CN109721321A - A kind of preparation method of ardealite based self-leveling material - Google Patents

A kind of preparation method of ardealite based self-leveling material Download PDF

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Publication number
CN109721321A
CN109721321A CN201910200439.1A CN201910200439A CN109721321A CN 109721321 A CN109721321 A CN 109721321A CN 201910200439 A CN201910200439 A CN 201910200439A CN 109721321 A CN109721321 A CN 109721321A
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ardealite
agent
preparation
based self
leveling material
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CN109721321B (en
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朱社凤
邓颖
陈艺芳
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Fujian green tree Energy Saving Technology Co., Ltd
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Hunan Seven Weft Technology Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/14Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing calcium sulfate cements
    • C04B28/142Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing calcium sulfate cements containing synthetic or waste calcium sulfate cements
    • C04B28/143Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing calcium sulfate cements containing synthetic or waste calcium sulfate cements the synthetic calcium sulfate being phosphogypsum
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00017Aspects relating to the protection of the environment
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/20Resistance against chemical, physical or biological attack
    • C04B2111/27Water resistance, i.e. waterproof or water-repellent materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2201/00Mortars, concrete or artificial stone characterised by specific physical values
    • C04B2201/50Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Curing Cements, Concrete, And Artificial Stone (AREA)

Abstract

The invention belongs to technical field of energy saving and environmental protection, more particularly to a kind of preparation method of ardealite based self-leveling material, be prepared by the substance of following weight percent: modified ardealite 40%-50%, PO42.5 cement 10%-15%, modified rubber powder 3%-5%, fiber 0.5%-2%, redispersable latex powder 3%-6%, water conservation stabilizer 0.3%-0.8%, powdery polycarboxylic acid water-reducing agent 0.1%-0.4%, moistening flatting agent 0.1%-0.5%, defoaming agent 0.001%-0.005%, surplus are steel slag or quartz sand.Ardealite based self-leveling material prepared by the present invention has the characteristics that intensity is high, waterproof performance is good, can also make full use of the wastes such as ardealite, waste old, be conducive to environmental protection.

Description

A kind of preparation method of ardealite based self-leveling material
Technical field
The present invention is a kind of divisional application of Chinese patent " ardealite based self-leveling material ", and the applying date is April 9 in 2017 Day, application No. is 201710226715.2.The invention belongs to technical field of energy saving and environmental protection, and in particular to a kind of ardealite base gravity flow Flat material and preparation method thereof.
Background technique
Ground is an important component of architectural engineering, and Self-leveling technology is a kind of ground construction technology, liquid Floor material under state trickles automatically after being scattered to ground, and on ground, trickling is to being filled and led up after low-lying, finally by full wafer Surface current drops down smooth rear static, condensation cure.The levelling technique of Self-leveling saves a large amount of people compared to artificial floor leveling technique Work, with the continuous improvement of human cost, gravity flowing levelling mortar competitiveness in terms of economy is increasing.Traditional gypsum base is certainly Levelling material is the related various auxiliary agents of addition using αsemiwatergypsum as main material, such as the preparation of retarder, water-reducing agent, water-retaining agent Made of a kind of air-setting self-leveling material.Since its water resistance is poor, at high cost, using being subject to certain restrictions.
Ardealite is that wet process manufactures the waste residue being discharged when phosphoric acid in phosphorous chemical industry, and 1 ton of phosphoric acid of every production is (with P2O5Meter) it generates about 4.5~5.5 tons of by-product ardealite, ardealite utilization rate is lower at present.It is most of to be disposed for stockpiling, the accumulation of a large amount of ardealites Not only land occupation, but also waste of resource endanger wherein the acidity contained and other harmful substances are easy to pollute surrounding enviroment It is extremely urgent to solve the problems, such as that ardealite accumulates for ecological environment.
In recent years, as private car quantity is increased sharply, accompanying this is the waste tire continually generated, currently, I The waste tire that state generates reaches several hundred million, if utilization is not added in so many waste old, there is also land occupation resource, harm The problem of ecological environment.
Summary of the invention
The present invention in view of the above-mentioned problems, providing one kind using ardealite is main substrate, waste rubber powder as auxiliary material, and Gypsum-based self-leveling material with preferable waterproof performance.
In order to achieve the above objectives, the present invention uses following technical scheme, and a kind of ardealite based self-leveling material, is by following The material composition of weight percent:
Modified ardealite: 40%-50%
Cement: 10%-15%
Modified rubber powder: 3%-5%
Fiber: 0.5%-2%
Redispersable latex powder: 3%-6%
It is retained stabilizer: 0.3%-0.8%
Water-reducing agent: 0.1%-0.4%
Moistening flatting agent: 0.1%-0.5%
Defoaming agent: 0.001%-0.005%
Surplus is hard material.
The preparation method of the modified ardealite is: by original state ardealite with account for changing for ardealite total weight 4%-6% Property agent be aged after mixing reaction 24-28h, then thermal activation 4h under the conditions of 140 DEG C, is down to after constant temperature in planetary mill Middle grinding 2min to obtain the final product.
The modifying agent is made of quick lime and compound modifying agent according to weight ratio 10-20:1.
Preferably, the compound modifying agent is sodium polyphosphate, stearic acid, itaconic acid, sodium ammonium triacetate, ethylenediamine tetramethyl Pitch one of sodium phosphate and diethanol amine or more than one.
It is furthermore preferred that the compound modifying agent is by stearic acid, itaconic acid and sodium ammonium triacetate according to weight ratio 1:1:1 group At.
The cement is PO42.5 cement.
The modified rubber powder refer to by rubber powder that fineness is 50-70 mesh mass fraction be 10% sodium hydroxide it is molten It is cleaned after impregnating 30-60min in liquid with clear water, then dries and obtain at 60-80 DEG C.
The fiber refers to one of short nylon fiber, basalt fibre, aromatic polyamide fibre.
Preferably, the fiber refers to that diameter is 10mm-20um, and length is the basalt fibre of 6mm-15mm.
The redispersable latex powder refers to vinyl acetate and ethylene higher fatty acids copolymerization rubber powder, acrylate and benzene second Alkene is copolymerized rubber powder, ethylene and one of vinyl chloride and vinyl laurate ternary polymerization rubber powder.
The water conservation stabilizer refers to one in methyl hydroxyethylcellulose ether, methylhydroxypropylcellulose ether and welan gum Kind.
The water-reducing agent is powdery polycarboxylic acid water-reducing agent.
The moistening flatting agent is polyether-modified dimethyl silicone polymer or organic silicon acrylic ester.
The defoaming agent is ethylenedistearamide or tributyl phosphate.
The hard material is one of steel slag or quartz sand.
Preferably, the quartzy grain fineness number is 100-200 mesh.
The surface of ardealite particle is adsorbed in the present invention after compound modifying agent incorporation, thus it is possible to vary when gypsum crystallization is grown Environment, prevent crystal form to longitudinal development, the crystal habit of product promoted to convert to ideal form;Self-leveling material is with thin layer It spreads out and puts in substrate surface, thinner thickness, ground layer can absorb many moisture, and large contact area with air, easily hard in slurry It dries out before change, mobile performance is caused to reduce, or even influence is normal hydrated, water conservation stabilizer can make system moisture excessive Be lost, keep normal hydrated and workability, can also improve viscosity coefficient, improve system stability, reduce laminated segregation, Grain sedimentation, bleeding phenomena such as, prevent self-leveling material because dehydration is too fast and cause insufficient material aquation, surface shedding, do The problems such as splitting;Sodium hydroxide solution can make to dispel the rubber additives such as the zinc stearate on rubber powder surface, make itself and gypsum base The binding force of material is stronger, rubber powder have retardance, alleviate self-leveling material system in as entringite formation and caused by it is swollen It is swollen, the water resistance of self-leveling material can also be improved;Moistening flatting agent can reduce system surface tension, increase system to substrate Wetting ability and the flowing levelability of itself;Latex powder can react after meeting water generates continuous film, is formed with gypsum slurry The mixture of interpenetrating body plays cementation, and transition region can be made more fine and close, the impermeability of material is greatly improved, in addition Emulsoid-film has hydrophobic effect, is improved the hydrophobic performance of material;Gypsum and cement in system can aquation generation calcium Aluminite and hydrated calcium silicate gel, with the progress of aquation, entringite is continuously increased with hydrated calcium silicate gel, hardenite intensity It is continuously improved, ettringite plays skeleton function in hardenite, and hydrated calcium silicate gel is then distributed in gap, to reduction hole Gap rate, the entringite of a large amount of hydraulicitys, hydrated calcium silicate gel are formed, the erosion work that can be hindered or weaken water to Self-leveling system With.
Beneficial effects of the present invention mainly have two o'clock:
(1) wastes such as ardealite, waste old can be made full use of, environmental protection is conducive to.
(2)) rational proportion of various raw material makes ardealite based self-leveling material of the present invention have intensity height, waterproofness Can be good the features such as.
Specific embodiment
In order to further illustrate the present invention, below with reference to embodiment to ardealite based self-leveling material provided by the invention into Row describe in detail, but it is to be understood that these description only for further illustrate the features and advantages of the present invention rather than it is right The limitation that the invention patent requires.
Embodiment 1
A kind of ardealite based self-leveling material is by the material composition of following weight percent: modified ardealite 40%, Cement 10%, modified rubber powder 3%, fiber 0.5%, redispersable latex powder 3%, water conservation stabilizer 0.3%, water-reducing agent 0.1%, moistening flatting agent 0.1%, defoaming agent 0.001%, surplus are hard material;
The preparation method of the modified ardealite is: by original state ardealite and the modifying agent for accounting for ardealite total weight 4% For 24 hours, then thermal activation 4h under the conditions of 140 DEG C, is down to after constant temperature the grinding in planetary mill for ageing reaction after mixing 2min to obtain the final product;
The modifying agent is made of quick lime and compound modifying agent according to weight ratio 10:1;
The compound modifying agent is sodium polyphosphate;
The cement is PO42.5 cement;
The sodium hydroxide solution that it is 10% in mass fraction by the rubber powder that fineness is 50 mesh that the modified rubber powder, which refers to, It is cleaned after middle immersion 30min with clear water, then dries and obtain at 60 DEG C;
The fiber refers to short nylon fiber;
The redispersable latex powder refers to that vinyl acetate and ethylene higher fatty acids are copolymerized rubber powder;
The water conservation stabilizer refers to methyl hydroxyethylcellulose ether;
The water-reducing agent is powdery polycarboxylic acid water-reducing agent;
The moistening flatting agent is polyether-modified dimethyl silicone polymer;
The defoaming agent is ethylenedistearamide;
The hard material is steel slag.
Embodiment 2
A kind of ardealite based self-leveling material is by the material composition of following weight percent: modified ardealite 50%, Cement 15%, modified rubber powder 5%, fiber 2%, redispersable latex powder 6%, water conservation stabilizer 0.8%, water-reducing agent 0.4%, Moistening flatting agent 0.5%, defoaming agent 0.005%, surplus are hard material;
The preparation method of the modified ardealite is: by original state ardealite and the modifying agent for accounting for ardealite total weight 6% Ageing reaction 28h after mixing, then thermal activation 4h under the conditions of 140 DEG C, is down to after constant temperature the grinding in planetary mill 2min to obtain the final product;
The modifying agent is made of quick lime and compound modifying agent according to weight ratio 20:1;
The compound modifying agent is made of ethylenediamine tetraacetic methene sodium phosphate and diethanol amine according to weight ratio 1:1;
The cement is PO42.5 cement;
The sodium hydroxide solution that it is 10% in mass fraction by the rubber powder that fineness is 70 mesh that the modified rubber powder, which refers to, It is cleaned after middle immersion 60min with clear water, then dries and obtain at 80 DEG C;
The fiber refers to aromatic polyamide fibre;
The redispersable latex powder refers to acrylate and styrene copolymerized rubber powder;
The water conservation stabilizer is methylhydroxypropylcellulose ether;
The water-reducing agent is powdery polycarboxylic acid water-reducing agent;
The moistening flatting agent is organic silicon acrylic ester;
The defoaming agent is tributyl phosphate;
The hard material is the quartz sand that steel fineness is 100 mesh.
Embodiment 3
A kind of ardealite based self-leveling material is by the material composition of following weight percent: modified ardealite 45%, Cement 12%, modified rubber powder 4%, fiber 1%, redispersable latex powder 4%, water conservation stabilizer 0.5%, water-reducing agent 0.3%, Moistening flatting agent 0.4%, defoaming agent 0.003%, surplus are hard material;
The preparation method of the modified ardealite is: by original state ardealite and the modifying agent for accounting for ardealite total weight 5% Ageing reaction 25h after mixing, then thermal activation 4h under the conditions of 140 DEG C, is down to after constant temperature the grinding in planetary mill 2min to obtain the final product;
The modifying agent is made of quick lime and compound modifying agent according to weight ratio 15:1;
The compound modifying agent is made of stearic acid, itaconic acid and sodium ammonium triacetate according to weight ratio 1:1:1;
The cement is PO42.5 cement;
The sodium hydroxide solution that it is 10% in mass fraction by the rubber powder that fineness is 60 mesh that the modified rubber powder, which refers to, It is cleaned after middle immersion 50min with clear water, then dries and obtain at 70 DEG C;
The fiber refers to that diameter is 10mm-20um, and length is the basalt fibre of 6mm-15mm;
The redispersable latex powder is ethylene and vinyl chloride and vinyl laurate ternary polymerization rubber powder;
The water conservation stabilizer is welan gum;
The water-reducing agent is powdery polycarboxylic acid water-reducing agent;
The moistening flatting agent is polyether-modified dimethyl silicone polymer;
The defoaming agent is ethylenedistearamide;
The hard material is the quartz sand that fineness is 150 mesh.
Embodiment 4
A kind of ardealite based self-leveling material is by the material composition of following weight percent: modified ardealite 48%, Cement 13%, modified rubber powder 4%, fiber 1.5%, redispersable latex powder 5%, water conservation stabilizer 0.6%, water-reducing agent 0.3%, moistening flatting agent 0.2%, defoaming agent 0.003%, surplus are hard material;
The preparation method of the modified ardealite is: by original state ardealite and the modification for accounting for ardealite total weight 4.5% Agent is aged reaction 27h after mixing, and then thermal activation 4h under the conditions of 140 DEG C, is down to after constant temperature the powder in planetary mill Grind 2min to obtain the final product;
The modifying agent is made of quick lime and compound modifying agent according to weight ratio 12:1;
The compound modifying agent is ethylenediamine tetraacetic methene sodium phosphate;
The cement is PO42.5 cement;
The sodium hydroxide solution that it is 10% in mass fraction by the rubber powder that fineness is 65 mesh that the modified rubber powder, which refers to, It is cleaned after middle immersion 40min with clear water, then dries and obtain at 70 DEG C;
The fiber refers to short nylon fiber;
The redispersable latex powder refers to acrylate and styrene copolymerized rubber powder;
The water conservation stabilizer refers to methylhydroxypropylcellulose ether;
The water-reducing agent is powdery polycarboxylic acid water-reducing agent;
The moistening flatting agent is organic silicon acrylic ester;
The defoaming agent is tributyl phosphate;
The hard material is steel slag.
Embodiment 5
A kind of ardealite based self-leveling material is by the material composition of following weight percent: modified ardealite 48%, Cement 13%, modified rubber powder 3.8%, fiber 1.2%, redispersable latex powder 5%, water conservation stabilizer 0.6%, water-reducing agent 0.3%, moistening flatting agent 0.3%, defoaming agent 0.003%, surplus are hard material.
Comparative example 1
A kind of ardealite based self-leveling material is by the material composition of following weight percent: ardealite 45%, cement 12%, modified rubber powder 4%, fiber 1%, redispersable latex powder 4%, water conservation stabilizer 0.5%, water-reducing agent 0.3%, wetting Levelling agent 0.4%, defoaming agent 0.003%, surplus are hard material;
The ardealite is original state ardealite;
The cement is PO42.5 cement;
The sodium hydroxide solution that it is 10% in mass fraction by the rubber powder that fineness is 60 mesh that the modified rubber powder, which refers to, It is cleaned after middle immersion 50min with clear water, then dries and obtain at 70 DEG C;
The fiber refers to that diameter is 10mm-20um, and length is the basalt fibre of 6mm-15mm;
The redispersable latex powder is ethylene and vinyl chloride and vinyl laurate ternary polymerization rubber powder;
The water conservation stabilizer is welan gum;
The water-reducing agent is powdery polycarboxylic acid water-reducing agent;
The moistening flatting agent is polyether-modified dimethyl silicone polymer;
The defoaming agent is ethylenedistearamide;
The hard material is the quartz sand that fineness is 150 mesh.
Comparative example 2
A kind of ardealite based self-leveling material is by the material composition of following weight percent: modified ardealite 45%, Cement 12%, rubber powder 4%, fiber 1%, redispersable latex powder 4%, water conservation stabilizer 0.5%, water-reducing agent 0.3%, wetting Levelling agent 0.4%, defoaming agent 0.003%, surplus are hard material;
The preparation method of the modified ardealite is: by original state ardealite and the modifying agent for accounting for ardealite total weight 5% Ageing reaction 25h after mixing, then thermal activation 4h under the conditions of 140 DEG C, is down to after constant temperature the grinding in planetary mill 2min to obtain the final product;
The modifying agent is made of quick lime and compound modifying agent according to weight ratio 15:1;
The compound modifying agent is made of stearic acid, itaconic acid and sodium ammonium triacetate according to weight ratio 1:1:1;
The cement is PO42.5 cement;
It is that 60 mesh obtain that the rubber powder, which is by waste tire grinding to fineness,;
The fiber refers to that diameter is 10mm-20um, and length is the basalt fibre of 6mm-15mm;
The redispersable latex powder is ethylene and vinyl chloride and vinyl laurate ternary polymerization rubber powder;
The water conservation stabilizer is welan gum;
The water-reducing agent is powdery polycarboxylic acid water-reducing agent;
The moistening flatting agent is polyether-modified dimethyl silicone polymer;
The defoaming agent is ethylenedistearamide;
The hard material is the quartz sand that fineness is 150 mesh.
Comparative example 3
A kind of ardealite based self-leveling material is by the material composition of following weight percent: modified ardealite 45%, Cement 12%, modified rubber powder 4%, fiber 1%, redispersable latex powder 4%, water conservation stabilizer 0.5%, water-reducing agent 0.3%, Defoaming agent 0.003%, surplus are hard material;
The preparation method of the modified ardealite is: by original state ardealite and the modifying agent for accounting for ardealite total weight 5% Ageing reaction 25h after mixing, then thermal activation 4h under the conditions of 140 DEG C, is down to after constant temperature the grinding in planetary mill 2min to obtain the final product;
The modifying agent is made of quick lime and compound modifying agent according to weight ratio 15:1;
The compound modifying agent is made of stearic acid, itaconic acid and sodium ammonium triacetate according to weight ratio 1:1:1;
The cement is PO42.5 cement;
The sodium hydroxide solution that it is 10% in mass fraction by the rubber powder that fineness is 60 mesh that the modified rubber powder, which refers to, It is cleaned after middle immersion 50min with clear water, then dries and obtain at 70 DEG C;
The fiber refers to that diameter is 10mm-20um, and length is the basalt fibre of 6mm-15mm;
The redispersable latex powder is ethylene and vinyl chloride and vinyl laurate ternary polymerization rubber powder;
The water conservation stabilizer is welan gum;
The water-reducing agent is powdery polycarboxylic acid water-reducing agent;
The defoaming agent is ethylenedistearamide;
The hard material is the quartz sand that fineness is 150 mesh.
Performance test
Reference standard JC/T1023-2007 " gypsum based self-leveling mortar " is to 1-5 of the embodiment of the present invention and comparative example 1-3 Some main performances of self-leveling material be tested, as a result see the table below 1.
1 gravity flowing levelling mortar performance of table

Claims (10)

1. a kind of preparation method of ardealite based self-leveling material, which is characterized in that be by the substance system of following weight percent It is standby to form: modified ardealite 40%-50%, PO42.5 cement 10%-15%, modified rubber powder 3%-5%, fiber 0.5%- 2%, redispersable latex powder 3%-6%, water conservation stabilizer 0.3%-0.8%, powdery polycarboxylic acid water-reducing agent 0.1%-0.4%, Moistening flatting agent 0.1%-0.5%, defoaming agent 0.001%-0.005%, surplus are steel slag or quartz sand;
Wherein, the modified ardealite is to mix original state ardealite with the modifying agent for accounting for ardealite total weight 4%-6% Ageing reaction 24-28h after even, then thermal activation 4h under the conditions of 140 DEG C, is down to after constant temperature the grinding 2min in planetary mill After be made;
It is that the rubber powder of 50-70 mesh soaks in the sodium hydroxide solution that mass fraction is 10% that the modified rubber powder, which is by fineness, It is cleaned after bubble 30-60min with clear water, is made after then being dried at 60-80 DEG C.
2. the preparation method of ardealite based self-leveling material according to claim 1, which is characterized in that the modifying agent It is made of quick lime and compound modifying agent according to weight ratio 10-20:1.
3. the preparation method of ardealite based self-leveling material according to claim 2, which is characterized in that the transformation of crystal Agent is one of sodium polyphosphate, stearic acid, itaconic acid, sodium ammonium triacetate, ethylenediamine tetraacetic methene sodium phosphate and diethanol amine Or more than one.
4. the preparation method of ardealite based self-leveling material according to claim 3, which is characterized in that the transformation of crystal Agent is made of stearic acid, itaconic acid and sodium ammonium triacetate according to weight ratio 1:1:1.
5. the preparation method of ardealite based self-leveling material according to claim 1, which is characterized in that the fiber is short One of nylon fiber, basalt fibre, aromatic polyamide fibre.
6. the preparation method of ardealite based self-leveling material according to claim 5, which is characterized in that the fiber refers to Diameter is 10mm-20um, and length is the basalt fibre of 6mm-15mm.
7. the preparation method of ardealite based self-leveling material according to claim 1, which is characterized in that described redispersible Latex powder is vinyl acetate and ethylene higher fatty acids copolymerization rubber powder, acrylate and styrene copolymerized rubber powder, ethylene and chloroethene One of alkene and vinyl laurate ternary polymerization rubber powder.
8. the preparation method of ardealite based self-leveling material according to claim 1, which is characterized in that the water conservation is stablized Agent is one of methyl hydroxyethylcellulose ether, methylhydroxypropylcellulose ether and welan gum.
9. the preparation method of ardealite based self-leveling material according to claim 1, which is characterized in that the wetting levelling Agent is polyether-modified dimethyl silicone polymer or organic silicon acrylic ester.
10. the preparation method of ardealite based self-leveling material according to claim 1, which is characterized in that the defoaming agent For ethylenedistearamide or tributyl phosphate.
CN201910200439.1A 2017-04-09 2017-04-09 Preparation method of phosphogypsum-based self-leveling material Active CN109721321B (en)

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CN107162553A (en) * 2017-07-19 2017-09-15 合肥广民建材有限公司 A kind of brushing gypsum and preparation method thereof
CN110436805B (en) * 2018-05-04 2021-09-21 北新集团建材股份有限公司 Caulking gypsum powder, preparation method thereof and phosphogypsum harmless treatment method
CN114573314B (en) * 2021-06-07 2023-04-25 瓮福化工科技有限公司 Phosphogypsum-based sound insulation self-leveling mortar and application thereof

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