CN109609892A - A kind of heat treatment process of automobile club - Google Patents
A kind of heat treatment process of automobile club Download PDFInfo
- Publication number
- CN109609892A CN109609892A CN201811596377.2A CN201811596377A CN109609892A CN 109609892 A CN109609892 A CN 109609892A CN 201811596377 A CN201811596377 A CN 201811596377A CN 109609892 A CN109609892 A CN 109609892A
- Authority
- CN
- China
- Prior art keywords
- furnace
- automobile club
- carburizing
- automobile
- heat treatment
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C8/00—Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C8/06—Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using gases
- C23C8/08—Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using gases only one element being applied
- C23C8/20—Carburising
- C23C8/22—Carburising of ferrous surfaces
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D1/00—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
- C21D1/18—Hardening; Quenching with or without subsequent tempering
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D1/00—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
- C21D1/68—Temporary coatings or embedding materials applied before or during heat treatment
- C21D1/70—Temporary coatings or embedding materials applied before or during heat treatment while heating or quenching
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D1/00—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
- C21D1/74—Methods of treatment in inert gas, controlled atmosphere, vacuum or pulverulent material
- C21D1/773—Methods of treatment in inert gas, controlled atmosphere, vacuum or pulverulent material under reduced pressure or vacuum
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D9/00—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
- C21D9/0075—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for rods of limited length
Abstract
The present invention relates to a kind of heat treatment process of automobile club comprising automobile club is placed in furnace by shove charge step;Temperature in furnace is increased to 860-880 DEG C, and keeps 100min by quenching Step;Carburization step, towards furnace in be added dropwise methanol solution, including a carburizing, the 10-50min of soaking time section after in-furnace temperature is increased to 860-880 DEG C, the time of carburizing is 25-30min;Secondary carburizing, the 50-75min of soaking time section, carburizing time 15-20min;Carburizing three times, the 75-90min of soaking time section, carburizing time 8-10min;It is quickly cooled down step, automobile club is placed in the quenching oil that oil temperature is 70 DEG C and is cooled down;Cleaning step cleans the quenching oil on automobile club;Tempering step reapposes automobile club in furnace, and the temperature in furnace is increased to 560-580 DEG C and keeps 120min;Automobile club is taken out and is cooled to room temperature out of furnace by cooling step.The invention can ensure that the carbon in methanol can sufficiently be merged with automobile club, be conducive to the structural strength for improving automobile club.
Description
Technical field
The present invention relates to the technical fields of automobile club, more particularly, to a kind of heat treatment process of automobile club.
Background technique
Automobile club is located in the steering system of automobile, plays connection, steering-effecting, and automobile club in the production process, needs
By raw material by blanking, forge, be heat-treated and be shaped to corresponding product after machine adds, in the whole process, raw material is formed
Heat treatment process in the process is particularly important.
Existing automobile club heat treatment process such as publication No. is a kind of heat treatment of automobile club of CN104088891A
Technique Chinese invention patent, it discloses a kind of heat treatment process automobile connecting bar of automobile club and its heat treatment processes, including
The process of ontology and heat treatment, the ontology are set as cylindrical structure, and outer ring middle section is set as circle hole shape, wound form
Spring structure, heat treatment process include it is carried out quenching plus average tempering, to obtain secondary troostite tissue, process
In be that should guarantee abundant austenitizing to the selection of hardening heat, keep thinner crystal grain again, crystal grain refinement can be mentioned significantly
The impact value of high spring steel the carbonitride of trace alloying element is added into steel, in heat to develop high-strength spring steel
Can be with fining austenite grains in treatment process, while also can produce precipitation strength effect, finally made annealing treatment.
Prior art among the above have the following deficiencies: due to automobile club play the role of in the car it is larger,
Therefore higher for the hardness requirement needs of automobile club itself, it needs to improve during heat treatment carbon containing in automobile club
Amount, but in above-mentioned automobile connecting bar heat treatment process, it is only merely the carbonitride for being quenched, and adding to automobile club
Also only it is merely the enhancing to spring steel structural strength, and then easily leads to the strength reduction of automobile club.
Summary of the invention
The object of the present invention is to provide a kind of heat treatment process of automobile club, to improve automobile club after heat treatment
Structural strength.
Foregoing invention purpose of the invention has the technical scheme that a kind of heat treatment of automobile club
Technique, comprising:
Step S1: shove charge step stacks automobile club on bracket and being successively placed in furnace;
Step S2: quenching Step, to carrying out heat temperature raising in furnace, so that the temperature in furnace is increased to 860-880 DEG C, and
100min is kept in 860-880 DEG C;
Step S3: carburization step, towards furnace in methanol solution, including a carburizing is added dropwise, be increased to 860- in in-furnace temperature
The 10-50min of soaking time section after 880 DEG C, the time of carburizing are 25-30min;Secondary carburizing, the 50- of soaking time section
75min, carburizing time 15-20min;Carburizing three times, the 75-90min of soaking time section, carburizing time 8-10min;
Step S4: being quickly cooled down step, by automobile club from being removed and placed in furnace in oil temperature in 70 DEG C of quenching oil
It is cooled down;
Step S5: cleaning step cleans the quenching oil on automobile club;
Step S6: tempering step reapposes automobile club in furnace, and to heat temperature raising is carried out in furnace, so that in furnace
Temperature be increased to keep 120min in 560-580 DEG C;
Step S7: automobile club is taken out and is cooled to room temperature out of furnace by cooling step.
By using above-mentioned technical proposal, when being heat-treated to automobile club, first automobile club is placed in furnace and incited somebody to action
In-furnace temperature is heated to 860-880 DEG C and continues 100min, during this lasting, by the way that methanol is added dropwise to automobile club
Solution carries out three times, the carburizing time of first time is most respectively as the carburizer to automobile club, and during dropwise addition
It is long, the automobile club not through over carburizing is rapidly entered when touching carbon, then twice the time by
Gradually successively decrease, so that the carbon in automobile club progressivelyes reach corresponding saturation state, later using being quickly cooled down and subsequent
Tempering step, and then can guarantee methanol in carbon can sufficiently be merged with automobile club, be conducive to improve automobile club
Structural strength.
The present invention is further arranged to: in the step S3, dissolved with tall oil fatty acid solution, methanol in the methanol of dropwise addition
Be 40:1-50:1 with the mass ratio of tall oil fatty acid solution, and in carburizing process methanol and tall oil fatty acid solution it is mixed
Conjunction solution rate of addition is 55-60mL/min.
By using above-mentioned technical proposal, by dissolving in tall oil fatty acid solution according to a certain percentage in methyl alcohol
Afterwards, the liveness of carbon in methanol can be improved, so that methanol can quickly be incorporated into automobile club when contacting automobile club,
To improve the carburizing efficiency of automobile club.
The present invention is further arranged to: in the step S3, carburizing depth 0.15-0.4mm.
By using above-mentioned technical proposal, during carrying out carburizing to automobile club, the depth of corresponding carburizing needs
Stringent control excessively easily leads to automobile club and becomes fragile, and very few to easily lead to carburizing effect poor, it usually needs holds carburizing depth
Between 0.15-0.4mm, so that carbon and the fusion of automobile club are best, be conducive to the intensity for improving automobile club.
The present invention is further arranged to: in the step S4, the quenching oil uses 109B quenching oil, and where quenching oil
Oil groove in be provided with blender, the blender is stirred the quenching oil in oil groove.
By using above-mentioned technical proposal, cooled down by using the 109B quenching oil for corresponding to automobile club, to add
Fastly to the cooling velocity of automobile club, and in cooling procedure, setting blender can be stirred quenching oil in oil groove, to add
The heat dissipation of fast quenching oil itself, and then quenching oil can be accelerated to the heat absorption of automobile club, to accelerate to the cold of automobile club
But speed.
The present invention is further arranged to: in the step S5, including cleaning agent cleaning step, clear water cleaning step and drying
Step, the cleaning agent in the cleaning agent cleaning step are that non-phosphor degreaser powder is mixed with water according to mass ratio 1:20-1:25
Solution.
By using above-mentioned technical proposal, automobile club is cleaned using non-phosphor degreaser amidin, may make automobile club
Quenching oil remained on surface is dissolved in into the solution, to accelerate the cleaning speed to quenching oil, improves the cleaning effect of automobile club
In addition rate easily removes remaining non-phosphor degreaser amidin on automobile club by washing away for water again.
The present invention is further arranged to: in the step S5, automobile club being placed in rinse bath and is cleaned, and cleaned
Multilayer spray pipe is set in slot, and every layer of injection pipe is uniformly arranged along the circumferential direction of rinse bath.
By using above-mentioned technical proposal, by the way that the injection pipe of multilayer is arranged, and every layer of injection pipe is uniformly arranged, so that right
Club can quickly clean each automobile club during jet cleaning, improve the efficiency of cleaning.
The present invention is further arranged to: in the step S6, automobile club being submerged initially in the 5- into benzotriazole solution
7min, benzotriazole solution mixed using benzotriazole crystal and 40-50 DEG C of hot water according to mass ratio 1:450-1:480 and
At, then be tempered.
By using above-mentioned technical proposal, benzotriazole solution, can be in metal material during contacting with metal material
Expect that surface forms one layer of polyphenoils, automobile club be introduced into benzotriazole solution to form corresponding polyphenoils,
To reduce the oxidation of automobile club face, and benzotriazole will do it decomposition in thermal histories, and then carry out to automobile club
It can avoid the residual of benzotriazole when tempering.
The present invention is further arranged to: in the step S7, including natural cooling step, vacuum cooled step, it is described from
In right cooling step, stop to the heating in furnace, so that in-furnace temperature slowly cools to 480-500 DEG C, the vacuum cooled step
In rapid, the automobile club after natural cooling is cooled to room temperature from removing and placing in furnace in vacuum environment.
By using above-mentioned technical proposal, during naturally cooling to 480-500 DEG C, due to the presence of furnace high-temperature,
Automobile club, which can be reduced, terminates the oxidation of rear surface in tempering, places in vacuum automobile club cool down later, with isolation
Oxygen in automobile club and air, and then can avoid oxidation of automobile club during being cooled to room temperature.
In conclusion advantageous effects of the invention are as follows:
It by the way that methanol is added dropwise to the automobile club after heating, and carries out respectively three times, the carburizing time longest of first time makes
Obtaining the automobile club not through over carburizing can rapidly enter when touching carbon, and then the time gradually passs twice
Subtract, enable the carbon in automobile club to progressively reach corresponding saturation state so that can guarantee the carbon in methanol with
Automobile club sufficiently merges, and is conducive to the structural strength for improving automobile club.
Detailed description of the invention
Fig. 1 is overall flow schematic diagram of the invention.
Specific embodiment
Below in conjunction with attached drawing, invention is further described in detail.
Referring to Fig.1, it is a kind of heat treatment process of automobile club disclosed by the invention, including step S1: shove charge step, it will
Automobile club is stacked on bracket and being successively placed in glowing furnace.
Step S2: quenching Step is internally heated heating to glowing furnace, so that the temperature in furnace is increased to 860-880
DEG C, it is preferably 870 DEG C in the present embodiment, and 100min is kept in 860-880 DEG C.
Step S3: carburization step, including a carburizing, the soaking time section after in-furnace temperature is increased to 860-880 DEG C
10-50min, the time of carburizing are 25-30min;Secondary carburizing, the 50-75min of soaking time section, carburizing time 15-
20min;Carburizing three times, the 75-90min of soaking time section, carburizing time 8-10min;A carburizing in the present embodiment
Time is preferably 28min, and the time of secondary carburizing is preferably 17min, and the time of carburizing is preferably 9min three times.
In step S3, carburizer used in carburizing process is methanol solution, and in order to improve in automobile automobile club
Carburizing efficiency, dissolved with tall oil fatty acid solution in the methanol solution being added dropwise, and methanol and tall oil fatty acid solution
Mass ratio is 40:1-50:1, is preferably 1:45 in the present embodiment, the mixing of methanol and tall oil fatty acid solution in carburizing process
Solution rate of addition is 55-60mL/min, and needs to guarantee that carburizing depth is 0.15-0.4mm, wherein being maintained at 0.25mm is most
It is good.
Step S4: it is quickly cooled down step, automobile club is removed and placed out of furnace in oil groove, oil is first equipped in oil groove
The 109B quenching oil that temperature is 70 DEG C, so that automobile club is entered in quenching oil and is rapidly cooled, and to guarantee that quenching oil exists
During cooling down to automobile club, quenching oil itself is able to carry out cooling to absorb more heats, the slot bottom of oil groove
It is additionally provided with blender, is entered in quenching oil after 30min in club, starting blender is stirred quenching oil, accelerates to quench
The heat dissipation of kerosene itself.
Step S5: cleaning step, including cleaning agent cleaning step, clear water cleaning step and baking step, to automobile ball
Quenching oil on bar is cleaned, and is dried later to automobile club;Wherein cleaning agent used in cleaning agent cleaning step
It for the solution that non-phosphor degreaser powder is mixed with water according to mass ratio 1:20-1:25, and is best with mass ratio 1:23;In addition it is
Automobile club is adequately cleaned in guarantee, and automobile club is placed in rinse bath and is cleaned, and is arranged in rinse bath more
Layer injection pipe, three layers be preferably arranged at equal intervals in the present embodiment, and every layer of several injection pipes are along the circumferential direction side of rinse bath
To being uniformly arranged.
Step S6: automobile club is submerged initially in the 5-7min into benzotriazole solution by tempering step, and benzotriazole solution is adopted
It is mixed with 40-50 DEG C of hot water according to mass ratio 1:450-1:480 with benzotriazole crystal, and is with mass ratio 1:460
Most preferably, then by automobile club it is placed in tempering furnace, and to heat temperature raising is carried out in tempering furnace, so that the temperature in furnace is increased to
120min is kept in 560-580 DEG C.
Step S7: automobile club is taken out and is cooled to room temperature out of furnace by cooling step, and including natural cooling step,
Vacuum cooled step in natural cooling step, stops to the heating in tempering furnace, so that tempering in-furnace temperature slowly cools to
It is 480-500 DEG C, in vacuum cooled step, the automobile club after natural cooling is cold in vacuum environment from removing and placing in furnace
But to room temperature, to be further reduced the oxidation of automobile club face.
The embodiment of present embodiment is presently preferred embodiments of the present invention, not limits protection of the invention according to this
Range, therefore: the equivalence changes that all structures under this invention, shape, principle are done, should all be covered by protection scope of the present invention it
It is interior.
Claims (8)
1. a kind of heat treatment process of automobile club, it is characterised in that: include:
Step S1: shove charge step stacks automobile club on bracket and being successively placed in furnace;
Step S2: quenching Step, to heat temperature raising is carried out in furnace, so that the temperature in furnace is increased to 860-880 DEG C, and in 860-
100min is kept in 880 DEG C;
Step S3: carburization step, towards furnace in methanol solution, including a carburizing is added dropwise, be increased to 860-880 DEG C in in-furnace temperature
The 10-50min of soaking time section afterwards, the time of carburizing are 25-30min;Secondary carburizing, the 50- of soaking time section
75min, carburizing time 15-20min;Carburizing three times, the 75-90min of soaking time section, carburizing time 8-10min;
Step S4: being quickly cooled down step, from being removed and placed in furnace in oil temperature is to carry out in 70 DEG C of quenching oil by automobile club
It is cooling;
Step S5: cleaning step cleans the quenching oil on automobile club;
Step S6: tempering step reapposes automobile club in furnace, and to heat temperature raising is carried out in furnace, so that the temperature in furnace
Degree is increased to keep 120min in 560-580 DEG C;
Step S7: automobile club is taken out and is cooled to room temperature out of furnace by cooling step.
2. a kind of heat treatment process of automobile club according to claim 1, it is characterised in that: in the step S3, drop
Dissolved with tall oil fatty acid solution in the methanol added, the mass ratio of methanol and tall oil fatty acid solution is 40:1-50:1, and is seeped
The mixed solution rate of addition of methanol and tall oil fatty acid solution is 55-60mL/min during carbon.
3. a kind of heat treatment process of automobile club according to claim 2, it is characterised in that: in the step S3, seep
Carbon depth is 0.15-0.4mm.
4. a kind of heat treatment process of automobile club according to claim 1, it is characterised in that: in the step S4, institute
Quenching oil is stated using 109B quenching oil, and is provided with blender in the oil groove where quenching oil, the blender is in oil groove
Quenching oil is stirred.
5. a kind of heat treatment process of automobile club according to claim 1, it is characterised in that: in the step S5, packet
Cleaning agent cleaning step, clear water cleaning step and baking step are included, the cleaning agent in the cleaning agent cleaning step is without phosphorus de-
The solution that cosmetics is mixed with water according to mass ratio 1:20-1:25.
6. a kind of heat treatment process of automobile club according to claim 5, it is characterised in that:, will in the step S5
Automobile club, which is placed in rinse bath, to be cleaned, and multilayer spray pipe is arranged in rinse bath, and every layer of injection pipe is along rinse bath
Circumferential direction is uniformly arranged.
7. a kind of heat treatment process of automobile club according to claim 1, it is characterised in that:, will in the step S6
Automobile club is submerged initially in the 5-7min into benzotriazole solution, and benzotriazole solution is using benzotriazole crystal and 40-50 DEG C
Hot water is mixed according to mass ratio 1:450-1:480, then is tempered.
8. a kind of heat treatment process of automobile club according to claim 1, it is characterised in that: in the step S7, packet
It includes natural cooling step, vacuum cooled step, in the natural cooling step, stops to the heating in furnace, so that in-furnace temperature
It slowly cools to 480-500 DEG C, in the vacuum cooled step, the automobile club after natural cooling is removed and placed out of furnace
It is cooled to room temperature in vacuum environment.
Priority Applications (1)
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CN201811596377.2A CN109609892A (en) | 2018-12-25 | 2018-12-25 | A kind of heat treatment process of automobile club |
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CN201811596377.2A CN109609892A (en) | 2018-12-25 | 2018-12-25 | A kind of heat treatment process of automobile club |
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CN109609892A true CN109609892A (en) | 2019-04-12 |
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ID=66012454
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CN201811596377.2A Pending CN109609892A (en) | 2018-12-25 | 2018-12-25 | A kind of heat treatment process of automobile club |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110169667A (en) * | 2019-04-27 | 2019-08-27 | 临海市创宇工艺有限公司 | A kind of processing technology of rattan chair |
CN110240482A (en) * | 2019-06-13 | 2019-09-17 | 浙江永灵液压机械有限公司 | A kind of blade pump stator inner surface heat treatment process |
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CN102254629A (en) * | 2011-05-10 | 2011-11-23 | 浙江省浦江县百川产业有限公司 | Production technology of copper-clad steel wire in soft state |
CN104088891A (en) * | 2014-06-29 | 2014-10-08 | 奉化市飞天人精密模具设计有限公司 | Automobile connection rod and thermal treatment process thereof |
CN108676992A (en) * | 2018-06-25 | 2018-10-19 | 温岭市万泰热处理厂(普通合伙) | A kind of heat treatment process of output shaft |
CN108866309A (en) * | 2018-07-23 | 2018-11-23 | 台州市众达热处理有限公司 | The separator and its heat treatment process of gear sheet |
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2018
- 2018-12-25 CN CN201811596377.2A patent/CN109609892A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102254629A (en) * | 2011-05-10 | 2011-11-23 | 浙江省浦江县百川产业有限公司 | Production technology of copper-clad steel wire in soft state |
CN104088891A (en) * | 2014-06-29 | 2014-10-08 | 奉化市飞天人精密模具设计有限公司 | Automobile connection rod and thermal treatment process thereof |
CN108676992A (en) * | 2018-06-25 | 2018-10-19 | 温岭市万泰热处理厂(普通合伙) | A kind of heat treatment process of output shaft |
CN108866309A (en) * | 2018-07-23 | 2018-11-23 | 台州市众达热处理有限公司 | The separator and its heat treatment process of gear sheet |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110169667A (en) * | 2019-04-27 | 2019-08-27 | 临海市创宇工艺有限公司 | A kind of processing technology of rattan chair |
CN110240482A (en) * | 2019-06-13 | 2019-09-17 | 浙江永灵液压机械有限公司 | A kind of blade pump stator inner surface heat treatment process |
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