CN108892469A - A kind of building decoration fire proofing material and preparation method thereof - Google Patents
A kind of building decoration fire proofing material and preparation method thereof Download PDFInfo
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- CN108892469A CN108892469A CN201811113854.5A CN201811113854A CN108892469A CN 108892469 A CN108892469 A CN 108892469A CN 201811113854 A CN201811113854 A CN 201811113854A CN 108892469 A CN108892469 A CN 108892469A
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- fire proofing
- building decoration
- proofing material
- decoration fire
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/34—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing cold phosphate binders
- C04B28/344—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing cold phosphate binders the phosphate binder being present in the starting composition solely as one or more phosphates
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/28—Fire resistance, i.e. materials resistant to accidental fires or high temperatures
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Fireproofing Substances (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a kind of building decoration fire proofing materials, are characterized in that：Including below according to the raw material of parts by weight：30-40 parts of kaolin, 10-25 parts of aluminium oxide, 20-30 parts of titanium dioxide, 10-20 parts of aluminum phosphate, 20-30 parts of calcium stearate, 20-35 parts of calamine.The invention also discloses the preparation methods of the building decoration fire proofing material.Building decoration fire proofing material compression strength performance prepared by the present invention is good, can satisfy the market demand, and have excellent flame retardant property, has a vast market foreground.
Description
Technical field
The present invention relates to a kind of building material technical field, specifically a kind of building decoration fire proofing material and its preparation side
Method.
Background technique
In construction and decoration or decoration process, it will use various materials, fire proofing material is also wherein.Fire proofing wood
Material, refer to prevent or retard flame sprawling performance material, be added to certain synthetic material with fire performance matrix
Or inherently there is high temperature resistant, heat-resisting, flame-retarding characteristic material.
In recent years, since building fire caused by thermal insulation material, ornament materials be not up to standard takes place frequently repeatedly, so, Wo Menyao
More pay attention to the fire protecting performance of construction material.In view of the severe situation of current building fire protection, proposes that a kind of flame retardant property is good and build
It is very necessary for building ornament materials.Therefore, the invention proposes a kind of building decoration fire proofing materials and preparation method thereof.
Summary of the invention
The purpose of the present invention is to provide a kind of building decoration fire proofing materials and preparation method thereof, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the present invention provides the following technical solutions：
A kind of building decoration fire proofing material, including below according to the raw material of parts by weight：30-40 parts of kaolin, aluminium oxide 10-
25 parts, 20-30 parts of titanium dioxide, 10-20 parts of aluminum phosphate, 20-30 parts of calcium stearate, 20-35 parts of calamine.
As a further solution of the present invention：Including below according to the raw material of parts by weight：30-35 parts of kaolin, aluminium oxide
15-25 parts, 25-30 parts of titanium dioxide, 10-15 parts of aluminum phosphate, 25-30 parts of calcium stearate, 25-35 parts of calamine.
As further scheme of the invention：Including below according to the raw material of parts by weight：32 parts of kaolin, aluminium oxide 20
Part, 38 parts of titanium dioxide, 15 parts of aluminum phosphate, 25 parts of calcium stearate, 30 parts of calamine.
The preparation method of the building decoration fire proofing material, steps are as follows：
1) kaolin, aluminium oxide and aluminum phosphate are weighed, be sieved to obtain mixture A after grinding, spare；
2) A is added in 500 parts of water, is dispersed with stirring and suspension slurry A is made；
3) titanium dioxide is weighed, is then added in suspension slurry A, stirs evenly, suspension slurry B is made；
4) calamine and calcium stearate are weighed, is merged, then grinding puts into suspension slurry B, is uniformly mixed system
Obtain mixture B；
5) mixture B microwave treatment is carried out then to be formed then in 80 DEG C of at a temperature of stir process, be aged 35h
Up to fire proofing material.
As further scheme of the invention：In step 4), the mixing time is 20-30min.
As further scheme of the invention：In step 5), the microwave treatment time is 10-15min.
As further scheme of the invention：In step 5), the stir process time is 30min.
The fire proofing material is preparing the purposes in building decoration fire-proof product.
Compared with prior art, the beneficial effects of the invention are as follows：
Building decoration fire proofing material compression strength performance prepared by the present invention is good, can satisfy the market demand, and have
Excellent flame retardant property, has a vast market foreground.
Specific embodiment
The technical solution of the patent is explained in further detail With reference to embodiment.
Embodiment 1
A kind of building decoration fire proofing material, including below according to the raw material of parts by weight：30 parts of kaolin, 10 parts of aluminium oxide,
20 parts of titanium dioxide, 10 parts of aluminum phosphate, 20 parts of calcium stearate, 20 parts of calamine.
In the present embodiment, the preparation method of the building decoration fire proofing material, steps are as follows：
1) kaolin, aluminium oxide and aluminum phosphate are weighed, be sieved to obtain mixture A after grinding, spare；
2) A is added in 500 parts of water, is dispersed with stirring and suspension slurry A is made；
3) titanium dioxide is weighed, is then added in suspension slurry A, stirs evenly, suspension slurry B is made；
4) calamine and calcium stearate are weighed, is merged, then grinding puts into suspension slurry B, is uniformly mixed system
Obtain mixture B；
5) mixture B microwave treatment is carried out then to be formed then in 80 DEG C of at a temperature of stir process, be aged 35h
Up to fire proofing material.
Wherein, in step 4), the mixing time is 20min；In step 5), the microwave treatment time is 10min；Step
It is rapid 5) in, the stir process time be 30min.
Embodiment 2
A kind of building decoration fire proofing material, including below according to the raw material of parts by weight：40 parts of kaolin, 25 parts of aluminium oxide,
30 parts of titanium dioxide, 20 parts of aluminum phosphate, 30 parts of calcium stearate, 35 parts of calamine.
In the present embodiment, the preparation method of the building decoration fire proofing material, steps are as follows：
1) kaolin, aluminium oxide and aluminum phosphate are weighed, be sieved to obtain mixture A after grinding, spare；
2) A is added in 500 parts of water, is dispersed with stirring and suspension slurry A is made；
3) titanium dioxide is weighed, is then added in suspension slurry A, stirs evenly, suspension slurry B is made；
4) calamine and calcium stearate are weighed, is merged, then grinding puts into suspension slurry B, is uniformly mixed system
Obtain mixture B；
5) mixture B microwave treatment is carried out then to be formed then in 80 DEG C of at a temperature of stir process, be aged 35h
Up to fire proofing material.
Wherein, in step 4), the mixing time is 30min；In step 5), the microwave treatment time is 15min；Step
It is rapid 5) in, the stir process time be 30min.
Embodiment 3
A kind of building decoration fire proofing material, including below according to the raw material of parts by weight：32 parts of kaolin, 20 parts of aluminium oxide,
38 parts of titanium dioxide, 15 parts of aluminum phosphate, 25 parts of calcium stearate, 30 parts of calamine.
In the present embodiment, the preparation method of the building decoration fire proofing material, steps are as follows：
1) kaolin, aluminium oxide and aluminum phosphate are weighed, be sieved to obtain mixture A after grinding, spare；
2) A is added in 500 parts of water, is dispersed with stirring and suspension slurry A is made；
3) titanium dioxide is weighed, is then added in suspension slurry A, stirs evenly, suspension slurry B is made；
4) calamine and calcium stearate are weighed, is merged, then grinding puts into suspension slurry B, is uniformly mixed system
Obtain mixture B；
5) mixture B microwave treatment is carried out then to be formed then in 80 DEG C of at a temperature of stir process, be aged 35h
Up to fire proofing material.
Wherein, in step 4), the mixing time is 25min；In step 5), the microwave treatment time is 15min；Step
It is rapid 5) in, the stir process time be 30min.
Embodiment 4
A kind of building decoration fire proofing material, including below according to the raw material of parts by weight：30 parts of kaolin, 15 parts of aluminium oxide,
25 parts of titanium dioxide, 10 parts of aluminum phosphate, 25 parts of calcium stearate, 25 parts of calamine.
In the present embodiment, the preparation method of the building decoration fire proofing material, steps are as follows：
1) kaolin, aluminium oxide and aluminum phosphate are weighed, be sieved to obtain mixture A after grinding, spare；
2) A is added in 500 parts of water, is dispersed with stirring and suspension slurry A is made；
3) titanium dioxide is weighed, is then added in suspension slurry A, stirs evenly, suspension slurry B is made；
4) calamine and calcium stearate are weighed, is merged, then grinding puts into suspension slurry B, is uniformly mixed system
Obtain mixture B；
5) mixture B microwave treatment is carried out then to be formed then in 80 DEG C of at a temperature of stir process, be aged 35h
Up to fire proofing material.
Wherein, in step 4), the mixing time is 20min；In step 5), the microwave treatment time is 10min；Step
It is rapid 5) in, the stir process time be 30min.
Embodiment 5
A kind of building decoration fire proofing material, including below according to the raw material of parts by weight：35 parts of kaolin, 25 parts of aluminium oxide,
30 parts of titanium dioxide, 15 parts of aluminum phosphate, 30 parts of calcium stearate, 35 parts of calamine.
In the present embodiment, the preparation method of the building decoration fire proofing material, steps are as follows：
1) kaolin, aluminium oxide and aluminum phosphate are weighed, be sieved to obtain mixture A after grinding, spare；
2) A is added in 500 parts of water, is dispersed with stirring and suspension slurry A is made；
3) titanium dioxide is weighed, is then added in suspension slurry A, stirs evenly, suspension slurry B is made；
4) calamine and calcium stearate are weighed, is merged, then grinding puts into suspension slurry B, is uniformly mixed system
Obtain mixture B；
5) mixture B microwave treatment is carried out then to be formed then in 80 DEG C of at a temperature of stir process, be aged 35h
Up to fire proofing material.
Wherein, in step 4), the mixing time is 30min；In step 5), the microwave treatment time is 15min；Step
It is rapid 5) in, the stir process time be 30min.
Comparative example 1
Compared with Example 3, calcium stearate is free of, other are same as Example 3.
Comparative example 2
Compared with Example 3, calamine is free of, other are same as Example 3.
Comparative example 3
Compared with Example 3, calcium stearate and calamine are free of, other are same as Example 3.
Comparative example 4
NCB type indoor ultrathin steel structure fireproof coating.
Building decoration fire proofing material prepared by embodiment 3 and comparative example 1-4 is tested for the property, test result such as table
Shown in 1.
1 performance test table of table
| Group | The fire endurance time (min) | Compression strength (MPa) | Flame retardant rating (grade) |
| Embodiment 3 | 88 | 5.2 | V-0 |
| Comparative example 1 | 65 | 4.5 | V-1 |
| Comparative example 2 | 71 | 4.9 | V-1 |
| Comparative example 3 | 60 | 4.2 | V-2 |
| Comparative example 4 | 76 | 4.6 | V-1 |
As can be seen that building decoration fire proofing material compression strength prepared by the present invention performance is good from result above, energy
Enough meet the market demand, and there is excellent flame retardant property, has a vast market foreground.
In addition, as can be seen that the present invention is by being added calcium stearate from the data comparison of embodiment 3 and comparative example 1-3
And calamine, calcium stearate and calamine cooperate, and are conducive to the flame retardant property for improving the building decoration fire proofing material.
The preferred embodiment of the patent is described in detail above, but this patent is not limited to above-mentioned embodiment party
Formula within the knowledge of one of ordinary skill in the art can also be under the premise of not departing from this patent objective
It makes a variety of changes.
Claims (8)
1. a kind of building decoration fire proofing material, which is characterized in that including below according to the raw material of parts by weight：30-40 parts of kaolin,
10-25 parts of aluminium oxide, 20-30 parts of titanium dioxide, 10-20 parts of aluminum phosphate, 20-30 parts of calcium stearate, 20-35 parts of calamine.
2. building decoration fire proofing material according to claim 1, which is characterized in that including below according to the original of parts by weight
Material：30-35 parts of kaolin, 15-25 parts of aluminium oxide, 25-30 parts of titanium dioxide, 10-15 parts of aluminum phosphate, 25-30 parts of calcium stearate, furnace
Sweet stone 25-35 parts.
3. building decoration fire proofing material according to claim 2, which is characterized in that including below according to the original of parts by weight
Material：32 parts of kaolin, 20 parts of aluminium oxide, 38 parts of titanium dioxide, 15 parts of aluminum phosphate, 25 parts of calcium stearate, 30 parts of calamine.
4. a kind of preparation method of building decoration fire proofing material a method according to any one of claims 1-3, which is characterized in that step is such as
Under：
1）Kaolin, aluminium oxide and aluminum phosphate are weighed, be sieved to obtain mixture A after grinding, spare；
2）A is added in 500 parts of water, is dispersed with stirring and suspension slurry A is made；
3）Titanium dioxide is weighed, is then added in suspension slurry A, stirs evenly, suspension slurry B is made；
4）Calamine and calcium stearate are weighed, is merged, then grinding is put into suspension slurry B, be uniformly mixed and be made mixed
Close object B；
5）Mixture B is carried out microwave treatment then to be formed then in 80 DEG C of at a temperature of stir process, be aged 35h to obtain the final product
Fire proofing material.
5. the preparation method of building decoration fire proofing material according to claim 4, which is characterized in that step 4）In, it is described
Mixing time is 20-30min.
6. the preparation method of building decoration fire proofing material according to claim 4, which is characterized in that step 5）In, it is described
Microwave treatment time is 10-15min.
7. the preparation method of building decoration fire proofing material according to claim 4, which is characterized in that step 5）In, it is described
The stir process time is 30min.
8. fire proofing material a method according to any one of claims 1-3 is preparing the purposes in building decoration fire-proof product.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811113854.5A CN108892469A (en) | 2018-09-25 | 2018-09-25 | A kind of building decoration fire proofing material and preparation method thereof |
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| CN201811113854.5A CN108892469A (en) | 2018-09-25 | 2018-09-25 | A kind of building decoration fire proofing material and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109762260A (en) * | 2018-11-29 | 2019-05-17 | 汪培杰 | A kind of building decoration fire proofing and preparation method thereof |
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| KR20130048740A (en) * | 2013-04-02 | 2013-05-10 | 이재환 | Liquid curable composition |
| CN105219145A (en) * | 2014-10-27 | 2016-01-06 | 济南大学 | A kind of high temperature resistant infrared external reflection thermal insulation material and preparation method thereof |
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Application publication date: 20181127 |