CN109774017A - A kind of acrylic leftover pieces and clast processing method and preparation method thereof - Google Patents

A kind of acrylic leftover pieces and clast processing method and preparation method thereof Download PDF

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Publication number
CN109774017A
CN109774017A CN201910162109.8A CN201910162109A CN109774017A CN 109774017 A CN109774017 A CN 109774017A CN 201910162109 A CN201910162109 A CN 201910162109A CN 109774017 A CN109774017 A CN 109774017A
Authority
CN
China
Prior art keywords
pellet
acrylic
crucible
clast
leftover pieces
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910162109.8A
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Chinese (zh)
Inventor
徐正青
李小华
刘强
陈家信
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anhui Maiming Acrylic Technology Co Ltd
Original Assignee
Anhui Maiming Acrylic Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anhui Maiming Acrylic Technology Co Ltd filed Critical Anhui Maiming Acrylic Technology Co Ltd
Priority to CN201910162109.8A priority Critical patent/CN109774017A/en
Publication of CN109774017A publication Critical patent/CN109774017A/en
Pending legal-status Critical Current

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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/62Plastics recycling; Rubber recycling

Abstract

The invention discloses a kind of acrylic leftover pieces and clast processing methods, specifically include following operating procedure: 1) recycling clast;2) it cleans;3) it cleans;4) primary colors is handled;5) it rinses;6) dry;7) melting remodeling;8) it stores.The present invention impregnates bulk material by cleaning solution, is cleaned by ultrasonic, the carving liquid, oil stain, stain being adhered on waste material in process can be removed, boiling is being carried out by the way that decolorising agent is added, the acrylic waste material of different colours can be reduced into primary colors, be conducive to that waste material is uniformly processed, improve waste disposal efficiency, then pass through melting remodeling, waste material is formed, can directly be used.

Description

A kind of acrylic leftover pieces and clast processing method and preparation method thereof
Technical field
The present invention relates to a kind of acrylic leftover pieces and clast processing methods and preparation method thereof, belong to organic glass recovery processing Technical field.
Background technique
Acrylic is called PMMA or organic glass, is originated from English acrylic (acrylic plastics), and chemical name is poly- first Base methyl acrylate.Acrylic is a kind of exploitation high molecular thermoplast earlier, and machine-shaping is more convenient, acrylic The molding mode of material mainly has cast molding and extrusion forming, can also be soft by its by reheating after acrylic material molding The mode of change is made the various shape of needs, and acrylic has the preferable transparency and a light transmittance, light transmittance up to 92%, Chemical stability and weatherability are preferable, very strong to natural environment adaptability.
In acrylic process, the waste materials such as a large amount of leftover pieces, clast can be generated, it, can if cannot recycle Generate vast resources waste.Existing acrylic clast recovery and treatment method is simple, and treatment effeciency is low.
Summary of the invention
Technical problem to be solved by the present invention lies in provide a kind of acrylic leftover pieces and clast processing method.
The technical problems to be solved by the invention take following technical scheme to realize:
A kind of acrylic leftover pieces and clast processing method, specifically include following operating procedure:
1) it recycles clast: the waste materials such as the leftover pieces, clout, clast that generate in acrylic process is collected;
2) it cleans: the big impurity (such as wooden unit, paper scrap, hair) being mixed in the waste material of centralized recovery being rejected, and passes through pulverizer Break process is carried out, it is spare to obtain acrylic pellet;
3) it cleans: pellet being placed in the rinse bath for being marked with the supersonic wave cleaning machine of cleaning solution and impregnated 1-2 hours, immersion terminates Afterwards, supersonic wave cleaning machine is opened, pellet is cleaned 20-30 minutes;
4) primary colors is handled: pellet being taken out from rinse bath and is drained, and pellet is put into cooker and is boiled, continues 1-3 Hour, the distilled water of its volume 3/4 is added in cooker, and the powdered sodium carbonate of distillation water quality 1-3% and taking off for 3-5% is added Toner;
5) it rinses: the pellet in cooker is taken out, and by distilled water to pellet repeated flushing 10-20 seconds, flushing water is returned Packaging film sealed envelope is used after receipts, is used for boiling;
6) dry: pellet being placed in 40-60 DEG C of baking oven by clean charging tray collection and is dried, it is cold that nature is taken out after drying But spare after;
7) melting remodeling: pellet after cooling is added into crucible, to vacuumize process is carried out in crucible, until crucible internal pressure After power is 0.05-0.07MPa, injected in crucible by nitrogen so that crucible external and internal pressure is identical, by intermediate frequency furnace to crucible into It goes and heats, heating temperature is 460-480 DEG C, continues 2-4 hours, so that the pellet in crucible all becomes to stop adding when molten state Heat, and fused materials are cast to the chilled glass die of preparatory surface filming, it is formed after cooling, obtains acrylic profile;
8) it stores: packaging film sealed envelope will be used after the recycling of acrylic profile, be staggeredly stacked, room temperature storage.
The cleaning solution weighs following material mixing for component by weight and forms: 1-3 parts of odium stearate, emulsifier 4-7 Part, 3-5 parts of sodium hydroxide, 20-30 parts of water.
The temperature of the cleaning solution is kept for 50-60 DEG C.
The beneficial effects of the present invention are: the present invention is conducive to by the way that acrylic waste material is carried out crushing granulation to granular original Material is handled, and is impregnated, is cleaned by ultrasonic to bulk material by cleaning solution, can removed and be adhered to waste material in process On carving liquid, oil stain, stain, by be added decolorising agent carry out boiling, the acrylic waste material of different colours can be restored At primary colors, be conducive to that waste material is uniformly processed, improve waste disposal efficiency, then by melting remodeling, by waste material carry out at Type can be used directly.
Specific embodiment
In order to be easy to understand to technical means, creative features, achievable purpose and effectiveness of the invention, below with reference to tool Body embodiment, the present invention is further explained.
Embodiment 1
A kind of acrylic leftover pieces and clast processing method, specifically include following operating procedure:
1) it recycles clast: the waste materials such as the leftover pieces, clout, clast that generate in acrylic process is collected;
2) it cleans: the big impurity (such as wooden unit, paper scrap, hair) being mixed in the waste material of centralized recovery being rejected, and passes through pulverizer Break process is carried out, it is spare to obtain acrylic pellet, and pellet diameter is less than 3mm;
3) it cleans: pellet being placed in the rinse bath for being marked with the supersonic wave cleaning machine of cleaning solution and impregnated 1 hour, after immersion, Supersonic wave cleaning machine is opened, pellet is cleaned 30 minutes;The cleaning solution be by weight component weigh following material mixing and At: 1-3 parts of odium stearate, 4-7 parts of emulsifier, 3-5 parts of sodium hydroxide, 20-30 parts of water;The temperature of cleaning solution is kept for 60 DEG C;
4) primary colors is handled: pellet being taken out from rinse bath and is drained, and pellet is put into cooker and is boiled, it is small to continue 3 When, the distilled water of its volume 3/4 is added in cooker, and the powdered sodium carbonate of distillation water quality 3% and 5% decolorising agent is added;
5) it rinses: the pellet in cooker is taken out, and by distilled water to pellet repeated flushing 20 seconds, after flushing water is recycled With packaging film sealed envelope, it to be used for boiling;
6) dry: pellet being placed in 40 DEG C of baking oven by clean charging tray collection and is dried, natural cooling is taken out after drying Afterwards, spare;
7) melting remodeling: pellet after cooling is added into crucible, to vacuumize process is carried out in crucible, until crucible internal pressure After power is 0.05MPa, injects in crucible by nitrogen, so that crucible external and internal pressure is identical, crucible is added by intermediate frequency furnace Heat, heating temperature are 460 DEG C, continue 4 hours, so that the pellet in crucible all becomes to stop heating when molten state, and will be melted Melt material to cast to the chilled glass die of preparatory surface filming, is formed after cooling, obtain acrylic profile;
8) it stores: packaging film sealed envelope will be used after the recycling of acrylic profile, be staggeredly stacked, room temperature storage.
Embodiment 2
A kind of acrylic leftover pieces and clast processing method, specifically include following operating procedure:
1) it recycles clast: the waste materials such as the leftover pieces, clout, clast that generate in acrylic process is collected;
2) it cleans: the big impurity (such as wooden unit, paper scrap, hair) being mixed in the waste material of centralized recovery being rejected, and passes through pulverizer Break process is carried out, it is spare to obtain acrylic pellet, and pellet diameter is less than 3mm;
3) it cleans: pellet being placed in the rinse bath for being marked with the supersonic wave cleaning machine of cleaning solution and impregnated 2 hours, after immersion, Supersonic wave cleaning machine is opened, pellet is cleaned 20 minutes;The cleaning solution be by weight component weigh following material mixing and At: 1-3 parts of odium stearate, 4-7 parts of emulsifier, 3-5 parts of sodium hydroxide, 20-30 parts of water;The temperature of cleaning solution is kept for 50 DEG C;
4) primary colors is handled: pellet being taken out from rinse bath and is drained, and pellet is put into cooker and is boiled, it is small to continue 1 When, the distilled water of its volume 3/4 is added in cooker, and the powdered sodium carbonate of distillation water quality 3% and 3% decolorising agent is added;
5) it rinses: the pellet in cooker is taken out, and by distilled water to pellet repeated flushing 10 seconds, after flushing water is recycled With packaging film sealed envelope, it to be used for boiling;
6) dry: pellet being placed in 60 DEG C of baking oven by clean charging tray collection and is dried, natural cooling is taken out after drying Afterwards, spare;
7) melting remodeling: pellet after cooling is added into crucible, to vacuumize process is carried out in crucible, until crucible internal pressure After power is 0.07MPa, injects in crucible by nitrogen, so that crucible external and internal pressure is identical, crucible is added by intermediate frequency furnace Heat, heating temperature are 480 DEG C, continue 2 hours, so that the pellet in crucible all becomes to stop heating when molten state, and will be melted Melt material to cast to the chilled glass die of preparatory surface filming, is formed after cooling, obtain acrylic profile;
8) it stores: packaging film sealed envelope will be used after the recycling of acrylic profile, be staggeredly stacked, room temperature storage.
Embodiment 3
A kind of acrylic leftover pieces and clast processing method, specifically include following operating procedure:
1) it recycles clast: the waste materials such as the leftover pieces, clout, clast that generate in acrylic process is collected;
2) it cleans: the big impurity (such as wooden unit, paper scrap, hair) being mixed in the waste material of centralized recovery being rejected, and passes through pulverizer Break process is carried out, it is spare to obtain acrylic pellet, and pellet diameter is less than 3mm;
3) it cleans: pellet being placed in the rinse bath for being marked with the supersonic wave cleaning machine of cleaning solution and impregnated 1.5 hours, immersion terminates Afterwards, supersonic wave cleaning machine is opened, pellet is cleaned 25 minutes;The cleaning solution is that component by weight weighs following material mixing It forms: 1-3 parts of odium stearate, 4-7 parts of emulsifier, 3-5 parts of sodium hydroxide, 20-30 parts of water;The temperature of cleaning solution is kept for 55 DEG C;
4) primary colors is handled: pellet being taken out from rinse bath and is drained, and pellet is put into cooker and is boiled, it is small to continue 2 When, the distilled water of its volume 3/4 is added in cooker, and the powdered sodium carbonate of distillation water quality 2% and 4% decolorising agent is added;
5) it rinses: the pellet in cooker is taken out, and by distilled water to pellet repeated flushing 15 seconds, after flushing water is recycled With packaging film sealed envelope, it to be used for boiling;
6) dry: pellet being placed in 50 DEG C of baking oven by clean charging tray collection and is dried, natural cooling is taken out after drying Afterwards, spare;
7) melting remodeling: pellet after cooling is added into crucible, to vacuumize process is carried out in crucible, until crucible internal pressure After power is 0.06MPa, injects in crucible by nitrogen, so that crucible external and internal pressure is identical, crucible is added by intermediate frequency furnace Heat, heating temperature are 470 DEG C, continue 3 hours, so that the pellet in crucible all becomes to stop heating when molten state, and will be melted Melt material to cast to the chilled glass die of preparatory surface filming, is formed after cooling, obtain acrylic profile;
8) it stores: packaging film sealed envelope will be used after the recycling of acrylic profile, be staggeredly stacked, room temperature storage.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, without departing from the spirit and scope of the present invention, this hair Bright to will also have various changes and improvements, these changes and improvements all fall within the protetion scope of the claimed invention.The present invention claims Protection scope is defined by the appending claims and its equivalent thereof.

Claims (3)

1. a kind of acrylic leftover pieces and clast processing method, it is characterised in that: specifically include following operating procedure:
1) it recycles clast: the waste materials such as the leftover pieces, clout, clast that generate in acrylic process is collected;
2) it cleans: the big impurity (such as wooden unit, paper scrap, hair) being mixed in the waste material of centralized recovery being rejected, and passes through pulverizer Break process is carried out, it is spare to obtain acrylic pellet;
3) it cleans: pellet being placed in the rinse bath for being marked with the supersonic wave cleaning machine of cleaning solution and impregnated 1-2 hours, immersion terminates Afterwards, supersonic wave cleaning machine is opened, pellet is cleaned 20-30 minutes;
4) primary colors is handled: pellet being taken out from rinse bath and is drained, and pellet is put into cooker and is boiled, continues 1-3 Hour, the distilled water of its volume 3/4 is added in cooker, and the powdered sodium carbonate of distillation water quality 1-3% and taking off for 3-5% is added Toner;
5) it rinses: the pellet in cooker is taken out, and by distilled water to pellet repeated flushing 10-20 seconds, flushing water is returned Packaging film sealed envelope is used after receipts, is used for boiling;
6) dry: pellet being placed in 40-60 DEG C of baking oven by clean charging tray collection and is dried, it is cold that nature is taken out after drying But spare after;
7) melting remodeling: pellet after cooling is added into crucible, to vacuumize process is carried out in crucible, until crucible internal pressure After power is 0.05-0.07MPa, injected in crucible by nitrogen so that crucible external and internal pressure is identical, by intermediate frequency furnace to crucible into It goes and heats, heating temperature is 460-480 DEG C, continues 2-4 hours, so that the pellet in crucible all becomes to stop adding when molten state Heat, and fused materials are cast to the chilled glass die of preparatory surface filming, it is formed after cooling, obtains acrylic profile;
8) it stores: packaging film sealed envelope will be used after the recycling of acrylic profile, be staggeredly stacked, room temperature storage.
2. a kind of acrylic leftover pieces and clast processing method, it is characterised in that: the cleaning solution is that component by weight weighs Following material mixing forms: 1-3 parts of odium stearate, 4-7 parts of emulsifier, 3-5 parts of sodium hydroxide, 20-30 parts of water.
3. a kind of acrylic leftover pieces and clast processing method, it is characterised in that: the temperature of the cleaning solution keeps 50-60 ℃。
CN201910162109.8A 2019-03-05 2019-03-05 A kind of acrylic leftover pieces and clast processing method and preparation method thereof Pending CN109774017A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910162109.8A CN109774017A (en) 2019-03-05 2019-03-05 A kind of acrylic leftover pieces and clast processing method and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201910162109.8A CN109774017A (en) 2019-03-05 2019-03-05 A kind of acrylic leftover pieces and clast processing method and preparation method thereof

Publications (1)

Publication Number Publication Date
CN109774017A true CN109774017A (en) 2019-05-21

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115193860A (en) * 2022-03-11 2022-10-18 南通市辉鑫玻璃纤维有限公司 Leftover material treatment method for glass fiber grinding wheel net piece

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1571810A (en) * 2001-10-16 2005-01-26 帝人株式会社 Method for recycling pet bottle
CN108262886A (en) * 2018-01-23 2018-07-10 滁州英诺信电器有限公司 Acrylic carves clast treatment process

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1571810A (en) * 2001-10-16 2005-01-26 帝人株式会社 Method for recycling pet bottle
CN108262886A (en) * 2018-01-23 2018-07-10 滁州英诺信电器有限公司 Acrylic carves clast treatment process

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
刘伟: "《废旧塑料回收利用技术创新发展研究》", 30 September 2018, 北京:科学技术文献出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115193860A (en) * 2022-03-11 2022-10-18 南通市辉鑫玻璃纤维有限公司 Leftover material treatment method for glass fiber grinding wheel net piece

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