CN109704723A - A kind of wear-resisting ageing-resistant soft ceramic tile - Google Patents
A kind of wear-resisting ageing-resistant soft ceramic tile Download PDFInfo
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- CN109704723A CN109704723A CN201910153838.7A CN201910153838A CN109704723A CN 109704723 A CN109704723 A CN 109704723A CN 201910153838 A CN201910153838 A CN 201910153838A CN 109704723 A CN109704723 A CN 109704723A
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- ceramic tile
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- resistant soft
- resisting ageing
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Abstract
The invention mainly relates to ceramic tile processing technique fields, a kind of wear-resisting ageing-resistant soft ceramic tile is disclosed, is prepared from the following raw materials: soil 165 ~ 175, attapulgite modified 43 ~ 45, gas phase of white carbon black 17 ~ 19, polypropylene fibre 6 ~ 8, polyethylene wax 1 ~ 3, nano zine oxide 1.6 ~ 1.8, nanometer anion powder 1.1 ~ 1.3；Wear-resisting ageing-resistant soft ceramic tile provided by the invention, intensity is high, and wearability is strong, avoids generating scratch in use process, while can be subjected to exposing to the weather, and delaying aging increases the practicability of soft ceramic tile；By soil and attapulgite modified mixing, using soil as primary raw material, mass production cost is saved, crushes and reduces partial size, and carry out humidification heating, keep soft ceramic tile quality exquisiteness, intensity high, avoids generating scratch in installation and use process.
Description
Technical field
The invention mainly relates to ceramic tile processing technique fields, more particularly to a kind of wear-resisting ageing-resistant soft ceramic tile.
Background technique
The raw material of traditional soft ceramic tile are to be burnt by 90% soil and 10% water-soluble additives by 400 DEG C or more high temperature
It ties.Soft ceramic tile be by the performance change of original soil, by light effect of irradiation be formed it is light come, obtained soft ceramic tile,
Softness, but wear no resistance, due to exposing to the weather when being easy to appear scratch, and being used in outdoor, it is easy to aging and change occur
Color influences the decorative effect of soft ceramic tile.
Existing 108275961 A of patent document CN discloses a kind of processing technology of porcelain tendre, and the soft ceramic tile made has
Certain flexibility and waterproofness, but obtained porcelain tendre is equally easy to appear scratch and aging phenomenon, practicability is not good enough；It is existing
102173652 A of patent document CN discloses a kind of preparation method of soft ceramic tile, and the soft ceramic tile being prepared has preferable resistance to
Hot and anti-flammability, but for it is outdoor when still it is easy to appear aging phenomena；And the biography being added in existing patent document
Soil of uniting is less, hence it is evident that improves production cost.
Summary of the invention
In order to make up the defect of prior art, the object of the present invention is to provide a kind of wear-resisting ageing-resistant soft ceramic tiles.
A kind of wear-resisting ageing-resistant soft ceramic tile, is made of raw material from the following weight: soil 165 ~ 175, attapulgite modified
43 ~ 45, gas phase of white carbon black 17 ~ 19, polypropylene fibre 6 ~ 8, polyethylene wax 1 ~ 3, nano zine oxide 1.6 ~ 1.8, nano-negative ion
Powder 1.1 ~ 1.3.
Described is attapulgite modified, and attapulgite is heated to 170 ~ 190 DEG C, keeps the temperature 20 ~ 30min, concave convex rod is added
The boric acid solution of native weight 15 ~ 20%, stirs evenly, and the butyl rubber of attapulgite weight 3 ~ 5% is added, continue to be heated to 230 ~
250 DEG C, 8 ~ 10min of insulated and stirred, 140 ~ 160 DEG C are cooled to the speed of 4 ~ 5 DEG C/min, 30 ~ 40min is kept the temperature, is down to naturally
Room temperature improves the adsorptivity and flexibility of attapulgite, enhances the intensity and wearability of soft ceramic tile, delays external environment to porcelain tendre
The accelerated ageing of brick obtains attapulgite modified.
The boric acid solution, concentration are 72 ~ 76mg/L, and temperature is 2 ~ 6 DEG C.
The polypropylene fibre, length are 30 ~ 35mm.
A kind of preparation method of wear-resisting ageing-resistant soft ceramic tile, comprising the following steps:
(1) soil and attapulgite modified is weighed by weight, using soil as primary raw material, is saved mass production cost, is crushed to
230 ~ 270 mesh, adjusting water content is 43 ~ 45%, is slowly heated to 160 ~ 180 DEG C, keeps soft ceramic tile quality exquisiteness, intensity high, avoids
Scratch is generated in installation and use process, obtains mixture A；
(2) gas phase of white carbon black and nano zine oxide are added in mixture A, are stirred 10 ~ 15min in 130 ~ 150 DEG C, make original
Material is sufficiently mixed and is crosslinked, and improves the intensity and flexibility of soft ceramic tile, can be avoided pollutant and ultraviolet light causes soft ceramic tile
Corrosion and oxidation, the generation of delaying aging phenomenon extend the service life of soft ceramic tile, obtain mixture B；
(3) polypropylene fibre, polyethylene wax and nanometer anion powder are added in mixture B, are stirred 10 in 160 ~ 180 DEG C
~ 15min can enhance the flexibility and antioxygenic property of soft ceramic tile, avoid soft ceramic tile oxidation impaired, obtain mixture C；
(4) mixture C is injected in mold, in 150 ~ 160 DEG C of compression mouldings, promotes full cross-linked between material, raising porcelain tendre
The intensity and wearability of brick, demoulding, obtain adobe；
(5) ethyl lactate solution for being 4 ~ 6% to adobe surface even spraying volume fraction infiltrates 2 ~ 3h in 50 ~ 70 DEG C of standings,
It slowly penetrates ethyl lactate inside adobe, promotes each ingredient in adobe to be cross-linked with each other, improve the intensity and flexibility of ceramic tile, prolong
Slow external world's corrosive elements cause aging to brick body, then at 140 ~ 150 DEG C of steam-cured 30 ~ 40min, improve the intensity of ceramic tile and wear-resisting
Property, it avoids ceramic tile from scratch occur, obtains wear-resisting ageing-resistant soft ceramic tile.
The compression moulding of the step (4), pressing time are 8 ~ 10min.
The ethyl lactate solution of the step (5), every 40 ~ 60min is spraying primary, and spray amount is adobe surface wettability but nothing
Liquid drips.
The application method of the wear-resisting ageing-resistant soft ceramic tile is used for internal wall brick and exterior wall tile.
The invention has the advantages that wear-resisting ageing-resistant soft ceramic tile provided by the invention, intensity is high, and wearability is strong, avoid using
Scratch is generated in the process, while can be subjected to exposing to the weather, and delaying aging increases the practicability of soft ceramic tile；By soil and modification
Attapulgite mixing saves mass production cost using soil as primary raw material, crushes and reduces partial size, and carry out humidification heating, makes
Soft ceramic tile quality is fine and smooth, intensity is high, avoids generating scratch in installation and use process；It is attapulgite modified to be added by attapulgite
Boric acid solution and butyl rubber are modified the adsorptivity and flexibility for improving attapulgite, enhance the intensity of soft ceramic tile and wear-resisting
Property, delay accelerated ageing of the external environment to soft ceramic tile；It adds gas phase of white carbon black and nano zine oxide and carries out high-temperature stirring,
So that raw material is sufficiently mixed and is crosslinked, improve the intensity and flexibility of soft ceramic tile, can be avoided pollutant and ultraviolet light to soft ceramic tile
It causes to corrode and aoxidize, the generation of delaying aging phenomenon extends the service life of soft ceramic tile；Add polypropylene fibre, poly- second
Alkene wax and nanometer anion powder simultaneously carry out high-temperature stirring, can enhance the flexibility and antioxygenic property of soft ceramic tile, avoid porcelain tendre
Brick oxidation is impaired；Material is injected after mold and carries out high-temperature high-pressure and is made type, promotes full cross-linked between material, improves soft ceramic tile
Intensity and wearability；Ethyl lactate solution is repeatedly sprayed to adobe surface after molding, slowly penetrates ethyl lactate inside adobe,
Promote each ingredient in adobe to be cross-linked with each other, improves the intensity and flexibility of ceramic tile, extraneous corrosive elements is delayed to cause brick body
Aging, carries out steam-cured after infiltration, improve the intensity and wearability of ceramic tile, ceramic tile is avoided scratch occur, improve the practical of soft ceramic tile
Property.
Specific embodiment
Illustrate the present invention with specific embodiment below.
Embodiment 1
A kind of wear-resisting ageing-resistant soft ceramic tile, is made of raw material from the following weight: soil 165, attapulgite modified 43, gas phase is white
Carbon black 17, polypropylene fibre 6, polyethylene wax 1, nano zine oxide 1.6, nanometer anion powder 1.1.
Described is attapulgite modified, and attapulgite is heated to 170 DEG C, keeps the temperature 20min, attapulgite weight is added
15% boric acid solution, stirs evenly, and the butyl rubber of attapulgite weight 3% is added, continues to be heated to 230 DEG C, insulated and stirred
8min is cooled to 140 DEG C with the speed of 4 DEG C/min, keeps the temperature 30min, be down to room temperature naturally, improve attapulgite adsorptivity and
Flexibility enhances the intensity and wearability of soft ceramic tile, and external environment is delayed to obtain modified attapulgite to the accelerated ageing of soft ceramic tile
Soil.
The boric acid solution, concentration 72mg/L, temperature are 2 DEG C.
The polypropylene fibre, length are 30 ~ 35mm.
A kind of preparation method of wear-resisting ageing-resistant soft ceramic tile, comprising the following steps:
(1) soil and attapulgite modified is weighed by weight, using soil as primary raw material, is saved mass production cost, is crushed to
230 mesh, adjusting water content is 43%, is slowly heated to 160 DEG C, keeps soft ceramic tile quality exquisiteness, intensity high, avoids installing and use
Scratch is generated in the process, obtains mixture A；
(2) gas phase of white carbon black and nano zine oxide are added in mixture A, are stirred 10min in 130 DEG C, keep raw material abundant
Mixing and crosslinking, improve the intensity and flexibility of soft ceramic tile, can be avoided pollutant and ultraviolet light to soft ceramic tile cause corrosion and
Oxidation, the generation of delaying aging phenomenon extend the service life of soft ceramic tile, obtain mixture B；
(3) polypropylene fibre, polyethylene wax and nanometer anion powder are added in mixture B, are stirred 10min in 160 DEG C,
The flexibility and antioxygenic property that soft ceramic tile can be enhanced avoid soft ceramic tile oxidation impaired, obtain mixture C；
(4) mixture C is injected in mold, in 150 DEG C of compression mouldings, pressing time 8min promotes sufficiently to hand between material
Connection, improves the intensity and wearability of soft ceramic tile, demoulds, obtains adobe；
(5) ethyl lactate solution for being 4% to adobe surface even spraying volume fraction infiltrates 2h, every 40min in 50 DEG C of standings
Spraying primary, spray amount is adobe surface wettability but no liquid is dripped, and slowly penetrates ethyl lactate inside adobe, promotes adobe
Interior each ingredient is cross-linked with each other, and improves the intensity and flexibility of ceramic tile, extraneous corrosive elements is delayed to cause aging to brick body, then at
140 DEG C of steam-cured 30min improve the intensity and wearability of ceramic tile, ceramic tile are avoided scratch occur, obtain wear-resisting ageing-resistant soft ceramic tile.
The application method of the wear-resisting ageing-resistant soft ceramic tile is used for internal wall brick and exterior wall tile.
Embodiment 2
A kind of wear-resisting ageing-resistant soft ceramic tile, is made of raw material from the following weight: soil 170, attapulgite modified 44, gas phase is white
Carbon black 18, polypropylene fibre 7, polyethylene wax 2, nano zine oxide 1.7, nanometer anion powder 1.2.
Described is attapulgite modified, and attapulgite is heated to 180 DEG C, keeps the temperature 25min, attapulgite weight is added
18% boric acid solution, stirs evenly, and the butyl rubber of attapulgite weight 4% is added, continues to be heated to 240 DEG C, insulated and stirred
9min is cooled to 150 DEG C with the speed of 4.5 DEG C/min, keeps the temperature 35min, be down to room temperature naturally, improve the adsorptivity of attapulgite
And flexibility, enhance the intensity and wearability of soft ceramic tile, external environment is delayed to obtain modified attapulgite to the accelerated ageing of soft ceramic tile
Soil.
The boric acid solution, concentration 74mg/L, temperature are 4 DEG C.
The polypropylene fibre, length are 30 ~ 35mm.
A kind of preparation method of wear-resisting ageing-resistant soft ceramic tile, comprising the following steps:
(1) soil and attapulgite modified is weighed by weight, using soil as primary raw material, is saved mass production cost, is crushed to
250 mesh, adjusting water content is 44%, is slowly heated to 170 DEG C, keeps soft ceramic tile quality exquisiteness, intensity high, avoids installing and use
Scratch is generated in the process, obtains mixture A；
(2) gas phase of white carbon black and nano zine oxide are added in mixture A, are stirred 13min in 140 DEG C, keep raw material abundant
Mixing and crosslinking, improve the intensity and flexibility of soft ceramic tile, can be avoided pollutant and ultraviolet light to soft ceramic tile cause corrosion and
Oxidation, the generation of delaying aging phenomenon extend the service life of soft ceramic tile, obtain mixture B；
(3) polypropylene fibre, polyethylene wax and nanometer anion powder are added in mixture B, are stirred 13min in 170 DEG C,
The flexibility and antioxygenic property that soft ceramic tile can be enhanced avoid soft ceramic tile oxidation impaired, obtain mixture C；
(4) mixture C is injected in mold, in 155 DEG C of compression mouldings, pressing time 9min promotes sufficiently to hand between material
Connection, improves the intensity and wearability of soft ceramic tile, demoulds, obtains adobe；
(5) ethyl lactate solution for being 5% to adobe surface even spraying volume fraction infiltrates 2.5h in 60 DEG C of standings, often
50min is spraying primary, and spray amount is adobe surface wettability but no liquid is dripped, and slowly penetrates ethyl lactate inside adobe, promotees
Each ingredient is cross-linked with each other in into adobe, improves the intensity and flexibility of ceramic tile, extraneous corrosive elements is delayed to cause always brick body
Change, then at 145 DEG C of steam-cured 35min, improves the intensity and wearability of ceramic tile, ceramic tile is avoided scratch occur, obtain wear-resisting ageing-resistant soft
Ceramic tile.
The application method of the wear-resisting ageing-resistant soft ceramic tile is used for internal wall brick and exterior wall tile.
Embodiment 3
A kind of wear-resisting ageing-resistant soft ceramic tile, is made of raw material from the following weight: soil 175, attapulgite modified 45, gas phase is white
Carbon black 19, polypropylene fibre 8, polyethylene wax 3, nano zine oxide 1.8, nanometer anion powder 1.3.
Described is attapulgite modified, and attapulgite is heated to 190 DEG C, keeps the temperature 30min, attapulgite weight is added
20% boric acid solution, stirs evenly, and the butyl rubber of attapulgite weight 5% is added, continues to be heated to 250 DEG C, insulated and stirred
10min is cooled to 160 DEG C with the speed of 5 DEG C/min, keeps the temperature 40min, be down to room temperature naturally, improve the adsorptivity of attapulgite
And flexibility, enhance the intensity and wearability of soft ceramic tile, external environment is delayed to obtain modified attapulgite to the accelerated ageing of soft ceramic tile
Soil.
The boric acid solution, concentration 76mg/L, temperature are 6 DEG C.
The polypropylene fibre, length are 30 ~ 35mm.
A kind of preparation method of wear-resisting ageing-resistant soft ceramic tile, comprising the following steps:
(1) soil and attapulgite modified is weighed by weight, using soil as primary raw material, is saved mass production cost, is crushed to
270 mesh, adjusting water content is 45%, is slowly heated to 180 DEG C, keeps soft ceramic tile quality exquisiteness, intensity high, avoids installing and use
Scratch is generated in the process, obtains mixture A；
(2) gas phase of white carbon black and nano zine oxide are added in mixture A, are stirred 15min in 150 DEG C, keep raw material abundant
Mixing and crosslinking, improve the intensity and flexibility of soft ceramic tile, can be avoided pollutant and ultraviolet light to soft ceramic tile cause corrosion and
Oxidation, the generation of delaying aging phenomenon extend the service life of soft ceramic tile, obtain mixture B；
(3) polypropylene fibre, polyethylene wax and nanometer anion powder are added in mixture B, are stirred 15min in 180 DEG C,
The flexibility and antioxygenic property that soft ceramic tile can be enhanced avoid soft ceramic tile oxidation impaired, obtain mixture C；
(4) mixture C is injected in mold, in 160 DEG C of compression mouldings, pressing time 10min promotes sufficiently to hand between material
Connection, improves the intensity and wearability of soft ceramic tile, demoulds, obtains adobe；
(5) ethyl lactate solution for being 6% to adobe surface even spraying volume fraction infiltrates 3h, every 60min in 70 DEG C of standings
Spraying primary, spray amount is adobe surface wettability but no liquid is dripped, and slowly penetrates ethyl lactate inside adobe, promotes adobe
Interior each ingredient is cross-linked with each other, and improves the intensity and flexibility of ceramic tile, extraneous corrosive elements is delayed to cause aging to brick body, then at
150 DEG C of steam-cured 40min improve the intensity and wearability of ceramic tile, ceramic tile are avoided scratch occur, obtain wear-resisting ageing-resistant soft ceramic tile.
The application method of the wear-resisting ageing-resistant soft ceramic tile is used for internal wall brick and exterior wall tile.
Comparative example 1
It is changed to attapulgite by attapulgite modified, remaining preparation method, with embodiment 1.
Comparative example 2
Remove polypropylene fibre, remaining preparation method, with embodiment 1.
Comparative example 3
Remove polyethylene wax, remaining preparation method, with embodiment 1.
Comparative example 4
Remove nano zine oxide, remaining preparation method, with embodiment 1.
Comparative example 5
Remove nanometer anion powder, remaining preparation method, with embodiment 1.
Comparative example 6
Removal step (2) and (3), all raw materials are added in step (1), remaining preparation method, with embodiment 1.
Comparative example 7
Remove the ethyl lactate solution in step (5), remaining preparation method, with embodiment 1.
Comparative example 8
Existing 108275961 A of patent document CN discloses a kind of processing technology of porcelain tendre.
Comparative example 9
Existing 102173652 A of patent document CN discloses a kind of preparation method of soft ceramic tile.
The performance of embodiment and comparative example soft ceramic tile:
According to the tensile strength and fracture of the method detection embodiment and comparative example soft ceramic tile of 102173652 A of patent document CN
Elongation, and the horizontal iron block for pulling weight 5kg carries out horizontal sliding on soft ceramic tile surface, horizontal velocity 0.5m/s is slided repeatedly
Dynamic 10 times, whether observation soft ceramic tile surface there is scratch, and the exterior wall tile of each group is exposed to the sun 100d in the sun, sees whether to send out
Raw weather stain, the performance of embodiment and comparative example soft ceramic tile are shown in Table 1.
Table 1: the performance of embodiment and comparative example soft ceramic tile
Note: "-" expression does not occur, and "+" indicates occur, and quantity is more, more serious.
Table 1 the result shows that, the wear-resisting ageing-resistant soft ceramic tile of embodiment, tensile strength, elongation at break, scratch and discoloration
Index is significantly better than that comparative example, illustrate wear-resisting ageing-resistant soft ceramic tile provided by the invention have good intensity, wearability and
Ageing-resistant performance.
Claims (8)
1. a kind of wear-resisting ageing-resistant soft ceramic tile, which is characterized in that be made of raw material from the following weight: soil 165 ~ 175 is modified
Attapulgite 43 ~ 45, polypropylene fibre 6 ~ 8, polyethylene wax 1 ~ 3, nano zine oxide 1.6 ~ 1.8, is received gas phase of white carbon black 17 ~ 19
Rice negative ion powder 1.1 ~ 1.3.
2. wear-resisting ageing-resistant soft ceramic tile according to claim 1, which is characterized in that described is attapulgite modified, will be concave-convex
Stick soil is heated to 170 ~ 190 DEG C, keeps the temperature 20 ~ 30min, and the boric acid solution of attapulgite weight 15 ~ 20% is added, stirs evenly, adds
The butyl rubber for entering attapulgite weight 3 ~ 5% continues to be heated to 230 ~ 250 DEG C, 8 ~ 10min of insulated and stirred, with 4 ~ 5 DEG C/min
Speed be cooled to 140 ~ 160 DEG C, keep the temperature 30 ~ 40min, be down to room temperature naturally, obtain attapulgite modified.
3. wear-resisting ageing-resistant soft ceramic tile according to claim 2, which is characterized in that the boric acid solution, concentration be 72 ~
76mg/L, temperature are 2 ~ 6 DEG C.
4. wear-resisting ageing-resistant soft ceramic tile according to claim 1, which is characterized in that the polypropylene fibre, length be 30 ~
35mm。
5. a kind of preparation method of ageing-resistant soft ceramic tile wear-resisting according to claim 1, which is characterized in that including following step
It is rapid:
(1) weigh soil and attapulgite modified by weight, be crushed to 230 ~ 270 mesh, adjusting water content is 43 ~ 45%, slowly plus
Heat obtains mixture A to 160 ~ 180 DEG C；
(2) gas phase of white carbon black and nano zine oxide are added in mixture A, are stirred 10 ~ 15min in 130 ~ 150 DEG C, obtain mixed
Close object B；
(3) polypropylene fibre, polyethylene wax and nanometer anion powder are added in mixture B, are stirred 10 in 160 ~ 180 DEG C
~ 15min, obtains mixture C；
(4) mixture C is injected in mold, in 150 ~ 160 DEG C of compression mouldings, demoulding obtains adobe；
(5) ethyl lactate solution for being 4 ~ 6% to adobe surface even spraying volume fraction infiltrates 2 ~ 3h in 50 ~ 70 DEG C of standings,
Then at 140 ~ 150 DEG C of steam-cured 30 ~ 40min, wear-resisting ageing-resistant soft ceramic tile is obtained.
6. the preparation method of wear-resisting ageing-resistant soft ceramic tile according to claim 5, which is characterized in that the pressure of the step (4)
Type is made, the pressing time is 8 ~ 10min.
7. the preparation method of wear-resisting ageing-resistant soft ceramic tile according to claim 5, which is characterized in that the cream of the step (5)
Acetate solution, every 40 ~ 60min is spraying primary, and spray amount is adobe surface wettability but no liquid is dripped.
8. a kind of application method of any one of claim 1 ~ 7 wear-resisting ageing-resistant soft ceramic tile, which is characterized in that be used for interior wall
Brick and exterior wall tile.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910153838.7A CN109704723A (en) | 2019-03-01 | 2019-03-01 | A kind of wear-resisting ageing-resistant soft ceramic tile |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910153838.7A CN109704723A (en) | 2019-03-01 | 2019-03-01 | A kind of wear-resisting ageing-resistant soft ceramic tile |
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| Publication Number | Publication Date |
|---|---|
| CN109704723A true CN109704723A (en) | 2019-05-03 |
Family
ID=66265989
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910153838.7A Withdrawn CN109704723A (en) | 2019-03-01 | 2019-03-01 | A kind of wear-resisting ageing-resistant soft ceramic tile |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111927019A (en) * | 2020-08-11 | 2020-11-13 | 深圳市维业装饰集团股份有限公司 | Decorative brick and manufacturing method and mounting method thereof |
| CN112500044A (en) * | 2020-12-04 | 2021-03-16 | 姚智 | Soft ceramic tile and preparation method thereof |
-
2019
- 2019-03-01 CN CN201910153838.7A patent/CN109704723A/en not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111927019A (en) * | 2020-08-11 | 2020-11-13 | 深圳市维业装饰集团股份有限公司 | Decorative brick and manufacturing method and mounting method thereof |
| CN112500044A (en) * | 2020-12-04 | 2021-03-16 | 姚智 | Soft ceramic tile and preparation method thereof |
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