CN109628209A - A kind of tea seed essence production technology - Google Patents
A kind of tea seed essence production technology Download PDFInfo
- Publication number
- CN109628209A CN109628209A CN201910010123.6A CN201910010123A CN109628209A CN 109628209 A CN109628209 A CN 109628209A CN 201910010123 A CN201910010123 A CN 201910010123A CN 109628209 A CN109628209 A CN 109628209A
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- CN
- China
- Prior art keywords
- tea seed
- long
- tube evaporator
- extraction
- production technology
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/006—Refining fats or fatty oils by extraction
Abstract
The invention discloses a kind of tea seed essence production technologies, methanol loop extraction including leached tea oil slag, precipitation Methanol Recovery, the drying of dregs of rice slag, the evaporation of the first long-tube evaporator, the evaporation of second long-tube evaporator, the concentration of multiple groups single-effect concentrator adds Kathon CG to get smart to tea seed, first long-tube evaporator, the second long-tube evaporator, multiple groups single-effect concentrator, desolventizing machine and dryer are energized using steam boiler, and steam boiler generates steam and carries out condensed water water circulation through condenser, cooling tower, circulating water pool.The tea seed essence production technology, the addition of Kathon CG solves the problems, such as that carbon dioxide generation causes flatulence, it can prevent albumen and polysaccharide from fermenting under the action of alien bacteria and lead to the problem of carbon dioxide, environmental protection and public nuisance free, meets the requirement of environmental protection production, and leftover bits and pieces drying is used as biological organic fertilizer, realize resource saving with recycle, entire production process, link is complete, can be used with popularity.
Description
Technical field
The invention belongs to tea seed processing technique fields, and in particular to a kind of tea seed essence production technology.
Background technique
China is the maximum country of tea-oil tree yield, there are about 3,670,000 hectares of oil tea resource, produces 64.5 ten thousand tons of oil tea seed per year.
Tea seed essence is present in tea seed and squeezes except the tea seed grouts that in residual residue cake of camellia oleifera seeds, annual 400000 tons or so of China after grease
It is thrown away, a considerable amount of tea seed essence is discarded, and causes greatly to waste.
Tea seed essence is jolted and is shaken, be easy to produce carbon dioxide due to long-distance transportation, and flatulence, existing tea seed essence are caused
Production in material utilization it is lower, there is pollution in production process, sustainable productivity is lower.
Summary of the invention
The purpose of the present invention is to provide a kind of tea seed essence production technologies, to solve mentioned above in the background art ask
Topic.
To achieve the above object, the invention provides the following technical scheme: a kind of tea seed essence production technology, including following step
It is rapid:
S1, leached tea oil slag is crushed, smashed leached tea oil slag powder is put into infuser, is extracted with methanol, uses dish
After piece centrifuge isolates tea grounds, extraction mixed liquor is obtained;
The wet dregs of rice are delivered in desolventizing machine through wet dregs of rice scraper plate pipeline in S2, infuser, and prolapse solvent is sent into condenser, are then sent
Enter Methanol Recovery week stock relocation carry out Methanol Recovery, Methanol Recovery week stock relocation communicated with methanol library, dregs of rice slag through the dregs of rice slag pipeline entrance
It is dried in dryer;
S3, mixed liquor is extracted in infuser when reaching 5 Baume degrees, filtered twice, be re-fed into the first long-tube evaporator and steam
Hair, until the evaporation of the second long-tube evaporator is re-fed into when 8 Baume degrees, until 12 Baume degrees, are re-fed into multiple groups single-effect concentrator and carry out
Concentration, is concentrated into 25 to 26 Baume degrees;
S4, after being concentrated by multiple groups single-effect concentrator, it is sent into hold-up tank, 0.3% Kathon CG is added to get smart to tea seed.
Preferably, it is 90% that extraction methanol concentration is carried out in step S1, and extraction is heated to reflux in 50 DEG C of hot bath
3-4h。
Preferably, the first long-tube evaporator operating pressure is 0.4-0.5mpa in step S3, and extraction mixeding liquid temperature is 90-
100 degree.
Preferably, the second long-tube evaporator operating pressure is 0.3 to 0.4mpa in step S3, and extraction mixeding liquid temperature is 85
To 95 degree.
Preferably, multiple groups single-effect concentrator operating pressure is 0.1-0.2mpa in step S3, and extraction mixeding liquid temperature is 80-
90 degree.
Preferably, the first long-tube evaporator, the second long-tube evaporator, multiple groups single-effect concentrator, desolventizing machine and dryer make
It is energized with steam boiler, steam boiler generates steam and carries out condensed water water circulation through condenser, cooling tower, circulating water pool.
Technical effect and advantage of the invention: the tea seed essence production technology, the addition of Kathon CG are solved since long range is transported
It is defeated, it jolts and shakes, make the vegetable protein and polysaccharide in tea seed essence, generate carbon dioxide under force, cause flatulence
Problem, can also play prevents albumen and polysaccharide from fermenting under the action of alien bacteria and leading to the problem of carbon dioxide, environmental protection
Nuisanceless, no chemical reaction is generated with waste water, obtains steam by biomass fuel, meets the requirement of environmental protection production, technique
Leftover bits and pieces after precipitation, drying are used as biological organic fertilizer, realize the saving of resource and recycle, entire production process, chain
It connects completely, can be used with popularity.
Detailed description of the invention
Fig. 1 is process flow chart of the invention.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
The present invention provides a kind of tea seed essence production technologies as shown in Figure 1, comprising the following steps:
S1, leached tea oil slag is crushed, smashed leached tea oil slag powder is put into infuser (can also wherein contain a small amount of straw), is used
Methanol is extracted, extraction with methanol concentration be 90%, be heated to reflux in 50 DEG C of hot bath extraction 3-4h, using disk from
After tea grounds is isolated in scheming, extraction mixed liquor is obtained;
The wet dregs of rice are delivered in desolventizing machine through wet dregs of rice scraper plate pipeline in S2, infuser, and prolapse solvent is sent into condenser, are then sent
Enter Methanol Recovery week stock relocation and carry out Methanol Recovery, Methanol Recovery technology is more mature, Methanol Recovery week stock relocation and methanol library
It communicates, dregs of rice slag enters in dryer through dregs of rice slag pipeline is dried, and the leftover bits and pieces after precipitation may be used as giving birth to after drying
Organic fertilizer is the first-class organic fertilizer of nuisanceless and organic agricultural fruits and vegetables;
S3, mixed liquor is extracted in infuser when reaching 5 Baume degrees, filtered twice, be re-fed into the first long-tube evaporator and steam
Hair, the first long-tube evaporator operating pressure are 0.4-0.5mpa, and extraction mixeding liquid temperature is 90-100 degree, until when 8 Baume degrees, then
It is sent into the evaporation of the second long-tube evaporator, the second long-tube evaporator operating pressure is 0.3 to 0.4mpa, and extraction mixeding liquid temperature is 85
To 95 degree, until 12 Baume degrees, are re-fed into multiple groups single-effect concentrator and are concentrated, multiple groups single-effect concentrator operating pressure is 0.1-
0.2mpa, extraction mixeding liquid temperature are 80-90 degree, are concentrated into 25 to 26 Baume degrees;
S4, after being concentrated by multiple groups single-effect concentrator, it is sent into hold-up tank, 0.3% Kathon CG is added to get to tea seed essence, adds
Add Kathon CG mainly to solve to jolt and shake due to long-distance transportation, makes the vegetable protein and polysaccharide in tea seed essence, in the work of power
With lower generation carbon dioxide, the problem of causing flatulence, a small amount of Kathon CG is added, effectively inhibits the generation of carbon dioxide, can also rise
Carbon dioxide is generated to preventing albumen and polysaccharide from generating physical change (commonly referred to as ferment) under the action of alien bacteria.
Specifically, the first long-tube evaporator, the second long-tube evaporator, multiple groups single-effect concentrator, desolventizing machine and dryer make
It is energized with steam boiler, obtains steam with biomass fuel, follow green, environmental protection, non-harmful production theory, steam
Boiler generates steam and carries out condensed water water circulation through condenser, cooling tower, circulating water pool.
Finally, it should be noted that the foregoing is only a preferred embodiment of the present invention, it is not intended to restrict the invention,
Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still may be used
To modify the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features,
All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in of the invention
Within protection scope.
Claims (6)
1. a kind of tea seed essence production technology, it is characterised in that: the following steps are included:
Leached tea oil slag is crushed, leached tea oil slag powder is put into infuser, is extracted with methanol, is separated using disk plate centrifuge
Out after tea grounds, extraction mixed liquor is obtained;
The wet dregs of rice are delivered in desolventizing machine through wet dregs of rice scraper plate pipeline in infuser, and prolapse solvent is sent into condenser, are subsequently sent to
Methanol Recovery week stock relocation carry out Methanol Recovery, Methanol Recovery week stock relocation communicated with methanol library, dregs of rice slag enters baking through dregs of rice slag pipeline
It is dried in dry machine;
It when extraction mixed liquor reaches 5 Baume degrees in infuser, is filtered twice, is re-fed into the evaporation of the first long-tube evaporator,
When to 8 Baume degrees, be re-fed into the evaporation of the second long-tube evaporator, until 12 Baume degrees, be re-fed into multiple groups single-effect concentrator carry out it is dense
Contracting, is concentrated into 25 to 26 Baume degrees;
After being concentrated by multiple groups single-effect concentrator, it is sent into hold-up tank, 0.3% Kathon CG is added to get smart to tea seed.
2. a kind of tea seed essence production technology according to claim 1, it is characterised in that: carry out extraction methanol in step S1
Concentration is 90%, and extraction 3-4h is heated to reflux in 50 DEG C of hot bath.
3. a kind of tea seed essence production technology according to claim 1, it is characterised in that: the first long-tube evaporator in step S3
Operating pressure is 0.4-0.5mpa, and extraction mixeding liquid temperature is 90-100 degree.
4. a kind of tea seed essence production technology according to claim 1, it is characterised in that: the second long-tube evaporator in step S3
Operating pressure is 0.3 to 0.4mpa, and extraction mixeding liquid temperature is 85 to 95 degree.
5. a kind of tea seed essence production technology according to claim 1, it is characterised in that: multiple groups single-effect concentrator in step S3
Operating pressure is 0.1-0.2mpa, and extraction mixeding liquid temperature is 80-90 degree.
6. a kind of tea seed essence production technology according to claim 1, it is characterised in that: the first long-tube evaporator, the second length
Pipe evaporator, multiple groups single-effect concentrator, desolventizing machine and dryer are energized using steam boiler, and steam boiler generates steam warp
Condenser, cooling tower, circulating water pool carry out condensed water water circulation.
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CN201910010123.6A CN109628209A (en) | 2019-01-07 | 2019-01-07 | A kind of tea seed essence production technology |
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CN201910010123.6A CN109628209A (en) | 2019-01-07 | 2019-01-07 | A kind of tea seed essence production technology |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111620925A (en) * | 2020-07-03 | 2020-09-04 | 蒋文昌 | Method for preparing tea saponin by continuous pipeline type ultrasonic wave |
CN111892640A (en) * | 2020-08-14 | 2020-11-06 | 蒋文昌 | Continuous pipeline type countercurrent extraction method for tea saponin |
Citations (8)
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CN201695016U (en) * | 2010-05-12 | 2011-01-05 | 黄山市徽山食用油业有限公司 | Tea seed oil leaching system in oil tea seed cake |
CN102002089A (en) * | 2010-11-12 | 2011-04-06 | 安徽映山红生物科技有限公司 | Process for extracting tea saponin from tea seed cakes or meal |
CN103031199A (en) * | 2012-12-03 | 2013-04-10 | 郭少海 | Desolventizing and drying method for camellia seed extract |
CN104531384A (en) * | 2015-01-09 | 2015-04-22 | 湖南新金浩茶油股份有限公司 | Tea saponin anti-bacterial detergent and preparing method thereof |
CN104629900A (en) * | 2015-01-28 | 2015-05-20 | 安徽嘉旗粮油工程技术有限公司 | Production method of synchronously extracting tea-seed oil and tea saponin from tea seed cakes |
CN105461780A (en) * | 2015-12-09 | 2016-04-06 | 中国林业科学研究院亚热带林业研究所 | Low-cost, efficient and continuous tea saponin extraction process |
CN106367216A (en) * | 2016-08-26 | 2017-02-01 | 华侨大学 | Tea saponin liquid detergent |
CN106565812A (en) * | 2016-09-26 | 2017-04-19 | 中国林业科学研究院亚热带林业研究所 | Efficient recovery process for tea saponin continuous extraction solvent |
-
2019
- 2019-01-07 CN CN201910010123.6A patent/CN109628209A/en active Pending
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN201695016U (en) * | 2010-05-12 | 2011-01-05 | 黄山市徽山食用油业有限公司 | Tea seed oil leaching system in oil tea seed cake |
CN102002089A (en) * | 2010-11-12 | 2011-04-06 | 安徽映山红生物科技有限公司 | Process for extracting tea saponin from tea seed cakes or meal |
CN103031199A (en) * | 2012-12-03 | 2013-04-10 | 郭少海 | Desolventizing and drying method for camellia seed extract |
CN104531384A (en) * | 2015-01-09 | 2015-04-22 | 湖南新金浩茶油股份有限公司 | Tea saponin anti-bacterial detergent and preparing method thereof |
CN104629900A (en) * | 2015-01-28 | 2015-05-20 | 安徽嘉旗粮油工程技术有限公司 | Production method of synchronously extracting tea-seed oil and tea saponin from tea seed cakes |
CN105461780A (en) * | 2015-12-09 | 2016-04-06 | 中国林业科学研究院亚热带林业研究所 | Low-cost, efficient and continuous tea saponin extraction process |
CN106367216A (en) * | 2016-08-26 | 2017-02-01 | 华侨大学 | Tea saponin liquid detergent |
CN106565812A (en) * | 2016-09-26 | 2017-04-19 | 中国林业科学研究院亚热带林业研究所 | Efficient recovery process for tea saponin continuous extraction solvent |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111620925A (en) * | 2020-07-03 | 2020-09-04 | 蒋文昌 | Method for preparing tea saponin by continuous pipeline type ultrasonic wave |
CN111892640A (en) * | 2020-08-14 | 2020-11-06 | 蒋文昌 | Continuous pipeline type countercurrent extraction method for tea saponin |
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Application publication date: 20190416 |
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