting treatment textile and silver nitrate solution it is anti-
It answers, the textile fabrics after being reacted.
Preferably, the preparation method of the environment-friendlyantibiotic antibiotic textile product can be with are as follows:
Step 1: by textile fabrics weight percent solubility be 0.05-0.5% burnett's solution in impregnation 30-
90min, the weight and burnett's solution weight ratio of textile fabrics are 1:10-50, and dipping temperature is 40-60 DEG C；
Step 2: dopamine hydrochloride buffer hybrid reaction, the textile fabrics after being reacted are added；
Step 3: the textile fabrics and silver nitrate solution hybrid reaction that reaction is obtained obtain antibacterial fabric.
Preferably, the concentration of the silver ammino solution is 0.01-0.5mol/L, and the reaction temperature of the silver ammino solution is 120-
250 DEG C, the reaction time is 20-50min, and the concentration of the glucose solution is 0.01-0.50mol/L.
Preferably, the concentration of the silver nitrate is 0.01-0.5mol/L, and the reaction temperature of the silver nitrate solution is 120-
250 DEG C, the reaction time is 20-50min, and the concentration of the glucose solution is 0.01-0.50mol/L.
Preferably, the concentration of the silver nitrate is 0.1-20mmol/L, and the reaction temperature of the silver nitrate solution is 120-
250 DEG C, the reaction time is 0.5-20h.
Preferably, the alkali in the aqueous slkali is preferably one or more of NaOH, KOH and NH4OH, the aqueous slkali
PH value be preferably 9-12.
Preferably, the dopamine hydrochloride buffer is prepared in accordance with the following methods: 25mg dopamine hydrochloride being taken to buffer
Liquid is dissolved in 20ml deionized water, and adjusting pH is 8.5, then takes 20mg dopamine to be added in dopamine hydrochloride buffer and obtain
Finished product.
Compared with prior art, beneficial effects of the present invention are as follows: the present invention on textile fabrics by being added zinc oxide
And Argent grain, so that the textile fabrics washability that the present invention obtains is good, and the method for preparing textile is simple, the production cycle
It is short；Antibacterial fabric of the invention has excellent antibiotic property and wearability, can satisfy the demand of people, be conducive to people
Use.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common
Technical staff's every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
A kind of preparation method of environment-friendlyantibiotic antibiotic textile product is obtained by the way that zinc oxide and Argent grain are added on textile fabrics
It arrives, comprising the following steps:
Step 1: by textile fabrics weight percent solubility be 0.05-0.5% burnett's solution in impregnation 30-
90min, the weight and burnett's solution weight ratio of textile fabrics are 1:10-50, and dipping temperature is 40-60 DEG C；
Step 2: silver ammino solution is added, then by textile fabrics impregnation 60min, washing is dried or dried, after being reacted
Textile fabrics；
Step 3: reaction being obtained into textile fabrics and mixes immersion with glucose solution, obtains antibacterial fabric.
A kind of preparation method of environment-friendlyantibiotic antibiotic textile product is obtained by the way that zinc oxide and Argent grain are added on textile fabrics
It arrives, comprising the following steps:
Step 1: by textile fabrics weight percent solubility be 0.05-0.5% burnett's solution in impregnation 30-
90min, the weight and burnett's solution weight ratio of textile fabrics are 1:10-50, and dipping temperature is 40-60 DEG C；
Step 2: be added aqueous slkali mixing carry out hydrophilicity-imparting treatment, by after hydrophilicity-imparting treatment textile and silver nitrate solution it is anti-
It answers, the textile fabrics after being reacted；
Step 3: the textile fabrics and glucose solution hybrid reaction that reaction is obtained obtain antibacterial fabric.
A kind of preparation method of environment-friendlyantibiotic antibiotic textile product is obtained by the way that zinc oxide and Argent grain are added on textile fabrics
It arrives, comprising the following steps:
Step 1: by textile fabrics weight percent solubility be 0.05-0.5% burnett's solution in impregnation 30-
90min, the weight and burnett's solution weight ratio of textile fabrics are 1:10-50, and dipping temperature is 40-60 DEG C；
Step 2: dopamine hydrochloride buffer hybrid reaction, the textile fabrics after being reacted are added；
Step 3: the textile fabrics and silver nitrate solution hybrid reaction that reaction is obtained obtain antibacterial fabric.
Embodiment 1
A kind of preparation method of environment-friendlyantibiotic antibiotic textile product is obtained by the way that zinc oxide and Argent grain are added on textile fabrics,
The following steps are included: step 1: by textile fabrics impregnation in the burnett's solution that weight percent solubility is 0.05%
90min, the weight and burnett's solution weight ratio of textile fabrics are 1:50, and dipping temperature is 60 DEG C；Step 2: it is molten that silver-colored ammonia is added
Liquid, then by textile fabrics impregnation 60min, washing is dried or is dried, the textile fabrics after being reacted；Step 3: will be anti-
It should obtain textile fabrics and mix immersion with glucose solution, obtain antibacterial fabric.
Embodiment 2
In embodiment 1, following steps are added:
The concentration of silver ammino solution is 0.01-0.5mol/L, and the reaction temperature of silver ammino solution is 120-250 DEG C, reaction time 20-
50min, the concentration of glucose solution are 0.01-0.50mol/L.
A kind of preparation method of environment-friendlyantibiotic antibiotic textile product is obtained by the way that zinc oxide and Argent grain are added on textile fabrics
It arrives, comprising the following steps: step 1: by textile fabrics in the burnett's solution that weight percent solubility is 0.05% at dipping
30min is managed, the weight and burnett's solution weight ratio of textile fabrics are 1:10, and dipping temperature is 40 DEG C；Step 2: silver-colored ammonia is added
Solution, then by textile fabrics impregnation 60min, washing is dried or is dried, the textile fabrics after being reacted；Step 3: will
Reaction obtains textile fabrics and mixes immersion with glucose solution, obtains antibacterial fabric.
Embodiment 3
A kind of preparation method of environment-friendlyantibiotic antibiotic textile product is obtained by the way that zinc oxide and Argent grain are added on textile fabrics,
Step 1: by textile fabrics weight percent solubility be 0.05% burnett's solution in impregnation 50min, textile fabrics
Weight and burnett's solution weight ratio be 1:20, dipping temperature be 40 DEG C；Step 2: aqueous slkali mixing is added and carries out hydrophiling
Processing, the textile after hydrophilicity-imparting treatment is reacted with silver nitrate solution, the textile fabrics after being reacted；Step 3: will react
Obtained textile fabrics and glucose solution hybrid reaction, obtain antibacterial fabric.
Embodiment 4
In embodiment 3, following steps are added:
The concentration of silver nitrate is 0.01-0.5mol/L, and the reaction temperature of silver nitrate solution is 120-250 DEG C, reaction time 20-
50min, the concentration of glucose solution are 0.01-0.50mol/L.
A kind of preparation method of environment-friendlyantibiotic antibiotic textile product is obtained by the way that zinc oxide and Argent grain are added on textile fabrics
It arrives, step 1: by textile fabrics, impregnation 90min, weaving are made in the burnett's solution that weight percent solubility is 0.5%
The weight and burnett's solution weight ratio of product are 1:50, and dipping temperature is 40 DEG C；Step 2: it is hydrophilic that aqueous slkali mixing progress is added
Change processing, the textile after hydrophilicity-imparting treatment is reacted with silver nitrate solution, the textile fabrics after being reacted；Step 3: will be anti-
The textile fabrics and glucose solution hybrid reaction that should be obtained, obtain antibacterial fabric.
Embodiment 5
A kind of preparation method of environment-friendlyantibiotic antibiotic textile product is obtained by the way that zinc oxide and Argent grain are added on textile fabrics,
Step 1: by textile fabrics weight percent solubility be 0.3% burnett's solution in impregnation 60min, textile fabrics
Weight and burnett's solution weight ratio are 1:30, and dipping temperature is 40 DEG C；Step 2: the mixing of dopamine hydrochloride buffer is added
Reaction, the textile fabrics after being reacted；Step 3: the textile fabrics and silver nitrate solution hybrid reaction that reaction is obtained obtain
Antibacterial fabric.
Embodiment 6
In embodiment 5, following steps are added:
Alkali in aqueous slkali is preferably one or more of NaOH, KOH and NH4OH, and the pH value of aqueous slkali is preferably 9-12.
A kind of preparation method of environment-friendlyantibiotic antibiotic textile product is obtained by the way that zinc oxide and Argent grain are added on textile fabrics
It arrives, step 1: by textile fabrics, impregnation 60min, weaving are made in the burnett's solution that weight percent solubility is 0.3%
The weight and burnett's solution weight ratio of product are 1:30, and dipping temperature is 40 DEG C；Step 2: dopamine hydrochloride buffer is added
Hybrid reaction, the textile fabrics after being reacted；Step 3: the textile fabrics and silver nitrate solution hybrid reaction that reaction is obtained,
Obtain antibacterial fabric.
Embodiment 7
In embodiment 6, following steps are added:
The concentration of silver nitrate is 0.1-20mmol/L, and the reaction temperature of silver nitrate solution is 120-250 DEG C, reaction time 0.5-
30h。
A kind of preparation method of environment-friendlyantibiotic antibiotic textile product is obtained by the way that zinc oxide and Argent grain are added on textile fabrics
It arrives, step 1: by textile fabrics, impregnation 35min, weaving are made in the burnett's solution that weight percent solubility is 0.4%
The weight and burnett's solution weight ratio of product are 1:25, and dipping temperature is 60 DEG C；Step 2: dopamine hydrochloride buffer is added
Hybrid reaction, the textile fabrics after being reacted；Step 3: the textile fabrics and silver nitrate solution hybrid reaction that reaction is obtained,
Obtain antibacterial fabric.
Embodiment 8
In embodiment 7, following steps are added:
Dopamine hydrochloride buffer is prepared in accordance with the following methods: 25mg dopamine hydrochloride buffer being taken to be dissolved in 20ml deionization
In water, and adjusting pH is 8.5, then takes 20mg dopamine to be added in dopamine hydrochloride buffer and obtain finished product.
A kind of preparation method of environment-friendlyantibiotic antibiotic textile product is obtained by the way that zinc oxide and Argent grain are added on textile fabrics
It arrives, step 1: by textile fabrics, impregnation 37min, weaving are made in the burnett's solution that weight percent solubility is 0.35%
The weight and burnett's solution weight ratio of product are 1:27, and dipping temperature is 41 DEG C；Step 2: dopamine hydrochloride buffer is added
Hybrid reaction, the textile fabrics after being reacted；Step 3: the textile fabrics and silver nitrate solution hybrid reaction that reaction is obtained,
Obtain antibacterial fabric.
It is washed in use, textile fabrics produced by the present invention are put into 49 DEG C of water according to AATCC-612006 washing standard
5 circulations, recycle 45min every time, and textile surface is observed after washing, the water-wash resistance weaved are observed, to implementation
The antibacterial textile fabrics that example is prepared carry out anti-Escherichia coli performance detection, compare common textile fabrics cotton fabric to large intestine
Bacillus does not resist effect, since silver is a kind of good antibacterial agent, if silver is reverted to cotton fabric by the way of certain
On, it will show good antibiotic property, and then improve bacteriostasis rate, and antibacterial textile fabrics provided by the invention are identical in silver concentration
When, antibiotic rate is greater than the antibiotic rate that silver is directly loaded in the textile obtained on textile, so that the weaving that the present invention obtains
Product washability is good, and the method for preparing textile is simple, with short production cycle；Antibacterial fabric of the invention has excellent
Antibiotic property and wearability, can satisfy the demand of people, be conducive to the use of people.
In summary: the preparation method of the environment-friendlyantibiotic antibiotic textile product, by textile fabrics be added zinc oxide and
Argent grain, so that the textile fabrics washability that the present invention obtains is good, and the method for preparing textile is simple, with short production cycle；
Antibacterial fabric of the invention has excellent antibiotic property and wearability, can satisfy the demand of people, be conducive to making for people
With, it solves current technique and prepares that the antibacterial fabric period is long, and antibacterial fabric washability is poor, the problem of antibiotic property difference.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (8)
1. a kind of preparation method of environment-friendlyantibiotic antibiotic textile product, by zinc oxide being added on textile fabrics and Argent grain obtains
It arrives, it is characterised in that: the following steps are included:
Step 1: by textile fabrics weight percent solubility be 0.05-0.5% burnett's solution in impregnation 30-
90min, the weight and burnett's solution weight ratio of textile fabrics are 1:10-50, and dipping temperature is 40-60 DEG C；
Step 2: silver ammino solution is added, then by textile fabrics impregnation 60min, washing is dried or dried, after being reacted
Textile fabrics；
Step 3: reaction being obtained into textile fabrics and mixes immersion with glucose solution, obtains antibacterial fabric.
2. a kind of preparation method of environment-friendlyantibiotic antibiotic textile product according to claim 1, it is characterised in that: the environmental protection
The preparation method of type antibacterial textile fabrics can be with are as follows:
Step 1: by textile fabrics weight percent solubility be 0.05-0.5% burnett's solution in impregnation 30-
90min, the weight and burnett's solution weight ratio of textile fabrics are 1:10-50, and dipping temperature is 40-60 DEG C；
Step 2: be added aqueous slkali mixing carry out hydrophilicity-imparting treatment, by after hydrophilicity-imparting treatment textile and silver nitrate solution it is anti-
It answers, the textile fabrics after being reacted；
Step 3: the textile fabrics and glucose solution hybrid reaction that reaction is obtained obtain antibacterial fabric.
3. a kind of preparation method of environment-friendlyantibiotic antibiotic textile product according to claim 1, it is characterised in that: the environmental protection
The preparation method of type antibacterial textile fabrics can be with are as follows:
Step 1: by textile fabrics weight percent solubility be 0.05-0.5% burnett's solution in impregnation 30-
90min, the weight and burnett's solution weight ratio of textile fabrics are 1:10-50, and dipping temperature is 40-60 DEG C；
Step 2: dopamine hydrochloride buffer hybrid reaction, the textile fabrics after being reacted are added；
Step 3: the textile fabrics and silver nitrate solution hybrid reaction that reaction is obtained obtain antibacterial fabric.
4. a kind of preparation method of environment-friendlyantibiotic antibiotic textile product according to claim 1, it is characterised in that: the silver ammonia
The concentration of solution is 0.01-0.5mol/L, and the reaction temperature of the silver ammino solution is 120-250 DEG C, and the reaction time is 20-
50min, the concentration of the glucose solution are 0.01-0.50mol/L.
5. a kind of preparation method of environment-friendlyantibiotic antibiotic textile product according to claim 2, it is characterised in that: the nitric acid
The concentration of silver is 0.01-0.5mol/L, and the reaction temperature of the silver nitrate solution is 120-250 DEG C, and the reaction time is 20-
50min, the concentration of the glucose solution are 0.01-0.50mol/L.
6. a kind of preparation method of environment-friendlyantibiotic antibiotic textile product according to claim 3, it is characterised in that: the nitric acid
The concentration of silver is 0.1-20mmol/L, and the reaction temperature of the silver nitrate solution is 120-250 DEG C, and the reaction time is 0.5-
20h。
7. a kind of preparation method of environment-friendlyantibiotic antibiotic textile product according to claim 2, it is characterised in that: the alkali soluble
Alkali in liquid is preferably one or more of NaOH, KOH and NH4OH, and the pH value of the aqueous slkali is preferably 9-12.
8. a kind of preparation method of environment-friendlyantibiotic antibiotic textile product according to claim 3, it is characterised in that: the DOPA
Amine hydrochlorate buffer is prepared in accordance with the following methods: take 25mg dopamine hydrochloride buffer to be dissolved in 20ml deionized water, and
Adjusting pH is 8.5, then takes 20mg dopamine to be added in dopamine hydrochloride buffer and obtain finished product.
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| CN201811649082.7A CN109778528A (en) | 2018-12-30 | 2018-12-30 | A kind of preparation method of environment-friendlyantibiotic antibiotic textile product |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110644239A (en) * | 2019-10-31 | 2020-01-03 | 南昌大学附属口腔医院(江西省口腔医院) | Antibacterial polylactic acid nanofiber and preparation method and application thereof |
| CN112760988A (en) * | 2021-01-22 | 2021-05-07 | 何成龙 | Antibacterial carpet fabric and preparation method thereof |
| CN114108307A (en) * | 2021-11-02 | 2022-03-01 | 盐城工学院 | Preparation method of zinc oxide modified fabric with dual functions of ultraviolet resistance and adsorptivity |
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| CN202786881U (en) * | 2012-04-17 | 2013-03-13 | 杭州云界环保科技有限公司 | Antibacterial fabric |
| CN103015166A (en) * | 2012-12-13 | 2013-04-03 | 北京航空航天大学 | Nano-silver antibacterial fabric and preparation method thereof |
| CN105568669A (en) * | 2015-12-31 | 2016-05-11 | 苏州榕绿纳米科技有限公司 | Antibiotic textile and production method thereof |
| CN107354716A (en) * | 2017-07-31 | 2017-11-17 | 陕西科技大学 | A kind of preparation method of the mould proof bafta of long acting antibiotic |
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|---|---|---|---|---|
| CN202786881U (en) * | 2012-04-17 | 2013-03-13 | 杭州云界环保科技有限公司 | Antibacterial fabric |
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| CN107354716A (en) * | 2017-07-31 | 2017-11-17 | 陕西科技大学 | A kind of preparation method of the mould proof bafta of long acting antibiotic |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110644239A (en) * | 2019-10-31 | 2020-01-03 | 南昌大学附属口腔医院(江西省口腔医院) | Antibacterial polylactic acid nanofiber and preparation method and application thereof |
| CN112760988A (en) * | 2021-01-22 | 2021-05-07 | 何成龙 | Antibacterial carpet fabric and preparation method thereof |
| CN114108307A (en) * | 2021-11-02 | 2022-03-01 | 盐城工学院 | Preparation method of zinc oxide modified fabric with dual functions of ultraviolet resistance and adsorptivity |
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