CN109673752A - Regulating menstruation and assisting pregnancy red date-walnut drink and preparation method thereof - Google Patents
Regulating menstruation and assisting pregnancy red date-walnut drink and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C11/00—Milk substitutes, e.g. coffee whitener compositions
- A23C11/02—Milk substitutes, e.g. coffee whitener compositions containing at least one non-milk component as source of fats or proteins
- A23C11/10—Milk substitutes, e.g. coffee whitener compositions containing at least one non-milk component as source of fats or proteins containing or not lactose but no other milk components as source of fats, carbohydrates or proteins
- A23C11/103—Milk substitutes, e.g. coffee whitener compositions containing at least one non-milk component as source of fats or proteins containing or not lactose but no other milk components as source of fats, carbohydrates or proteins containing only proteins from pulses, oilseeds or nuts, e.g. nut milk
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
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- A23C2240/00—Use or particular additives or ingredients
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Abstract
The invention discloses regulating menstruation and assisting pregnancy red date-walnut drinks and preparation method thereof, the regulating menstruation and assisting pregnancy red date-walnut drink is raw material using motherwort, Radix Salviae Miltiorrhizae, China rose, walnut, jujube, Radix Angelicae Sinensis, radix rehmanniae preparata, semen sojae atricolor, safflower, brown sugar, honey etc., is prepared by infusion, sterilization.Regulating menstruation and assisting pregnancy red date-walnut drink of the present invention is prepared by irreplaceable secret prescription handed down in the family from generation to generation, belongs to nourishing conditioning product, has effects that following: 1. adjust endocrine disorder；2. adjust menstruation postponement, blood stasis, amount less, palace cold, color it is dark；3. adjusting dysmenorrhea, premenstrual swollen breasts, paramenia；4. palace, warm palace are supported in pregnancy difficulty, pregnant preceding menstruation regulating；5. activating microcirculation and removing stasis medicinal delays menopause；6. production and post-abortion miscellaneous disease and uterus maintenance.
Description
Technical field
The present invention relates to drink with function technical fields, more particularly to regulating menstruation and assisting pregnancy red date-walnut drink and preparation method thereof.
Background technique
By operating pressure, the various aspects such as big, environmental pollution, unbalanced nutrition are influenced modern female, the generation of endocrine system disease
Rate obviously increases, and common are: amenorrhoea, Stein-Leventhal syndrome, premature ovarian failure, hyperprolactinemia, ovulation failure etc..Inferior colliculus
Brain-pituitary and ovary s function is normally the foundation basis of ovulatory cycle, any one position occurs dysfunction and all may
Cause not ovulate, ovulatory dysfunction, causes amenorrhea, oligomenorrhea, function blood, infertile etc..Current clinic anovulatory is not
Pregnant disease patient mostly uses western medicine, but often less effective.Kidney deficiency fertility is the warm gasification function due to decline of kidney-YANG
Deficiency causes internal organs physiological function to inhibit, and in utero ecological environment is low and the pathological state of a kind of excess of yin due to yang insufficiency that reflects.
Walnut Milk be using walnut kernel as primary raw material, through mashing, filtering, homogeneous, sterilization, with etc. milkiness shape made of techniques
Protein beverage, rich in protein, vitamin and mineral great variety of goods, nutritive value is higher.Studies have shown that the Walnut Milk Central Asia is oily
It is acid, linolenic acid, phosphorus, magnesium, iron, sodium, iodine, manganese, glutamic acid, aspartic acid, alanine, serine, cystine, valine, different bright
The content of the nutriments such as propylhomoserin is close to or higher than that breast milk, especially ω -6 are fatty acid (linoleic acid) and ω -3 is fatty acid
(linolenic acid) content is close to nutritionist's recommended range.
Walnut Milk have preferable medical care effect, can prevent and treat hyperlipidemia, hypertension, hypoferric anemia, artery sclerosis,
The diseases such as diabetes；Drink Walnut Milk more, not only can be with brain tonic and intelligence development, face nursing and life prolonging, but also senile dementia can be prevented, prevented
Cancer anticancer.Walnut Milk is vegetable food and is rich in vegetable protein, a large number of studies show that, the people of diet mainly based on plant food
Healthier, the probability for obtaining chronic disease is lower.In addition, higher vegetable protein uptake rate, can reduce hip fracture generation
Probability.On the other hand, Walnut Milk is basic food, can mitigate the negative consequence of acid food；And some Asia human bodies
Interior not have lactase, whens dairy products such as milk drink, will appear allergic problem, but Walnut Milk does not have this problem, is conducive to human body and disappears
Change and absorbs.
Summary of the invention
The first technical problem to be solved by the present invention is to provide a kind of preparation method of regulating menstruation and assisting pregnancy red date-walnut drink, with
Jujube, walnut and draft Chinese medicinal plant are primary raw material, and the pure and fresh jujube juice of flavor and Walnut Milk full of nutrition are carried out
The complementation of flavor and nutrition, develop it is a kind of with excellent flavor, protein beverage full of nutrition, with regulating menstruation and assisting pregnancy function.
The present invention discloses a kind of preparation method of regulating menstruation and assisting pregnancy red date-walnut drink, comprising the following steps:
Step A: by 10~20g of motherwort, 1~3g of Radix Salviae Miltiorrhizae, 5~20g of China rose, 60~200g of walnut, jujube 30~
70g, 3~10g of Radix Angelicae Sinensis, 5~10g of radix rehmanniae preparata, 10~40g of semen sojae atricolor, 2~10g of safflower are mixed well, and obtain mixture；By mixture
With mass ratio 1:(10~50) it impregnates 2~3 hours into the water, it squeezes the juice, filtrate A and filter residue A is collected in filtering respectively；By filtrate A
12~24 hours are placed at room temperature for, is filtered again, collects liquor B and filter residue B respectively；Liquor B is spare as medical fluid, filter residue A and filter
Slag B mixing is spare as the dregs of a decoction；
Step B: by the dregs of a decoction and medical fluid with mass ratio 1:(30~80) it mixes well, in 50~80 DEG C 30~60 points of infusion
Clock, filtering collect liquor C as stoste；
Step C: brown sugar and honey are added into stoste, wherein brown sugar accounts for the 1~2% of stock solution quality, and honey accounts for stoste matter
The 0.5~2% of amount after infusion 60~300 minutes, is placed at room temperature for 12~24 hours in 60~90 DEG C；
Step D: then it is canned, it is sterilized 10~20 minutes in 80~90 DEG C, obtains the regulating menstruation and assisting pregnancy red date-walnut drink.
Further, the present invention discloses a kind of preparation method of regulating menstruation and assisting pregnancy red date-walnut drink, comprising the following steps:
Step A: by 10~20g of motherwort, 1~3g of Radix Salviae Miltiorrhizae, 5~20g of China rose, 60~200g of walnut, jujube 30~
70g, 3~10g of Radix Angelicae Sinensis, 5~10g of radix rehmanniae preparata, 10~40g of semen sojae atricolor, 2~10g of safflower are mixed well, and obtain mixture；By mixture
With mass ratio 1:(10~50) it impregnates 2~3 hours into the water, it squeezes the juice, filtrate A and filter residue A is collected in filtering respectively；By filtrate A
12~24 hours are placed at room temperature for, is filtered again, collects liquor B and filter residue B respectively；Liquor B is spare as medical fluid, filter residue A and filter
Slag B mixing is spare as the dregs of a decoction；
Step B: by the dregs of a decoction and medical fluid with mass ratio 1:(30~80) it mixes well, in 50~80 DEG C 30~60 points of infusion
Liquor C is collected in clock, filtering；
Step C: vulcanized ester is inoculated in fluid nutrient medium with volume ratio 5~10%, is fermented 5~7 days in 24~30 DEG C,
Obtain fermentation liquid；The wherein fluid nutrient medium composition are as follows: 50~100g/L of potato, 10~20g/L of glucose, biphosphate
0.3~1g/L of potassium, 0.2~0.5g/L of magnesium sulfate, surplus are water；By fermentation liquid in 50~70 DEG C ultrasonic extraction 30~40 minutes,
Filtering, obtains sulphur bacterium solution；By liquor C and sulphur bacterium solution with volume ratio (8~20): 1 mixing obtains mixed liquor；To mixed liquor
The middle sucrose that mixed liquor quality 2~4% is added, mixes well as stoste；
Step D: brown sugar and honey are added into stoste, wherein brown sugar accounts for the 1~2% of stock solution quality, and honey accounts for stoste matter
The 0.5~2% of amount after infusion 60~300 minutes, is placed at room temperature for 12~24 hours in 60~90 DEG C；
Step E: then it is canned, it is sterilized 10~20 minutes in 80~90 DEG C, obtains the regulating menstruation and assisting pregnancy red date-walnut drink.
Further, the present invention discloses a kind of preparation method of regulating menstruation and assisting pregnancy red date-walnut drink, comprising the following steps:
Step A: by 10~20g of motherwort, 1~3g of Radix Salviae Miltiorrhizae, 5~20g of China rose, 60~200g of walnut, jujube 30~
70g, 3~10g of Radix Angelicae Sinensis, 5~10g of radix rehmanniae preparata, 10~40g of semen sojae atricolor, 2~10g of safflower are mixed well, and obtain mixture；By mixture
With mass ratio 1:(10~50) it impregnates 2~3 hours into the water, it squeezes the juice, filtrate A and filter residue A is collected in filtering respectively；By filtrate A
12~24 hours are placed at room temperature for, is filtered again, collects liquor B and filter residue B respectively；Liquor B is spare as medical fluid, filter residue A and filter
Slag B mixing is spare as the dregs of a decoction；
Step B: by the dregs of a decoction and medical fluid with mass ratio 1:(30~80) it mixes well, in 50~80 DEG C 30~60 points of infusion
Liquor C is collected in clock, filtering；
Step C: vulcanized ester is inoculated in fluid nutrient medium with volume ratio 5~10%, is fermented 5~7 days in 24~30 DEG C,
Obtain fermentation liquid；The wherein fluid nutrient medium composition are as follows: 50~100g/L of potato, 10~20g/L of glucose, biphosphate
0.3~1g/L of potassium, 0.2~0.5g/L of magnesium sulfate, surplus are water；By fermentation liquid in 50~70 DEG C ultrasonic extraction 30~40 minutes,
Filtering, obtains sulphur bacterium solution；By liquor C and sulphur bacterium solution with volume ratio (8~20): 1 mixing obtains mixed liquor；To mixed liquor
The middle sucrose that mixed liquor quality 2~4% is added, mixes well as stoste；
Step D: brown sugar and honey are added into stoste, wherein brown sugar accounts for the 1~2% of stock solution quality, and honey accounts for stoste matter
Amount 0.5~2%, in 60~90 DEG C infusion 60~300 minutes；Continue that protein particle and stabilizer, stabilizer are added thereto
Account for the 0.3~0.5% of stock solution quality, protein particle account for 40~50 DEG C of 1~3%, the Yu Wendu of stock solution quality, homogenization pressure 20~
40MPa homogeneous 10~after twenty minutes, it is placed at room temperature for 12~24 hours；
Step E: then it is canned, it is sterilized 10~20 minutes in 80~90 DEG C, obtains the regulating menstruation and assisting pregnancy red date-walnut drink.
In some technical solutions of the invention, the protein particle is soybean protein particle, is prepared using following procedure
Obtain: soybean protein isolate be dispersed in water to the dispersion liquid that mass fraction 10~20% is prepared, using mass fraction 1~
5% salt acid for adjusting pH is placed in agitating and heating 20~60 minutes in 85~95 DEG C of water-bath, then takes out certainly to 3.0~7.0
It is so cooled to room temperature, obtains soybean protein particle dispersion liquid；By soybean protein particle dispersion liquid homogeneous 10~20 minutes, homogeneous temperature
50~70 DEG C of degree, then 30~60MPa of homogenization pressure is spray-dried, and obtains protein particle.
The soybean protein isolate can both be obtained by commercially available method, can also be obtained by homemade method, example
Such as: defatted soybean meal being smashed it through into 40~60 meshes, obtains defatted soybean meal powder；By defatted soybean meal powder with
Mass volume ratio 1:(10~30) (g/mL) mix with water, using the sodium hydrate aqueous solution of 1~5mol/L adjust pH to 8.0~
9.0, it is centrifugated after being stirred at room temperature 2~3 hours, takes supernatant；By supernatant with the salt acid for adjusting pH of 1~5mol/L to 4.0
It is centrifugated again after~4.5, takes precipitating；To precipitate with mass ratio 1:(10~30) it is multiple soluble in water using 1~5mol/L's
Sodium hydrate aqueous solution adjusts pH to 7.0~8.0, is placed in deionized water after dialysing 24~48 hours and is freeze-dried, and obtains big
Beans protein isolate.
In some technical solutions of the invention, the protein particle is compound protein particle, is prepared using following methods
Obtain: by soybean protein isolate and albumen with mass ratio (1~2): (1~2) is uniformly mixed, and is dispersed in water and is prepared
The dispersion liquid of soybean protein isolate and albumen total mass fraction 10~20% is adjusted using the hydrochloric acid of mass fraction 1~5%
PH to 3.0~7.0 is placed in agitating and heating 20~60 minutes in 85~95 DEG C of water-bath, then takes out cooled to room temperature,
Obtain compound protein particle dispersion liquid；By compound protein particle dispersion liquid homogeneous 10~20 minutes, 50~70 DEG C of homogenizing temperature,
Matter 30~60MPa of pressure, is then spray-dried, and obtains protein particle.
Further, the sucrose is substituted using sugar alcohol, and the sugar alcohol is xylitol, D-sorbite, maltitol, red moss
One of sugar alcohol.
Further, the sugar alcohol is maltitol.
Further, the stabilizer be sodium carboxymethylcellulose, it is carboxymethyl curdlan gum, corn fiber gum, water-soluble big
One of beans polysaccharide, esterification soybean polyoses or a variety of mixtures.Preferably, the stabilizer is corn fiber gum and esterification
The mixture that soybean polyoses are formed with mass ratio 1:1.
Commercially available soluble soybean polysaccharide had both can be used in soluble soybean polysaccharide, can also be with referenced patent application number
201310011231.8 embodiment one be prepared.
Further, the esterification soybean polyoses are prepared using following methods: soluble soybean polysaccharide is dissolved in
Water prepares the soluble soybean polysaccharide solution of mass fraction 10~20%, is heated to 40~60 DEG C, uses mass fraction 1~5%
Sodium hydrate aqueous solution adjust pH to 8.0~9.0；In 40~60 DEG C of addition octenyl succinic acid anhydrides, and it is stirred to react 30~
50 minutes, the mass ratio of octenyl succinic acid anhydride and soluble soybean polysaccharide was 1:(5~10), pass through addition matter in reaction process
The sodium hydrate aqueous solution for measuring score 1~5% maintains pH 8.0~9.0；After reaction, using mass fraction 1~5%
To 4.0~5.0, dialysis is freeze-dried salt acid for adjusting pH after 24~48 hours, obtains esterification soybean polyoses.
The second technical problem to be solved by the present invention is to provide a kind of regulating menstruation and assisting pregnancy red date-walnut drink, and use is any of the above-described
The preparation method of regulating menstruation and assisting pregnancy red date-walnut drink described in is process.
Regulating menstruation and assisting pregnancy red date-walnut drink of the present invention is prepared by irreplaceable secret prescription handed down in the family from generation to generation, belongs to nourishing conditioning
Product have effects that following: 1. adjust endocrine disorder；2. adjust menstruation postponement, blood stasis, amount less, palace cold, color it is dark；3. adjusting dysmenorrhea, warp
Fore udder distending pain, paramenia；4. palace, warm palace are supported in pregnancy difficulty, pregnant preceding menstruation regulating；5. activating microcirculation and removing stasis medicinal delays menopause；6. production
It is conserved with post-abortion miscellaneous disease and uterus.
Specific embodiment
Raw material is described below in embodiment:
Motherwort, source area Anhui, the auspicious bright hall medicine company of producer's Bozhou City sell Co., Ltd.
Radix Salviae Miltiorrhizae, source area Shaanxi, producer's Bozhou City Liu Xiang medicine company sell Co., Ltd.
China rose, kind are Chinese rose, place of production Shandong.
Walnut, kind Shanxi dragon No. 1, place of production Shanxi.
Jujube, kind Xinzheng jujube, place of production Henan.
Radix Angelicae Sinensis, source area Gansu, Bozhou City An Qiao pharmaceutcal corporation, Ltd, producer.
Radix rehmanniae preparata, source area Henan, producer's Bozhou City morning hydrargyrum oxydatum crudum industry sell Co., Ltd.
Semen sojae atricolor, source area Anhui, Anhui Hui Cui ecological agriculture development Co., Ltd, producer.
Safflower, source area Xinjiang, the poly- spring hall Chinese medicine of producer's Bozhou City sell Co., Ltd.
Brown sugar, Shijiazhuang City Zhong Xing sugar industry Co., Ltd, producer.
Honey, the honey of various flowers that specifically used producer Sheng Beite bee product Co., Ltd provides, source area Jiangsu.
Vulcanized ester, the medicinal material business department, family of producer Dali ganoderma lucidum, source area Yunnan.
Sucrose, producer Langfang Kang Puhui tie up Science and Technology Ltd., food-grade.
Corn fiber gum, with reference to " extraction, property and its application of corn fiber gum " (grain and feed industries, Li Ping,
2014No.11) in the method for 1.1CFG.1 be prepared.
Soybean protein isolate, food-grade, Henan Kai Ji trade Co., Ltd, producer.
Albumen, Shanghai Nai Jin Industrial Co., Ltd., producer, food-grade, brand HH.
Maltitol, No. CAS: 585-88-6, food-grade.
D-sorbite, No. CAS: 50-70-4, food-grade.
Xylitol, No. CAS: 87-99-0, food-grade.
Antierythrite, No. CAS: 149-32-6, food-grade.
The embodiment one of soluble soybean polysaccharide, referenced patent application number 201310011231.8 is prepared.
Octenyl succinic acid anhydride, No. CAS: 26680-54-6.
In the case where the present invention does not illustrate, speed of agitator is 100 revs/min.
In the case where the present invention does not illustrate, the actual conditions of freeze-drying are as follows: -80 DEG C of pre-freezing temperature, pre-freeze
Time 2 h, -60 DEG C of cryogenic temperature, cooling time 24 hours, absolute pressure 100Pa.
Embodiment 1
The preparation method of regulating menstruation and assisting pregnancy red date-walnut drink, comprising the following steps:
Step A: by motherwort 10g, Radix Salviae Miltiorrhizae 2g, China rose 10g, walnut 180g, jujube 60g, Radix Angelicae Sinensis 5g, radix rehmanniae preparata 5g, black
Beans 20g, safflower 4g are mixed well, and obtain mixture；Mixture is impregnated 2 hours into the water with mass ratio 1:30, with 2300
Rev/min juicing 2 minutes, using 200 mesh nylon cloths filter, respectively collect filtrate A and filter residue A；It is small that filtrate A is placed at room temperature for 12
When, the filtering of 200 mesh nylon cloths is reused, collects liquor B and filter residue B respectively；Liquor B is spare as medical fluid, filter residue A and filter residue
B mixing is spare as the dregs of a decoction；
Step B: the dregs of a decoction and medical fluid are mixed well with mass ratio 1:40, in 80 DEG C infusion 30 minutes, use 200 mesh nylon
Cloth filtering collects liquor C as stoste；
Step C: brown sugar and honey are added into stoste, wherein brown sugar accounts for the 2% of stock solution quality, and honey accounts for stock solution quality
0.5%, after infusion 300 minutes, 12 hours are placed at room temperature in 60 DEG C；
Step D: then it is canned, it is sterilized 15 minutes in 85 DEG C, obtains the regulating menstruation and assisting pregnancy red date-walnut drink.
Embodiment 2
The preparation method of regulating menstruation and assisting pregnancy red date-walnut drink, comprising the following steps:
Step A: by motherwort 10g, Radix Salviae Miltiorrhizae 2g, China rose 10g, walnut 180g, jujube 60g, Radix Angelicae Sinensis 5g, radix rehmanniae preparata 5g, black
Beans 20g, safflower 4g are mixed well, and obtain mixture；Mixture is impregnated 2 hours into the water with mass ratio 1:30, with 2300
Rev/min juicing 2 minutes, using 200 mesh nylon cloths filter, respectively collect filtrate A and filter residue A；It is small that filtrate A is placed at room temperature for 12
When, the filtering of 200 mesh nylon cloths is reused, collects liquor B and filter residue B respectively；Liquor B is spare as medical fluid, filter residue A and filter residue
B mixing is spare as the dregs of a decoction；
Step B: the dregs of a decoction and medical fluid are mixed well with mass ratio 1:40, in 80 DEG C infusion 30 minutes, use 200 mesh nylon
Cloth filtering, collects liquor C；
Step C: vulcanized ester is inoculated in fluid nutrient medium with volume ratio 7.5%, is fermented 7 days, is fermented in 24 DEG C
Liquid；The wherein fluid nutrient medium composition are as follows: potato 100g/L, glucose 20g/L, potassium dihydrogen phosphate 1g/L, magnesium sulfate
0.5g/L, surplus are water；Fermentation liquid is extracted 30 minutes under conditions of 60 DEG C, ultrasonic power 300W, is allowed in vulcanized ester mycelia
Nutriment release, then filtered with the nylon cloths of 200 mesh, obtain sulphur bacterium solution；By liquor C and sulphur bacterium solution with body
Product is mixed than 10:1, obtains mixed liquor；The sucrose of mixed liquor quality 4% is added into mixed liquor, mixes well as stoste；
Step D: brown sugar and honey are added into stoste, wherein brown sugar accounts for the 2% of stock solution quality, and honey accounts for stock solution quality
0.5%, after infusion 300 minutes, 12 hours are placed at room temperature in 60 DEG C；
Step E: then it is canned, it is sterilized 15 minutes in 85 DEG C, obtains the regulating menstruation and assisting pregnancy red date-walnut drink.
Embodiment 3
The preparation method of regulating menstruation and assisting pregnancy red date-walnut drink, comprising the following steps:
Step A: by motherwort 10g, Radix Salviae Miltiorrhizae 2g, China rose 10g, walnut 180g, jujube 60g, Radix Angelicae Sinensis 5g, radix rehmanniae preparata 5g, black
Beans 20g, safflower 4g are mixed well, and obtain mixture；Mixture is impregnated 2 hours into the water with mass ratio 1:30, with 2300
Rev/min juicing 2 minutes, using 200 mesh nylon cloths filter, respectively collect filtrate A and filter residue A；It is small that filtrate A is placed at room temperature for 12
When, the filtering of 200 mesh nylon cloths is reused, collects liquor B and filter residue B respectively；Liquor B is spare as medical fluid, filter residue A and filter residue
B mixing is spare as the dregs of a decoction；
Step B: the dregs of a decoction and medical fluid are mixed well with mass ratio 1:40, in 80 DEG C infusion 30 minutes, use 200 mesh nylon
Cloth filtering collects liquor C as stoste；
Step C: vulcanized ester is inoculated in fluid nutrient medium with volume ratio 7.5%, is fermented 7 days, is fermented in 24 DEG C
Liquid；The wherein fluid nutrient medium composition are as follows: potato 100g/L, glucose 20g/L, potassium dihydrogen phosphate 1g/L, magnesium sulfate
0.5g/L, surplus are water；Fermentation liquid is extracted 30 minutes under conditions of 60 DEG C, ultrasonic power 300W, is allowed in vulcanized ester mycelia
Nutriment release, then filtered with the nylon cloths of 200 mesh, obtain sulphur bacterium solution；By liquor C and sulphur bacterium solution with body
Product is mixed than 10:1, obtains mixed liquor；The sucrose of mixed liquor quality 4% is added into mixed liquor, mixes well as stoste；
Step D: brown sugar and honey are added into stoste, wherein brown sugar accounts for the 2% of stock solution quality, and honey accounts for stock solution quality
0.5%, in 60 DEG C infusion 300 minutes；Continue that protein particle is added thereto and corn fiber gum, corn fiber gum account for stoste matter
The 0.3% of amount, protein particle accounts for the 2% of stock solution quality, and after ten minutes in temperature 50 C, homogenization pressure 30MPa homogeneous, room temperature is put
It sets 12 hours；
Step E: then it is canned, it is sterilized 15 minutes in 85 DEG C, obtains the regulating menstruation and assisting pregnancy red date-walnut drink.
The protein particle is soybean protein particle, is prepared using following procedure: dispersing soybean protein isolate in
The dispersion liquid of mass fraction 15% is prepared in deionized water, using the salt acid for adjusting pH of mass fraction 1% to 4.5, is placed in
Agitating and heating 60 minutes, then take out cooled to room temperature in 95 DEG C of water-bath, obtain soybean protein particle dispersion liquid；It will
Soybean protein particle dispersion liquid homogeneous 20 minutes, 50 DEG C of homogenizing temperature, then homogenization pressure 50MPa is spray-dried, and obtains soybean
Protein particle, wherein the process conditions being spray-dried: 180 DEG C of inlet temperature, 110 DEG C of outlet temperature, sample introduction flow 3mL/min,
Air velocity 600L/h.
Embodiment 4
The preparation method of regulating menstruation and assisting pregnancy red date-walnut drink, comprising the following steps:
Step A: by motherwort 10g, Radix Salviae Miltiorrhizae 2g, China rose 10g, walnut 180g, jujube 60g, Radix Angelicae Sinensis 5g, radix rehmanniae preparata 5g, black
Beans 20g, safflower 4g are mixed well, and obtain mixture；Mixture is impregnated 2 hours into the water with mass ratio 1:30, with 2300
Rev/min juicing 2 minutes, using 200 mesh nylon cloths filter, respectively collect filtrate A and filter residue A；It is small that filtrate A is placed at room temperature for 12
When, the filtering of 200 mesh nylon cloths is reused, collects liquor B and filter residue B respectively；Liquor B is spare as medical fluid, filter residue A and filter residue
B mixing is spare as the dregs of a decoction；
Step B: the dregs of a decoction and medical fluid are mixed well with mass ratio 1:40, in 80 DEG C infusion 30 minutes, use 200 mesh nylon
Cloth filtering collects liquor C as stoste；
Step C: vulcanized ester is inoculated in fluid nutrient medium with volume ratio 7.5%, is fermented 7 days, is fermented in 24 DEG C
Liquid；The wherein fluid nutrient medium composition are as follows: potato 100g/L, glucose 20g/L, potassium dihydrogen phosphate 1g/L, magnesium sulfate
0.5g/L, surplus are water；Fermentation liquid is extracted 30 minutes under conditions of 60 DEG C, ultrasonic power 300W, is allowed in vulcanized ester mycelia
Nutriment release, then filtered with the nylon cloths of 200 mesh, obtain sulphur bacterium solution；By liquor C and sulphur bacterium solution with body
Product is mixed than 10:1, obtains mixed liquor；The sucrose of mixed liquor quality 4% is added into mixed liquor, mixes well as stoste；
Step D: brown sugar and honey are added into stoste, wherein brown sugar accounts for the 2% of stock solution quality, and honey accounts for stock solution quality
0.5%, in 60 DEG C infusion 300 minutes；Continue that protein particle is added thereto and corn fiber gum, corn fiber gum account for stoste matter
The 0.3% of amount, protein particle accounts for the 2% of stock solution quality, and after ten minutes in temperature 50 C, homogenization pressure 30MPa homogeneous, room temperature is put
It sets 12 hours；
Step E: then it is canned, it is sterilized 15 minutes in 85 DEG C, obtains the regulating menstruation and assisting pregnancy red date-walnut drink.
The protein particle is compound protein particle, is prepared using following methods: by soybean protein isolate and egg white
Albumen is uniformly mixed with mass ratio 2:1, is scattered in deionized water and soybean protein isolate and albumen gross mass is prepared
The dispersion liquid of score 15% is placed in agitating and heating in 95 DEG C of water-bath using the salt acid for adjusting pH of mass fraction 1% to 4.5
60 minutes, cooled to room temperature is then taken out, obtains compound protein particle dispersion liquid；By compound protein particle dispersion liquid homogeneous
20 minutes, 50 DEG C of homogenizing temperature, then homogenization pressure 50MPa was spray-dried, and compound protein particle was obtained, wherein being spray-dried
Process conditions: 180 DEG C of inlet temperature, 110 DEG C of outlet temperature, sample introduction flow 3mL/min, air velocity 600L/h.
Embodiment 5~8
The preparation method of regulating menstruation and assisting pregnancy red date-walnut drink, comprising the following steps:
Step A: by motherwort 10g, Radix Salviae Miltiorrhizae 2g, China rose 10g, walnut 180g, jujube 60g, Radix Angelicae Sinensis 5g, radix rehmanniae preparata 5g, black
Beans 20g, safflower 4g are mixed well, and obtain mixture；Mixture is impregnated 2 hours into the water with mass ratio 1:30, with 2300
Rev/min juicing 2 minutes, using 200 mesh nylon cloths filter, respectively collect filtrate A and filter residue A；It is small that filtrate A is placed at room temperature for 12
When, the filtering of 200 mesh nylon cloths is reused, collects liquor B and filter residue B respectively；Liquor B is spare as medical fluid, filter residue A and filter residue
B mixing is spare as the dregs of a decoction；
Step B: the dregs of a decoction and medical fluid are mixed well with mass ratio 1:40, in 80 DEG C infusion 30 minutes, use 200 mesh nylon
Cloth filtering collects liquor C as stoste；
Step C: vulcanized ester is inoculated in fluid nutrient medium with volume ratio 7.5%, is fermented 7 days, is fermented in 24 DEG C
Liquid；The wherein fluid nutrient medium composition are as follows: potato 100g/L, glucose 20g/L, potassium dihydrogen phosphate 1g/L, magnesium sulfate
0.5g/L, surplus are water；Fermentation liquid is extracted 30 minutes under conditions of 60 DEG C, ultrasonic power 300W, is allowed in vulcanized ester mycelia
Nutriment release, then filtered with the nylon cloths of 200 mesh, obtain sulphur bacterium solution；By liquor C and sulphur bacterium solution with body
Product is mixed than 10:1, obtains mixed liquor；The sugar alcohol of mixed liquor quality 4% is added into mixed liquor, mixes well as stoste；
Step D: brown sugar and honey are added into stoste, wherein brown sugar accounts for the 2% of stock solution quality, and honey accounts for stock solution quality
0.5%, in 60 DEG C infusion 300 minutes；Continue that protein particle is added thereto and corn fiber gum, corn fiber gum account for stoste matter
The 0.3% of amount, protein particle accounts for the 2% of stock solution quality, and after ten minutes in temperature 50 C, homogenization pressure 30MPa homogeneous, room temperature is put
It sets 12 hours；
Step E: then it is canned, it is sterilized 15 minutes in 85 DEG C, obtains the regulating menstruation and assisting pregnancy red date-walnut drink.
The protein particle is compound protein particle, is prepared using following methods: by soybean protein isolate and egg white
Albumen is uniformly mixed with mass ratio 2:1, is scattered in deionized water and soybean protein isolate and albumen gross mass is prepared
The dispersion liquid of score 15% is placed in agitating and heating in 95 DEG C of water-bath using the salt acid for adjusting pH of mass fraction 1% to 4.5
60 minutes, cooled to room temperature is then taken out, obtains compound protein particle dispersion liquid；By compound protein particle dispersion liquid homogeneous
20 minutes, 50 DEG C of homogenizing temperature, then homogenization pressure 50MPa was spray-dried, and compound protein particle was obtained, wherein being spray-dried
Process conditions: 180 DEG C of inlet temperature, 110 DEG C of outlet temperature, sample introduction flow 3mL/min, air velocity 600L/h.
The difference of embodiment 5~8 is: the sugar alcohol type that embodiment 5~8 uses is different, and embodiment 5 uses maltose
Alcohol, embodiment 6 use D-sorbite, and embodiment 7 uses xylitol, and embodiment 8 uses antierythrite.
As it can be seen from table 1 compared with embodiment 4 uses sucrose, menstruation regulating that embodiment 5~8 is obtained using four kinds of sugar alcohols
It helps pregnant red date-walnut drink centrifugation rate smaller, shows the high stability for the regulating menstruation and assisting pregnancy red date-walnut drink that sugar alcohol obtains,
This may be because protein denaturation and thickener hydrolysis degree are serious in 4 sterilization process of embodiment, and Zeta potential and viscosity become
Change larger.And regulating menstruation and assisting pregnancy red date-walnut drink steadiness is 5 maltitols of embodiment > embodiment, 6 mountain in embodiment 5~8
Pears sugar alcohol > 7 xylitols of embodiment > embodiment, 8 antierythrite, it may be possible to which, because maltitol molecular weight is larger, viscosity is maximum, egg
White matter decline and fat floating rate are slower, and hydroxy number is relatively fewer, and shielding action is weaker, Zeta potential absolute value compared with
Greatly.
Embodiment 9
The preparation method of regulating menstruation and assisting pregnancy red date-walnut drink, comprising the following steps:
Step A: by motherwort 10g, Radix Salviae Miltiorrhizae 2g, China rose 10g, walnut 180g, jujube 60g, Radix Angelicae Sinensis 5g, radix rehmanniae preparata 5g, black
Beans 20g, safflower 4g are mixed well, and obtain mixture；Mixture is impregnated 2 hours into the water with mass ratio 1:30, with 2300
Rev/min juicing 2 minutes, using 200 mesh nylon cloths filter, respectively collect filtrate A and filter residue A；It is small that filtrate A is placed at room temperature for 12
When, the filtering of 200 mesh nylon cloths is reused, collects liquor B and filter residue B respectively；Liquor B is spare as medical fluid, filter residue A and filter residue
B mixing is spare as the dregs of a decoction；
Step B: the dregs of a decoction and medical fluid are mixed well with mass ratio 1:40, in 80 DEG C infusion 30 minutes, use 200 mesh nylon
Cloth filtering collects liquor C as stoste；
Step C: vulcanized ester is inoculated in fluid nutrient medium with volume ratio 7.5%, is fermented 7 days, is fermented in 24 DEG C
Liquid；The wherein fluid nutrient medium composition are as follows: potato 100g/L, glucose 20g/L, potassium dihydrogen phosphate 1g/L, magnesium sulfate
0.5g/L, surplus are water；Fermentation liquid is extracted 30 minutes under conditions of 60 DEG C, ultrasonic power 300W, is allowed in vulcanized ester mycelia
Nutriment release, then filtered with the nylon cloths of 200 mesh, obtain sulphur bacterium solution；By liquor C and sulphur bacterium solution with body
Product is mixed than 10:1, obtains mixed liquor；The maltitol of mixed liquor quality 4% is added into mixed liquor, mixes well as original
Liquid；
Step D: brown sugar and honey are added into stoste, wherein brown sugar accounts for the 2% of stock solution quality, and honey accounts for stock solution quality
0.5%, in 60 DEG C infusion 300 minutes；Continue that protein particle and soluble soybean polysaccharide, soluble soybean polysaccharide are added thereto
The 0.3% of stock solution quality is accounted for, protein particle accounted for the 2% of stock solution quality, in temperature 50 C, homogenization pressure 30MPa homogeneous 10 minutes
Afterwards, 12 hours are placed at room temperature for；
Step E: then it is canned, it is sterilized 15 minutes in 85 DEG C, obtains the regulating menstruation and assisting pregnancy red date-walnut drink.
The protein particle is compound protein particle, is prepared using following methods: by soybean protein isolate and egg white
Albumen is uniformly mixed with mass ratio 2:1, is scattered in deionized water and soybean protein isolate and albumen gross mass is prepared
The dispersion liquid of score 15% is placed in agitating and heating in 95 DEG C of water-bath using the salt acid for adjusting pH of mass fraction 1% to 4.5
60 minutes, cooled to room temperature is then taken out, obtains compound protein particle dispersion liquid；By compound protein particle dispersion liquid homogeneous
20 minutes, 50 DEG C of homogenizing temperature, then homogenization pressure 50MPa was spray-dried, and compound protein particle was obtained, wherein being spray-dried
Process conditions: 180 DEG C of inlet temperature, 110 DEG C of outlet temperature, sample introduction flow 3mL/min, air velocity 600L/h.
Embodiment 10
The preparation method of regulating menstruation and assisting pregnancy red date-walnut drink, comprising the following steps:
Step A: by motherwort 10g, Radix Salviae Miltiorrhizae 2g, China rose 10g, walnut 180g, jujube 60g, Radix Angelicae Sinensis 5g, radix rehmanniae preparata 5g, black
Beans 20g, safflower 4g are mixed well, and obtain mixture；Mixture is impregnated 2 hours into the water with mass ratio 1:30, with 2300
Rev/min juicing 2 minutes, using 200 mesh nylon cloths filter, respectively collect filtrate A and filter residue A；It is small that filtrate A is placed at room temperature for 12
When, the filtering of 200 mesh nylon cloths is reused, collects liquor B and filter residue B respectively；Liquor B is spare as medical fluid, filter residue A and filter residue
B mixing is spare as the dregs of a decoction；
Step B: the dregs of a decoction and medical fluid are mixed well with mass ratio 1:40, in 80 DEG C infusion 30 minutes, use 200 mesh nylon
Cloth filtering collects liquor C as stoste；
Step C: vulcanized ester is inoculated in fluid nutrient medium with volume ratio 7.5%, is fermented 7 days, is fermented in 24 DEG C
Liquid；The wherein fluid nutrient medium composition are as follows: potato 100g/L, glucose 20g/L, potassium dihydrogen phosphate 1g/L, magnesium sulfate
0.5g/L, surplus are water；Fermentation liquid is extracted 30 minutes under conditions of 60 DEG C, ultrasonic power 300W, is allowed in vulcanized ester mycelia
Nutriment release, then filtered with the nylon cloths of 200 mesh, obtain sulphur bacterium solution；By liquor C and sulphur bacterium solution with body
Product is mixed than 10:1, obtains mixed liquor；The maltitol of mixed liquor quality 4% is added into mixed liquor, mixes well as original
Liquid；
Step D: brown sugar and honey are added into stoste, wherein brown sugar accounts for the 2% of stock solution quality, and honey accounts for stock solution quality
0.5%, in 60 DEG C infusion 300 minutes；Continue that protein particle and esterification soybean polyoses are added thereto, esterification soybean polyoses account for original
The 0.3% of liquid quality, protein particle account for the 2% of stock solution quality, after ten minutes in temperature 50 C, homogenization pressure 30MPa homogeneous, room
Temperature is placed 12 hours；
Step E: then it is canned, it is sterilized 15 minutes in 85 DEG C, obtains the regulating menstruation and assisting pregnancy red date-walnut drink.
The protein particle is compound protein particle, is prepared using following methods: by soybean protein isolate and egg white
Albumen is uniformly mixed with mass ratio 2:1, is scattered in deionized water and soybean protein isolate and albumen gross mass is prepared
The dispersion liquid of score 15% is placed in agitating and heating in 95 DEG C of water-bath using the salt acid for adjusting pH of mass fraction 1% to 4.5
60 minutes, cooled to room temperature is then taken out, obtains compound protein particle dispersion liquid；By compound protein particle dispersion liquid homogeneous
20 minutes, 50 DEG C of homogenizing temperature, then homogenization pressure 50MPa was spray-dried, and compound protein particle was obtained, wherein being spray-dried
Process conditions: 180 DEG C of inlet temperature, 110 DEG C of outlet temperature, sample introduction flow 3mL/min, air velocity 600L/h.
The esterification soybean polyoses are prepared using following methods: soluble soybean polysaccharide is dissolved in deionized water system
The soluble soybean polysaccharide solution of standby mass fraction 10%, is heated to 40 DEG C with 2 DEG C/min, uses the hydrogen-oxygen of mass fraction 1%
Change sodium water solution and adjusts pH to 8.5；In 40 DEG C of addition octenyl succinic acid anhydrides, and 35 minutes are stirred to react, ocentyl succinic
The mass ratio of acid anhydride and soluble soybean polysaccharide is 1:7, passes through the sodium hydrate aqueous solution of addition mass fraction 1% in reaction process
Maintain pH 8.5；After reaction, using the salt acid for adjusting pH of mass fraction 1% to 5.0, using shutting off molecular weight 500KD's
Bag filter is freeze-dried after dialysing 48 hours, obtains esterification soybean polyoses.
Embodiment 11
The preparation method of regulating menstruation and assisting pregnancy red date-walnut drink, comprising the following steps:
Step A: by motherwort 10g, Radix Salviae Miltiorrhizae 2g, China rose 10g, walnut 180g, jujube 60g, Radix Angelicae Sinensis 5g, radix rehmanniae preparata 5g, black
Beans 20g, safflower 4g are mixed well, and obtain mixture；Mixture is impregnated 2 hours into the water with mass ratio 1:30, with 2300
Rev/min juicing 2 minutes, using 200 mesh nylon cloths filter, respectively collect filtrate A and filter residue A；It is small that filtrate A is placed at room temperature for 12
When, the filtering of 200 mesh nylon cloths is reused, collects liquor B and filter residue B respectively；Liquor B is spare as medical fluid, filter residue A and filter residue
B mixing is spare as the dregs of a decoction；
Step B: the dregs of a decoction and medical fluid are mixed well with mass ratio 1:40, in 80 DEG C infusion 30 minutes, use 200 mesh nylon
Cloth filtering collects liquor C as stoste；
Step C: vulcanized ester is inoculated in fluid nutrient medium with volume ratio 7.5%, is fermented 7 days, is fermented in 24 DEG C
Liquid；The wherein fluid nutrient medium composition are as follows: potato 100g/L, glucose 20g/L, potassium dihydrogen phosphate 1g/L, magnesium sulfate
0.5g/L, surplus are water；Fermentation liquid is extracted 30 minutes under conditions of 60 DEG C, ultrasonic power 300W, is allowed in vulcanized ester mycelia
Nutriment release, then filtered with the nylon cloths of 200 mesh, obtain sulphur bacterium solution；By liquor C and sulphur bacterium solution with body
Product is mixed than 10:1, obtains mixed liquor；The maltitol of mixed liquor quality 4% is added into mixed liquor, mixes well as original
Liquid；
Step D: brown sugar and honey are added into stoste, wherein brown sugar accounts for the 2% of stock solution quality, and honey accounts for stock solution quality
0.5%, in 60 DEG C infusion 300 minutes；Continue that protein particle is added thereto and stabilizer, stabilizer account for stock solution quality
0.3%, protein particle accounts for the 2% of stock solution quality, and the stabilizer is corn fiber gum and esterification soybean polyoses with mass ratio 1:1
The mixture of composition after ten minutes in temperature 50 C, homogenization pressure 30MPa homogeneous is placed at room temperature for 12 hours；
Step E: then it is canned, it is sterilized 15 minutes in 85 DEG C, obtains the regulating menstruation and assisting pregnancy red date-walnut drink.
The protein particle is compound protein particle, is prepared using following methods: by soybean protein isolate and egg white
Albumen is uniformly mixed with mass ratio 2:1, is scattered in deionized water and soybean protein isolate and albumen gross mass is prepared
The dispersion liquid of score 15% is placed in agitating and heating in 95 DEG C of water-bath using the salt acid for adjusting pH of mass fraction 1% to 4.5
60 minutes, cooled to room temperature is then taken out, obtains compound protein particle dispersion liquid；By compound protein particle dispersion liquid homogeneous
20 minutes, 50 DEG C of homogenizing temperature, then homogenization pressure 50MPa was spray-dried, and compound protein particle was obtained, wherein being spray-dried
Process conditions: 180 DEG C of inlet temperature, 110 DEG C of outlet temperature, sample introduction flow 3mL/min, air velocity 600L/h.
The esterification soybean polyoses are prepared using following methods: soluble soybean polysaccharide is dissolved in deionized water system
The soluble soybean polysaccharide solution of standby mass fraction 10%, is heated to 40 DEG C with 2 DEG C/min, uses the hydrogen-oxygen of mass fraction 1%
Change sodium water solution and adjusts pH to 8.5；In 40 DEG C of addition octenyl succinic acid anhydrides, and 35 minutes are stirred to react, ocentyl succinic
The mass ratio of acid anhydride and soluble soybean polysaccharide is 1:7, passes through the sodium hydrate aqueous solution of addition mass fraction 1% in reaction process
Maintain pH 8.5；After reaction, using the salt acid for adjusting pH of mass fraction 1% to 5.0, using shutting off molecular weight 500KD's
Bag filter is freeze-dried after dialysing 48 hours, obtains esterification soybean polyoses.
Test case 1
The stability of 2~11 regulating menstruation and assisting pregnancy red date-walnut drink of embodiment is measured:
(1) measurement of centrifugation rate: 50mL centrifuge tube is dry to constant weight, quality m1 is weighed, 10g tune is accurately weighed
It is helped pregnant red date-walnut drink (quality m2) in centrifuge tube, is centrifuged 20 minutes with 6980 revs/min, supernatant liquid is outwelled (on
Layer fat is disposed simultaneously), centrifugation pipe outer wall is dried, is inverted 5 minutes, accurately weighs quality m3.Calculation formula are as follows: centrifugation is heavy
Shallow lake rate (%)=(m3-m1)/m2 × 100.
(2) measurement of Zeta potential: by zeta potential instrument, (model DT-1202, producer's instrument think odd Beijing development in science and technology
Co., Ltd) it is measured, 100 times are diluted with deionized water, takes appropriate amount of sample in cuvette, sets decentralized medium as water,
Dispersed phase is protein, refractive index 1.450, equilibration time 30s, parallel determination 3 times.
(3) measurement of viscosity: II+Pro rotational viscometer of Brookfield DV- (the scientific instrument in producer, silent west, Shanghai is utilized
Device Co., Ltd) measurement, using ULA rotor, 25 DEG C of temperature, 100 revs/min of revolving speed.
Specific test result is shown in Table 1.
1 regulating menstruation and assisting pregnancy red date-walnut drink stability test table of table
Test case 2
The curative effect of embodiment 1,11 regulating menstruation and assisting pregnancy red date-walnut drink of embodiment 2, embodiment 5 and embodiment is surveyed
Examination.
Research object is 40 anovulatory infertility (kidney deficiency palace cold type) patients, is classified as four groups at random.Every group
Patient's general information (age, the course of disease and body-mass index) compares no significant difference (P > 0.05), there is comparativity.
Diagnose, be included in it is as follows with exclusion criteria: diagnostic criteria: referring in " the infertile diagnosis and treatment guide of elder women " about ovulation
Obstruction type sterility treatment standard.It is included in standard: 1. meeting anovulatory infertility (kidney deficiency palace cold type) diagnostic criteria；2. from
It is willing to participate in and signs Written informed consent；3. not with other severe genitor systemic disease, communicable disease and malignant tumours.
Exclusion criteria: anovulatory infertility (kidney deficiency palace cold type) diagnostic criteria is not 1. met；2. refusal participates in research or does not sign
Written informed consent；3. concurrent other serious Organ Failure, reproductive system, communicable disease and malignant tumours.
The infertile clinical manifestation of kidney deficiency palace cold type has soreness of waist abdomen cold expanding, and chilly, cold limbs, leukorrhagia is thin, and the menstrual cycle is disorderly
Unrest or phase of spreading out are unlikely, unsmooth through row, and the few color of amount is black or dysmenorrhea, pulse condition are heavy late or heavy carefully powerless.Auxiliary examination: 1. basal body temperature is surveyed
It is fixed, be not true to type for diphasic curve or luteal phase be stepped risings, and liter and it is unstable；Or high phase lack of luteal phase 10 days, or be in
Monophasic curve.2. bilanual gynecological examination, uterus is normal or less than normal, or merges other gynaecological imflammations.Tune is taken after making a definite diagnosis daily
Helped pregnant red date-walnut drink, each 50mL, 2 times a day.
The preceding integral of tcm syndrome curative effect determinate standard: therapeutic index (n)=(being integrated after integral-treatment before treating)/treatment ×
100%, n >=90% is recovery from illness；66.67%≤n < 90% is effective；33.3%≤n < 66.67% is effective；N < 33.3%
It is invalid.All patient base's body temperature (BBT) of time-and-motion study are carried out by professional B ultrasound technical staff after the course for the treatment of, records and compares
Compared with two groups of patient's ovulation rates.
Specific test result is shown in Table 2.
2 regulating menstruation and assisting pregnancy red date-walnut drink curative effect of table tests table
Regulating menstruation and assisting pregnancy red date-walnut drink of the present invention is prepared by irreplaceable secret prescription handed down in the family from generation to generation, belongs to nourishing conditioning
Product have effects that following: 1. adjust endocrine disorder；2. adjust menstruation postponement, blood stasis, amount less, palace cold, color it is dark；3. adjusting dysmenorrhea, warp
Fore udder distending pain, paramenia；4. palace, warm palace are supported in pregnancy difficulty, pregnant preceding menstruation regulating；5. activating microcirculation and removing stasis medicinal delays menopause；6. production
It is conserved with post-abortion miscellaneous disease and uterus.
It should be appreciated that although this specification is described in terms of embodiments, but not each embodiment only includes one
A independent technical solution, for the sake of this narrating mode of specification is used for the purpose of clearly, those skilled in the art should be incited somebody to action
As a whole, the technical solutions in the various embodiments may also be suitably combined for specification, and forming those skilled in the art can
With the other embodiments of understanding.
Claims (10)
1. the preparation method of regulating menstruation and assisting pregnancy red date-walnut drink, which comprises the following steps:
Step A: by 10~20g of motherwort, 1~3g of Radix Salviae Miltiorrhizae, 5~20g of China rose, 60~200g of walnut, 30~70g of jujube, when
Return 3~10g, 5~10g of radix rehmanniae preparata, 10~40g of semen sojae atricolor, 2~10g of safflower to mix well, obtains mixture；By mixture with quality
Than 1:(10~50) it impregnates 2~3 hours into the water, it squeezes the juice, filtrate A and filter residue A is collected in filtering respectively；Filtrate A room temperature is put
It sets 12~24 hours, filters again, collect liquor B and filter residue B respectively；Liquor B is spare as medical fluid, filter residue A and filter residue B mixing
It is spare as the dregs of a decoction；
Step B: by the dregs of a decoction and medical fluid with mass ratio 1:(30~80) mix well, in 50~80 DEG C infusion 30~60 minutes, mistake
Filter collects liquor C as stoste；
Step C: brown sugar and honey are added into stoste, wherein brown sugar accounts for the 1~2% of stock solution quality, and honey accounts for stock solution quality
0.5~2%, after infusion 60~300 minutes, 12~24 hours are placed at room temperature in 60~90 DEG C；
Step D: then it is canned, it is sterilized 10~20 minutes in 80~90 DEG C, obtains the regulating menstruation and assisting pregnancy red date-walnut drink.
2. the preparation method of regulating menstruation and assisting pregnancy red date-walnut drink, which comprises the following steps:
Step A: by 10~20g of motherwort, 1~3g of Radix Salviae Miltiorrhizae, 5~20g of China rose, 60~200g of walnut, 30~70g of jujube, when
Return 3~10g, 5~10g of radix rehmanniae preparata, 10~40g of semen sojae atricolor, 2~10g of safflower to mix well, obtains mixture；By mixture with quality
Than 1:(10~50) it impregnates 2~3 hours into the water, it squeezes the juice, filtrate A and filter residue A is collected in filtering respectively；Filtrate A room temperature is put
It sets 12~24 hours, filters again, collect liquor B and filter residue B respectively；Liquor B is spare as medical fluid, filter residue A and filter residue B mixing
It is spare as the dregs of a decoction；
Step B: by the dregs of a decoction and medical fluid with mass ratio 1:(30~80) mix well, in 50~80 DEG C infusion 30~60 minutes, mistake
Liquor C is collected in filter；
Step C: vulcanized ester is inoculated in fluid nutrient medium with volume ratio 5~10%, is fermented 5~7 days in 24~30 DEG C, is obtained
Fermentation liquid；The wherein fluid nutrient medium composition are as follows: 50~100g/L of potato, 10~20g/L of glucose, potassium dihydrogen phosphate
0.3~1g/L, 0.2~0.5g/L of magnesium sulfate, surplus are water；By fermentation liquid in 50~70 DEG C ultrasonic extraction 30~40 minutes, mistake
Filter, obtains sulphur bacterium solution；By liquor C and sulphur bacterium solution with volume ratio (8~20): 1 mixing obtains mixed liquor；Into mixed liquor
The sucrose of mixed liquor quality 2~4% is added, mixes well as stoste；
Step D: brown sugar and honey are added into stoste, wherein brown sugar accounts for the 1~2% of stock solution quality, and honey accounts for stock solution quality
0.5~2%, after infusion 60~300 minutes, 12~24 hours are placed at room temperature in 60~90 DEG C；
Step E: then it is canned, it is sterilized 10~20 minutes in 80~90 DEG C, obtains the regulating menstruation and assisting pregnancy red date-walnut drink.
3. the preparation method of regulating menstruation and assisting pregnancy red date-walnut drink, which comprises the following steps:
Step A: by 10~20g of motherwort, 1~3g of Radix Salviae Miltiorrhizae, 5~20g of China rose, 60~200g of walnut, 30~70g of jujube, when
Return 3~10g, 5~10g of radix rehmanniae preparata, 10~40g of semen sojae atricolor, 2~10g of safflower to mix well, obtains mixture；By mixture with quality
Than 1:(10~50) it impregnates 2~3 hours into the water, it squeezes the juice, filtrate A and filter residue A is collected in filtering respectively；Filtrate A room temperature is put
It sets 12~24 hours, filters again, collect liquor B and filter residue B respectively；Liquor B is spare as medical fluid, filter residue A and filter residue B mixing
It is spare as the dregs of a decoction；
Step B: by the dregs of a decoction and medical fluid with mass ratio 1:(30~80) mix well, in 50~80 DEG C infusion 30~60 minutes, mistake
Liquor C is collected in filter；
Step C: vulcanized ester is inoculated in fluid nutrient medium with volume ratio 5~10%, is fermented 5~7 days in 24~30 DEG C, is obtained
Fermentation liquid；The wherein fluid nutrient medium composition are as follows: 50~100g/L of potato, 10~20g/L of glucose, potassium dihydrogen phosphate
0.3~1g/L, 0.2~0.5g/L of magnesium sulfate, surplus are water；By fermentation liquid in 50~70 DEG C ultrasonic extraction 30~40 minutes, mistake
Filter, obtains sulphur bacterium solution；By liquor C and sulphur bacterium solution with volume ratio (8~20): 1 mixing obtains mixed liquor；Into mixed liquor
The sucrose of mixed liquor quality 2~4% is added, mixes well as stoste；
Step D: brown sugar and honey are added into stoste, wherein brown sugar accounts for the 1~2% of stock solution quality, and honey accounts for stock solution quality
0.5~2%, in 60~90 DEG C infusion 60~300 minutes；Continue that protein particle is added thereto and stabilizer, stabilizer account for original
The 0.3~0.5% of liquid quality, protein particle account for 40~50 DEG C of 1~3%, the Yu Wendu of stock solution quality, homogenization pressure 20~
40MPa homogeneous 10~after twenty minutes, it is placed at room temperature for 12~24 hours；
Step E: then it is canned, it is sterilized 10~20 minutes in 80~90 DEG C, obtains the regulating menstruation and assisting pregnancy red date-walnut drink.
4. the preparation method of regulating menstruation and assisting pregnancy red date-walnut drink according to claim 3, which is characterized in that the protein particle
It for soybean protein particle, is prepared using following procedure: soybean protein isolate being dispersed in water, mass fraction is prepared
10~20% dispersion liquid is placed in 85~95 DEG C of water-bath using the salt acid for adjusting pH of mass fraction 1~5% to 3.0~7.0
Agitating and heating 20~60 minutes in pot, cooled to room temperature is then taken out, soybean protein particle dispersion liquid is obtained；By soybean egg
White particle dispersion liquid homogeneous 10~20 minutes, 50~70 DEG C of homogenizing temperature, then 30~60MPa of homogenization pressure is spray-dried, obtains
Obtain protein particle.
5. the preparation method of regulating menstruation and assisting pregnancy red date-walnut drink according to claim 3, which is characterized in that the protein particle
It for compound protein particle, is prepared using following methods: by soybean protein isolate and albumen with mass ratio (1~2): (1
~2) it is uniformly mixed, is dispersed in water the dispersion that soybean protein isolate and albumen total mass fraction 10~20% is prepared
Liquid is placed in agitating and heating 20 in 85~95 DEG C of water-bath using the salt acid for adjusting pH of mass fraction 1~5% to 3.0~7.0
~60 minutes, cooled to room temperature is then taken out, obtains compound protein particle dispersion liquid；Compound protein particle dispersion liquid is equal
Matter 10~20 minutes, 50~70 DEG C of homogenizing temperature, then 30~60MPa of homogenization pressure was spray-dried, and obtained protein particle.
6. the preparation method of regulating menstruation and assisting pregnancy red date-walnut drink according to any one of claim 3~5, which is characterized in that
The sucrose is substituted using sugar alcohol, and the sugar alcohol is one of xylitol, D-sorbite, maltitol, antierythrite.
7. the preparation method of regulating menstruation and assisting pregnancy red date-walnut drink according to claim 6, which is characterized in that the sugar alcohol is wheat
Bud sugar alcohol.
8. the preparation method of regulating menstruation and assisting pregnancy red date-walnut drink according to claim 3, which is characterized in that the stabilizer is
Sodium carboxymethylcellulose, carboxymethyl curdlan gum, corn fiber gum, soluble soybean polysaccharide, esterification one of soybean polyoses or
A variety of mixtures.
9. the preparation method of regulating menstruation and assisting pregnancy red date-walnut drink according to claim 8, which is characterized in that the esterification soybean
Polysaccharide is prepared using following methods: soluble soybean polysaccharide is dissolved in the water solubility that water prepares mass fraction 10~20%
Soybean polyoses solution is heated to 40~60 DEG C, using mass fraction 1~5% sodium hydrate aqueous solution adjust pH to 8.0~
9.0；In 40~60 DEG C of addition octenyl succinic acid anhydrides, and it is stirred to react 30~50 minutes, octenyl succinic acid anhydride and water solubility
The mass ratio of soybean polyoses is 1:(5~10), pass through the sodium hydrate aqueous solution of addition mass fraction 1~5% in reaction process
Maintain pH 8.0~9.0；After reaction, using the salt acid for adjusting pH of mass fraction 1~5% to 4.0~5.0, dialysis 24~
It is freeze-dried after 48 hours, obtains esterification soybean polyoses.
10. regulating menstruation and assisting pregnancy red date-walnut drink, which is characterized in that red using regulating menstruation and assisting pregnancy according to any one of claims 1 to 9
The preparation method of jujube walnut drink is process.
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| CN201910114183.2A Pending CN109673752A (en) | 2019-02-14 | 2019-02-14 | Regulating menstruation and assisting pregnancy red date-walnut drink and preparation method thereof |
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| CN111110838A (en) * | 2019-12-24 | 2020-05-08 | 华南师范大学 | Tilapia streptococcus agalactiae vaccine and preparation method thereof |
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