CN109771366A - Hair conditioner and preparation process are repaired in a kind of moisturizing - Google Patents
Hair conditioner and preparation process are repaired in a kind of moisturizing Download PDFInfo
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- CN109771366A CN109771366A CN201910241175.4A CN201910241175A CN109771366A CN 109771366 A CN109771366 A CN 109771366A CN 201910241175 A CN201910241175 A CN 201910241175A CN 109771366 A CN109771366 A CN 109771366A
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Abstract
The invention discloses a kind of moisturizings to repair hair conditioner and preparation process, is mixed by component A and component B 1:2 in mass ratio;The component A is to be prepared by Radix Angelicae Sinensis 20-30 parts by weight, fleece-flower root 10-15 parts by weight, Chinese gall 20-30 parts by weight, fruit of glossy privet 5-10 parts by weight, radix scrophulariae 4-8 parts by weight, cassia seed 3-6 parts by weight through composite bacteria fermentation;The component B is prepared by enzymatic hydrolysis aloe powder 15-20 parts by weight, hydrolysis of keratin 10-15 parts by weight, avenabeta glucosan 12-16 parts by weight, compound amino acid 8-12 parts by weight, polyglutamic acid sodium 3-6 parts by weight, cetearyl alcohol acid 5-9 parts by weight, vitamin 0.5-1 parts by weight.Hair conditioner of the present invention is safe and non-stimulating, is easily absorbed by scalp, can repair impaired hair scale piece, it is withered, matt to solve the problems, such as hair, and can supplement nutrition needed for hair, promotes natural on-off cycles of hair growth.
Description
Technical field
The present invention relates to Cosmetic Manufacture technical fields, and in particular to hair conditioner and preparation process are repaired in a kind of moisturizing.
Background technique
Hair conditioner makes hair keep natural balance wet, keeps the skin wet, when for hair jag, drying or being not easy to comb,
Hair moisture is helped to maintain, electrostatic is reduced and increases gloss.The hair surface layer of health is by one group of complete hair scale piece and nature
The grease of secretion constitutes the protective film of hair, and the natural protective film of this layer can all be destroyed by excessively washing reason, boiling hot dye, exposure in sunshine, causes
Cortex water loss keeps hair withered, follows the string and flexibility.Hair conditioner is only commonly used, could persistently form hair
Protective film, so that hair is escaped injury.
Currently, hair conditioner on the market contains preservative mostly, long-time service will cause harm, and hair conditioner to human body
Interior chemical substance after contacting with the air, can block pore or cause the generation of dandruff.
Based on this, it is necessary to select a kind of to be nutrition needed for hair supplement, so that hair is wet, submissive, and natural
It does not stimulate, the hair conditioner of hair follicle will not be blocked.
It is to disclose a kind of moisturizing in CN104771348A to repair hair conditioner and preparation method thereof in China Patent Publication No.,
Moisturizing reparation hair conditioner is dry by the infrared heating to Chinese medicine and Mechanical Crushing combines obtained, described Chinese medicine by weight
Amount includes following ingredient: 8-15 parts of ginger, 3-9 parts of the tuber of multiflower knotweed, 4-8 parts of ginkgo, 6-15 parts of Chinese gall, 3-7 parts of the fruit of glossy privet, Semen sesami nigrum
5-12 parts, it is 1-6 parts of pseudo-ginseng, 2-5 parts of the root bark of tree peony, 2-4 parts of cationic surfactant, 1-2 parts of thickener, 0.1-0.5 parts of essence, white
200-600 parts of wine, 2-4 parts of folium artemisiae argyi, 1-3 parts of borneol and 3-6 parts of shrubalthea leaf.The hair conditioner has certain hair care and nourishing effect, but
Due to lacking protein, amino acid, vitamins and other nutritious components, hair care and nourishing effect is limited, while used in the hair conditioner
Cationic surfactant, essence, white wine etc. are chemicals, have certain damage to hair.
Summary of the invention
In order to solve the problems in the existing technology, the present invention provides a kind of moisturizings to repair hair conditioner and preparation work
Skill, by mutually assembling the plant component of fermentation with containing nutritional ingredients such as protein, amino acid, natural mild, safety is stingless
Swash, easily absorbed by scalp, impaired hair scale piece can be repaired, it is withered, matt to solve the problems, such as hair, and battalion needed for hair can be supplemented
It supports, promotes natural on-off cycles of hair growth, while having effects that water conservation, hair is made to have wet, soft feeling.
It is of the existing technology in order to solve the problems, such as, it adopts the following technical scheme that
A kind of moisturizing reparation hair conditioner, the hair conditioner are mixed by component A and component B 1:2 in mass ratio;
The component A is by Radix Angelicae Sinensis 20-30 parts by weight, fleece-flower root 10-15 parts by weight, Chinese gall 20-30 parts by weight, glossy privet
Sub- 5-10 parts by weight, radix scrophulariae 4-8 parts by weight, cassia seed 3-6 parts by weight are prepared through composite bacteria fermentation;
The component B is by enzymatic hydrolysis aloe powder 15-20 parts by weight, hydrolysis of keratin 10-15 parts by weight, avenabeta glucosan
12-16 parts by weight, compound amino acid 8-12 parts by weight, polyglutamic acid sodium 3-6 parts by weight, cetearyl alcohol acid 5-9 parts by weight, dimension life
Plain 0.5-1 parts by weight are prepared;
Wherein, the composite bacteria agent be bacillus licheniformis, Phanerochaete chrysosporium and candidiasis in mass ratio
3:2:1 composition.
Preferably, the component A is by 25 parts by weight of Radix Angelicae Sinensis, 12.5 parts by weight of the fleece-flower root, 25 parts by weight of Chinese gall, glossy privet
Sub 7.5 parts by weight, 6 parts by weight of radix scrophulariae, 4.5 parts by weight of cassia seed are prepared through the fermentation of composite fermentation microbial inoculum;
Preferably, the component B is by 18 parts by weight of enzymatic hydrolysis aloe powder, 12.5 parts by weight of hydrolysis of keratin, oat β-Portugal
14 parts by weight of glycan, 10 parts by weight of compound amino acid, 4.5 parts by weight of polyglutamic acid sodium, cetearyl alcohol sour 7 parts by weight, vitamin
0.8 parts by weight are prepared.
Preferably, the enzymatic hydrolysis aloe powder the preparation method comprises the following steps: by aloe grinds, cross 50 meshes, be subsequently placed in enzymatic hydrolysis
In tank, the pure water of 2-4 times of aloe powder weight is added, and neutral proteinase and amylase is added, warming while stirring to 45-55
DEG C, and 20-25min is reacted at such a temperature, it is then freeze-dried to get enzymatic hydrolysis aloe powder.
Preferably, the compound amino acid is by alanine, glutamic acid, isoleucine and glycine according to mass ratio 1:1:
1:2 is mixed with.
Preferably, the preparation method of the component A includes the following steps:
(1) Radix Angelicae Sinensis, the fleece-flower root, Chinese gall, the fruit of glossy privet, radix scrophulariae and cassia seed are weighed by weight, after being mixed uniformly
It crushed 20-40 mesh, the pure water of mixture weight 35% be then added, stirs evenly;
(2) composite bacteria agent after activation is added in the mixture stirred to get to step (1), continues to stir evenly, then
Ferment 4-6h at 30-34 DEG C, is passed through air, ventilatory capacity 5L/min into mixture in the process;Then adjustment fermentation
The temperature of mixture, ferment 4-6h at 38-42 DEG C, is passed through air, ventilatory capacity 2L/min into mixture at this;Next
The temperature for adjusting fermentation material, is left to ferment 8-10h at 45-50 DEG C;
(3) tunning made from step (2) is subjected to low temperature drying, then be crushed into powder, cross 20-40 mesh to get group
Divide A.
Preferably, the preparation method of the component B includes the following steps:
(1) it by enzymatic hydrolysis aloe powder and the cetearyl alcohol acid of formula ratio, after weighing in proportion, is added with agitating device not
It becomes rusty in steel kettle, is dissolved by heating completely under the stirring of revolving speed 30-40rpm, and constant temperature disinfection 10-15min at a temperature of 70 DEG C, so
The compound amino acid and polyglutamic acid sodium for adding formula ratio afterwards, stir evenly, obtain mixture A;
(2) by the hydrolysis of keratin of formula ratio, avenabeta glucosan and vitamin, after weighing in proportion, it is added to emulsification
In pot, it is heated with stirring to 50-60 DEG C, is extracted into stainless steel homogeneous kettle by strainer later, continues to be heated to 75-85 DEG C, and
15-25min is kept the temperature at this temperature, obtains mixture B;
(3) mixture A and mixture B are put into homogenizer, and the homogeneous 10-15min at 300-400rpm, later will
Revolving speed reduction of speed is cooled to room temperature to get component B to 100-150rpm under the revolving speed.
Preferably, the present invention also provides the preparation processes that hair conditioner is repaired in above-mentioned moisturizing, comprising: counts, claims in mass ratio
It takes component A and component B to be placed in dispersion tank, is ultrasonically treated 10-15min, it is cooling, it takes out, stands 30-50min to get the guarantor
Wet reparation hair conditioner.
Preferably, the condition of the ultrasonic treatment are as follows: with 5kHz, 500W, pulse working time 4s, intermittent time 2s, 24-
28 DEG C of processing 10-15min.
Compared with prior art, the present invention it has the advantages that
1, the present invention is by mutually assembling the plant component of fermentation with containing nutritional ingredients such as protein, amino acid, naturally
Mildly, safe and non-stimulating, it is easily absorbed by scalp, impaired hair scale piece can be repaired, it is withered, matt to solve the problems, such as hair, and can mend
Nutrition needed for hair is filled, promotes natural on-off cycles of hair growth, while having effects that water conservation, hair is made to have wet, soft feeling;
2, the present invention is by carrying out fermentation process for natural plant component, so that the active constituent in plant component fills
Divide and release, secondary metabolite abundant is generated, to achieve the purpose that hair care and nourishing, while the activity in the plant component
It cooperates between ingredient, has the function of synergy, impaired hair scale piece can be repaired, solve the problems, such as that hair is withered, matt,
Have the function that consolidate;And be added enzymatic hydrolysis aloe powder, hydrolysis of keratin and compound amino acid can supplement scalp needed for egg
The nutritional ingredients such as white matter, amino acid, and the ingredient is easily absorbed by scalp, nutrition hair, to promote the growth of hair;
3, the avenabeta glucosan that the present invention is added a kind of natural water-retaining agent and emollients, can assist moisture content combination scalp
Keratin in cuticula has preferable water retention, prevents hair moisture from evaporating, and keeps the submissive silk of hair sliding, meanwhile, oat
Beta glucan has certain anti-static electrification, can avoid hair since electrostatic interaction adsorbs dust, keeps hair cleaning;
4, polyglutamic acid sodium of the invention has splendid moisturizing, storage capacity, replenishing water and preserving moisture and the scalp that can releive, and grows
The effect of supporting scalp, promoting hair growth and oil-control;
5, the collaboration of hair conditioner each component is repaired in moisturizing of the present invention, and moistening effect is good, and safe and non-stimulating, while the present invention protects
The preparation method for sending out element is simple, can promote the use of.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, technical solution of the present invention will be carried out below
Clear, complete description.Obviously, the described embodiment is only a part of the embodiment of the present invention, instead of all the embodiments.
Based on the embodiments of the present invention, those of ordinary skill in the art obtained institute without making creative work
There are other embodiments, belongs to the range that the present invention is protected.
Embodiment 1
Hair conditioner is repaired in the moisturizing of the present embodiment, which is mixed by component A and component B 1:2 in mass ratio;
The component A is by 20 parts by weight of Radix Angelicae Sinensis, 10 parts by weight of the fleece-flower root, 20 parts by weight of Chinese gall, 5 weight of the fruit of glossy privet
Part, 4 parts by weight of radix scrophulariae, 3 parts by weight of cassia seed are prepared through composite bacteria fermentation;
The component B is by 15 parts by weight of enzymatic hydrolysis aloe powder, 10 parts by weight of hydrolysis of keratin, 12 weight of avenabeta glucosan
Part, sour 5 parts by weight of 8 parts by weight of compound amino acid, 3 parts by weight of polyglutamic acid sodium, cetearyl alcohol, the preparation of 0.5 parts by weight of vitamin
It forms;
Wherein, the composite bacteria agent be bacillus licheniformis, Phanerochaete chrysosporium and candidiasis in mass ratio
3:2:1 composition.
Wherein, the enzymatic hydrolysis aloe powder the preparation method comprises the following steps: by aloe grinds, cross 50 meshes, be subsequently placed in enzymatic vessel
In, 2 times of aloe powder weight of pure water is added, and neutral proteinase and amylase is added, warming while stirring is to 45 DEG C, and at this
At a temperature of react 20min, be then freeze-dried to get enzymatic hydrolysis aloe powder.
Wherein, the compound amino acid is by alanine, glutamic acid, isoleucine and glycine according to mass ratio 1:1:1:
2 are mixed with.
Wherein, the preparation method of the component A includes the following steps:
(1) Radix Angelicae Sinensis, the fleece-flower root, Chinese gall, the fruit of glossy privet, radix scrophulariae and cassia seed are weighed by weight, after being mixed uniformly
It crushed 20-40 mesh, the pure water of mixture weight 35% be then added, stirs evenly;
(2) composite bacteria agent after activation is added in the mixture stirred to get to step (1), continues to stir evenly, then
Ferment 4h at 30 DEG C, is passed through air, ventilatory capacity 5L/min into mixture in the process;Then adjust fermenting mixture
Temperature, ferment 4-6h at 38 DEG C, is passed through air, ventilatory capacity 2L/min into mixture at this;Next adjustment fermentation
The temperature of object is left to ferment 8h at 45 DEG C;
(3) tunning made from step (2) is subjected to low temperature drying, then be crushed into powder, cross 20-40 mesh to get group
Divide A.
Wherein, the preparation method of the component B includes the following steps:
(1) it by enzymatic hydrolysis aloe powder and the cetearyl alcohol acid of formula ratio, after weighing in proportion, is added with agitating device not
It becomes rusty in steel kettle, is dissolved by heating completely under the stirring of revolving speed 30rpm, and constant temperature disinfection 10min at a temperature of 70 DEG C, then added again
The compound amino acid and polyglutamic acid sodium for entering formula ratio, stir evenly, obtain mixture A;
(2) by the hydrolysis of keratin of formula ratio, avenabeta glucosan and vitamin, after weighing in proportion, it is added to emulsification
In pot, 50 DEG C are heated with stirring to, is extracted into stainless steel homogeneous kettle by strainer later, continues to be heated to 75 DEG C, and in the temperature
Lower heat preservation 15min, obtains mixture B;
(3) mixture A and mixture B are put into homogenizer, and homogeneous 10min at 3,000 rpm, later drop revolving speed
Speed is cooled to room temperature to get component B to 100rpm under the revolving speed.
Wherein, the present invention also provides the preparation processes that hair conditioner is repaired in above-mentioned moisturizing, comprising: counts, weighs in mass ratio
Component A and component B are placed in dispersion tank, are ultrasonically treated 10min, cooling, are taken out, and are stood 30min and are protected to get the moisturizing reparation
Hair element.
Wherein, the condition of the ultrasonic treatment are as follows: with 5kHz, 500W, pulse working time 4s, intermittent time 2s, 24 DEG C
Handle 10min.
Embodiment 2
Hair conditioner is repaired in the moisturizing of the present embodiment, which is mixed by component A and component B 1:2 in mass ratio;
The component A is by 30 parts by weight of Radix Angelicae Sinensis, 15 parts by weight of the fleece-flower root, 30 parts by weight of Chinese gall, 10 weight of the fruit of glossy privet
Part, 8 parts by weight of radix scrophulariae, 6 parts by weight of cassia seed are prepared through composite bacteria fermentation;
The component B is by 20 parts by weight of enzymatic hydrolysis aloe powder, 15 parts by weight of hydrolysis of keratin, 16 weight of avenabeta glucosan
Part, 12 parts by weight of compound amino acid, 6 parts by weight of polyglutamic acid sodium, cetearyl alcohol sour 9 parts by weight, vitamin 0.5-1 parts by weight system
It is standby to form;
Wherein, the composite bacteria agent be bacillus licheniformis, Phanerochaete chrysosporium and candidiasis in mass ratio
3:2:1 composition.
Wherein, the enzymatic hydrolysis aloe powder the preparation method comprises the following steps: by aloe grinds, cross 50 meshes, be subsequently placed in enzymatic vessel
In, 4 times of aloe powder weight of pure water is added, and neutral proteinase and amylase is added, warming while stirring is to 55 DEG C, and at this
At a temperature of react 25min, be then freeze-dried to get enzymatic hydrolysis aloe powder.
Wherein, the compound amino acid is by alanine, glutamic acid, isoleucine and glycine according to mass ratio 1:1:1:
2 are mixed with.
Wherein, the preparation method of the component A includes the following steps:
(1) Radix Angelicae Sinensis, the fleece-flower root, Chinese gall, the fruit of glossy privet, radix scrophulariae and cassia seed are weighed by weight, after being mixed uniformly
It crushed 20-40 mesh, the pure water of mixture weight 35% be then added, stirs evenly;
(2) composite bacteria agent after activation is added in the mixture stirred to get to step (1), continues to stir evenly, then
Ferment 6h at 34 DEG C, is passed through air, ventilatory capacity 5L/min into mixture in the process;Then adjust fermenting mixture
Temperature, ferment 6h at 42 DEG C, is passed through air, ventilatory capacity 2L/min into mixture at this;Next adjustment fermentation material
Temperature, be left to ferment 10h at 50 DEG C;
(3) tunning made from step (2) is subjected to low temperature drying, then be crushed into powder, cross 20-40 mesh to get group
Divide A.
Wherein, the preparation method of the component B includes the following steps:
(1) it by enzymatic hydrolysis aloe powder and the cetearyl alcohol acid of formula ratio, after weighing in proportion, is added with agitating device not
It becomes rusty in steel kettle, is dissolved by heating completely under the stirring of revolving speed 40rpm, and constant temperature disinfection 15min at a temperature of 70 DEG C, then added again
The compound amino acid and polyglutamic acid sodium for entering formula ratio, stir evenly, obtain mixture A;
(2) by the hydrolysis of keratin of formula ratio, avenabeta glucosan and vitamin, after weighing in proportion, it is added to emulsification
In pot, 60 DEG C are heated with stirring to, is extracted into stainless steel homogeneous kettle by strainer later, continues to be heated to 85 DEG C, and in the temperature
Lower heat preservation 25min, obtains mixture B;
(3) mixture A and mixture B are put into homogenizer, and the homogeneous 15min at 400rpm, later drop revolving speed
Speed is cooled to room temperature to get component B to 150rpm under the revolving speed.
Wherein, the present invention also provides the preparation processes that hair conditioner is repaired in above-mentioned moisturizing, comprising: counts, weighs in mass ratio
Component A and component B are placed in dispersion tank, are ultrasonically treated 15min, cooling, are taken out, and are stood 50min and are protected to get the moisturizing reparation
Hair element.
Wherein, the condition of the ultrasonic treatment are as follows: with 5kHz, 500W, pulse working time 4s, intermittent time 2s, 28 DEG C
Handle 15min.
Embodiment 3
Hair conditioner is repaired in the moisturizing of the present embodiment, which is mixed by component A and component B 1:2 in mass ratio;
The component A is by 25 parts by weight of Radix Angelicae Sinensis, 12.5 parts by weight of the fleece-flower root, 25 parts by weight of Chinese gall, 7.5 weight of the fruit of glossy privet
Amount part, 6 parts by weight of radix scrophulariae, 4.5 parts by weight of cassia seed are prepared through the fermentation of composite fermentation microbial inoculum;
The component B is by 18 parts by weight of enzymatic hydrolysis aloe powder, 12.5 parts by weight of hydrolysis of keratin, 14 weight of avenabeta glucosan
Measure part, 10 parts by weight of compound amino acid, 4.5 parts by weight of polyglutamic acid sodium, cetearyl alcohol sour 7 parts by weight, 0.8 parts by weight of vitamin
It is prepared;
Wherein, the composite bacteria agent be bacillus licheniformis, Phanerochaete chrysosporium and candidiasis in mass ratio
3:2:1 composition.
Wherein, the enzymatic hydrolysis aloe powder the preparation method comprises the following steps: by aloe grinds, cross 50 meshes, be subsequently placed in enzymatic vessel
In, 3 times of aloe powder weight of pure water is added, and neutral proteinase and amylase is added, warming while stirring is to 50 DEG C, and at this
At a temperature of react 23min, be then freeze-dried to get enzymatic hydrolysis aloe powder.
Wherein, the compound amino acid is by alanine, glutamic acid, isoleucine and glycine according to mass ratio 1:1:1:
2 are mixed with.
Wherein, the preparation method of the component A includes the following steps:
(1) Radix Angelicae Sinensis, the fleece-flower root, Chinese gall, the fruit of glossy privet, radix scrophulariae and cassia seed are weighed by weight, after being mixed uniformly
It crushed 20-40 mesh, the pure water of mixture weight 35% be then added, stirs evenly;
(2) composite bacteria agent after activation is added in the mixture stirred to get to step (1), continues to stir evenly, then
Ferment 5h at 32 DEG C, is passed through air, ventilatory capacity 5L/min into mixture in the process;Then adjust fermenting mixture
Temperature, ferment 5h at 40 DEG C, is passed through air, ventilatory capacity 2L/min into mixture at this;Next adjustment fermentation material
Temperature, be left to ferment 9h at 48 DEG C;
(3) tunning made from step (2) is subjected to low temperature drying, then be crushed into powder, cross 20-40 mesh to get group
Divide A.
Wherein, the preparation method of the component B includes the following steps:
(1) it by enzymatic hydrolysis aloe powder and the cetearyl alcohol acid of formula ratio, after weighing in proportion, is added with agitating device not
It becomes rusty in steel kettle, is dissolved by heating completely under the stirring of revolving speed 35rpm, and constant temperature disinfection 13min at a temperature of 70 DEG C, then added again
The compound amino acid and polyglutamic acid sodium for entering formula ratio, stir evenly, obtain mixture A;
(2) by the hydrolysis of keratin of formula ratio, avenabeta glucosan and vitamin, after weighing in proportion, it is added to emulsification
In pot, 55 DEG C are heated with stirring to, is extracted into stainless steel homogeneous kettle by strainer later, continues to be heated to 80 DEG C, and in the temperature
Lower heat preservation 20min, obtains mixture B;
(3) mixture A and mixture B are put into homogenizer, and the homogeneous 13min at 350rpm, later drop revolving speed
Speed is cooled to room temperature to get component B to 125rpm under the revolving speed.
Wherein, the present invention also provides the preparation processes that hair conditioner is repaired in above-mentioned moisturizing, comprising: counts, weighs in mass ratio
Component A and component B are placed in dispersion tank, are ultrasonically treated 13min, cooling, are taken out, and are stood 40min and are protected to get the moisturizing reparation
Hair element.
Wherein, the condition of the ultrasonic treatment are as follows: with 5kHz, 500W, pulse working time 4s, intermittent time 2s, 26 DEG C
Handle 13min.
Embodiment 4
Hair conditioner is repaired in the moisturizing of the present embodiment, which is mixed by component A and component B 1:2 in mass ratio;
The component A is by 23 parts by weight of Radix Angelicae Sinensis, 11 parts by weight of the fleece-flower root, 22 parts by weight of Chinese gall, 6 weight of the fruit of glossy privet
Part, 5 parts by weight of radix scrophulariae, 4 parts by weight of cassia seed are prepared through composite bacteria fermentation;
The component B is by 16 parts by weight of enzymatic hydrolysis aloe powder, 11 parts by weight of hydrolysis of keratin, 13 weight of avenabeta glucosan
Part, sour 6 parts by weight of 9 parts by weight of compound amino acid, 4 parts by weight of polyglutamic acid sodium, cetearyl alcohol, the preparation of 0.6 parts by weight of vitamin
It forms;
Wherein, the composite bacteria agent be bacillus licheniformis, Phanerochaete chrysosporium and candidiasis in mass ratio
3:2:1 composition.
Wherein, the enzymatic hydrolysis aloe powder the preparation method comprises the following steps: by aloe grinds, cross 50 meshes, be subsequently placed in enzymatic vessel
In, 2.5 times of aloe powder weight of pure water is added, and neutral proteinase and amylase is added, warming while stirring to 48 DEG C, and
22min is reacted at this temperature, is then freeze-dried to get enzymatic hydrolysis aloe powder.
Wherein, the compound amino acid is by alanine, glutamic acid, isoleucine and glycine according to mass ratio 1:1:1:
2 are mixed with.
Wherein, the preparation method of the component A includes the following steps:
(1) Radix Angelicae Sinensis, the fleece-flower root, Chinese gall, the fruit of glossy privet, radix scrophulariae and cassia seed are weighed by weight, after being mixed uniformly
It crushed 20-40 mesh, the pure water of mixture weight 35% be then added, stirs evenly;
(2) composite bacteria agent after activation is added in the mixture stirred to get to step (1), continues to stir evenly, then
Ferment 4.5h at 31 DEG C, is passed through air, ventilatory capacity 5L/min into mixture in the process;Then adjustment fermentation mixing
The temperature of object, ferment 4.5h at 39 DEG C, is passed through air, ventilatory capacity 2L/min into mixture at this;Next adjustment hair
The temperature of ferment object is left to ferment 8.5h at 46 DEG C;
(3) tunning made from step (2) is subjected to low temperature drying, then be crushed into powder, cross 20-40 mesh to get group
Divide A.
Wherein, the preparation method of the component B includes the following steps:
(1) it by enzymatic hydrolysis aloe powder and the cetearyl alcohol acid of formula ratio, after weighing in proportion, is added with agitating device not
It becomes rusty in steel kettle, is dissolved by heating completely under the stirring of revolving speed 33rpm, and constant temperature disinfection 11min at a temperature of 70 DEG C, then added again
The compound amino acid and polyglutamic acid sodium for entering formula ratio, stir evenly, obtain mixture A;
(2) by the hydrolysis of keratin of formula ratio, avenabeta glucosan and vitamin, after weighing in proportion, it is added to emulsification
In pot, 53 DEG C are heated with stirring to, is extracted into stainless steel homogeneous kettle by strainer later, continues to be heated to 78 DEG C, and in the temperature
Lower heat preservation 18min, obtains mixture B;
(3) mixture A and mixture B are put into homogenizer, and the homogeneous 12min at 330rpm, later drop revolving speed
Speed is cooled to room temperature to get component B to 110rpm under the revolving speed.
Wherein, the present invention also provides the preparation processes that hair conditioner is repaired in above-mentioned moisturizing, comprising: counts, weighs in mass ratio
Component A and component B are placed in dispersion tank, are ultrasonically treated 12min, cooling, are taken out, and are stood 35min and are protected to get the moisturizing reparation
Hair element.
Wherein, the condition of the ultrasonic treatment are as follows: with 5kHz, 500W, pulse working time 4s, intermittent time 2s, 25 DEG C
Handle 12min.
Embodiment 5
Hair conditioner is repaired in the moisturizing of the present embodiment, which is mixed by component A and component B 1:2 in mass ratio;
The component A is by 28 parts by weight of Radix Angelicae Sinensis, 14 parts by weight of the fleece-flower root, 28 parts by weight of Chinese gall, 9 weight of the fruit of glossy privet
Part, 7 parts by weight of radix scrophulariae, 5 parts by weight of cassia seed are prepared through composite bacteria fermentation;
The component B is by 19 parts by weight of enzymatic hydrolysis aloe powder, 14 parts by weight of hydrolysis of keratin, 15 weight of avenabeta glucosan
Part, sour 8 parts by weight of 11 parts by weight of compound amino acid, 5 parts by weight of polyglutamic acid sodium, cetearyl alcohol, the preparation of 0.9 parts by weight of vitamin
It forms;
Wherein, the composite bacteria agent be bacillus licheniformis, Phanerochaete chrysosporium and candidiasis in mass ratio
3:2:1 composition.
Wherein, the enzymatic hydrolysis aloe powder the preparation method comprises the following steps: by aloe grinds, cross 50 meshes, be subsequently placed in enzymatic vessel
In, 3.5 times of aloe powder weight of pure water is added, and neutral proteinase and amylase is added, warming while stirring to 52 DEG C, and
24min is reacted at this temperature, is then freeze-dried to get enzymatic hydrolysis aloe powder.
Wherein, the compound amino acid is by alanine, glutamic acid, isoleucine and glycine according to mass ratio 1:1:1:
2 are mixed with.
Wherein, the preparation method of the component A includes the following steps:
(1) Radix Angelicae Sinensis, the fleece-flower root, Chinese gall, the fruit of glossy privet, radix scrophulariae and cassia seed are weighed by weight, after being mixed uniformly
It crushed 20-40 mesh, the pure water of mixture weight 35% be then added, stirs evenly;
(2) composite bacteria agent after activation is added in the mixture stirred to get to step (1), continues to stir evenly, then
Ferment 5.5h at 33 DEG C, is passed through air, ventilatory capacity 5L/min into mixture in the process;Then adjustment fermentation mixing
The temperature of object, ferment 4-6h at 41 DEG C, is passed through air, ventilatory capacity 2L/min into mixture at this;Next adjustment hair
The temperature of ferment object is left to ferment 9.5h at 48 DEG C;
(3) tunning made from step (2) is subjected to low temperature drying, then be crushed into powder, cross 20-40 mesh to get group
Divide A.
Wherein, the preparation method of the component B includes the following steps:
(1) it by enzymatic hydrolysis aloe powder and the cetearyl alcohol acid of formula ratio, after weighing in proportion, is added with agitating device not
It becomes rusty in steel kettle, is dissolved by heating completely under the stirring of revolving speed 38rpm, and constant temperature disinfection 14min at a temperature of 70 DEG C, then added again
The compound amino acid and polyglutamic acid sodium for entering formula ratio, stir evenly, obtain mixture A;
(2) by the hydrolysis of keratin of formula ratio, avenabeta glucosan and vitamin, after weighing in proportion, it is added to emulsification
In pot, 58 DEG C are heated with stirring to, is extracted into stainless steel homogeneous kettle by strainer later, continues to be heated to 83 DEG C, and in the temperature
Lower heat preservation 22min, obtains mixture B;
(3) mixture A and mixture B are put into homogenizer, and the homogeneous 14min at 380rpm, later drop revolving speed
Speed is cooled to room temperature to get component B to 140rpm under the revolving speed.
Wherein, the present invention also provides the preparation processes that hair conditioner is repaired in above-mentioned moisturizing, comprising: counts, weighs in mass ratio
Component A and component B are placed in dispersion tank, are ultrasonically treated 14min, cooling, are taken out, and are stood 45min and are protected to get the moisturizing reparation
Hair element.
Wherein, the condition of the ultrasonic treatment are as follows: with 5kHz, 500W, pulse working time 4s, intermittent time 2s, 27 DEG C
Handle 14min.
Comparative example 1
Except by the composite bacteria agent in component A and in addition to fermentation step saves, other material content agent preparation steps are the same as embodiment 1
Unanimously.
Comparative example 2
In addition to it will digest aloe powder, hydrolysis of keratin saves, other material contents and preparation step are consistent with embodiment 1.
Comparative example 3
In addition to saving avenabeta glucosan, other material contents and preparation step are consistent with embodiment 1.
Comparative example 4
In addition to saving compound amino acid, other material contents and preparation step are consistent with embodiment 1.
Experimental example 1
Hair conditioner made from embodiment 1-5 and comparative example 1-4 is subjected to repairing effect verifying, steps are as follows for specific experiment:
(1) taking length is the hair of 10cm, and every 10 are one group, totally 9 groups.Use quality dense respectively in each group hair chosen
The sodium dodecyl sulfate solution 2g of degree 3% is cleaned, and carries out mechanical rubbing 5 minutes to each group hair, then under the microscope
Observation each group hair surface hair scale piece eucaryotic cell structure destroys situation and counts, marks.
(2) above-mentioned each group hair is soaked in respectively in hair conditioner made from embodiment 1-5 and comparative example 1-4, and constantly
Agitation, respectively 5 minutes, 10 minutes, 15 minutes, after twenty minutes take out, rinsed 3 times with clear water, it is 1 minute every time, then natural
It dries.
(3) each group hair after drying is observed under the microscope respectively, in counting step (1) mark hair surface by
Damage hair scale piece eucaryotic cell structure repairs situation and calculates repair rate:
Repair rate=reparation hair scale piece total number of cells/impaired hair scale piece total number of cells × 100%
Specific hair surface is damaged hair scale piece eucaryotic cell structure reparation result (percentage is repair rate in table) and is shown in Table 1:
Table 1
Test item | 5 minutes | 10 minutes | 15 minutes | 20 minutes |
Embodiment 1 | 68% | 78% | 83% | 86% |
Embodiment 2 | 70% | 81% | 85% | 88% |
Embodiment 3 | 72% | 83% | 87% | 90% |
Embodiment 4 | 71% | 81% | 85% | 87% |
Embodiment 5 | 70% | 81% | 86% | 89% |
Comparative example 1 | 55% | 63% | 66% | 70% |
Comparative example 2 | 60% | 69% | 71% | 74% |
Comparative example 3 | 64% | 72% | 78% | 81% |
Comparative example 4 | 66% | 74% | 79% | 83% |
As shown in Table 1, it is good to repair hair conditioner repairing effect for moisturizing of the invention, wherein moisturizing reparation made from embodiment 3
Hair conditioner effect is optimal, and from comparative example 1-4 it is found that by carrying out fermentation process to plant component and being added into hair conditioner
The repairing effect of hair conditioner can be improved in enzymatic hydrolysis aloe powder, hydrolysis of keratin, avenabeta glucosan, compound amino acid.
Experimental example 2
The hair conditioner of the above embodiments 1-5 and comparative example 1-3 are subjected to hair care effect measurement to hair swatch, it is specific to survey
Method for testing is as follows:
The relative humidity for testing environment is 40-60%, and the tested long 30cm of hair is all from the same female volunteer, year
Age 25 years old, long hair, natural straight hair (being unstained).
By hair using embodiment 1-5 and comparative example 1-4 hair conditioner coating uniformly, and gently rub 2min, then with 30
DEG C clear water rinse 5min, wet hair sample is placed under 25 DEG C of temperature, 50%RH damp condition and tested after naturally dry 3h.
The standard specifically tested: using surface specific resistance tester, referring to standard GB/T/T16801-1997 and GB/
It is quiet to evaluate the anti-hair of above-mentioned hair conditioner with surface specific resistance drop for the method that T14342-93 is measured the softening agent of fabric
Electrical property, surface specific resistance drop is bigger, shows that antistatic property is better.
Using LDY type anti-static instrument, referring to FZ/T01042-1996 textile material antistatic property measuring method, when with decaying
Between T1/2 (s) evaluate the above-mentioned anti-hair antistatic property of hair conditioner, half-life period is shorter, shows that above-mentioned hair conditioner antistatic property is got over
It is good.
Friction factor μ after being stated hair conditioner in use using Y151 fiber type friction factor analyzer measurement hair, is rubbed
Resistance and its normal pressure ratio are wiped static friction factor μ s, the ratio between mean kinetic friction force and its normal pressure are dynamic friction factor μ d.It rubs
Wiping factor is smaller, shows that the flatness of hair is better, cardability is also better.
The hair gloss after using above-mentioned hair conditioner is measured using hair-brightness determination instrument, units gloss degree is bigger,
Show that hair gloss is better.
Each sample repeats to survey 3 times, takes its average value.
Specifically test that the results are shown in Table 2:
Table 2
As shown in Table 2, using hair conditioner provided by the invention cleaning after hair can significantly improve its easy cardability and
Glossiness, wherein the effect of embodiment 3 is optimal, and by comparative example 1-4 it is found that by carrying out fermentation process to plant component
And enzymatic hydrolysis aloe powder, hydrolysis of keratin, avenabeta glucosan, compound amino acid is added into hair conditioner, the easy of hair can be improved
Cardability and glossiness.
In conclusion the present invention provides a kind of moisturizings to repair hair conditioner and preparation process, by the plant that will ferment at
Divide and is mutually assembled with containing nutritional ingredients such as protein, amino acid, it is natural mild, it is safe and non-stimulating, it is easily absorbed, can repair by scalp
It is withered, matt to solve the problems, such as hair, and can supplement nutrition needed for hair for impaired hair scale piece, promotes natural on-off cycles of hair growth, has simultaneously
It is retained effect, hair is made to have wet, soft feeling.
Specific embodiments of the present invention are described above.It is to be appreciated that the invention is not limited to above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring substantive content of the invention.
Claims (9)
1. hair conditioner is repaired in a kind of moisturizing, which is characterized in that the hair conditioner by component A and component B 1:2 in mass ratio mixing and
At;
The component A is by Radix Angelicae Sinensis 20-30 parts by weight, fleece-flower root 10-15 parts by weight, Chinese gall 20-30 parts by weight, fruit of glossy privet 5-
10 parts by weight, radix scrophulariae 4-8 parts by weight, cassia seed 3-6 parts by weight are prepared through composite bacteria fermentation;
The component B is by enzymatic hydrolysis aloe powder 15-20 parts by weight, hydrolysis of keratin 10-15 parts by weight, avenabeta glucosan 12-
16 parts by weight, compound amino acid 8-12 parts by weight, polyglutamic acid sodium 3-6 parts by weight, cetearyl alcohol acid 5-9 parts by weight, vitamin
0.5-1 parts by weight are prepared;
Wherein, the composite bacteria agent is bacillus licheniformis, Phanerochaete chrysosporium and candidiasis 3:2:1 in mass ratio
Composition.
2. hair conditioner is repaired in moisturizing according to claim 1, which is characterized in that the component A be by 25 parts by weight of Radix Angelicae Sinensis,
12.5 parts by weight of the fleece-flower root, 25 parts by weight of Chinese gall, 7.5 parts by weight of the fruit of glossy privet, 6 parts by weight of radix scrophulariae, 4.5 parts by weight of cassia seed warp
The fermentation of composite fermentation microbial inoculum is prepared.
3. hair conditioner is repaired in moisturizing according to claim 1, which is characterized in that the component B is by enzymatic hydrolysis aloe powder 18
Parts by weight, 12.5 parts by weight of hydrolysis of keratin, 14 parts by weight of avenabeta glucosan, 10 parts by weight of compound amino acid, polyglutamic acid
Sour 7 parts by weight of 4.5 parts by weight of sodium, cetearyl alcohol, 0.8 parts by weight of vitamin are prepared.
4. hair conditioner is repaired in moisturizing according to claim 1, which is characterized in that the preparation method of the enzymatic hydrolysis aloe powder
Are as follows: by aloe grinds, 50 meshes are crossed, are subsequently placed in enzymatic vessel, the pure water of 2-4 times of aloe powder weight is added, and in addition
Property protease and amylase, warming while stirring react 20-25min to 45-55 DEG C at such a temperature, are then freeze-dried,
Up to enzymatic hydrolysis aloe powder.
5. hair conditioner is repaired in moisturizing according to claim 1, which is characterized in that the compound amino acid be by alanine,
Glutamic acid, isoleucine and glycine are mixed with according to mass ratio 1:1:1:2.
6. hair conditioner is repaired in moisturizing according to claim 1, which is characterized in that the preparation method of the component A includes such as
Lower step:
(1) Radix Angelicae Sinensis, the fleece-flower root, Chinese gall, the fruit of glossy privet, radix scrophulariae and cassia seed are weighed by weight, are crushed after being mixed uniformly
20-40 mesh is crossed, the pure water of mixture weight 35% is then added, stirs evenly;
(2) composite bacteria agent after activation is added in the mixture stirred to get to step (1), continues to stir evenly, then in 30-
Ferment 4-6h at 34 DEG C, is passed through air, ventilatory capacity 5L/min into mixture in the process;Then adjust fermenting mixture
Temperature, ferment 4-6h at 38-42 DEG C, is passed through air, ventilatory capacity 2L/min into mixture at this;Next adjustment hair
The temperature of ferment object is left to ferment 8-10h at 45-50 DEG C;
(3) tunning made from step (2) is subjected to low temperature drying, then be crushed into powder, cross 20-40 mesh to get component A.
7. hair conditioner is repaired in moisturizing according to claim 1, which is characterized in that the preparation method of the component B includes such as
Lower step:
(1) by enzymatic hydrolysis aloe powder and the cetearyl alcohol acid of formula ratio, after weighing in proportion, the stainless steel for having agitating device is added
In kettle, dissolved by heating completely under the stirring of revolving speed 30-40rpm, and constant temperature disinfection 10-15min at a temperature of 70 DEG C, then again
The compound amino acid and polyglutamic acid sodium of formula ratio is added, stirs evenly, obtains mixture A;
(2) it by the hydrolysis of keratin of formula ratio, avenabeta glucosan and vitamin, after weighing in proportion, is added in emulsion pot,
It is heated with stirring to 50-60 DEG C, is extracted into stainless steel homogeneous kettle by strainer later, continues to be heated to 75-85 DEG C, and in the temperature
Lower heat preservation 15-25min, obtains mixture B;
(3) mixture A and mixture B are put into homogenizer, and the homogeneous 10-15min at 300-400rpm, later by revolving speed
Reduction of speed is cooled to room temperature to get component B to 100-150rpm under the revolving speed.
8. the preparation process that hair conditioner is repaired in moisturizing according to claim 1-7 characterized by comprising press
Mass ratio meter, weighs component A and component B is placed in dispersion tank, is ultrasonically treated 10-15min, cooling, takes out, stands 30-
50min repairs hair conditioner to get the moisturizing.
9. the preparation process that hair conditioner is repaired in moisturizing according to claim 8, which is characterized in that the item of the ultrasonic treatment
Part are as follows: with 5kHz, 500W, 2s, 24-28 DEG C of pulse working time 4s, intermittent time processing 10-15min.
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Cited By (2)
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CN111617015A (en) * | 2020-06-19 | 2020-09-04 | 黄河三角洲京博化工研究院有限公司 | Antibacterial and itching-relieving enzyme hair conditioner and preparation method thereof |
CN113576954A (en) * | 2021-08-31 | 2021-11-02 | 苏州博克生物科技股份有限公司 | Plant-based damaged repair hair conditioner and plant processing technology thereof |
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2019
- 2019-03-28 CN CN201910241175.4A patent/CN109771366A/en active Pending
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN111617015A (en) * | 2020-06-19 | 2020-09-04 | 黄河三角洲京博化工研究院有限公司 | Antibacterial and itching-relieving enzyme hair conditioner and preparation method thereof |
CN113576954A (en) * | 2021-08-31 | 2021-11-02 | 苏州博克生物科技股份有限公司 | Plant-based damaged repair hair conditioner and plant processing technology thereof |
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