CN109700673A - A kind of acid effect clean skin product and preparation method thereof containing alkaline particle - Google Patents
A kind of acid effect clean skin product and preparation method thereof containing alkaline particle Download PDFInfo
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- CN109700673A CN109700673A CN201910145846.7A CN201910145846A CN109700673A CN 109700673 A CN109700673 A CN 109700673A CN 201910145846 A CN201910145846 A CN 201910145846A CN 109700673 A CN109700673 A CN 109700673A
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Abstract
The present invention relates to cosmetic technical fields, provide a kind of acid effect clean skin product and preparation method thereof containing alkaline particle.A kind of preparation method of acid effect clean skin product containing alkaline particle is formulated as follows: being free of the non-soap based substrate of preservative skin-cleaning articles；Acidulant substance；Matrix stablizes conditioner；Alkaline particle；It is uniformly mixed and filters after being weighed according to the formula.The present invention also provides a kind of acid effect clean skin product containing alkaline particle.
Description
Technical field
The present invention relates to cosmetic technical field more particularly to a kind of acid effect clean skin product containing alkaline particle and its
Preparation method.
Background technique
Daily life, we be unable to do without the articles for daily use such as chemical article, especially cosmetics, detergent, dish washing liquid.
According to 2007 Nian8Yue27 State General Administration for Quality Supervision announce " cosmetics mark administrative provisions ", cosmetics refer to
It smears, sprinkling or other similar method, intersperses among any position of human body surface, such as skin, hair, refer to toenail, lips and teeth,
To reach cleaning, maintenance, beauty, modification and change appearance, or amendment human scent, the chemistry for the purpose of maintaining a good state
Industrial goods or fine chemical product.
Cleaning products are the products that everybody will face daily, and for most of people seeking beauties, cleaning daily is twice
Face is minimum number, and common people had a bath at-three days two days, touch cleaning supplies.Male will almost use daily
Shaving Products, to have the function that clean beard.
Furthermore enter and leave kitchen, toilet at us, meet with friend, party perhaps the rest of short time or
In air-conditioned room, the time stayed by computer, by TV, perhaps in colder outside enter warm room or from warm
Room enters colder space, etc..Our mankind be one like movement life, the state of time changing oneself, when
The characteristics of making us become more comfortable at quarter, being our mankind.
The amphiphilic structure of surfactant is excellent promotion skin cutaneous permeable agent, and it is exactly excellent that preservative is senior
Skin-absorbent agents.Therefore, the cleaning products containing surfactant and preservative are most easily to make tight skin, stimulation and mistake
Quick product.
Data show that white-collar Ms almost uses 8-12 clean skin product, non-physiology in physiology phase daily
5-8 clean skin product is used when the phase daily.With irritation and hypersensitive cleaning supplies, while consumer is also increased to rear
The use of road cosmetics, such as toner, essence, lotion, cream.The inappropriate use of these products is not suitable for using, more
Aggravate the burden of skin.
Therefore, how when consumer uses cleaning supplies, the product without containing preservative, for people seeking beauty and people
Health be just particularly important.
It is well known that nonexpondable cosmetics, the cosmetics if do not added preservative are easy to be contaminated by bacterial, otherwise
Disposable product must be carried out under absolute cleanliness environment to fill, in this way to production environment, production cost, packing cost,
Environmental pollution and carbon emission etc. can all cause very big influence.
Summary of the invention
It is an object of the invention to overcome the above-mentioned prior art, it is clean to provide a kind of acid effect containing alkaline particle
Skin product and preparation method thereof.
In order to solve the above technical problems, invention uses technical solution as described below.A kind of acid function containing alkaline particle
The preparation method of clean skin product is imitated, is formulated as follows:
Without the non-soap based substrate of preservative skin-cleaning articles: 80-95 parts by weight；
Acidulant substance: 5-15 parts by weight；
Matrix stablizes conditioner: 0.001-5 parts by weight；
Alkaline particle: 0.01-14.999 parts by weight；
It is uniformly mixed and filters after being weighed according to the formula.
Preferably, the pH value of the 0.01-5% aqueous solution of the acidulant substance is 1-4.
Preferably, the acidulant substance is citric acid and derivative, Glycolic acid and derivative, lactic acid and derivative, apple
Tartaric acid and derivative, acetic acid and derivative, lactobionic acid and derivative, gluconic acid and derivative, tartaric acid and health object, amino acid and
Derivative, salicylic acid and derivative, oleic acid and derivative, linoleic acid and derivative, linolenic acid and derivative phosphoric acid and its derivative
The combination of one or more of object.
Preferably, the matrix stablize conditioner be one of cellulose, starch, glue, carbohydrate, peptides, protein or
Several combinations.
Preferably, the matrix stablizes the pH value of the aqueous solution of conditioner less than 8.
Preferably, the alkaline particle is sodium hydroxide, potassium hydroxide, calcium hydroxide, ammonium hydroxide, organic amine, alkalescence potassium
The combination of one or more of salt, alkaline sodium salt, basic ammonium salts, alkaline organic ammonium salt.
Preferably, described to be uniformly mixed to be carried out at 15-100 DEG C.
Preferably, the filter screen being filtered into using -15000 mesh of 300 mesh, pressure are to carry out under normal pressure -1.0MPa.
A kind of acid effect clean skin product containing alkaline particle is produced using above-mentioned acid effect clean skin containing alkaline particle
The preparation method of product is prepared.
Preferably, the pH value of acid effect clean skin product containing alkaline particle is less than 4.
The beneficial effects of the present invention are:
The present invention is exactly to have invented a kind of acid effect clean skin product containing alkaline particle, can be used for multiple times, and is reduced anti-
Injury of the rotten agent to skin.
Specific embodiment
To make those skilled in the art that the purposes, technical schemes and advantages of invention be more clearly understood, below
Invention is further elaborated in conjunction with the embodiments.
A kind of preparation method of acid effect clean skin product containing alkaline particle is formulated as follows:
Without the non-soap based substrate of preservative skin-cleaning articles: 80-95 parts by weight；
Acidulant substance: 5-15 parts by weight；
Matrix stablizes conditioner: 0.001-5 parts by weight；
Alkaline particle: 0.01-14.999 parts by weight；
It is uniformly mixed and filters after being weighed according to the formula.
Of the invention is that cosmetics or daily use chemicals engineer are intelligible clean without the non-soap based substrate of preservative skin-cleaning articles
Skin matrix can be anionic surfactant, amphitypy surfactant, nonionic surfactant and special surface activity
Shampoo, shower cream, shaving cream, facial cleanser, the hand cleanser etc. of agent composition, pH value is less than 10.
Acidulant substance of the invention can be citric acid and derivative, Glycolic acid and derivative, lactic acid and derivative, apple
Tartaric acid and derivative, acetic acid and derivative, lactobionic acid and derivative, gluconic acid and derivative, tartaric acid and health object, amino acid and
Derivative, salicylic acid and derivative, oleic acid and derivative, linoleic acid and derivative, linolenic acid and derivative phosphoric acid and its derivative
The combination of one or more of object.It is characterized in that the pH value of aqueous solution 0.01-5% between 1-4, includes 1 and 4.
Matrix of the invention stablize conditioner can for one of cellulose, starch, glue, carbohydrate, peptides, protein or
Several combinations.Wherein cellulose, starch, glue, carbohydrate, peptides, protein can be it is natural synthesis and it is semi-synthetic
Cellulose, starch, glue, carbohydrate, peptides, protein.The pH value of its aqueous solution is less than 8.
Alkaline particle of the invention can be sodium hydroxide, potassium hydroxide, calcium hydroxide, ammonium hydroxide, organic amine, alkalescence potassium
The combination of one or more of salt, alkaline sodium salt, basic ammonium salts, alkaline organic ammonium salt.
Preferably, described to be uniformly mixed to be carried out at 15-100 DEG C.The mistake being filtered into using -15000 mesh of 300 mesh
Strainer, pressure are to carry out under normal pressure -1.0MPa.
Acid effect clean skin product containing alkaline particle of the invention has a characteristic that
PH value is less than 4；
Without containing preservative；
When using this product, taking-up product is used conventionally, it can be with the pH=such as tap water, pure water, vegetable juice, fruit syrup
Liquid mixing between 5-8, mixed pH value is greater than 4, it is still further preferred that pH=5.8；
In use, alkaline particle can occur physically or chemically to react with matrix, make the pH of product between 4-8.
Its effect of effect clean skin product of the invention can treat and prevent acne, treats and prevents sun-induced skin
Skin lesion, the various skin diseases of adjuvant treatment.
Some specific embodiments are provided below
Embodiment 1
Shampoo without preservative: unit: g
1) without preservative hair washing water-based (surfactant activity object total amount 25%): 91；
2) gluconolactone 5, potassium dihydrogen phosphate 2.5；
3) sodium alginate 0.5；
4) sodium metasilicate 1；
Above-mentioned substance is uniformly mixed according to prescription quality at 15 DEG C.It then is 300 mesh with filter screen, pressure is
Natural filtration, as gained.
Embodiment 2
Without preservative face cleaning gel: unit: g
1) preservative face cleaning gel matrix (surfactant activity object total amount 15%) is free of: 93.8；
2) Glycolic acid 5, lactic acid 0.5；
3) xanthan gum 0.5；
4) sodium hydroxide 0.2；
Above-mentioned substance is uniformly mixed according to prescription quality at 50 DEG C.It then is 15000 mesh, pressure with filter screen
For 0.5MPa filtering, as gained.
Embodiment 3
Hand cleanser without preservative: unit: g
1) preservative hand cleanser matrix (surfactant activity object total amount 15%) is free of: 89；
2) sodium dihydrogen citrate 2, sodium lactate 3；
3) highland barley polysaccharide 1；
4) triethanolamine 5；
Above-mentioned substance is uniformly mixed according to prescription quality at 100 DEG C.It then is 800 mesh, pressure with filter screen
For 0.5MPa filtering, as gained.
Embodiment 4
Without preservative shaving liquid: unit: g
1) preservative shaving liquid matrix (surfactant activity object total amount 8%) is free of: 93.5；
2) Glycolic acid 2.5, sodium lactate 3；
3) xanthan gum 0.5；
4) sodium acetate 0.5；
Embodiment 5
Facial cleanser: unit: g is emulsified without preservative
1) without preservative emulsification facial cleanser matrix: 92；
2) lactobionic acid 3, gluconolactone 3；
3) polysaccharide 0.5；
4) sodium salicylate 2；
Above-mentioned substance is uniformly mixed according to prescription quality at 75 DEG C.It then is 500 mesh with filter screen, pressure is
Natural filtration, as gained.
Embodiment 6
Without preservative surfactant makeup remover: unit: g
1) without preservative emulsification facial cleanser matrix: 92；
2) linoleic acid 3, gluconolactone 3；
3) polysaccharide 0.5；
4) potassium hydroxide 2；
Above-mentioned substance is uniformly mixed according to prescription quality at 75 DEG C.It then is 500 mesh with filter screen, pressure is
Natural filtration, as gained.
Confirmatory experiment:
Test the experiment of 7-12 Microbial Challenge
Above-mentioned experiment is subjected to Microbial Challenge experiment, is selected respectively thin as provided by food of Zhejiang Province and drug inspection
Bacterium includes: Escherichia coli, staphylococcus aureus, hay bacillus, Bacillus megatherium, Pseudomonas aeruginosa.Mould includes: black song
Mould, aspergillus flavus, discoloration aspergillus, Penicillium citrinum, Paecilomyces varioti, cladosporium herbarum, Chaetomium globosum, Trichoderma viride.According to international CT FA
The Microbial Challenge testing standard that (international cosmetic, essence and detergent association) is recommended, result are from the 7th day, 14 days, 28
Its observation quantity is that the preservation challenge of the 0. visible facial cleanser using acidization preparation is successful.
Test the experiment of 13-18 foam height
High measure is carried out using matrix and prepared product of the foam height tester WH010XA-G type to experiment 1-6.As a result
As shown in the table
| Experiment 1 | Experiment 2 | Experiment 3 | Experiment 4 | Experiment 5 | Experiment 6 | |
| Matrix/mm | 132 | 107 | 112 | 50 | 48 | 38 |
| Prepared product/mm | 128 | 110 | 109 | 55 | 47 | 40 |
As can be seen from the above table, matrix and the foam height of primary standard substance do not change substantially.
Test 19-24 efficacy validation
18-60 years old super quick skin crowd, 60 people are selected, every 10 people is a group, uses experiment 1-6 in half side face at random
Product, it is control group that corresponding face, which is clear water, is used continuously 28 days.
The result shows that all human facial skins do not occur allergic phenomena.
Test 25-30 efficacy validation
The daylight crowd that do not tolerate for 18-60 years old, 60 people are selected, every 10 people is a group, uses experiment in half side face at random
1-6 product, corresponding face are control group for face cleaning product of releiving, and are used continuously 28 days.
Before this product, swim 2 hours in Sanya, Hainan seawater.
The result shows that all human facial skins daylight inflammatory phenomena do not occur using what experiment 1-6 was formulated per capita, and make
With clear water control group, all occurs the performance of daylight inflammation in various degree.
Test 31-36 efficacy validation
18-60 years old skin acne crowd, 60 people are selected, every 10 people is a group, uses experiment 1-6 in half side face at random
Product, corresponding face are acne clean skin product control group, are used continuously 3 days.
The result shows that being clearly better or curing occur in people of all human facial skins using experiment 1-6 formula, acne,
It is substantially better than control group.
Specific embodiments of the present invention are described above.It is to be appreciated that the invention is not limited to above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring substantive content of the invention.
Claims (10)
1. a kind of preparation method of acid effect clean skin product containing alkaline particle, it is characterised in that:
Its formula is as follows:
Without the non-soap based substrate of preservative skin-cleaning articles: 80-95 parts by weight；
Acidulant substance: 5-15 parts by weight；
Matrix stablizes conditioner: 0.001-5 parts by weight；
Alkaline particle: 0.01-14.999 parts by weight；
It is uniformly mixed and filters after being weighed according to the formula.
2. the preparation method of acid effect clean skin product containing alkaline particle as described in claim 1, it is characterised in that: described
The pH value of the 0.01-5% aqueous solution of acidulant substance is 1-4.
3. the preparation method of acid effect clean skin product containing alkaline particle as claimed in claim 2, it is characterised in that: described
Acidulant substance be citric acid and derivative, Glycolic acid and derivative, lactic acid and derivative, malic acid and derivative, acetic acid and
Derivative, lactobionic acid and derivative, gluconic acid and derivative, tartaric acid and health object, amino acid and derivative, salicylic acid and derivative
The group of one or more of object, oleic acid and derivative, linoleic acid and derivative, linolenic acid and derivative phosphoric acid and its derivative
It closes.
4. the preparation method of acid effect clean skin product containing alkaline particle as described in claim 1, it is characterised in that: described
Matrix stablizes the combination that conditioner is one or more of cellulose, starch, glue, carbohydrate, peptides, protein.
5. the preparation method of acid effect clean skin product containing alkaline particle as claimed in claim 4, it is characterised in that: described
Matrix stablizes the pH value of the aqueous solution of conditioner less than 8.
6. the preparation method of acid effect clean skin product containing alkaline particle as described in claim 1, it is characterised in that: described
Alkaline particle be sodium hydroxide, potassium hydroxide, calcium hydroxide, ammonium hydroxide, organic amine, alkaline potassium salt, alkaline sodium salt, alkaline ammonium
The combination of one or more of salt, alkaline organic ammonium salt.
7. the preparation method of acid effect clean skin product containing alkaline particle as described in claim 1, it is characterised in that: described
It is uniformly mixed to be carried out at 15-100 DEG C.
8. the preparation method of acid effect clean skin product containing alkaline particle as described in claim 1, it is characterised in that: described
It is filtered into the filter screen using -15000 mesh of 300 mesh, pressure is to carry out under normal pressure -1.0MPa.
9. a kind of acid effect clean skin product containing alkaline particle, it is characterised in that: using described in any one of claim 1-8
The preparation method of acid effect clean skin product containing alkaline particle is prepared.
10. acid effect clean skin product containing alkaline particle as claimed in claim 9, it is characterised in that: its pH value is less than 4.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910145846.7A CN109700673A (en) | 2019-02-27 | 2019-02-27 | A kind of acid effect clean skin product and preparation method thereof containing alkaline particle |
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| CN201910145846.7A CN109700673A (en) | 2019-02-27 | 2019-02-27 | A kind of acid effect clean skin product and preparation method thereof containing alkaline particle |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102429827A (en) * | 2011-11-30 | 2012-05-02 | 江南大学 | Preservative-free liquid detergents |
| CN108066194A (en) * | 2016-11-08 | 2018-05-25 | 宋丛恺 | A kind of shaving creme compositions |
-
2019
- 2019-02-27 CN CN201910145846.7A patent/CN109700673A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102429827A (en) * | 2011-11-30 | 2012-05-02 | 江南大学 | Preservative-free liquid detergents |
| CN108066194A (en) * | 2016-11-08 | 2018-05-25 | 宋丛恺 | A kind of shaving creme compositions |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB02 | Change of applicant information |
Address after: 518000, room five, floor 192, 501 Chongqing Road, Heping community, Fuyong street, Baoan District, Guangdong, Shenzhen Applicant after: Shenzhen Xiandi Cosmetics Co., Ltd Address before: 518000, room five, floor 192, 501 Chongqing Road, Heping community, Fuyong street, Baoan District, Guangdong, Shenzhen Applicant before: SHENZHEN SANDA COSMETICS Co.,Ltd. |
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190503 |
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| RJ01 | Rejection of invention patent application after publication |