CN109762260A - A kind of building decoration fire proofing and preparation method thereof - Google Patents
A kind of building decoration fire proofing and preparation method thereof Download PDFInfo
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- CN109762260A CN109762260A CN201811446644.8A CN201811446644A CN109762260A CN 109762260 A CN109762260 A CN 109762260A CN 201811446644 A CN201811446644 A CN 201811446644A CN 109762260 A CN109762260 A CN 109762260A
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Abstract
The present invention relates to building decoration technology fields, specifically a kind of building decoration fire proofing, is characterized in that: including below according to the raw material of parts by weight: 15-25 parts of polystyrene resin, 10-20 parts of waterglass, 15-20 parts of butyryl citric acid tri-n-hexyl ester, 5-15 parts of titanium dioxide, 5-12 parts of carbide slag, 6-10 parts of nano-grade aluminum hydroxide, 5-8 parts of hydrotalcite, 5-8 parts of montmorillonite.The invention also discloses the preparation methods of the building decoration fire proofing.Building decoration fire proofing prepared by the present invention has excellent flame retardant property, but also has good compression strength, can satisfy the market demand, has a vast market foreground.
Description
Technical field
The present invention relates to building decoration technology field, specifically a kind of building decoration fire proofing and preparation method thereof.
Background technique
Building decoration is to protect the main structure of building, the physical property for improving building, using function and beautification
Building, the various treatment processes that the surfaces externally and internally of building and space are carried out using decorating and renovating material or jewelry.Building
Decoration is indispensable a part in people's life.Architectural decoration has become three big mainstay industries in construction industry
One of, it is a labour intensive profession.Architectural decoration is the gradually rise with real estate upsurge, and Fast Growth gets up
Rising industry.
The building fire due to caused by ornament materials is not up to standard occurs in succession, in order to reduce security risk, so building
Ornament materials has to excellent flame retardant property.In consideration of it, the invention proposes a kind of building decoration fire proofing and its systems
Preparation Method.
Summary of the invention
The purpose of the present invention is to provide a kind of building decoration fire proofings and preparation method thereof, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the invention provides the following technical scheme:
A kind of building decoration fire proofing, including below according to the raw material of parts by weight: 15-25 parts of polystyrene resin, water
10-20 parts of glass, 15-20 parts of butyryl citric acid tri-n-hexyl ester, 5-15 parts of titanium dioxide, 5-12 parts of carbide slag, nanoscale hydroxide
6-10 parts of aluminium, 5-8 parts of hydrotalcite, 5-8 parts of montmorillonite.
As a further solution of the present invention: including below according to the raw material of parts by weight: 18-23 parts of polystyrene resin,
12-18 parts of waterglass, 15-17 parts of butyryl citric acid tri-n-hexyl ester, 7-15 parts of titanium dioxide, 5-10 parts of carbide slag, nanoscale hydrogen-oxygen
Change aluminium 7-10 parts, 5-7 parts of hydrotalcite, 5-7 parts of montmorillonite.
As further scheme of the invention: including below according to the raw material of parts by weight: 20 parts of polystyrene resin, water
16 parts of glass, 16 parts of butyryl citric acid tri-n-hexyl ester, 10 parts of titanium dioxide, 8 parts of carbide slag, 8 parts of nano-grade aluminum hydroxide, hydrotalcite
6 parts, 6 parts of montmorillonite.
The preparation method of the building decoration fire proofing, steps are as follows:
1) polystyrene resin, waterglass, butyryl citric acid tri-n-hexyl ester, titanium dioxide, calcium carbide are successively taken according to parts by weight
Slag, nano-grade aluminum hydroxide, hydrotalcite and montmorillonite, it is spare；
2) titanium dioxide taken in step 1) and carbide slag are mixed, grinds 30min, obtains material A, it is spare；
3) polystyrene resin taken in step 1) and waterglass are mixed, the stir process 20- at a temperature of 65 DEG C
30min obtains material B, spare；
4) material A and material B are mixed, adds the butyryl citric acid tri-n-hexyl ester taken in step 1), nanoscale hydrogen
Aluminium oxide, hydrotalcite and montmorillonite, 70 DEG C at a temperature of stir 10min, obtain material C；
5) material C is subjected to microwave treatment and obtains material D then in 80-90 DEG C of at a temperature of stir process 20min；
6) material D is formed, and is aged to get the building decoration fire proofing.
As the present invention further scheme: in step 5), microwave treatment time 20min, microwave power is
1000W。
As further scheme of the invention: in step 6), digestion time 30-35h.
The building decoration fire proofing is preparing the purposes in dalle product.
A kind of dalle based on the building decoration fire proofing.
Compared with prior art, the beneficial effects of the present invention are:
Building decoration fire proofing prepared by the present invention has excellent flame retardant property, but also has good pressure resistance
Degree, can satisfy the market demand, has a vast market foreground.
Specific embodiment
The technical solution of the patent is explained in further detail With reference to embodiment.
Embodiment 1
A kind of building decoration fire proofing, including below according to the raw material of parts by weight: 15 parts of polystyrene resin, waterglass
10 parts, 15 parts of butyryl citric acid tri-n-hexyl ester, 5 parts of titanium dioxide, 5 parts of carbide slag, 6 parts of nano-grade aluminum hydroxide, 5 parts of hydrotalcite,
5 parts of montmorillonite.
In the present embodiment, the preparation method of the building decoration fire proofing, steps are as follows:
1) polystyrene resin, waterglass, butyryl citric acid tri-n-hexyl ester, titanium dioxide, calcium carbide are successively taken according to parts by weight
Slag, nano-grade aluminum hydroxide, hydrotalcite and montmorillonite, it is spare；
2) titanium dioxide taken in step 1) and carbide slag are mixed, grinds 30min, obtains material A, it is spare；
3) polystyrene resin taken in step 1) and waterglass are mixed, the stir process at a temperature of 65 DEG C
20min obtains material B, spare；
4) material A and material B are mixed, adds the butyryl citric acid tri-n-hexyl ester taken in step 1), nanoscale hydrogen
Aluminium oxide, hydrotalcite and montmorillonite, 70 DEG C at a temperature of stir 10min, obtain material C；
5) material C is subjected to microwave treatment and obtains material D then in 80 DEG C of at a temperature of stir process 20min；
6) material D is formed, and is aged to get the building decoration fire proofing.
Wherein, in step 5), microwave treatment time 20min, microwave power 1000W；In step 6), digestion time is
30h。
The building decoration fire proofing is preparing the purposes in dalle product.
A kind of dalle based on the building decoration fire proofing.
Embodiment 2
A kind of building decoration fire proofing, including below according to the raw material of parts by weight: 18 parts of polystyrene resin, waterglass
12 parts, 15 parts of butyryl citric acid tri-n-hexyl ester, 7 parts of titanium dioxide, 5 parts of carbide slag, 7 parts of nano-grade aluminum hydroxide, 5 parts of hydrotalcite,
5 parts of montmorillonite.
In the present embodiment, the preparation method of the building decoration fire proofing, steps are as follows:
1) polystyrene resin, waterglass, butyryl citric acid tri-n-hexyl ester, titanium dioxide, calcium carbide are successively taken according to parts by weight
Slag, nano-grade aluminum hydroxide, hydrotalcite and montmorillonite, it is spare；
2) titanium dioxide taken in step 1) and carbide slag are mixed, grinds 30min, obtains material A, it is spare；
3) polystyrene resin taken in step 1) and waterglass are mixed, the stir process at a temperature of 65 DEG C
22min obtains material B, spare；
4) material A and material B are mixed, adds the butyryl citric acid tri-n-hexyl ester taken in step 1), nanoscale hydrogen
Aluminium oxide, hydrotalcite and montmorillonite, 70 DEG C at a temperature of stir 10min, obtain material C；
5) material C is subjected to microwave treatment and obtains material D then in 83 DEG C of at a temperature of stir process 20min；
6) material D is formed, and is aged to get the building decoration fire proofing.
Wherein, in step 5), microwave treatment time 20min, microwave power 1000W；In step 6), digestion time is
31h。
The building decoration fire proofing is preparing the purposes in dalle product.
A kind of dalle based on the building decoration fire proofing.
Embodiment 3
A kind of building decoration fire proofing, including below according to the raw material of parts by weight: 20 parts of polystyrene resin, waterglass
16 parts, 16 parts of butyryl citric acid tri-n-hexyl ester, 10 parts of titanium dioxide, 8 parts of carbide slag, 8 parts of nano-grade aluminum hydroxide, 6 parts of hydrotalcite,
6 parts of montmorillonite.
In the present embodiment, the preparation method of the building decoration fire proofing, steps are as follows:
1) polystyrene resin, waterglass, butyryl citric acid tri-n-hexyl ester, titanium dioxide, calcium carbide are successively taken according to parts by weight
Slag, nano-grade aluminum hydroxide, hydrotalcite and montmorillonite, it is spare；
2) titanium dioxide taken in step 1) and carbide slag are mixed, grinds 30min, obtains material A, it is spare；
3) polystyrene resin taken in step 1) and waterglass are mixed, the stir process at a temperature of 65 DEG C
25min obtains material B, spare；
4) material A and material B are mixed, adds the butyryl citric acid tri-n-hexyl ester taken in step 1), nanoscale hydrogen
Aluminium oxide, hydrotalcite and montmorillonite, 70 DEG C at a temperature of stir 10min, obtain material C；
5) material C is subjected to microwave treatment and obtains material D then in 85 DEG C of at a temperature of stir process 20min；
6) material D is formed, and is aged to get the building decoration fire proofing.
Wherein, in step 5), microwave treatment time 20min, microwave power 1000W；In step 6), digestion time is
32h。
The building decoration fire proofing is preparing the purposes in dalle product.
A kind of dalle based on the building decoration fire proofing.
Embodiment 4
A kind of building decoration fire proofing, including below according to the raw material of parts by weight: 23 parts of polystyrene resin, waterglass
18 parts, 17 parts of butyryl citric acid tri-n-hexyl ester, 15 parts of titanium dioxide, 10 parts of carbide slag, 10 parts of nano-grade aluminum hydroxide, hydrotalcite 7
Part, 7 parts of montmorillonite.
In the present embodiment, the preparation method of the building decoration fire proofing, steps are as follows:
1) polystyrene resin, waterglass, butyryl citric acid tri-n-hexyl ester, titanium dioxide, calcium carbide are successively taken according to parts by weight
Slag, nano-grade aluminum hydroxide, hydrotalcite and montmorillonite, it is spare；
2) titanium dioxide taken in step 1) and carbide slag are mixed, grinds 30min, obtains material A, it is spare；
3) polystyrene resin taken in step 1) and waterglass are mixed, the stir process at a temperature of 65 DEG C
27min obtains material B, spare；
4) material A and material B are mixed, adds the butyryl citric acid tri-n-hexyl ester taken in step 1), nanoscale hydrogen
Aluminium oxide, hydrotalcite and montmorillonite, 70 DEG C at a temperature of stir 10min, obtain material C；
5) material C is subjected to microwave treatment and obtains material D then in 87 DEG C of at a temperature of stir process 20min；
6) material D is formed, and is aged to get the building decoration fire proofing.
Wherein, in step 5), microwave treatment time 20min, microwave power 1000W；In step 6), digestion time is
34h。
The building decoration fire proofing is preparing the purposes in dalle product.
A kind of dalle based on the building decoration fire proofing.
Embodiment 5
A kind of building decoration fire proofing, including below according to the raw material of parts by weight: 25 parts of polystyrene resin, waterglass
20 parts, 20 parts of butyryl citric acid tri-n-hexyl ester, 15 parts of titanium dioxide, 12 parts of carbide slag, 10 parts of nano-grade aluminum hydroxide, hydrotalcite 8
Part, 8 parts of montmorillonite.
In the present embodiment, the preparation method of the building decoration fire proofing, steps are as follows:
1) polystyrene resin, waterglass, butyryl citric acid tri-n-hexyl ester, titanium dioxide, calcium carbide are successively taken according to parts by weight
Slag, nano-grade aluminum hydroxide, hydrotalcite and montmorillonite, it is spare；
2) titanium dioxide taken in step 1) and carbide slag are mixed, grinds 30min, obtains material A, it is spare；
3) polystyrene resin taken in step 1) and waterglass are mixed, the stir process at a temperature of 65 DEG C
30min obtains material B, spare；
4) material A and material B are mixed, adds the butyryl citric acid tri-n-hexyl ester taken in step 1), nanoscale hydrogen
Aluminium oxide, hydrotalcite and montmorillonite, 70 DEG C at a temperature of stir 10min, obtain material C；
5) material C is subjected to microwave treatment and obtains material D then in 90 DEG C of at a temperature of stir process 20min；
6) material D is formed, and is aged to get the building decoration fire proofing.
Wherein, in step 5), microwave treatment time 20min, microwave power 1000W；In step 6), digestion time is
35h。
The building decoration fire proofing is preparing the purposes in dalle product.
A kind of dalle based on the building decoration fire proofing.
Comparative example 1
Compared with Example 3, carbide slag is free of, other are same as Example 3.
Comparative example 2
Compared with Example 3, nano-grade aluminum hydroxide is free of, other are same as Example 3.
Comparative example 3
Compared with Example 3, carbide slag and nano-grade aluminum hydroxide are free of, other are same as Example 3.
Comparative example 4
Common buildings currently on the market decorate fire proofing.
Building decoration described in building decoration fire proofing prepared by embodiment 3, comparative example 1-3 and comparative example 4 is hindered
Combustible material is tested for the property.The test method of flame retardant property: in laboratory, burn on alcolhol burner 10 minutes respectively into
Row, observes combustion case, and test result is as shown in table 1.
1 performance test table of table
As can be seen that building decoration fire proofing prepared by the present invention has excellent flame retardant property from result above,
But also there is good compression strength, performance decorates fire proofing better than existing building, can satisfy the market demand, has wide
Wealthy market prospects.
In addition, from the data comparison of embodiment 3 and comparative example 1-3 as can be seen that the present invention by be added carbide slag and
Nano-grade aluminum hydroxide, carbide slag and nano-grade aluminum hydroxide cooperate, and are conducive to the resistance for improving building decoration fire proofing
Fire performance.
The preferred embodiment of the patent is described in detail above, but this patent is not limited to above-mentioned embodiment party
Formula within the knowledge of one of ordinary skill in the art can also be under the premise of not departing from this patent objective
It makes a variety of changes.
Claims (8)
1. a kind of building decoration fire proofing, which is characterized in that including below according to the raw material of parts by weight: polystyrene resin
15-25 parts, 10-20 parts of waterglass, 15-20 parts of butyryl citric acid tri-n-hexyl ester, 5-15 parts of titanium dioxide, 5-12 parts of carbide slag, receive
6-10 parts of meter level aluminium hydroxide, 5-8 parts of hydrotalcite, 5-8 parts of montmorillonite.
2. building decoration fire proofing according to claim 1, which is characterized in that including below according to the original of parts by weight
Material: 18-23 parts of polystyrene resin, 12-18 parts of waterglass, 15-17 parts of butyryl citric acid tri-n-hexyl ester, 7-15 parts of titanium dioxide,
5-10 parts of carbide slag, 7-10 parts of nano-grade aluminum hydroxide, 5-7 parts of hydrotalcite, 5-7 parts of montmorillonite.
3. building decoration fire proofing according to claim 2, which is characterized in that including below according to the original of parts by weight
Material: 20 parts of polystyrene resin, 16 parts of butyryl citric acid tri-n-hexyl ester, 10 parts of titanium dioxide, 8 parts of carbide slag, is received 16 parts of waterglass
8 parts of meter level aluminium hydroxide, 6 parts of hydrotalcite, 6 parts of montmorillonite.
4. a kind of preparation method of building decoration fire proofing a method according to any one of claims 1-3, which is characterized in that step is such as
Under:
1) polystyrene resin is successively taken according to parts by weight, waterglass, butyryl citric acid tri-n-hexyl ester, titanium dioxide, carbide slag, is received
Meter level aluminium hydroxide, hydrotalcite and montmorillonite, it is spare；
2) titanium dioxide taken in step 1) and carbide slag are mixed, grinds 30min, obtains material A, it is spare；
3) polystyrene resin taken in step 1) and waterglass are mixed, in 65 DEG C of at a temperature of stir process 20-
30min obtains material B, spare；
4) material A and material B are mixed, adds the butyryl citric acid tri-n-hexyl ester taken in step 1), nanoscale hydroxide
Aluminium, hydrotalcite and montmorillonite, 70 DEG C at a temperature of stir 10min, obtain material C；
5) material C is subjected to microwave treatment and obtains material D then in 80-90 DEG C of at a temperature of stir process 20min；
6) material D is formed, and is aged to get the building decoration fire proofing.
5. the preparation method of building decoration fire proofing according to claim 4, which is characterized in that in step 5), microwave
The processing time is 20min, microwave power 1000W.
6. the preparation method of building decoration fire proofing according to claim 4, which is characterized in that in step 6), ageing
Time is 30-35h.
7. building decoration fire proofing a method according to any one of claims 1-3 is preparing the purposes in dalle product.
8. a kind of dalle based on building decoration fire proofing a method according to any one of claims 1-3.
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| CN201811446644.8A CN109762260A (en) | 2018-11-29 | 2018-11-29 | A kind of building decoration fire proofing and preparation method thereof |
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| CN201811446644.8A CN109762260A (en) | 2018-11-29 | 2018-11-29 | A kind of building decoration fire proofing and preparation method thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103435927A (en) * | 2013-09-11 | 2013-12-11 | 安徽中瑞节能装饰材料集团有限公司 | A-grade flame retardant modified polystyrene board and preparation method thereof |
| CN106517984A (en) * | 2016-11-10 | 2017-03-22 | 申家海 | Building decoration fireproof material and its preparation method and application |
| CN108892469A (en) * | 2018-09-25 | 2018-11-27 | 张连军 | A kind of building decoration fire proofing material and preparation method thereof |
-
2018
- 2018-11-29 CN CN201811446644.8A patent/CN109762260A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103435927A (en) * | 2013-09-11 | 2013-12-11 | 安徽中瑞节能装饰材料集团有限公司 | A-grade flame retardant modified polystyrene board and preparation method thereof |
| CN106517984A (en) * | 2016-11-10 | 2017-03-22 | 申家海 | Building decoration fireproof material and its preparation method and application |
| CN108892469A (en) * | 2018-09-25 | 2018-11-27 | 张连军 | A kind of building decoration fire proofing material and preparation method thereof |
Non-Patent Citations (1)
| Title |
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| 张书华等: "《高性能电缆材料及其应用技术》", 30 November 2015, 上海交通大学出版社 * |
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Application publication date: 20190517 |