CN109667144A - A kind of antibacterial quilt cover and its production technology - Google Patents
A kind of antibacterial quilt cover and its production technology Download PDFInfo
- Publication number
- CN109667144A CN109667144A CN201811537515.XA CN201811537515A CN109667144A CN 109667144 A CN109667144 A CN 109667144A CN 201811537515 A CN201811537515 A CN 201811537515A CN 109667144 A CN109667144 A CN 109667144A
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- quilt cover
- antibacterial
- production technology
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- 238000005516 engineering process Methods 0.000 title claims abstract description 30
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- 238000001035 drying Methods 0.000 claims abstract description 12
- 239000004744 fabric Substances 0.000 claims abstract description 4
- 238000007654 immersion Methods 0.000 claims abstract description 4
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 44
- 239000000843 powder Substances 0.000 claims description 42
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 31
- 239000000284 extract Substances 0.000 claims description 30
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 28
- 239000011787 zinc oxide Substances 0.000 claims description 22
- 239000003242 anti bacterial agent Substances 0.000 claims description 21
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- 229940088710 antibiotic agent Drugs 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
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- 125000002057 carboxymethyl group Chemical group [H]OC(=O)C([H])([H])[*] 0.000 description 1
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- D06B19/0005—Fixing of chemicals, e.g. dyestuffs, on textile materials
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- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
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- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/44—Oxides or hydroxides of elements of Groups 2 or 12 of the Periodic Table; Zincates; Cadmates
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- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
- D06M13/51—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond
- D06M13/513—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond with at least one carbon-silicon bond
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- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
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- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
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- D10B2401/13—Physical properties anti-allergenic or anti-bacterial
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Abstract
The invention discloses a kind of antibacterial sheet and its production technologies.The production technology of antibacterial sheet is the following steps are included: S1, fabric prepare: prepare to have printed and dyed by cover facing material;S2, quilt cover material treatment: will be immersed in antibiotic finishing solution by cover facing material, and water-bath ratio is 1:5-10, and soaking temperature is 45-55 DEG C, soaking time 20-30min;S3, pad drying: by being padded by cover facing material after immersion, pick-up 40-60%, be placed on 70-80 DEG C at a temperature of dry 2-4h, the dry 5-10min at 90-100 DEG C;S4, gas steam fixed: the gas at 105-110 DEG C that is placed in by cover facing material after drying is steamed 5-10min, naturally dry after taking-up.Preparation method of the invention has easy to operate, and the quilt cover prepared has anti-microbial property good, and the advantage that washability is good.
Description
Technical field
The present invention relates to bedding technical fields, more specifically, it relates to a kind of antibacterial quilt cover and its production technology.
Background technique
Quilt cover, household items usually necessary for every family are covered in the outside of core, due to the body of human daily secretion
The metabolins such as liquid, sweat and grease are easily adhered on quilt cover, so that quilt cover is become the breeding ground of dust mite, bacterium, are greatly affected
The health of body.
Therefore it develops that a kind of anti-microbial property is good and the antibacterial quilt cover of water-tolerant, is problem to be solved.
Summary of the invention
In view of the deficienciess of the prior art, the first purpose of this invention is to provide a kind of production work of antibacterial quilt cover
Skill can prepare that anti-microbial property is good with easy to operate, and the advantages of the quilt cover of water-tolerant.
Second object of the present invention is to provide a kind of antibacterial quilt cover, good with anti-microbial property, and water-tolerant
Advantage.
To realize above-mentioned first purpose, the present invention provides the following technical scheme that a kind of production technology of antibacterial quilt cover,
Characterized by comprising the following steps:
S1, fabric prepare: prepare printed and dyed by cover facing material;
S2, quilt cover material treatment: will be immersed in antibiotic finishing solution by cover facing material, and water-bath ratio is 1:5-10, soaking temperature 45-
55 DEG C, soaking time 20-30min;
S3, pad drying: by being padded by cover facing material after immersion, pick-up 40-60%, be placed on 70-80 DEG C
At a temperature of dry 2-4h, the dry 5-10min at 90-100 DEG C;
S4, gas steam fixed: the gas at 105-110 DEG C that is placed in by cover facing material after drying is steamed 5-10min, naturally dry after taking-up.
It by using above-mentioned technical proposal, will be impregnated in antibiotic finishing solution by cover facing material, and make soaking temperature 45-55
DEG C, the movement of antimicrobial molecule in antibiotic finishing solution can be accelerated, enter antimicrobial molecule by inside cover facing material, and uniform adhesion is in quilt
On cover facing material, then will be padded by cover facing material, when antimicrobial molecule is relatively firm is adhered on quilt cover, increase washability, make
After being housed in cleaning repeatedly, still there is good anti-microbial property, improve Durability of antimicrobial effect, after being steamed using gas to drying is padded
It is handled by cover facing material, can make more soft by cover facing material, and antimicrobial component anchored at by inside cover facing material, increased resistance to
Wash performance.
Further, the antimicrobial treatment solution comprises the following components in parts by weight: 5-10 parts of antibacterial agents, 200-250 parts of water,
5-10 parts of adhesives, 1-5 parts of Herba Senecionis Scandentis extracts, 1-5 parts of tuckahoe extracts, 1-3 parts of Ostholes.
By using above-mentioned technical proposal, since Herba Senecionis Scandentis extract has broad spectrum antibiotic activity, and contained by climbing groundsel
Brass constituents all have stronger inhibiting effect, Fu to staphylococcus aureus, Bacterium enteritidis, hemolytic streptococcus etc.
Siberian cocklebur extract all has inhibiting effect, snake to staphylococcus aureus, staphylococcus albus, Escherichia coli, alpha streptococcus etc.
Machine tool element has broad-spectrum antibacterial action, and three cooperates, and can be improved the antibacterial effect of quilt cover, while adhesive is for increasing
The viscosity of antimicrobial component is tightly adhered to antimicrobial component by cover facing material, to increase by the washability of cover facing material, makes to be housed in
After cleaning repeatedly, still there is good anti-microbial property.
Further, the antibacterial agent comprises the following components in parts by weight: 5.5-8 parts of zinc oxide, 1-3 parts of copper oxide, 5-
10 parts of chitins, 5-10 parts of zeolite powders, 1-5 parts of silica whites, 10-20 parts of ethyl alcohol, 20-30 parts of water, 5-10 parts of vinyl trimethoxies
Base silane, 1-5 part acrylic acid ester emulsion.
By using above-mentioned technical proposal, the antibacterial effect of zinc oxide is good, all has in the case where having light or unglazed irradiation
Preferable antibacterial effect, zinc oxide can lead to the dissolution of cellular content by destroying bacterial cell membrane, and obstruction is conducive to thin
The synthesis of bacterium metabolism enzyme destroys gene, so that bacterium is lost its biological activity, furthermore zinc oxide may also interfere with peptide
The synthesis of glycan, the formation of block cell wall inhibit the procreation and growth of cell, zinc oxide and copper oxide collective effect, antibacterial
Effect increases, and zeolite powder and silica white have porous structure, after mixing with zinc oxide, copper oxide, can carry copper oxide and oxygen
To change zinc to enter by inside cover facing material, increase zinc oxide, copper oxide and the adherency fastness by cover facing material, acrylate have viscosity,
The viscosity that antibacterial agent can be increased adheres to zinc oxide and copper oxide securely, and vinyltrimethoxysilane can be improved on quilt cover
The cementability of fiber and acrylic acid ester emulsion improves the washing fastness of antibiotic effective ingredient.
Further, the antibacterial agent is made of following methods: (1) by zinc oxide, copper oxide, zeolite powder, chitin, silicon
Rubber powder is added to the water, and is warming up to 20-30 DEG C, stirs 30-40min, and centrifugation calcines centrifugal sediment at 1100-1200 DEG C
0.5-0.8h, it is cooling after powder at 20-30nm powder;
(2) powder is added in acrylic acid ester emulsion, stirs 20-40min, vinyltrimethoxysilane and ethyl alcohol is added, stirs
10-20min is mixed, is centrifuged, taking precipitate, and dry 10-15min.
By using above-mentioned technical proposal, zinc oxide, copper oxide and chitin etc. are mixed first, make zinc oxide, oxidation
Copper and chitin are calcined after centrifugation well into the hole of zeolite powder and silica white, remove moisture removal, then with acrylic acid ester emulsion
Mixing improves the viscosity of the antimicrobial components such as zinc oxide, adds vinyltrimethoxysilane, improve acrylic acid ester emulsion and by
The viscosity of cover increases the washability of quilt cover.
It further, is 20-60kHz in frequency before the middle centrifugation of the step (1), power is super under conditions of being 300-800W
Sonication 20-30min.
By using above-mentioned technical proposal, ultrasonic treatment can make each stock dispersion more evenly, make zinc oxide, copper oxide and first
Shell element prevents to reunite or settle well into the hole of zeolite powder and silica white.
Further, described adhesive is one of tapioca, sodium carboxymethylcellulose, modified guar gum or several
The composition of kind.
By using above-mentioned technical proposal, tapioca have very high spike viscosity so that antimicrobial component be adhered to by
On cover facing material, the aqueous solution of sodium carboxymethylcellulose has viscosity, can dramatically increase the viscosity of antibiotic finishing solution, modified Guar
Bean gum is cooperateed with tapioca, be can be improved the viscosity of antibiotic finishing solution, is adhered to antimicrobial component on quilt cover, improves quilt cover
Washability and Durability of antimicrobial effect.
Further, the Herba Senecionis Scandentis extract is made of following methods:
(1) to the ethyl alcohol that 10-100 parts of mass fractions of addition are 50-60% in 5-10 parts of climbing groundsel herb powder, 20- is impregnated
For 24 hours, it is filtered after being ultrasonically treated 10-20min, obtains filtrate;
(2) filter residue obtained by step (1) is taken, 8-10 times is added and measures the ethyl alcohol that mass fraction is 50-60%, according in step (1)
Method processing, merges 2 filtrates, is concentrated by evaporation, is extracted with ether, 10-12h under conditions of being placed in 1-4 DEG C, filters, and filtrate is cold
It is lyophilized dry, powder is made, obtains Herba Senecionis Scandentis extract.
Further, it is mixed by cover facing material by 25-50wt% banana fiber and 50-75wt% Sheng-bast fiber in the step S1
Weaving is made.
By using above-mentioned technical proposal, banana fiber has light weight, good luster, the function that water imbibition is strong and antibiotic property is strong
Can, Sheng-bast fiber has natural antibacterial, suppression mite property, is made of antibacterials, has broad spectrum activity, using with anti-microbial property
Raw material, improve the anti-microbial property and Durability of antimicrobial effect of sheet.
Further, the antimicrobial treatment solution further includes 5-10 parts of dispersing agents.
By using above-mentioned technical proposal, dispersing agent can be such that antibacterial agent, tuckahoe extracts, Osthole and climbing groundsel mentions
It takes object fully dispersed in water, prevents the particulate component in antibacterial agent, tuckahoe extracts, Osthole and Herba Senecionis Scandentis extract heavy
Drop or cohesion.
To realize above-mentioned second purpose, the present invention provides the following technical scheme that a kind of antibacterial sheet, by antibacterial sheet
Production technology be prepared.
In conclusion the invention has the following advantages:
The first, since method of the invention will carry out gas steaming by cover facing material after drying, antimicrobial component can be improved and by cover facing material
Bonding intensity, increase the antibacterial washability of quilt cover, improve Durability of antimicrobial effect, and improve the pliability of quilt cover.
The second, antibiotic finish is made using Herba Senecionis Scandentis extract, tuckahoe extracts, Osthole and adhesive in the present invention
Liquid, Herba Senecionis Scandentis extract, tuckahoe extracts and Osthole all have good anti-microbial property, to staphylococcus aureus, greatly
The bacteriums such as enterobacteria and staphylococcus albus have stronger inhibiting effect, and adhesive can increase the viscosity of antimicrobial component, make
When being immersed in antibiotic finishing solution by cover facing material, antimicrobial component can be tightly adhered on quilt cover, increase the anti-microbial property of quilt cover
And washability.
Third, the present invention make antibacterial agent, zinc oxide and copper oxide phase using raw materials such as zinc oxide, copper oxide and chitins
Mutually collaboration, antibacterial effect are enhanced, and the antibacterial deodourizing performance of chitin can also further enhance the anti-microbial property of quilt cover,
Zeolite powder and silica white can make zinc oxide, copper oxide and chitin enter the anti-microbial property for inside cover facing material, being improved quilt cover.
Specific embodiment
Invention is further described in detail with reference to embodiments.
The preparation example 1-3 of antibacterial agent
Zinc oxide and copper oxide are that analysis is pure in preparation example 1-3, and zeolite powder is selected from what Lingshou County Hui Mao mineral products processing factory sold
The zeolite powder that article No. is 8888, chitin are selected from the XJH2858 type chitin that Xin Jiehui Biotechnology Co., Ltd in Nanjing sells,
Silica white is selected from the GF254 type silica white that Qingdao Shuo Yuan silica gel Science and Technology Ltd. sells, and acrylic acid ester emulsion is selected from Guangzhou
The SY-2403 type acrylic acid ester emulsion that Sui Yue trade Co., Ltd sells, fatty alcohol polyoxyethylene ether are selected from the prosperous indigo plant in Xingtai
The MOA-5 type fatty alcohol polyoxyethylene ether that star Science and Technology Ltd. sells, vinyltrimethoxysilane are selected from Dongguan City Chang Ping
The A-171 type vinyltrimethoxysilane that sunlight letter plasticizing business department sells.
Preparation example 1:(1) according to the proportion in table 1, by 5.5kg zinc oxide, 1kg copper oxide, 5kg zeolite powder, 5kg crust
Element, 1kg silica white are added to the water, and are warming up to 20 DEG C, stir 30min, are 20kHz in frequency, power surpasses under conditions of being 300W
Centrifugal sediment is calcined 0.5h by sonication 20min, centrifugation at 1100 DEG C, it is cooling after powder at 20nm powder;
(2) powder is added in 1kg acrylic acid ester emulsion, stirs 20min, 5kg vinyltrimethoxysilane, stirring is added
10min, centrifugation, taking precipitate, and dry 10min.
The raw material proportioning of antibacterial agent in 1 preparation example 1-3 of table
Preparation example 2:(1) according to the proportion in table 1, by 7kg zinc oxide, 2kg copper oxide, 8kg zeolite powder, 8kg chitin, 3kg
Silica white is added to the water, and is warming up to 25 DEG C, stirs 35min, is 40kHz in frequency, power is ultrasonically treated under conditions of being 450W
Centrifugal sediment is calcined 0.65h by 25min, centrifugation at 1150 DEG C, it is cooling after powder at 25nm powder;(2) powder is added
Enter in 3kg acrylic acid ester emulsion, stir 30min, 8kg vinyltrimethoxysilane is added, stir 15min, centrifugation takes precipitating
Object, and dry 13min.
Preparation example 3:(1) according to the proportion in table 1, by 8kg zinc oxide, 3kg copper oxide, 10kg zeolite powder, 10kg crust
Element, 5kg silica white are added to the water, and are warming up to 30 DEG C, stir 40min, are 60kHz in frequency, power surpasses under conditions of being 800W
Centrifugal sediment is calcined 0.8h by sonication 30min, centrifugation at 1200 DEG C, it is cooling after powder at 30nm powder;
(2) powder is added in 5kg acrylic acid ester emulsion, stirs 40min, 10kg vinyltrimethoxysilane, stirring is added
20min, centrifugation, taking precipitate, and dry 15min.
The preparation example 4-6 of Herba Senecionis Scandentis extract
Preparation example 4:(1) ethyl alcohol that 10kg mass fraction is 50% is added into climbing groundsel herb powder 5kg, impregnate 20h, ultrasound
It is filtered after processing 10min, obtains filtrate;
(2) filter residue obtained by step (1) is taken, the ethyl alcohol that 8 times of amount mass fractions are 50% is added, at the method in step (1)
Reason, merges 2 filtrates, is concentrated by evaporation, is extracted with ether, 10h under conditions of being placed in 1 DEG C, filters, and filtrate freeze-drying is made
Powder obtains Herba Senecionis Scandentis extract.
Preparation example 5:(1) ethyl alcohol that 80kg mass fraction is 55% is added into climbing groundsel herb powder 8kg, 22h is impregnated,
It is filtered after ultrasonic treatment 15min, obtains filtrate;
(2) filter residue obtained by step (1) is taken, the ethyl alcohol that 9 times of amount mass fractions are 55% is added, at the method in step (1)
Reason, merges 2 filtrates, is concentrated by evaporation, is extracted with ether, 11h under conditions of being placed in 3 DEG C, filters, and filtrate freeze-drying is made
Powder obtains Herba Senecionis Scandentis extract.
Preparation example 5:(1) ethyl alcohol that 100kg mass fraction is 60% is added into climbing groundsel herb powder 10kg, it impregnates
For 24 hours, it is filtered after being ultrasonically treated 20min, obtains filtrate;
(2) filter residue obtained by step (1) is taken, the ethyl alcohol that 10 times of amount mass fractions are 60% is added, at the method in step (1)
Reason, merges 2 filtrates, is concentrated by evaporation, is extracted with ether, 12h under conditions of being placed in 4 DEG C, filters, and filtrate freeze-drying is made
Powder obtains Herba Senecionis Scandentis extract.
Embodiment
Tuckahoe extracts are selected from the tuckahoe extracts that the article No. that Hao Chen Biotechnology Co., Ltd in Shaanxi sells is 10, cnidium monnieri
The Osthole that sub- element is SF selected from the article No. that Shaanxi Sen Fu natural product Co., Ltd sells, tapioca are selected from Jinan perseverance and rise
The tapioca that the article No. that Chemical Co., Ltd. sells is 001, modified guar gum are selected from Renqiu City Hao Chun Chemical Co., Ltd.
The modified guar gum of the RQHC-01 type of sale, sodium carboxymethylcellulose are selected from German-Chinese Chemical Industry Science Co., Ltd, Foshan City and sell
N-611 type sodium carboxymethylcellulose, it is poly- that Sodium Polyacrylate is selected from the GY-303 type that Changzhou Run Yang Chemical Co., Ltd. sells
Sodium acrylate, lauryl sodium sulfate are selected from the K-12 type lauryl sodium sulfate that Chun Jia trade Co., Ltd in Guangzhou sells.
A kind of embodiment 1: production technology of antibacterial quilt cover, comprising the following steps:
S1, fabric prepare: prepare to have printed and dyed by cover facing material, by cover facing material by the banana fiber and 75wt% of 25wt%
Sheng-bast fiber hybrid woven forms;
S2, quilt cover material treatment: will be immersed in antibiotic finishing solution by cover facing material, and water-bath ratio is 1:5, and soaking temperature is 45 DEG C,
Soaking time is 20min;
Antibiotic finishing solution according to the proportion in table 1, by 5kg antibacterial agent, 200kg water, 5kg adhesive, 1kg Herba Senecionis Scandentis extract,
1kg tuckahoe extracts and 1kg Osthole are mixed, and antibacterial agent is prepared by preparation example 1, and Herba Senecionis Scandentis extract is by preparing
Example 4 is prepared, and adhesive is tapioca, and dispersing agent is Sodium Polyacrylate;
S3, pad drying: by being padded by cover facing material after immersion, pick-up 40%, be placed at a temperature of 70 DEG C
Dry 2h, the dry 5min at 90 DEG C;
S4, gas steam fixed: the gas at 105 DEG C that is placed in by cover facing material after drying is steamed 5min, naturally dry after taking-up.
The raw material proportioning of antibiotic finishing solution in 2 embodiment 1-5 of table
Embodiment 2-5: a kind of production technology of antibacterial quilt cover, the difference from embodiment 1 is that, the raw material proportioning of antibiotic finishing solution
As shown in table 2.
Embodiment 6: a kind of production technology of antibacterial quilt cover, the difference from embodiment 1 is that, in S1 by cover facing material by
The banana fiber of 35wt% and the Sheng-bast fiber hybrid woven of 65wt% form;
It is immersed in antibiotic finishing solution in S2 by cover facing material, water-bath ratio is 1:8, and soaking temperature is 50 DEG C, and soaking time is
25min;Antibacterial agent is prepared by preparation example 2, and Herba Senecionis Scandentis extract is prepared by preparation example 5, and adhesive is modified Guar
Bean gum, dispersing agent are lauryl sodium sulfate;
Pick-up is 50% in S3, be placed on 75 DEG C at a temperature of dry 3h, the dry 8min at 95 DEG C;
Temperature of being steamed by cover facing material gas after drying in S4 is 108 DEG C, and gas steams the time for 8min.
Embodiment 7: a kind of production technology of antibacterial quilt cover, the difference from embodiment 1 is that, in S1 by cover facing material by
The banana fiber of 50wt% and the Sheng-bast fiber hybrid woven of 50wt% form;
It is immersed in antibiotic finishing solution in S2 by cover facing material, water-bath ratio is 1:10, and soaking temperature is 55 DEG C, and soaking time is
30min;Antibacterial agent is prepared by preparation example 3, and Herba Senecionis Scandentis extract is prepared by preparation example 6, and adhesive is that carboxymethyl is fine
Plain sodium is tieed up, dispersing agent is fatty alcohol polyoxyethylene ether;
Pick-up is 60% in S3, be placed on 80 DEG C at a temperature of dry 4h, the dry 10min at 100 DEG C;
Temperature of being steamed by cover facing material gas after drying in S4 is 110 DEG C, and gas steams the time for 10min.
Comparative example
Comparative example 1: a kind of production technology of antibacterial quilt cover, the difference from embodiment 1 is that, a thousand li is not added in antibiotic finishing solution
Light extraction object.
Comparative example 2: a kind of production technology of antibacterial quilt cover, the difference from embodiment 1 is that, it is not added in antibiotic finishing solution
Tuckahoe extracts.
Comparative example 3: a kind of production technology of antibacterial quilt cover, the difference from embodiment 1 is that, it is not added in antibiotic finishing solution
Osthole.
Comparative example 4: a kind of production technology of antibacterial quilt cover, the difference from embodiment 1 is that, it is not added in antibiotic finishing solution
Adhesive.
Comparative example 5: a kind of production technology of antibacterial quilt cover, the difference from embodiment 1 is that, it is not added in antibiotic finishing solution
Antibacterial agent.
Comparative example 6: a kind of production technology of antibacterial quilt cover, the difference from embodiment 1 is that, the antibacterial in antibiotic finishing solution
Zeolite powder and silica white are not added in agent raw material.
Comparative example 7: a kind of production technology of antibacterial quilt cover, the difference from embodiment 1 is that, the antibacterial in antibiotic finishing solution
Acrylic acid ester emulsion is not added in agent raw material.
Performance detection test
According in embodiment 1-7 and comparative example 1-7 method prepare antibacterial sheet, and according to GB/T15981-1995 " disinfection with
The evaluation method and standard of sterilization effect " detection antibacterial sheet anti-microbial property, and according to GB/T3921-2008 " textile color
Fastness test fastness to soaping " in method soap, detection washing 10 times, washing 20 times and wash 30 antibiotic properties
Can, testing result is as shown in table 3.
The antibacterial effect and washability test result of antibacterial sheet in table 3 embodiment 1-7 and comparative example 1-7
There is good anti-microbial property according to quilt cover made from method in embodiment 1-7 it can be seen from data in table 3, not
Before cleaning, 93.62% or more is reached to the bacteriostasis rate of staphylococcus aureus, 97.28% is reached to the bacteriostasis rate of Escherichia coli
More than, 92.28% or more, and the suppression after washing 30 times, to staphylococcus aureus are reached to the bacteriostasis rate of Candida albicans
Bacterium rate is still up to 92.08% or more, to the bacteriostasis rates of Escherichia coli still up to 97.05% or more, to Candida albicans
Bacteriostasis rate is up to 92.01% or more, and it is good according to the anti-microbial property of quilt cover made from embodiment 1-7 to illustrate, and washability is good, is washing
After washing 30 times, still there is preferable anti-microbial property.
Comparative example 1 because being not added with Herba Senecionis Scandentis extract in antibiotic finishing solution, the anti-microbial property of quilt cover compared with Example 1 compared with
Difference, and after washing 30 times, 85.17% is followed successively by the bacteriostasis rate of staphylococcus aureus, Escherichia coli and Candida albicans,
85.76% and 81.29%, washability is poor, illustrates that Herba Senecionis Scandentis extract can be improved the antibiotic property and washability of quilt cover.
Comparative example 2 is because being not added with tuckahoe extracts in antibiotic finishing solution, quilt cover is before cleaning to staphylococcus aureus, big
The bacteriostasis rate of enterobacteria and Candida albicans is followed successively by 87.65%, 88.86% and 84.87%, compared with Example 1 bacteriostasis rate
It reduces, and after cleaning 30 times, 85.32% is reduced to the bacteriostasis rate of staphylococcus aureus, to the bacteriostasis rate of Escherichia coli
It is reduced to 85.22%, 82.17%, after cleaning is reduced to the bacteriostasis rate of Candida albicans, bacteriostasis rate decline is very fast, illustrates Fu
Siberian cocklebur extract can be improved the anti-microbial property and washability of quilt cover.
Comparative example 3 because being not added with Osthole in antibiotic finishing solution, the antibiotic property of quilt cover before not cleaning with 1 phase of embodiment
It is poor, and after cleaning 30 times, bacteriostasis rate decline is very fast, and after cleaning 30 times, and bacteriostasis rate compared with Example 1, differs larger,
Illustrate that Osthole can be improved the anti-microbial property and washability of quilt cover.
Comparative example 4 is housed in front of not cleaning because being not added with adhesive in antibiotic finishing solution to staphylococcus aureus, large intestine
The bacteriostasis rate of bacillus and Candida albicans is higher, with do not cleaned in embodiment 1 before be not much different, cleaning 30 times after, under bacteriostasis rate
Drop is obvious, illustrates that adhesive can be improved the washability of quilt cover.
Comparative example 5 is because being not added with antibacterial agent in antibiotic finishing solution, the anti-microbial property of quilt cover is not before cleaning, with embodiment 1
Compared to poor, and after washing 30 times, bacteriostasis rate decline is obvious, is reduced to 83.18% to the bacteriostasis rate of staphylococcus aureus, right
The bacteriostasis rate of Escherichia coli is reduced to 82.31%, is reduced to 81.92% to the bacteriostasis rate of Candida albicans, illustrates antibacterial agent not
It only can be improved the anti-microbial property of quilt cover, moreover it is possible to which the washability for improving quilt cover makes after being housed in cleaning 30 times, still has higher
Anti-microbial property.
For comparative example 6 because being not added with zeolite powder and silica white in antibacterial agent, it is poor to be housed in the anti-microbial property before not cleaning, and
Compared with antibiotic property is not before clean after cleaning 30 times, anti-microbial property decline is very fast, illustrate zeolite powder and silica white can be improved by
The anti-microbial property and washability of cover.
Comparative example 7 is housed in the anti-microbial property before not cleaning and embodiment 1 because being not added with acrylic acid ester emulsion in antibacterial agent
Compared to no large change, the bacteriostasis rate to staphylococcus aureus is 93.65%, and the bacteriostasis rate to Escherichia coli is 97.23%,
Bacteriostasis rate to Candida albicans is 92.31%, and after washing 30 times, the bacteriostasis rate to staphylococcus aureus is only
85.16%, the bacteriostasis rate to Escherichia coli is only 89.54%, and the bacteriostasis rate to Candida albicans is only 86.21%, decline compared with
Be it is obvious, illustrate that acrylate can be improved the washability of quilt cover, still there is good antibacterial after making to be housed in cleaning 30 times
Performance.
This specific embodiment is only explanation of the invention, is not limitation of the present invention, those skilled in the art
Member can according to need the modification that not creative contribution is made to the present embodiment after reading this specification, but as long as at this
All by the protection of Patent Law in the scope of the claims of invention.
Claims (10)
1. a kind of production technology of antibacterial quilt cover, which comprises the following steps:
S1, fabric prepare: prepare printed and dyed by cover facing material;
S2, quilt cover material treatment: will be immersed in antibiotic finishing solution by cover facing material, and water-bath ratio is 1:5-10, soaking temperature 45-
55 DEG C, soaking time 20-30min;
S3, pad drying: by being padded by cover facing material after immersion, pick-up 40-60%, the temperature for being placed on 70-80 DEG C
Degree lower dry 2-4h, the dry 5-10min at 90-100 DEG C;
S4, gas steam fixed: the gas at 105-110 DEG C that is placed in by cover facing material after drying is steamed 5-10min, naturally dry after taking-up.
2. the production technology of antibacterial quilt cover according to claim 1, which is characterized in that the antimicrobial treatment solution includes following
The component of parts by weight: 5-10 parts of antibacterial agents, 200-250 parts of water, 5-10 parts of adhesives, 1-5 parts of Herba Senecionis Scandentis extracts, 1-5 parts of Fu
Siberian cocklebur extract, 1-3 part Osthole.
3. the production technology of antibacterial quilt cover according to claim 2, which is characterized in that the antibacterial agent includes following weight
The component of part: 5.5-8 parts of zinc oxide, 1-3 parts of copper oxide, 5-10 parts of chitins, 5-10 parts of zeolite powders, 1-5 parts of silica whites, 10-
20 parts of ethyl alcohol, 20-30 parts of water, 5-10 parts of vinyltrimethoxysilanes, 1-5 parts of acrylic acid ester emulsions.
4. the production technology of antibacterial quilt cover according to claim 3, which is characterized in that the antibacterial agent is by following methods system
At: (1) zinc oxide, copper oxide, zeolite powder, chitin, silica white are added to the water, are warming up to 20-30 DEG C, stirs 30-
Centrifugal sediment is calcined 0.5-0.8h by 40min, centrifugation at 1100-1200 DEG C, it is cooling after powder at 20-30nm powder;
(2) powder is added in acrylic acid ester emulsion, stirs 20-40min, vinyltrimethoxysilane and ethyl alcohol is added, stirs
10-20min is mixed, is centrifuged, taking precipitate, and dry 10-15min.
5. the production technology of antibacterial quilt cover according to claim 4, which is characterized in that in the step (1) before centrifugation
Frequency is 20-60kHz, and power is ultrasonically treated 20-30min under conditions of being 300-800W.
6. the production technology of antibacterial quilt cover according to claim 2, which is characterized in that described adhesive be tapioca,
The composition of one or more of sodium carboxymethylcellulose, modified guar gum.
7. the production technology of antibacterial quilt cover according to claim 2, which is characterized in that the Herba Senecionis Scandentis extract is by following
Method is made:
(1) to the ethyl alcohol that 10-100 parts of mass fractions of addition are 50-60% in 5-10 parts of climbing groundsel herb powder, 20-24h is impregnated,
It is filtered after ultrasonic treatment 10-20min, obtains filtrate;
(2) filter residue obtained by step (1) is taken, 8-10 times is added and measures the ethyl alcohol that mass fraction is 50-60%, according to the side in step (1)
Method processing, merges 2 filtrates, is concentrated by evaporation, is extracted with ether, 10-12h under conditions of being placed in 1-4 DEG C, filters, filtrate freezing
It is dry, powder is made, obtains Herba Senecionis Scandentis extract.
8. the production technology of antibacterial quilt cover according to claim 2, which is characterized in that the antimicrobial treatment solution further includes 5-
10 parts of dispersing agents.
9. the production technology of antibacterial quilt cover according to claim 1, which is characterized in that in the step S1 by cover facing material by
25-50wt% banana fiber and 50-75wt% Sheng-bast fiber hybrid woven form.
10. a kind of antibacterial quilt cover, which is characterized in that by the production technology system of the antibacterial quilt cover as described in claim 1-9 is any
It is standby to form.
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN111379161A (en) * | 2020-04-18 | 2020-07-07 | 广州宇然膜丽无纺制品有限公司 | Preparation method of silver ion antibacterial non-woven fabric |
CN112323496A (en) * | 2020-11-13 | 2021-02-05 | 苏州斯诺服饰有限公司 | Preparation method of antibacterial fabric, fabric prepared by using preparation method and windproof clothes |
CN112482039A (en) * | 2020-11-24 | 2021-03-12 | 桐乡市汇中纺织有限公司 | Environment-friendly imitated leather fabric and preparation process thereof |
CN112522977A (en) * | 2020-11-24 | 2021-03-19 | 桐乡市汇中纺织有限公司 | Environment-friendly gold stamping process for garment fabric |
CN112545761A (en) * | 2020-12-01 | 2021-03-26 | 张�杰 | Antibacterial paper diaper and production process thereof |
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CN106319974A (en) * | 2016-08-17 | 2017-01-11 | 浙江慧德新材料有限公司 | Production process of antibacterial quilt cover fabric |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
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CN111379161A (en) * | 2020-04-18 | 2020-07-07 | 广州宇然膜丽无纺制品有限公司 | Preparation method of silver ion antibacterial non-woven fabric |
CN111379161B (en) * | 2020-04-18 | 2021-05-04 | 广州宇然膜丽无纺制品有限公司 | Preparation method of silver ion antibacterial non-woven fabric |
CN112323496A (en) * | 2020-11-13 | 2021-02-05 | 苏州斯诺服饰有限公司 | Preparation method of antibacterial fabric, fabric prepared by using preparation method and windproof clothes |
CN112482039A (en) * | 2020-11-24 | 2021-03-12 | 桐乡市汇中纺织有限公司 | Environment-friendly imitated leather fabric and preparation process thereof |
CN112522977A (en) * | 2020-11-24 | 2021-03-19 | 桐乡市汇中纺织有限公司 | Environment-friendly gold stamping process for garment fabric |
CN112545761A (en) * | 2020-12-01 | 2021-03-26 | 张�杰 | Antibacterial paper diaper and production process thereof |
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Application publication date: 20190423 |