CN109735176A - A kind of preparation method of energy conservation and environmental protection building thermal-insulating coating - Google Patents
A kind of preparation method of energy conservation and environmental protection building thermal-insulating coating Download PDFInfo
- Publication number
- CN109735176A CN109735176A CN201910016789.2A CN201910016789A CN109735176A CN 109735176 A CN109735176 A CN 109735176A CN 201910016789 A CN201910016789 A CN 201910016789A CN 109735176 A CN109735176 A CN 109735176A
- Authority
- CN
- China
- Prior art keywords
- parts
- environmental protection
- insulating coating
- energy conservation
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Paints Or Removers (AREA)
Abstract
The invention discloses a kind of preparation methods of energy conservation and environmental protection building thermal-insulating coating, are related to building materials field, mainly for solving the problems, such as that traditional thermal insulation coatings are at high cost and can generate a large amount of unwanted volatile matter；This method mainly includes eight steps.The present invention can be effectively reduced the production cost of thermal insulation coatings, while reasonable raw material proportioning, can substantially reduce the volatile quantity of harmful substance, agree with current energy-saving and environment-friendly development topic, have a vast market foreground with higher practical value, be worth of widely use.
Description
Technical field
The present invention relates to a kind of building materials field, the preparation method of specifically a kind of energy conservation and environmental protection building thermal-insulating coating.
Background technique
Thermal insulation coatings thermal insulation coatings are a kind of novel thermal insulation materials, are realized by low thermal conductivity and high thermal resistance heat-insulated
Heat preservation a kind of coating, have waterproof, anticracking, sound insulation, fire prevention, fire-retardant, wear-resisting, insulation, antiacid alkali, it is light-weight, easy for construction,
The features such as long service life.Thermal insulation coatings can extensively should be in building, chemical industry, petroleum, electric power, metallurgy, ship, light textile, storage, friendship
The industries such as logical, space flight, are mainly used for heat-insulated or heat preservation (cold insulation) occasion, and coating has good adhesive force, easy construction,
Can be used for steel, cast iron, zinc-plated, aluminium, copper, magnesium, armored concrete, stone material, timber, brick and tile, ceramics, glass, textile, plastics,
Paper and various coating surfaces.It is a kind of anti-enzyme environmental protection of heat-proof insulation waterproof fire retardant anticorrosion insulation acid and alkali-resistance with a relatively high cost performance
Energy-saving coating.
In recent years, the development of thermal insulation coatings is more swift and violent, but there are more disadvantages, such as higher cost, and can generate
A large amount of toxic volatile substances do not agree with current energy-saving and environment-friendly development topic.
Summary of the invention
The purpose of the present invention is to provide a kind of preparation methods of energy conservation and environmental protection building thermal-insulating coating, to solve above-mentioned ask
Topic.
To achieve the above object, the invention provides the following technical scheme:
A kind of preparation method of energy conservation and environmental protection building thermal-insulating coating, comprising the following steps:
1) the following raw material according to parts by weight: 11-19 parts of talcum powder, 5-11 parts of silica, 13-21 parts of Chinese wistaria leaf, dispersing agent is weighed
0.8-1.7 parts, 0.9-1.7 parts of thickener, 14-21 parts of Corvic lotion, 7-13 parts of Phenolic resin emulsion；
2) mashing processing, isolated residue and slurries are carried out to Chinese wistaria leaf；
3) 4-9 times of quality times of dehydrated alcohol is added in slurries, is extracted in the environment of 67-81 DEG C twice, merging mentions twice
Liquid is taken, extracting solution is concentrated into the 15-25% of original volume, obtains extracting solution；
4) by silica in the environment of 600-800 DEG C frying 13-21min, then crush, sieve with 100 mesh sieve, obtain Cab-O-sil；
5) merge talcum powder, Cab-O-sil and residue, obtain solid-phase mixture after mixing；
6) merge Corvic lotion, Phenolic resin emulsion and extracting solution, thickener is added, obtains liquid phase after being sufficiently mixed
Mixture；
7) solid-phase mixture and liquid phase mixture merging are placed in processor for ultrasonic wave, while dispersing agent is added, in 89-
It is ultrasonically treated 34-47min in the environment of 106 DEG C, temperature is then promoted to 115-127 DEG C and continues to be ultrasonically treated 5-12min, is obtained
To solidliquid mixture；
8) solidliquid mixture is stood into 8-13h, remove lower sediment to get.
Based on the above technical solution, the present invention also provides following optional technical solutions:
In a kind of optinal plan: weighing the following raw material according to parts by weight: 15-17 parts of talcum powder, silica in the step 1)
7-9 parts, 15-19 parts of Chinese wistaria leaf, 1.1-1.4 parts of dispersing agent, 1.2-1.4 parts of thickener, 16-19 parts of Corvic lotion,
9-11 parts of Phenolic resin emulsion.
In a kind of optinal plan: weighing the following raw material according to parts by weight: 16 parts of talcum powder, silica in the step 1)
8 parts, 17 parts of Chinese wistaria leaf, 1.3 parts of dispersing agent, 1.3 parts of thickener, 18 parts of Corvic lotion, 10 parts of Phenolic resin emulsion.
In a kind of optinal plan: the dispersing agent is mixed by tripolyphosphate ammonium and calgon.
In a kind of optinal plan: the dispersing agent mixed by tripolyphosphate ammonium and calgon by weight 3:2 and
At.
In a kind of optinal plan: the thickener is hydroxypropyl methyl cellulose.
In a kind of optinal plan: ultrasonication power is 800-1100W in the step 5).
Compared to the prior art, beneficial effects of the present invention are as follows:
The present invention can be effectively reduced the production cost of thermal insulation coatings, while reasonable raw material proportioning, can substantially reduce nuisance
The volatile quantity of matter agrees with current energy-saving and environment-friendly development topic, have a vast market foreground with higher practical value, be worth
It promotes the use of.
Specific embodiment
Each embodiment cited by the present invention is only to illustrate the present invention, is not used to limit the scope of the present invention.To this
Any modification apparent easy to know or change are without departure from spirit and scope of the invention made by invention.
Embodiment 1
In the embodiment of the present invention, a kind of preparation method of energy conservation and environmental protection building thermal-insulating coating, comprising the following steps:
1) the following raw material according to parts by weight: 11 parts of talcum powder, 5 parts of silica, 13 parts of Chinese wistaria leaf, 0.8 part of dispersing agent, thickening is weighed
0.9 part of agent, 14 parts of Corvic lotion, 7 parts of Phenolic resin emulsion；
2) mashing processing, isolated residue and slurries are carried out to Chinese wistaria leaf；
3) dehydrated alcohol of 4 times of quality times is added in slurries, is extracted in the environment of 67 DEG C twice, merges extracting solution twice,
Extracting solution is concentrated into the 15% of original volume, obtains extracting solution；
4) by silica in the environment of 600 DEG C frying 13min, then crush, sieve with 100 mesh sieve, obtain Cab-O-sil；
5) merge talcum powder, Cab-O-sil and residue, obtain solid-phase mixture after mixing；
6) merge Corvic lotion, Phenolic resin emulsion and extracting solution, thickener is added, obtains liquid phase after being sufficiently mixed
Mixture；
7) solid-phase mixture and liquid phase mixture merging are placed in processor for ultrasonic wave, while dispersing agent is added, at 89 DEG C
In the environment of be ultrasonically treated 34min, then by temperature be promoted to 115 DEG C continue be ultrasonically treated 5min, obtain solidliquid mixture；
8) solidliquid mixture is stood into 8h, remove lower sediment to get.
The dispersing agent mixes by weight 1:1 by tripolyphosphate ammonium and calgon
The thickener is hydroxypropyl methyl cellulose.
Ultrasonication power is 800W in the step 5).
Embodiment 2
In the embodiment of the present invention, a kind of preparation method of energy conservation and environmental protection building thermal-insulating coating, comprising the following steps:
1) the following raw material according to parts by weight: 15 parts of talcum powder, 7 parts of silica, 15 parts of Chinese wistaria leaf, 1.1 parts of dispersing agent, thickening is weighed
1.2 parts of agent, 16 parts of Corvic lotion, 9 parts of Phenolic resin emulsion；
2) mashing processing, isolated residue and slurries are carried out to Chinese wistaria leaf；
3) dehydrated alcohol of 6 times of quality times is added in slurries, is extracted in the environment of 71 DEG C twice, merges extracting solution twice,
Extracting solution is concentrated into the 20% of original volume, obtains extracting solution；
4) by silica in the environment of 650 DEG C frying 16min, then crush, sieve with 100 mesh sieve, obtain Cab-O-sil；
5) merge talcum powder, Cab-O-sil and residue, obtain solid-phase mixture after mixing；
6) merge Corvic lotion, Phenolic resin emulsion and extracting solution, thickener is added, obtains liquid phase after being sufficiently mixed
Mixture；
7) solid-phase mixture and liquid phase mixture merging are placed in processor for ultrasonic wave, while dispersing agent is added, at 92 DEG C
In the environment of be ultrasonically treated 42min, then by temperature be promoted to 120 DEG C continue be ultrasonically treated 8min, obtain solidliquid mixture；
8) solidliquid mixture is stood into 11h, remove lower sediment to get.
The dispersing agent mixes by weight 2:1 by tripolyphosphate ammonium and calgon
The thickener is hydroxypropyl methyl cellulose.
Ultrasonication power is 900W in the step 5).
Embodiment 3
In the embodiment of the present invention, a kind of preparation method of energy conservation and environmental protection building thermal-insulating coating, comprising the following steps:
1) the following raw material according to parts by weight: 16 parts of talcum powder, 8 parts of silica, 17 parts of Chinese wistaria leaf, 1.3 parts of dispersing agent, thickening is weighed
1.3 parts of agent, 18 parts of Corvic lotion, 10 parts of Phenolic resin emulsion；
2) mashing processing, isolated residue and slurries are carried out to Chinese wistaria leaf；
3) dehydrated alcohol of 7 times of quality times is added in slurries, is extracted in the environment of 72 DEG C twice, merges extracting solution twice,
Extracting solution is concentrated into the 20% of original volume, obtains extracting solution；
4) by silica in the environment of 700 DEG C frying 18min, then crush, sieve with 100 mesh sieve, obtain Cab-O-sil；
5) merge talcum powder, Cab-O-sil and residue, obtain solid-phase mixture after mixing；
6) merge Corvic lotion, Phenolic resin emulsion and extracting solution, thickener is added, obtains liquid phase after being sufficiently mixed
Mixture；
7) solid-phase mixture and liquid phase mixture merging are placed in processor for ultrasonic wave, while dispersing agent is added, at 92 DEG C
In the environment of be ultrasonically treated 38min, then by temperature be promoted to 118 DEG C continue be ultrasonically treated 10min, obtain solidliquid mixture；
8) solidliquid mixture is stood into 11h, remove lower sediment to get.
The dispersing agent mixes by weight 3:2 by tripolyphosphate ammonium and calgon
The thickener is hydroxypropyl methyl cellulose.
Ultrasonication power is 1000W in the step 5).
Embodiment 4
In the embodiment of the present invention, a kind of preparation method of energy conservation and environmental protection building thermal-insulating coating, comprising the following steps:
1) the following raw material according to parts by weight: 17 parts of talcum powder, 9 parts of silica, 19 parts of Chinese wistaria leaf, 1.4 parts of dispersing agent, thickening is weighed
1.4 parts of agent, 19 parts of Corvic lotion, 11 parts of Phenolic resin emulsion；
2) mashing processing, isolated residue and slurries are carried out to Chinese wistaria leaf；
3) dehydrated alcohol of 9 times of quality times is added in slurries, is extracted in the environment of 77 DEG C twice, merges extracting solution twice,
Extracting solution is concentrated into the 22% of original volume, obtains extracting solution；
4) by silica in the environment of 700 DEG C frying 19min, then crush, sieve with 100 mesh sieve, obtain Cab-O-sil；
5) merge talcum powder, Cab-O-sil and residue, obtain solid-phase mixture after mixing；
6) merge Corvic lotion, Phenolic resin emulsion and extracting solution, thickener is added, obtains liquid phase after being sufficiently mixed
Mixture；
7) solid-phase mixture and liquid phase mixture merging are placed in processor for ultrasonic wave, while dispersing agent is added, at 98 DEG C
In the environment of be ultrasonically treated 42min, then by temperature be promoted to 122 DEG C continue be ultrasonically treated 9min, obtain solidliquid mixture；
8) solidliquid mixture is stood into 12h, remove lower sediment to get.
The dispersing agent mixes by weight 3:4 by tripolyphosphate ammonium and calgon
The thickener is hydroxypropyl methyl cellulose.
Ultrasonication power is 1000W in the step 5).
Embodiment 5
In the embodiment of the present invention, a kind of preparation method of energy conservation and environmental protection building thermal-insulating coating, comprising the following steps:
1) weigh the following raw material according to parts by weight: 19 parts of talcum powder, 21 parts of Chinese wistaria leaf, 1.7 parts of dispersing agent, increases 11 parts of silica
Thick dose 1.7 parts, 21 parts of Corvic lotion, 13 parts of Phenolic resin emulsion；
2) mashing processing, isolated residue and slurries are carried out to Chinese wistaria leaf；
3) dehydrated alcohol of 9 times of quality times is added in slurries, is extracted in the environment of 81 DEG C twice, merges extracting solution twice,
Extracting solution is concentrated into the 25% of original volume, obtains extracting solution；
4) by silica in the environment of 800 DEG C frying 21min, then crush, sieve with 100 mesh sieve, obtain Cab-O-sil；
5) merge talcum powder, Cab-O-sil and residue, obtain solid-phase mixture after mixing；
6) merge Corvic lotion, Phenolic resin emulsion and extracting solution, thickener is added, obtains liquid phase after being sufficiently mixed
Mixture；
7) solid-phase mixture and liquid phase mixture merging are placed in processor for ultrasonic wave, while dispersing agent is added, at 106 DEG C
In the environment of be ultrasonically treated 47min, then by temperature be promoted to 127 DEG C continue be ultrasonically treated 12min, obtain solidliquid mixture；
8) solidliquid mixture is stood into 13h, remove lower sediment to get.
The dispersing agent mixes by weight 1:1 by tripolyphosphate ammonium and calgon
The thickener is hydroxypropyl methyl cellulose.
Ultrasonication power is 1100W in the step 5).
The above, the only specific embodiment of the disclosure, but the protection scope of the disclosure is not limited thereto, it is any
Those familiar with the art can easily think of the change or the replacement in the technical scope that the disclosure discloses, and should all contain
It covers within the protection scope of the disclosure.Therefore, the protection scope of the disclosure should be subject to the protection scope in claims.
Claims (7)
1. a kind of preparation method of energy conservation and environmental protection building thermal-insulating coating, which comprises the following steps:
1) the following raw material according to parts by weight: 11-19 parts of talcum powder, 5-11 parts of silica, 13-21 parts of Chinese wistaria leaf, dispersing agent is weighed
0.8-1.7 parts, 0.9-1.7 parts of thickener, 14-21 parts of Corvic lotion, 7-13 parts of Phenolic resin emulsion；
2) mashing processing, isolated residue and slurries are carried out to Chinese wistaria leaf；
3) 4-9 times of quality times of dehydrated alcohol is added in slurries, is extracted in the environment of 67-81 DEG C twice, merging mentions twice
Liquid is taken, extracting solution is concentrated into the 15-25% of original volume, obtains extracting solution；
4) by silica in the environment of 600-800 DEG C frying 13-21min, then crush, sieve with 100 mesh sieve, obtain Cab-O-sil；
5) merge talcum powder, Cab-O-sil and residue, obtain solid-phase mixture after mixing；
6) merge Corvic lotion, Phenolic resin emulsion and extracting solution, thickener is added, obtains liquid phase after being sufficiently mixed
Mixture；
7) solid-phase mixture and liquid phase mixture merging are placed in processor for ultrasonic wave, while dispersing agent is added, in 89-
It is ultrasonically treated 34-47min in the environment of 106 DEG C, temperature is then promoted to 115-127 DEG C and continues to be ultrasonically treated 5-12min, is obtained
To solidliquid mixture；
8) solidliquid mixture is stood into 8-13h, remove lower sediment to get.
2. the preparation method of energy conservation and environmental protection building thermal-insulating coating according to claim 1, which is characterized in that the step 1)
In weigh the following raw material according to parts by weight: 15-17 parts of talcum powder, 7-9 parts of silica, 15-19 parts of Chinese wistaria leaf, dispersing agent 1.1-
1.4 parts, 1.2-1.4 parts of thickener, 16-19 parts of Corvic lotion, 9-11 parts of Phenolic resin emulsion.
3. the preparation method of energy conservation and environmental protection building thermal-insulating coating according to claim 1, which is characterized in that the step 1)
In weigh the following raw material according to parts by weight: 16 parts of talcum powder, 8 parts of silica, 17 parts of Chinese wistaria leaf, 1.3 parts of dispersing agent, thickener
1.3 parts, 18 parts of Corvic lotion, 10 parts of Phenolic resin emulsion.
4. the preparation method of energy conservation and environmental protection building thermal-insulating coating according to claim 1, which is characterized in that the dispersing agent
It is mixed by tripolyphosphate ammonium and calgon.
5. the preparation method of energy conservation and environmental protection building thermal-insulating coating according to claim 4, which is characterized in that the dispersing agent
It is mixed by tripolyphosphate ammonium and calgon by weight 3:2.
6. the preparation method of energy conservation and environmental protection building thermal-insulating coating according to claim 1, which is characterized in that the thickener
For hydroxypropyl methyl cellulose.
7. the preparation method of energy conservation and environmental protection building thermal-insulating coating according to claim 1, which is characterized in that the step 5)
Middle ultrasonication power is 800-1100W.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910016789.2A CN109735176A (en) | 2019-01-08 | 2019-01-08 | A kind of preparation method of energy conservation and environmental protection building thermal-insulating coating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910016789.2A CN109735176A (en) | 2019-01-08 | 2019-01-08 | A kind of preparation method of energy conservation and environmental protection building thermal-insulating coating |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109735176A true CN109735176A (en) | 2019-05-10 |
Family
ID=66363822
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910016789.2A Pending CN109735176A (en) | 2019-01-08 | 2019-01-08 | A kind of preparation method of energy conservation and environmental protection building thermal-insulating coating |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109735176A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1191235A (en) * | 1998-03-17 | 1998-08-26 | 孙枝荣 | Internal wall paint and products thereof |
| CN106189558A (en) * | 2016-07-14 | 2016-12-07 | 阜南县宏泰工艺品有限公司 | A kind of high rigidity anticorrosion straw treatment fluid and preparation method thereof |
| CN106280775A (en) * | 2016-08-17 | 2017-01-04 | 安徽顺驰电缆有限公司 | A kind of fire retardant coating of aquosity cable and preparation method thereof |
| CN107201067A (en) * | 2017-07-07 | 2017-09-26 | 北京志盛威华化工有限公司 | A kind of thermostable heat-isolating coating and preparation method thereof |
| CN107793816A (en) * | 2017-10-26 | 2018-03-13 | 山东圣泉新材料股份有限公司 | A kind of multi-functional latex paint and its preparation method and application |
-
2019
- 2019-01-08 CN CN201910016789.2A patent/CN109735176A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1191235A (en) * | 1998-03-17 | 1998-08-26 | 孙枝荣 | Internal wall paint and products thereof |
| CN106189558A (en) * | 2016-07-14 | 2016-12-07 | 阜南县宏泰工艺品有限公司 | A kind of high rigidity anticorrosion straw treatment fluid and preparation method thereof |
| CN106280775A (en) * | 2016-08-17 | 2017-01-04 | 安徽顺驰电缆有限公司 | A kind of fire retardant coating of aquosity cable and preparation method thereof |
| CN107201067A (en) * | 2017-07-07 | 2017-09-26 | 北京志盛威华化工有限公司 | A kind of thermostable heat-isolating coating and preparation method thereof |
| CN107793816A (en) * | 2017-10-26 | 2018-03-13 | 山东圣泉新材料股份有限公司 | A kind of multi-functional latex paint and its preparation method and application |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN100554394C (en) | Bearing scavenger specially of substituting coal oil and preparation method thereof | |
| CN102992720A (en) | External wall waterproof cracking-prevention flexible putty and preparation method thereof | |
| CN104193251B (en) | A kind of anti-corrosive antibacterial thermal insulation mortar and preparation method thereof | |
| CN105236893B (en) | One kind mixes ultralight pearlite heat-insulation plate of iron tailings and preparation method thereof | |
| CN102060461B (en) | Cement composite grinding aid and preparation method thereof | |
| CN103641427B (en) | A kind of foam type heat insulation material of Steel slag-cement-gypsum-swool wool compound and preparation method | |
| CN103723959A (en) | Inorganic, insulating and energy-saving material | |
| CN109735176A (en) | A kind of preparation method of energy conservation and environmental protection building thermal-insulating coating | |
| CN102992674A (en) | Water-proof agent for building and preparation method thereof | |
| CN102134423B (en) | Polystyrene-magnetic absorbent composite wave-absorbing coating and preparation method thereof | |
| CN102219452A (en) | Pumice straw lightweight aggregate concrete and preparation method thereof | |
| CN110590232B (en) | Antibiotic artificial stone and use its operating room wallboard | |
| CN102021093A (en) | Low temperature two-in-one type washing drier for dishwasher and preparation method thereof | |
| CN102603252B (en) | Jetting type foaming inorganic light energy-saving material | |
| CN103848599B (en) | A kind of aluminium oxide/zinc oxide composite thermal insulation mortar and preparation method thereof | |
| CN106995293A (en) | Multifunction wall board preparation method | |
| CN106148940A (en) | A kind of preparation method of environment-friendly type high aluminum zinc/silver stearate composite coating | |
| CN105967732A (en) | Mothproof insulation building gypsum powder with high compressive strength and manufacture method thereof | |
| CN104556865A (en) | Preparation method of light-weight composite fiber foamed concrete | |
| CN102503236A (en) | Composite concrete waterproofing agent | |
| CN106149974B (en) | A kind of keel shoe for cement foamed heat-insulation wall plate | |
| CN107117875A (en) | A kind of geo-polymer construction material and preparation method thereof | |
| CN104098301B (en) | A kind of light dolomite/montmorillonite Composite light cellular partition board and preparation method thereof | |
| CN103058596A (en) | Autoclaved aerated concrete | |
| CN105084819A (en) | Phenolic foam board interface agent and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190510 |