CN109574124A - A kind of environment-friendly type clarifying agent and its preparation process - Google Patents
A kind of environment-friendly type clarifying agent and its preparation process Download PDFInfo
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- CN109574124A CN109574124A CN201910068212.6A CN201910068212A CN109574124A CN 109574124 A CN109574124 A CN 109574124A CN 201910068212 A CN201910068212 A CN 201910068212A CN 109574124 A CN109574124 A CN 109574124A
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/281—Treatment of water, waste water, or sewage by sorption using inorganic sorbents
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/06—Aluminium; Calcium; Magnesium; Compounds thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
- B01J20/041—Oxides or hydroxides
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
- B01J20/045—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium containing sulfur, e.g. sulfates, thiosulfates, gypsum
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/12—Naturally occurring clays or bleaching earth
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
- B01J20/24—Naturally occurring macromolecular compounds, e.g. humic acids or their derivatives
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/283—Treatment of water, waste water, or sewage by sorption using coal, charred products, or inorganic mixtures containing them
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/286—Treatment of water, waste water, or sewage by sorption using natural organic sorbents or derivatives thereof
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/50—Treatment of water, waste water, or sewage by addition or application of a germicide or by oligodynamic treatment
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
- B01J2220/46—Materials comprising a mixture of inorganic and organic materials
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
- B01J2220/48—Sorbents characterised by the starting material used for their preparation
- B01J2220/4806—Sorbents characterised by the starting material used for their preparation the starting material being of inorganic character
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- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
- B01J2220/48—Sorbents characterised by the starting material used for their preparation
- B01J2220/4812—Sorbents characterised by the starting material used for their preparation the starting material being of organic character
- B01J2220/4825—Polysaccharides or cellulose materials, e.g. starch, chitin, sawdust, wood, straw, cotton
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Abstract
The invention discloses a kind of environment-friendly type clarifying agents, its raw material includes: 20-30 parts of Potassium aluminum sulfate dodecahydrate, 5-17 parts of chitosan, 10-20 parts of bentonite, 3-8 parts of activated carbon, 6-10 parts of biogas residue, 3-8 parts of lime, 5-9 parts of pomelo peel, 3-5 parts of Radix Glycyrrhizae, 9-15 parts of nano magnesia, 24-30 parts of distilled water by weight, and the present invention relates to technical field of sewage purification.The environment-friendly type clarifying agent and its preparation process, by adding Potassium aluminum sulfate dodecahydrate, bentonite and chitosan make the clarifying agent to the various gases in water, liquid and organic substance impurity have good adsorption capacity, by adding lime, pomelo peel and licorice extract have good bactericidal effect to sewage, the clarifying agent raw material is easy to get, without any toxicity, it will not have any impact to the health of operator, use scope is very extensive, it can be adapted for various lives and the purification of trade effluent, clarifying agent production simultaneously is simple, largely reduce production cost.
Description
Technical field
The present invention relates to technical field of sewage purification, specially a kind of environment-friendly type clarifying agent and its preparation process.
Background technique
Sewage treatment is that sewage is made to reach the mistake for being discharged into that a certain water body or the water quality requirement reused purify it
Journey, it is each that sewage treatment is widely used in building, agricultural, traffic, the energy, petrochemical industry, environmental protection, urban landscape, medical treatment, food and drink etc.
The daily life of common people is also come into field more and more, is classified by sewage source, and it is dirty that sewage treatment is generally divided into production
Water process and sanitary sewage disposal, production waste includes trade effluent, rural sewage and medical sewage etc., and sanitary sewage is just
It is the sewage that daily life generates, refers to the complex mixture of various forms of inorganic matters and organic matter, in aquaculture, supports
Contain impurity in the pool if growing, seriously affects aquatic products yield, clarifying agent is the cleanser used in sewage disposal process, existing
Clarifying agent effect be not very well, and it is inconvenient to use.
Traditional clarifying agent cannot have good absorption to various gases, liquid and the organic substance impurity in water simultaneously
Ability does not have good bactericidal effect to sewage, and clarifying agent expensive starting materials, some raw materials are toxic, can be to operator
Health has any impact, and use scope is single, it is not possible to suitable for various lives and the clarification of trade effluent, simultaneously
Making step is many and diverse, needs to expend a large amount of manpowers, largely increases production cost.
Summary of the invention
(1) the technical issues of solving
In view of the deficiencies of the prior art, it the present invention provides a kind of environment-friendly type clarifying agent and its preparation process, solves clear
Clear agent cannot simultaneously adsorb plurality of impurities, and use scope is single, does not sterilize to sewage, and manufacturing process is many and diverse,
The problem of high production cost.
(2) technical solution
In order to achieve the above object, the present invention is achieved by the following technical programs: a kind of environment-friendly type clarifying agent, raw material
Include: by weight 20-30 parts of Potassium aluminum sulfate dodecahydrate, 5-17 parts of chitosan, 10-20 parts of bentonite, 3-8 parts of activated carbon,
6-10 parts of biogas residue, 3-8 parts of lime, 5-9 parts of pomelo peel, 3-5 parts of Radix Glycyrrhizae, 9-15 parts of nano magnesia, 24-30 parts of distilled water.
Preferably, raw material includes following component: 20 parts of Potassium aluminum sulfate dodecahydrate, 10 parts of bentonite, is lived at 5 parts of chitosan
Property 8 parts of carbon, 10 parts of biogas residue, 8 parts of lime, 9 parts of pomelo peel, 5 parts of Radix Glycyrrhizae, 15 parts of nano magnesia, 30 parts of distilled water.
Preferably, raw material includes following component: 25 parts of Potassium aluminum sulfate dodecahydrate, 15 parts of bentonite, is lived at 11 parts of chitosan
Property 5 parts of carbon, 8 parts of biogas residue, 6 parts of lime, 7 parts of pomelo peel, 4 parts of Radix Glycyrrhizae, 12 parts of nano magnesia, 27 parts of distilled water.
Preferably, raw material includes following component: 30 parts of Potassium aluminum sulfate dodecahydrate, 20 parts of bentonite, is lived at 17 parts of chitosan
Property 3 parts of carbon, 6 parts of biogas residue, 3 parts of lime, 5 parts of pomelo peel, 3 parts of Radix Glycyrrhizae, 9 parts of nano magnesia, 24 parts of distilled water.
Preferably, the active carbon is biogas residue or charcoal is one of the active carbon that raw material is made into.
Potassium aluminum sulfate dodecahydrate is also known as alum, and adsorption capacity is very strong, can adsorb the impurity to suspend in water, and formed and sunk
It forms sediment, makes clarification of water.
Chitosan has very strong adsorption capacity, the material of many low molecular weights, such as metal ion, cholesterol, glycerol three
Ester, cholic acid and organic mercury etc. can be adsorbed by chitosan, and chitosan can not only adsorb magnesium, potassium, and can adsorb zinc,
Calcium, mercury and uranium, while having good fungistatic effect.
Bentonite has strong hygroscopicity and dilatancy, and the water of adsorbable 8-15 times of own vol, volume expansion can
Up to several times to 30 times, it can be dispersed into as a form of gel and suspension in an aqueous medium, this medium solution has certain viscosity, touching
Denaturation and lubricity, have stronger cation exchange capacity (CEC), there is certain adsorption capacity to various gases, liquid, organic substance,
For maximal absorptive capacity up to 5 times of itself weight, the admixture of it and water, mud or fine sand has plasticity and cohesiveness.
The invention also discloses a kind of preparation processes of environment-friendly type clarifying agent, specifically includes the following steps:
S1, choose raw material Potassium aluminum sulfate dodecahydrate, chitosan, bentonite, activated carbon, biogas residue, lime, pomelo peel, Radix Glycyrrhizae,
Nano magnesia, distilled water weigh raw material by its weight ratio respectively；
S2, bentonite weighed in S1 and lime are added in disintegrating apparatus, are crushed to 80-125 mesh, it will be weighed in S1
Pomelo peel and Radix Glycyrrhizae are added in disintegrating apparatus, are crushed to 60-70 mesh；
S3, distilled water weighed in S1 is added in heating equipment, reaches 100 DEG C to water temperature, is added into heating equipment
The pomelo peel crushed in S2 and Radix Glycyrrhizae, heating time control in 5-10min, obtain mixed liquor, mixed liquor is poured into filter plant,
Pomelo peel residue and Glycyrrhiza uralensisFisch residue have been filtered, mixed extract is obtained；
S4, Potassium aluminum sulfate dodecahydrate weighed in S1, chitosan, activated carbon, biogas residue and nano magnesia are added and stirred
In equipment, the swelling crushed in S2 is added into mixing plant after stirring 3-5min in 100-110r/min for stirring rate control
Soil and lime, stirring rate control are included in mixing made from S3 into mixing plant after stirring 4-6min in 115-125r/min
Extracting solution, stirring rate control obtain cementitious compositions in 60-80r/min, mixing time 6-8min；
S5, it will be made in S4 in cementitious compositions addition drying equipment, temperature control is in 200-300 DEG C, drying time
60-80min obtains semi-finished product clarifying agent, is granulated using pelletizer to semi-finished product clarifying agent, in 3-5mm between particle, is obtained into
Product environment-friendly type clarifying agent.
(3) beneficial effect
The present invention provides a kind of environment-friendly type clarifying agent and its preparation processes.Have compared with prior art following beneficial to effect
Fruit: the environment-friendly type clarifying agent and its preparation process, by its raw material include: by weight 20-30 parts of Potassium aluminum sulfate dodecahydrate,
5-17 parts of chitosan, 10-20 parts of bentonite, 3-8 parts of activated carbon, 6-10 parts of biogas residue, 3-8 parts of lime, 5-9 parts of pomelo peel, Radix Glycyrrhizae
3-5 parts, 9-15 parts of nano magnesia, 24-30 parts of distilled water, S1, choose raw material Potassium aluminum sulfate dodecahydrate, chitosan, bentonite,
Activated carbon, biogas residue, lime, pomelo peel, Radix Glycyrrhizae, nano magnesia, distilled water weigh raw material by its weight ratio respectively, S2, by S1
In weighed bentonite and lime be added in disintegrating apparatus, be crushed to 80-125 mesh, pomelo peel weighed in S1 and Radix Glycyrrhizae added
Enter in disintegrating apparatus, is crushed to 60-70 mesh, S3, distilled water weighed in S1 is added in heating equipment, reaches 100 to water temperature
DEG C, the pomelo peel crushed in S2 and Radix Glycyrrhizae are added into heating equipment, S4, gathers Potassium aluminum sulfate dodecahydrate weighed in S1, shell
Sugar, activated carbon, biogas residue and nano magnesia are added in mixing plant, and cementitious compositions addition drying equipment S5, will be made in S4
In, temperature control is at 200-300 DEG C, it can be achieved that making the clarification by addition Potassium aluminum sulfate dodecahydrate, bentonite and chitosan
Agent has good adsorption capacity to various gases, liquid and the organic substance impurity in water, passes through addition lime, pomelo peel and sweet
Careless extracting solution has good bactericidal effect to sewage, which is easy to get, environmental protection and without any toxicity, will not be to operator
The health of member has any impact, and use scope is very extensive, can be adapted for various lives and trade effluent
Clarification, while clarifying agent production is simple, does not need to expend a large amount of manpowers, largely reduces production cost, will clarify
Agent is manufactured into graininess, facilitates the use of operator.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common
Technical staff's every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
The embodiment of the present invention provides three kinds of technical solutions: a kind of preparation process of environment-friendly type clarifying agent specifically includes following
Embodiment:
Embodiment 1
S1,20 parts of raw material Potassium aluminum sulfate dodecahydrate, 5 parts of chitosan, 10 parts of bentonite, 8 parts of activated carbon, biogas residue 10 are chosen
Part, 8 parts of lime, 9 parts of pomelo peel, 5 parts of Radix Glycyrrhizae, 15 parts of nano magnesia, 30 parts of distilled water, weigh original by its weight ratio respectively
Material；
S2,10 parts of bentonites weighed in S1 and 8 parts of lime are added in disintegrating apparatus, are crushed to 80 mesh, will claim in S1
The 9 parts of pomelo peels and 5 portions of Radix Glycyrrhizaes taken are added in disintegrating apparatus, are crushed to 60 mesh；
S3,30 parts of distilled water weighed in S1 is added in heating equipment, 100 DEG C is reached to water temperature, into heating equipment
The pomelo peel crushed in S2 and Radix Glycyrrhizae is added, heating time controls in 5min, obtains mixed liquor, mixed liquor is poured into filter plant
In, pomelo peel residue and Glycyrrhiza uralensisFisch residue have been filtered, mixed extract is obtained；
S4, by 20 parts of Potassium aluminum sulfate dodecahydrates weighed in S1,5 parts of chitosans, 8 parts of activated carbon, 10 parts of biogas residues and 15 parts
Nano magnesia is added in mixing plant, and S2 is added into mixing plant after stirring 3min in 100r/min for stirring rate control
The bentonite and lime of middle crushing, stirring rate control are included in S3 into mixing plant after 115r/min, stirring 4min and are made
Mixed extract, stirring rate control in 60r/min, mixing time 6min obtains cementitious compositions；
S5, it will be made in S4 in cementitious compositions addition drying equipment, temperature control is in 200 DEG C, drying time
60min obtains semi-finished product clarifying agent, is granulated using pelletizer to semi-finished product clarifying agent, in 3mm between particle, obtains finished product ring
Guarantor's type clarifying agent.
Embodiment 2
S1,25 parts of raw material Potassium aluminum sulfate dodecahydrate, 11 parts of chitosan, 15 parts of bentonite, 5 parts of activated carbon, biogas residue 8 are chosen
Part, 6 parts of lime, 7 parts of pomelo peel, 4 parts of Radix Glycyrrhizae, 12 parts of nano magnesia, 27 parts of distilled water, weigh original by its weight ratio respectively
Material；
S2,15 parts of bentonites weighed in S1 and 6 parts of lime are added in disintegrating apparatus, are crushed to 100 mesh, will claim in S1
The 7 parts of pomelo peels and 4 portions of Radix Glycyrrhizaes taken are added in disintegrating apparatus, are crushed to 65 mesh；
S3,27 parts of distilled water weighed in S1 is added in heating equipment, 100 DEG C is reached to water temperature, into heating equipment
The pomelo peel crushed in S2 and Radix Glycyrrhizae is added, heating time controls in 7min, obtains mixed liquor, mixed liquor is poured into filter plant
In, pomelo peel residue and Glycyrrhiza uralensisFisch residue have been filtered, mixed extract is obtained；
S4, by 25 parts of Potassium aluminum sulfate dodecahydrates weighed in S1,11 parts of chitosans, 5 parts of activated carbon, 8 parts of biogas residues and 12 parts
Nano magnesia is added in mixing plant, and S2 is added into mixing plant after stirring 4min in 105r/min for stirring rate control
The bentonite and lime of middle crushing, stirring rate control are included in S3 into mixing plant after 120r/min, stirring 5min and are made
Mixed extract, stirring rate control in 70r/min, mixing time 7min obtains cementitious compositions；
S5, it will be made in S4 in cementitious compositions addition drying equipment, temperature control is in 250 DEG C, drying time
70min obtains semi-finished product clarifying agent, is granulated using pelletizer to semi-finished product clarifying agent, in 4mm between particle, obtains finished product ring
Guarantor's type clarifying agent.
Embodiment 3
S1,30 parts of raw material Potassium aluminum sulfate dodecahydrate, 17 parts of chitosan, 20 parts of bentonite, 3 parts of activated carbon, biogas residue 6 are chosen
Part, 3 parts of lime, 5 parts of pomelo peel, 3 parts of Radix Glycyrrhizae, 9 parts of nano magnesia, 24 parts of distilled water, weigh raw material by its weight ratio respectively；
S2,20 parts of bentonites weighed in S1 and 3 parts of lime are added in disintegrating apparatus, are crushed to 125 mesh, will claim in S1
The 5 parts of pomelo peels and 3 portions of Radix Glycyrrhizaes taken are added in disintegrating apparatus, are crushed to 70 mesh；
S3,24 parts of distilled water weighed in S1 is added in heating equipment, 100 DEG C is reached to water temperature, into heating equipment
The pomelo peel crushed in S2 and Radix Glycyrrhizae is added, heating time controls in 10min, obtains mixed liquor, mixed liquor is poured into filter plant
In, pomelo peel residue and Glycyrrhiza uralensisFisch residue have been filtered, mixed extract is obtained；
S4,30 parts of Potassium aluminum sulfate dodecahydrates weighed in S1,17 parts of chitosans, 3 parts of activated carbon, 6 parts of biogas residues and 9 parts are received
Rice magnesia is added in mixing plant, and stirring rate control is added in S2 after stirring 5min into mixing plant in 110r/min
The bentonite and lime of crushing, stirring rate control are included in made from S3 after stirring 6min into mixing plant in 125r/min
Mixed extract, stirring rate control obtain cementitious compositions in 80r/min, mixing time 8min；
S5, it will be made in S4 in cementitious compositions addition drying equipment, temperature control is in 300 DEG C, drying time
80min obtains semi-finished product clarifying agent, is granulated using pelletizer to semi-finished product clarifying agent, in 5mm between particle, obtains finished product ring
Guarantor's type clarifying agent.
Effect example
Certain South China's aquaculture quotient, severe water pollution, inside choose wherein three containing a large amount of harmful poisonous impurity
A culture pond is used continuously 5 days, obtains through water quality detection respectively using environment-friendly type clarifying agent made from embodiment 1-3, uses
Gas, liquid and organic substance impurity in embodiment 2 in the culture pond of environment-friendly type clarifying agent obtained are obviously implemented than using
Gas, liquid and organic substance impurity in example 1 and embodiment 3 in the culture pond of environment-friendly type clarifying agent obtained is few, to sum up institute
It states and show that environment-friendly type clarifying agent effect obtained is best in embodiment 2.
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality
Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation
In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to
Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those
Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment
Intrinsic element.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (6)
1. a kind of environment-friendly type clarifying agent, it is characterised in that: its raw material include: by weight 20-30 parts of Potassium aluminum sulfate dodecahydrate,
5-17 parts of chitosan, 10-20 parts of bentonite, 3-8 parts of activated carbon, 6-10 parts of biogas residue, 3-8 parts of lime, 5-9 parts of pomelo peel, Radix Glycyrrhizae
3-5 parts, 9-15 parts of nano magnesia, 24-30 parts of distilled water.
2. a kind of environment-friendly type clarifying agent according to claim 1, it is characterised in that: 20 parts of Potassium aluminum sulfate dodecahydrate, shell are poly-
Sugar 5 parts, 10 parts of bentonite, 8 parts of activated carbon, 10 parts of biogas residue, 8 parts of lime, 9 parts of pomelo peel, 5 parts of Radix Glycyrrhizae, 15 parts of nano magnesia,
30 parts of distilled water.
3. a kind of environment-friendly type clarifying agent according to claim 1, it is characterised in that: 25 parts of Potassium aluminum sulfate dodecahydrate, shell are poly-
Sugar 11 parts, 15 parts of bentonite, 5 parts of activated carbon, 8 parts of biogas residue, 6 parts of lime, 7 parts of pomelo peel, 4 parts of Radix Glycyrrhizae, 12 parts of nano magnesia,
27 parts of distilled water.
4. a kind of environment-friendly type clarifying agent according to claim 1, it is characterised in that: 30 parts of Potassium aluminum sulfate dodecahydrate, shell are poly-
Sugar 17 parts, 20 parts of bentonite, 3 parts of activated carbon, 6 parts of biogas residue, 3 parts of lime, 5 parts of pomelo peel, 3 parts of Radix Glycyrrhizae, 9 parts of nano magnesia,
24 parts of distilled water.
5. a kind of environment-friendly type clarifying agent according to any one of claims 1-4, it is characterised in that: the active carbon is natural pond
Slag or charcoal are one of the active carbon that raw material is made into.
6. a kind of environment-friendly type clarifying agent described in -5 any one according to claim 1, it is characterised in that: its preparation process is specific
The following steps are included:
S1, raw material Potassium aluminum sulfate dodecahydrate, chitosan, bentonite, activated carbon, biogas residue, lime, pomelo peel, Radix Glycyrrhizae, nanometer are chosen
Magnesia, distilled water weigh raw material by its weight ratio respectively；
S2, bentonite weighed in S1 and lime are added in disintegrating apparatus, 80-125 mesh are crushed to, by shaddock weighed in S1
Skin and Radix Glycyrrhizae are added in disintegrating apparatus, are crushed to 60-70 mesh；
S3, distilled water weighed in S1 is added in heating equipment, reaches 100 DEG C to water temperature, is added in S2 into heating equipment
The pomelo peel of crushing and Radix Glycyrrhizae, heating time control in 5-10min, obtain mixed liquor, mixed liquor is poured into filter plant, by shaddock
Sub- skin residue and Glycyrrhiza uralensisFisch residue have filtered, and obtain mixed extract；
S4, mixing plant is added in Potassium aluminum sulfate dodecahydrate weighed in S1, chitosan, activated carbon, biogas residue and nano magnesia
In, stirring rate control in 100-110r/min, stir be added into mixing plant after 3-5min the bentonite crushed in S2 and
Lime, stirring rate control are included in mixing extraction made from S3 into mixing plant after stirring 4-6min in 115-125r/min
Liquid, stirring rate control obtain cementitious compositions in 60-80r/min, mixing time 6-8min；
S5, cementitious compositions will be made in S4 and will be added in drying equipment, temperature control is at 200-300 DEG C, drying time 60-
80min obtains semi-finished product clarifying agent, is granulated using pelletizer to semi-finished product clarifying agent, in 3-5mm between particle, obtains finished product
Environment-friendly type clarifying agent.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110624515A (en) * | 2019-10-22 | 2019-12-31 | 泸州老窖股份有限公司 | Fruit wine clarifying agent and preparation method thereof |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5433865A (en) * | 1994-03-31 | 1995-07-18 | Laurent; Edward L. | Method for treating process waste streams by use of natural flocculants |
| CN105858782A (en) * | 2016-04-19 | 2016-08-17 | 肥东县柯文斌家庭农场 | Chinese herbal medicine water body clarifying agent |
| CN105858736A (en) * | 2016-04-13 | 2016-08-17 | 吴申龙 | Composite sewage treatment agent based on natural ores and biogas residues, and preparation method thereof |
| CN106430370A (en) * | 2016-12-05 | 2017-02-22 | 郑州诚合信息技术有限公司 | High-efficiency sewage treatment agent and preparation method thereof |
| CN106745447A (en) * | 2016-11-25 | 2017-05-31 | 南宁市黑晶信息技术有限公司 | A kind of heavy metal-polluted water process flocculant |
| CN106865652A (en) * | 2017-04-11 | 2017-06-20 | 安徽省明美矿物化工有限公司 | A kind of concave convex rod water quality cleansing agent and preparation method |
| CN106915777A (en) * | 2015-12-24 | 2017-07-04 | 天津绿格瑞科技发展有限公司 | A kind of sewage-treating agent |
| CN107285454A (en) * | 2017-07-03 | 2017-10-24 | 安徽国能亿盛环保科技有限公司 | A kind of Industrial waste water treatment agent |
-
2019
- 2019-01-24 CN CN201910068212.6A patent/CN109574124A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5433865A (en) * | 1994-03-31 | 1995-07-18 | Laurent; Edward L. | Method for treating process waste streams by use of natural flocculants |
| CN106915777A (en) * | 2015-12-24 | 2017-07-04 | 天津绿格瑞科技发展有限公司 | A kind of sewage-treating agent |
| CN105858736A (en) * | 2016-04-13 | 2016-08-17 | 吴申龙 | Composite sewage treatment agent based on natural ores and biogas residues, and preparation method thereof |
| CN105858782A (en) * | 2016-04-19 | 2016-08-17 | 肥东县柯文斌家庭农场 | Chinese herbal medicine water body clarifying agent |
| CN106745447A (en) * | 2016-11-25 | 2017-05-31 | 南宁市黑晶信息技术有限公司 | A kind of heavy metal-polluted water process flocculant |
| CN106430370A (en) * | 2016-12-05 | 2017-02-22 | 郑州诚合信息技术有限公司 | High-efficiency sewage treatment agent and preparation method thereof |
| CN106865652A (en) * | 2017-04-11 | 2017-06-20 | 安徽省明美矿物化工有限公司 | A kind of concave convex rod water quality cleansing agent and preparation method |
| CN107285454A (en) * | 2017-07-03 | 2017-10-24 | 安徽国能亿盛环保科技有限公司 | A kind of Industrial waste water treatment agent |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110624515A (en) * | 2019-10-22 | 2019-12-31 | 泸州老窖股份有限公司 | Fruit wine clarifying agent and preparation method thereof |
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