CN109652187A - A kind of water-base cutting fluid and preparation method thereof - Google Patents

A kind of water-base cutting fluid and preparation method thereof Download PDF

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Publication number
CN109652187A
CN109652187A CN201910024381.XA CN201910024381A CN109652187A CN 109652187 A CN109652187 A CN 109652187A CN 201910024381 A CN201910024381 A CN 201910024381A CN 109652187 A CN109652187 A CN 109652187A
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Prior art keywords
parts
water
cutting fluid
base cutting
dimethicone
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CN201910024381.XA
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Chinese (zh)
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唐鹏飞
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Hunan Jintai Inspection & Inspection Co Ltd
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Hunan Jintai Inspection & Inspection Co Ltd
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Priority to CN201910024381.XA priority Critical patent/CN109652187A/en
Publication of CN109652187A publication Critical patent/CN109652187A/en
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M173/00—Lubricating compositions containing more than 10% water
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/16—Paraffin waxes; Petrolatum, e.g. slack wax
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C10M2207/127—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids polycarboxylic
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C10M2209/104—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing two carbon atoms only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/08—Amides
    • C10M2215/082—Amides containing hydroxyl groups; Alkoxylated derivatives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/22—Heterocyclic nitrogen compounds
    • C10M2215/223—Five-membered rings containing nitrogen and carbon only
    • C10M2215/224—Imidazoles
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04—Phosphate esters
    • C10M2223/045—Metal containing thio derivatives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/041—Siloxanes with specific structure containing aliphatic substituents
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/64—Environmental friendly compositions
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working
    • C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

A kind of water-base cutting fluid, by weight, including following components: 8-10 parts of triethanolamine oleate；4-6 parts of calcium dodecyl benzene sulfonate；2-3 parts of polyethylene glycol；15-25 parts of paraffin oil；30-40 parts of deionized water；7-9 parts of zinc dialkyl dithiophosphate；5-6 parts of dodecenylsuccinic acid；2-3 parts of cation moiety corrosion inhibiter of N- alkyl benzimidazole；0.5-1 parts of dimethicone.The method for preparing above-mentioned water-base cutting fluid, the following steps are included: triethanolamine oleate, calcium dodecyl benzene sulfonate, paraffin oil, dimethicone are added in deionized water, unlatching is stirred and heated to 70-74 DEG C, 2h is cooled to room temperature later, then zinc dialkyl dithiophosphate, dodecenylsuccinic acid, N- alkyl benzimidazole cation moiety corrosion inhibiter is added, continues to stir 70-110min up to water-base cutting fluid.Water-base cutting fluid in the present invention is free of nitrite, carboxaldehyde radicals, the chlorinated paraffin being harmful to the human body, and rustless property, abrasion resistance, extreme pressure property are more excellent, has extremely wide application prospect.

Description

A kind of water-base cutting fluid and preparation method thereof
Technical field
The present invention relates to a kind of cutting fluid, in particular to a kind of water-base cutting fluid and preparation method thereof.
Background technique
Cutting fluid is a kind of liquid for intermetallic composite coating, it has the functions such as cooling, lubrication, antirust, cleaning, can be improved Machining accuracy, reduction tool wear etc., are metal and its alloy in the various machinings such as cutting, grinding, punching press, rolling and drawing Necessity in the process.
Cutting fluid can be divided into oil type and aqua type according to composition and medium, and wherein the starting of oil type cutting fluid is more early, Through more mature, and water-base cutting fluid starting relatively late, performance is not excellent enough, and containing be harmful to the human body nitrite, Carboxaldehyde radicals and chlorinated paraffin are easy to be detrimental to health.With country to the reinforcement of environmental requirement and people to inherently safe Attention, green water-base cutting fluid become development inexorable trend.Since water-base cutting fluid is metal cutting, grinds in process As cooling and lubrication cutter and workpiece industrial type fluid, therefore it must have preferable rustless property and extreme pressure property Energy.And although existing most water-base cutting fluid has good abrasion resistance, its rustless property and extreme pressure property are but owed It is good, so that the requirement of practical application be not achieved.
Summary of the invention
The technical problem to be solved in the present invention is that providing a kind of with the water base of excellent rustless property and extreme pressure property Cutting fluid.
To solve the above-mentioned problems, using following technical scheme: a kind of water-base cutting fluid, by weight, including it is following Component: 8-10 parts of triethanolamine oleate；4-6 parts of calcium dodecyl benzene sulfonate；2-3 parts of polyethylene glycol；15-25 parts of paraffin oil；It goes 30-40 parts of ionized water；7-9 parts of zinc dialkyl dithiophosphate；5-6 parts of dodecenylsuccinic acid；N- alkyl benzimidazole quinoline sun 2-3 parts of ion corrosion inhibiter；0.5-1 parts of dimethicone.
Preferably, above-mentioned water-base cutting fluid includes following components: 9 parts of triethanolamine oleate；Calcium dodecyl benzene sulfonate 5 Part；2.5 parts of polyethylene glycol；20 parts of paraffin oil；35 parts of deionized water；8 parts of zinc dialkyl dithiophosphate；Dodecenylsuccinic acid 5.5 part；2.5 parts of corrosion inhibiter of N- alkyl benzimidazole cation moiety；0.75 part of dimethicone.
The method for preparing above-mentioned water-base cutting fluid, comprising the following steps: by triethanolamine oleate, dodecyl benzene sulfonic acid Calcium, polyethylene glycol, paraffin oil, dimethicone are added in deionized water, and unlatching is stirred and heated to 70-74 DEG C, and 2h is later cold But to room temperature, zinc dialkyl dithiophosphate, dodecenylsuccinic acid, N- alkyl benzimidazole cation moiety inhibition is then added Agent continues 70-110min of stirring up to water-base cutting fluid.
Compared to the prior art, the invention has the following advantages: the water-base cutting fluid in the present invention is relative to tradition The component of cutting fluid, it is more environmentally protective without the nitrite, carboxaldehyde radicals, chlorinated paraffin being harmful to the human body, and various components After compounding according to a certain percentage, the rustless property of the water-base cutting fluid being finally prepared, abrasion resistance, extreme pressure property are more It is excellent, there is extremely wide application prospect.
Specific embodiment
Embodiment is given below so that the present invention to be specifically described, it is necessary to which indicated herein is following embodiment It is used to further illustrate the present invention, should not be understood as limiting the scope of the invention, the ordinary skill in the field Personnel still fall within protection scope of the present invention to some nonessential improvement of the invention made or adjustment according to this embodiment.
Embodiment 1
A kind of water-base cutting fluid, by weight, including following components: 8 parts of triethanolamine oleate；Calcium dodecyl benzene sulfonate 4 Part；2 parts of polyethylene glycol；15 parts of paraffin oil；30 parts of deionized water；7 parts of zinc dialkyl dithiophosphate；Dodecenylsuccinic acid 5 Part；2 parts of corrosion inhibiter of N- alkyl benzimidazole cation moiety；0.5 part of dimethicone.
Above-mentioned water-base cutting fluid the preparation method is as follows: by triethanolamine oleate, calcium dodecyl benzene sulfonate, poly- second two Alcohol, paraffin oil, dimethicone are added in deionized water, and unlatching is stirred and heated to 70-74 DEG C, and 2h is cooled to room temperature later, Then zinc dialkyl dithiophosphate, dodecenylsuccinic acid, N- alkyl benzimidazole cation moiety corrosion inhibiter is added, continues to stir 90min is mixed up to water-base cutting fluid.
Embodiment 2
A kind of water-base cutting fluid, by weight, including following components: 10 parts of triethanolamine oleate；Calcium dodecyl benzene sulfonate 6 Part；3 parts of polyethylene glycol；25 parts of paraffin oil；40 parts of deionized water；9 parts of zinc dialkyl dithiophosphate；Dodecenylsuccinic acid 6 Part；3 parts of corrosion inhibiter of N- alkyl benzimidazole cation moiety；1 part of dimethicone.
Above-mentioned water-base cutting fluid the preparation method is as follows: by triethanolamine oleate, calcium dodecyl benzene sulfonate, poly- second two Alcohol, paraffin oil, dimethicone are added in deionized water, and unlatching is stirred and heated to 70-74 DEG C, and 2h is cooled to room temperature later, Then zinc dialkyl dithiophosphate, dodecenylsuccinic acid, N- alkyl benzimidazole cation moiety corrosion inhibiter is added, continues to stir 90min is mixed up to water-base cutting fluid.
Embodiment 3
A kind of water-base cutting fluid, by weight, including following components: 9 parts of triethanolamine oleate；Calcium dodecyl benzene sulfonate 5 Part；2.5 parts of polyethylene glycol；20 parts of paraffin oil；35 parts of deionized water；8 parts of zinc dialkyl dithiophosphate；Dodecenylsuccinic acid 5.5 part；2.5 parts of corrosion inhibiter of N- alkyl benzimidazole cation moiety；0.75 part of dimethicone.
Above-mentioned water-base cutting fluid the preparation method is as follows: by triethanolamine oleate, calcium dodecyl benzene sulfonate, poly- second two Alcohol, paraffin oil, dimethicone are added in deionized water, and unlatching is stirred and heated to 70-74 DEG C, and 2h is cooled to room temperature later, Then zinc dialkyl dithiophosphate, dodecenylsuccinic acid, N- alkyl benzimidazole cation moiety corrosion inhibiter is added, continues to stir 90min is mixed up to water-base cutting fluid.
Performance data test method:
1) the water-base cutting fluid sample being prepared is taken, carries out four balls experiment test its extreme pressure value P using four-ball testerB。
2) take the water-base cutting fluid sample being prepared, using four-ball tester carry out four balls experiment test its room temperature, Wear scar diameter under the conditions of 1450 revs/min of the speed of mainshaft, load 519N.
3) the water-base cutting fluid sample being prepared is taken, coating records it and open to iron plate outer surface at being 25 DEG C in temperature Begin the time got rusty.
The performance data test result of water-base cutting fluid in above-described embodiment 1-3 is recorded into the following table 1.
By upper table 1 it is found that the extreme pressure property P of the water-base cutting fluid in the present inventionBTest result can reach 870N or more, wear Spot diameter can reach 0.26mm hereinafter, the antirust duration can reach 43h or more, extreme pressure property, abrasion resistance and antirust Performance is more excellent.

Claims (3)

1. a kind of water-base cutting fluid, which is characterized in that by weight, including following components: 8-10 parts of triethanolamine oleate；Ten 4-6 parts of dialkyl benzene sulfonic acids calcium；2-3 parts of polyethylene glycol；15-25 parts of paraffin oil；30-40 parts of deionized water；Dialkyl dithio 7-9 parts of trbasic zinc phosphate；5-6 parts of dodecenylsuccinic acid；2-3 parts of cation moiety corrosion inhibiter of N- alkyl benzimidazole；Dimethicone 0.5-1 parts.
2. water-base cutting fluid according to claim 1, which is characterized in that including following components: 9 parts of triethanolamine oleate； 5 parts of calcium dodecyl benzene sulfonate；2.5 parts of polyethylene glycol；20 parts of paraffin oil；35 parts of deionized water；Zinc dialkyl dithiophosphate 8 Part；5.5 parts of dodecenylsuccinic acid；2.5 parts of corrosion inhibiter of N- alkyl benzimidazole cation moiety；0.75 part of dimethicone.
3. the method for preparing water-base cutting fluid of any of claims 1 or 2, which comprises the following steps: by oleic acid three Ethanol amine, calcium dodecyl benzene sulfonate, polyethylene glycol, paraffin oil, dimethicone are added in deionized water, open and stir and add To 70-74 DEG C, 2h is cooled to room temperature heat later, and zinc dialkyl dithiophosphate, dodecenylsuccinic acid, N- alkyl is then added Benzimidazole cation moiety corrosion inhibiter continues 70-110min of stirring up to water-base cutting fluid.
CN201910024381.XA 2019-01-10 2019-01-10 A kind of water-base cutting fluid and preparation method thereof Pending CN109652187A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115637189A (en) * 2022-11-14 2023-01-24 俄美达（武汉）有限公司 Preparation method of magnesium alloy cutting fluid based on porous carbon material

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115637189A (en) * 2022-11-14 2023-01-24 俄美达（武汉）有限公司 Preparation method of magnesium alloy cutting fluid based on porous carbon material
CN115637189B (en) * 2022-11-14 2023-08-29 俄美达（武汉）有限公司 Preparation method of magnesium alloy cutting fluid based on porous carbon material

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Application publication date: 20190419