CN109567171A - A kind of water solube powder and preparation method thereof containing pearl - Google Patents
A kind of water solube powder and preparation method thereof containing pearl Download PDFInfo
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- CN109567171A CN109567171A CN201910035776.XA CN201910035776A CN109567171A CN 109567171 A CN109567171 A CN 109567171A CN 201910035776 A CN201910035776 A CN 201910035776A CN 109567171 A CN109567171 A CN 109567171A
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- pearl
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- water solube
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- 239000000843 powder Substances 0.000 title claims abstract description 153
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 117
- 238000002360 preparation method Methods 0.000 title claims abstract description 29
- 235000018290 Musa x paradisiaca Nutrition 0.000 claims abstract description 29
- 241001465754 Metazoa Species 0.000 claims abstract description 25
- 235000007164 Oryza sativa Nutrition 0.000 claims abstract description 24
- 235000009566 rice Nutrition 0.000 claims abstract description 24
- 239000002994 raw material Substances 0.000 claims abstract description 16
- 240000007594 Oryza sativa Species 0.000 claims abstract 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 174
- 235000019441 ethanol Nutrition 0.000 claims description 64
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 44
- 239000000284 extract Substances 0.000 claims description 43
- 238000001914 filtration Methods 0.000 claims description 32
- 241000234295 Musa Species 0.000 claims description 28
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 24
- 239000004310 lactic acid Substances 0.000 claims description 22
- 235000014655 lactic acid Nutrition 0.000 claims description 22
- 238000003756 stirring Methods 0.000 claims description 21
- 239000002253 acid Substances 0.000 claims description 20
- 108090000526 Papain Proteins 0.000 claims description 18
- 239000004365 Protease Substances 0.000 claims description 18
- 239000000706 filtrate Substances 0.000 claims description 18
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 claims description 18
- 235000013372 meat Nutrition 0.000 claims description 18
- 229940055729 papain Drugs 0.000 claims description 17
- 235000019834 papain Nutrition 0.000 claims description 17
- 238000010992 reflux Methods 0.000 claims description 16
- 230000001954 sterilising effect Effects 0.000 claims description 16
- 230000007071 enzymatic hydrolysis Effects 0.000 claims description 15
- 238000006047 enzymatic hydrolysis reaction Methods 0.000 claims description 15
- 244000063299 Bacillus subtilis Species 0.000 claims description 10
- 235000014469 Bacillus subtilis Nutrition 0.000 claims description 10
- 241000186000 Bifidobacterium Species 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 9
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 claims description 8
- 239000006286 aqueous extract Substances 0.000 claims description 8
- 239000001632 sodium acetate Substances 0.000 claims description 8
- 235000017281 sodium acetate Nutrition 0.000 claims description 8
- 238000004659 sterilization and disinfection Methods 0.000 claims description 8
- 241000237536 Mytilus edulis Species 0.000 claims description 7
- 239000013505 freshwater Substances 0.000 claims description 7
- 235000020638 mussel Nutrition 0.000 claims description 7
- 239000000047 product Substances 0.000 claims description 4
- 241000894006 Bacteria Species 0.000 claims description 2
- 238000010792 warming Methods 0.000 claims description 2
- 239000006071 cream Substances 0.000 claims 2
- 235000015110 jellies Nutrition 0.000 claims 1
- 239000008274 jelly Substances 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 20
- 230000037182 bone density Effects 0.000 abstract description 17
- 208000001132 Osteoporosis Diseases 0.000 abstract description 13
- 230000000050 nutritive effect Effects 0.000 abstract description 9
- 235000016709 nutrition Nutrition 0.000 abstract description 6
- 230000008569 process Effects 0.000 abstract description 5
- 230000035764 nutrition Effects 0.000 abstract description 4
- 238000012545 processing Methods 0.000 abstract description 3
- 238000010276 construction Methods 0.000 abstract description 2
- 230000003993 interaction Effects 0.000 abstract description 2
- 230000007774 longterm Effects 0.000 abstract description 2
- 239000003755 preservative agent Substances 0.000 abstract description 2
- 230000002335 preservative effect Effects 0.000 abstract description 2
- 240000008790 Musa x paradisiaca Species 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000002893 slag Substances 0.000 description 28
- 241000209094 Oryza Species 0.000 description 20
- 238000000605 extraction Methods 0.000 description 20
- 230000000052 comparative effect Effects 0.000 description 18
- 239000007788 liquid Substances 0.000 description 13
- 230000007062 hydrolysis Effects 0.000 description 11
- 238000006460 hydrolysis reaction Methods 0.000 description 11
- 108090000790 Enzymes Proteins 0.000 description 9
- 102000004190 Enzymes Human genes 0.000 description 9
- 235000013361 beverage Nutrition 0.000 description 9
- 230000000694 effects Effects 0.000 description 9
- 229940088598 enzyme Drugs 0.000 description 9
- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical compound NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 description 8
- 150000001413 amino acids Chemical class 0.000 description 7
- 238000002474 experimental method Methods 0.000 description 5
- 239000004615 ingredient Substances 0.000 description 5
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 4
- MKYBYDHXWVHEJW-UHFFFAOYSA-N N-[1-oxo-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propan-2-yl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(C(C)NC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 MKYBYDHXWVHEJW-UHFFFAOYSA-N 0.000 description 4
- 230000009286 beneficial effect Effects 0.000 description 4
- 239000011575 calcium Substances 0.000 description 4
- 229910052791 calcium Inorganic materials 0.000 description 4
- 238000011160 research Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 229960003080 taurine Drugs 0.000 description 4
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 3
- 206010006956 Calcium deficiency Diseases 0.000 description 3
- 230000000975 bioactive effect Effects 0.000 description 3
- 210000000988 bone and bone Anatomy 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 239000002158 endotoxin Substances 0.000 description 3
- 238000000855 fermentation Methods 0.000 description 3
- 230000004151 fermentation Effects 0.000 description 3
- 229920006008 lipopolysaccharide Polymers 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 102000004169 proteins and genes Human genes 0.000 description 3
- 108090000623 proteins and genes Proteins 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 230000001225 therapeutic effect Effects 0.000 description 3
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 230000035622 drinking Effects 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 235000015097 nutrients Nutrition 0.000 description 2
- 230000000717 retained effect Effects 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 230000001502 supplementing effect Effects 0.000 description 2
- MSWZFWKMSRAUBD-GASJEMHNSA-N 2-amino-2-deoxy-D-galactopyranose Chemical compound N[C@H]1C(O)O[C@H](CO)[C@H](O)[C@@H]1O MSWZFWKMSRAUBD-GASJEMHNSA-N 0.000 description 1
- 244000189799 Asimina triloba Species 0.000 description 1
- 235000006264 Asimina triloba Nutrition 0.000 description 1
- 241001037822 Bacillus bacterium Species 0.000 description 1
- 208000031872 Body Remains Diseases 0.000 description 1
- 235000009467 Carica papaya Nutrition 0.000 description 1
- 108010059892 Cellulase Proteins 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 239000004471 Glycine Substances 0.000 description 1
- 102000011782 Keratins Human genes 0.000 description 1
- 108010076876 Keratins Proteins 0.000 description 1
- AHLPHDHHMVZTML-BYPYZUCNSA-N L-Ornithine Chemical compound NCCC[C@H](N)C(O)=O AHLPHDHHMVZTML-BYPYZUCNSA-N 0.000 description 1
- 239000004367 Lipase Substances 0.000 description 1
- 102000004882 Lipase Human genes 0.000 description 1
- 108090001060 Lipase Proteins 0.000 description 1
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
- 208000007101 Muscle Cramp Diseases 0.000 description 1
- AHLPHDHHMVZTML-UHFFFAOYSA-N Orn-delta-NH2 Natural products NCCCC(N)C(O)=O AHLPHDHHMVZTML-UHFFFAOYSA-N 0.000 description 1
- UTJLXEIPEHZYQJ-UHFFFAOYSA-N Ornithine Natural products OC(=O)C(C)CCCN UTJLXEIPEHZYQJ-UHFFFAOYSA-N 0.000 description 1
- 108091005804 Peptidases Proteins 0.000 description 1
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 description 1
- 238000005903 acid hydrolysis reaction Methods 0.000 description 1
- 239000011149 active material Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- MSWZFWKMSRAUBD-UHFFFAOYSA-N beta-D-galactosamine Natural products NC1C(O)OC(CO)C(O)C1O MSWZFWKMSRAUBD-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 235000021466 carotenoid Nutrition 0.000 description 1
- 150000001747 carotenoids Chemical class 0.000 description 1
- 229940106157 cellulase Drugs 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 210000004211 gastric acid Anatomy 0.000 description 1
- 229960002449 glycine Drugs 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 230000003834 intracellular effect Effects 0.000 description 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 235000019421 lipase Nutrition 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 150000007522 mineralic acids Chemical class 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 229960003104 ornithine Drugs 0.000 description 1
- 238000000053 physical method Methods 0.000 description 1
- -1 porphyrin iron Amine Chemical class 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 235000019419 proteases Nutrition 0.000 description 1
- 230000017854 proteolysis Effects 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 229910052712 strontium Inorganic materials 0.000 description 1
- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 239000002344 surface layer Substances 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L17/00—Food-from-the-sea products; Fish products; Fish meal; Fish-egg substitutes; Preparation or treatment thereof
- A23L17/65—Addition of, or treatment with, microorganisms or enzymes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L17/00—Food-from-the-sea products; Fish products; Fish meal; Fish-egg substitutes; Preparation or treatment thereof
- A23L17/70—Comminuted, e.g. emulsified, fish products; Processed products therefrom such as pastes, reformed or compressed products
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/01—Instant products; Powders; Flakes; Granules
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/56—Materials from animals other than mammals
- A61K35/618—Molluscs, e.g. fresh-water molluscs, oysters, clams, squids, octopus, cuttlefish, snails or slugs
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P19/00—Drugs for skeletal disorders
- A61P19/08—Drugs for skeletal disorders for bone diseases, e.g. rachitism, Paget's disease
- A61P19/10—Drugs for skeletal disorders for bone diseases, e.g. rachitism, Paget's disease for osteoporosis
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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Abstract
The invention discloses a kind of water solube powders containing pearl, including following component and respective mass percentage: pearl powder 35-45%, aquatic animal muddy flesh 25-40%, banana 8-13%, fig 5-10%, fermented glutinous rice 7-12%.Preparation method of the invention is simple, process is short, and processing cost is low, reduces the nutrition of nutriment in process and loses, interaction is formed between present invention heating raw material, and retain intact nutrition, retain original shape, color and construction, is not required to add any preservative, the mouthfeel and nutritive value of the water solube powder containing pearl are fully ensured that, water solube powder of the gained containing pearl is applicable in any crowd, and long-term reference can also treat osteoporosis, increases bone density.
Description
Technical field
The invention belongs to pearl powder technical fields, and in particular to a kind of water solube powder and preparation method thereof containing pearl.
Background technique
Pearl is one of the rare medicinal herbs in motherland's medicine treasure-house, in the early time since processing technology falls behind, by mechanically
It is processed into pearl powder, low through gastric acid and trypsase decomposition absorptivity after taking, utility value is too small.Since the eighties in last century
With scientific and technological progress, people are engaged in the analysis of pearl and nacre effective component and its deep research and development of processing method, application
Patent is more.Effective component calcium carbonate about 92% in pearl and nacre, organic matter about 5%, including 18 kinds of amino acid (with
Taurine, ornithine and glycine are more), carotenoid (referring to yellow pearl), gucosamine, galactosamine, porphyrin iron
Amine, keratin etc. are separately just right highest quality containing elements, the proportions of these elements such as lithium, strontium, titaniums.And inorganic calcium is
By smooth, the hard surface layer that hard shell albumen is bonded, how by they resolve into easily digested amino acid,
Water soluble pearl calcium always is the hot spot of research.
In recent years, it is attempted to prepare liquid pearl by Hydrolyze method.But in existing pearl extracting method, there are all
More time limits.Such as number of patent application: there are many defects in 94104047.X and 94113159.9, and some stresses to add the progress of freshwater mussel meat
Enzymatic hydrolysis is handled using high temperature (180 DEG C -220 DEG C) and the physical method of high pressure (6-7 atmospheric pressure), it is in pearl and nacre
It accounts for most inorganic calcium to fail to obtain due attention and utilization, water soluble pearl calcium content is too low in product.Secondly, production work
The cumbersome complexity of skill, process is too long, even one week three days or more (such as application number: 93102321.1), unfavorable industrialized production.
At present by solid pearl be prepared into the most common method of liquid pearl be using sour water solution, basic hydrolysis, enzymatic hydrolysis or
It is to combine sour water solution and enzymatic hydrolysis, is prepared into liquid pearl as patent No. zl91100778.4 discloses a kind of solid pearl
Method papain hydrolysis is then added, makes hard shell proteolysis at amino acid mainly by inorganic acid solution.But
Using the method, other effective components of pearl are not extracted, and nutrient composition content is far from enough, the nutrition in pearl
Ingredient is easy to be destroyed, and the source of albumen source and other effective components is difficult, and the utilization rate of pearl effective component is low, and straight
It connects to obtain liquid pearl, condition of storage is harsh, and transport is inconvenient.
Summary of the invention
It is a kind of containing the water solube powder of pearl and its preparation side the purpose of the present invention is overcoming the deficiencies of the prior art and provide
Method.
The present invention provides a kind of water solube powders containing pearl, including following component and respective mass percentage: precious
Pearl powder 35-45%, aquatic animal muddy flesh 25-40%, banana 8-13%, fig 5-10%, fermented glutinous rice 7-12%.
Preferably, including following component and respective mass percentage: pearl powder 40%, aquatic animal muddy flesh 34% are fragrant
Any of several broadleaf plants 8%, fig 8%, fermented glutinous rice 10%.
The present invention also provides a kind of preparation methods of water solube powder containing pearl, comprising the following steps:
1) pearl original powder crushes to obtain pearl powder, and ethanol solution is added into pearl powder, is warming up to 70-100 DEG C and is returned
Stream extracts, and extracting solution and filter residue is obtained by filtration；
2) aquatic animal meat is quick-frozen at -15~-8 DEG C, then rub into aquatic animal muddy flesh；
3) acid iodide and lactic acid are added into filter residue, is stirred at 60-70 DEG C, adjusting pH is neutrality；It is added aquatic dynamic
Papain and trypsase is added in object muddy flesh, banana and water, and adjusting pH is neutrality, and enzymatic hydrolysis is stirred at 30-35 DEG C, is killed
Filtrate is obtained by filtration in bacterium；
4) fig is put into triangular flask, is added and is equivalent to 2 times of total mass of raw material of water, 121 DEG C of sterilizing 30min, so
Bacillus subtilis and Bifidobacterium bacterium solution are added afterwards, is carried out fermented and cultured 10 days at 30 DEG C after mixing, obtains tunning,
In tunning plus water, acetic acid is then added and sodium acetate solution adjusts pH, water is carried out at 60 DEG C and is mentioned, during Aqueous extracts are adjusted to
After property, fig extract is obtained；
5) extracting solution, filtrate and fig extract are mixed, concentration adds fermented glutinous rice, stirs evenly, dry, powder
It is broken, it sterilizes to get the water solube powder containing pearl.
Preferably, the fineness of pearl powder described in step 1) is 300-400 mesh.
Preferably, the volumetric concentration of ethanol solution described in step 1) is 30-80%.
Preferably, the mass ratio of pearl powder described in step 1) and ethanol solution is 1:5-8.
Preferably, aquatic animal meat described in step 2) is freshwater mussel meat or spiral shell.
Preferably, step 2) the quick-frozen time is 45-60min.
Preferably, the additional amount of the step 3) lactic acid is 2-4 times of filter residue quality, and the additional amount of acid iodide is filter residue quality
0.2-0.4 times.
Preferably, the molar concentration of the step 3) lactic acid is 5-8mol/L.
In water solube powder of the present invention containing pearl be added water quality and pearl powder, aquatic animal muddy flesh, banana,
The ratio of the sum of this 6 kinds of material qualities of fig, fermented glutinous rice is 1-3:1.
At present by solid pearl be prepared into the most common method of liquid pearl be using sour water solution, basic hydrolysis, enzymatic hydrolysis or
It is acid-enzymatic isolation method.But all there are the following problems for these existing methods: the effective component of pearl is not extracted
Come, nutrient composition content is far from enough, and the nutritional ingredient in pearl is easy to be destroyed during acid hydrolysis, egg
The source of Bai Laiyuan and other effective components is difficult, and the utilization rate of pearl effective component is low.
The inventor of the present application found through research that pearl powder first to be carried out to refluxing extraction in ethanol solution, and control temperature
Degree is 70-100 DEG C, can extract the part effective component in pearl powder, the later period is avoided to be destroyed.The application reflux
It extracts 3 times, and the volumetric concentration of refluxing extraction ethyl alcohol and Extracting temperature all change every time, extracts for the first time dense with volume
Degree is the ethanol solution of 30-40%, and Extracting temperature is 80-90 DEG C, and the mass ratio of pearl powder and ethanol solution is 1:5-8, filtering
It obtains extracting solution I and extracts slag I；The ethanol solution that it is 80% with volumetric concentration that second, which is extracted, Extracting temperature is 100 DEG C, precious
The mass ratio of pearl powder and ethanol solution is 1:5-8, and extracting solution II is obtained by filtration and extracts slag II；Third time is extracted and uses volumetric concentration
For the ethanol solution of 50-60%, Extracting temperature is 70 DEG C, and the mass ratio of pearl powder and ethanol solution is 1:5-8, is obtained by filtration and mentions
It takes liquid III and extracts slag III；The merging of extracting solution I, extracting solution II and extracting solution III is obtained into extracting solution, extracting slag III is filter residue.
The part effective component in pearl powder can be made sufficiently to extract using the extracting method of the application, especially taurine, mentioned
The high nutritive value of final drink, supplementing calcium element can health care bone be loose, fractures, has a pain in the back, leg cramps.
In the preparation method of the application, by aquatic animal meat in -15~-8 DEG C of quick-frozen 45-60min, so that internal albumen
Matter, a variety of amino acid, lipopolysaccharides, multivitamin, microelement and the bioactive substances such as enzyme beneficial to human body remain original
Activity is not destroyed.
Acid iodide and lactic acid is added in the application in filter residue, is conducive to being fully hydrolyzed for pearl raw material, makes the degree of hydrolysis more
Then aquatic animal muddy flesh, banana and papain and trypsase is added in height, can not only by banana it is effective at
Divide hydrolysis, increases the nutritive value of drink, additionally it is possible to be fully hydrolyzed to pearl powder using the enzyme wherein contained.This Shen
Please inventors discovered through research that, compared to the prior art in be only added lactic acid and papain carry out acidolysis and enzyme
Solution, acid iodide and the common acidolysis of lactic acid is added in the application, and banana, papain and trypsase is added and digests jointly, this
Kind method for hydrolysis is more advantageous to being fully hydrolyzed for raw material, and the degree of hydrolysis is higher, can also increase the nutritional ingredient of final drink,
Health-care effect more preferably, can be avoided osteoporosis caused by calcium deficiency.
The application uses acid iodide and lactic acid collective effect, is hydrolyzed to pearl, microorganism can be made to be in pH value smaller
Environment in, be more than their adaptable ranges of institute, there is bactericidal effect；The two cooperation simultaneously keeps the effective component of pearl abundant
It extracts.
The application by pearl powder with ethanol solution refluxing extraction 3 times, and every time the volumetric concentration of refluxing extraction ethyl alcohol and
Extracting temperature all changes, and extracting solution and filter residue is obtained by filtration；Acid iodide and lactic acid are added in filter residue, is added after acidolysis aquatic dynamic
Object muddy flesh, banana and water add papain and trypsase, and stirring enzymatic hydrolysis finally adds fermented glutinous rice, and stirring is equal
It is even, it dry, pulverize, obtain the water solube powder containing pearl.The present invention makes the battalion of pearl and aquatic animal meat by above-mentioned way
Feeding substance is largely retained in final water solube powder, and loss is less, and the water solube powder containing pearl of preparation is brewed into
Taste is dense after drink, fragrant in taste, and very tasty and refreshing, and nutritive value is high, strong health-care function, deep to be liked by the majority of consumers, can
Treat osteoporosis.
Fig in the application is not extracted using the method that conventional water mentions, and bacillus subtilis and bifid is added
Bacillus bacterium solution progress fermentation process, a large amount of protease secreted during the fermentation using bacillus subtilis and Bifidobacterium,
Cellulase, lipase and pectase, make cell rupture, so that the effective component be conducive in fig is discharged from intracellular, make
Active principle, active material are able to extract and utilize to the maximum extent.And the application mentions the further water of product after fermentation,
Directly extracting in water in compared to the prior art, hydrochloric acid, which is added, can increase the dissolution of material effective component in water
Degree, makes it be more easier to be extracted；And the temperature that water mentions is 60 DEG C, the temperature decocted well below water in the prior art
Degree, can protect to the maximum extent the effective component of Chinese medicine material from destroy, especially to thermo-responsive aromatics volatile oil,
Protein, vitamin, amino acid, microelement etc. solve Chinese medicine and the conventional machining process such as are decocting, boiling, enduring, refining, steaming, soaking
In, active constituent is easy to the problem destroyed.
The final products of the application are the water solube powder containing pearl, storage and convenient transportation.
The preparation method of fermented glutinous rice of the present invention is the prior art.
The present invention most preferably component of the water solube powder containing pearl and respective mass percentage is as follows: fineness is
The pearl powder 40% of 400 mesh, aquatic animal muddy flesh 34%, banana 8%, fig 8%, fermented glutinous rice 10%.
And most preferably the water solube powder containing pearl the preparation method is as follows:
1) pearl original powder crushes to obtain pearl powder, and with ethanol solution refluxing extraction 3 times, first time extraction is with volumetric concentration
30% ethanol solution, Extracting temperature are 85 DEG C, and the mass ratio of pearl powder and ethanol solution is 1:6, and I He of extracting solution is obtained by filtration
Extract slag I；The ethanol solution that it is 80% with volumetric concentration that second, which is extracted, Extracting temperature are 100 DEG C, pearl powder and ethanol solution
Mass ratio be 1:5, be obtained by filtration extracting solution II and extract slag II；The ethyl alcohol that it is 55% with volumetric concentration that third time, which is extracted, is molten
Liquid, Extracting temperature are 70 DEG C, and the mass ratio of pearl powder and ethanol solution is 1:8, and extracting solution III is obtained by filtration and extracts slag III；It will
Extracting solution I, extracting solution II and the merging of extracting solution III obtain extracting solution, and extracting slag III is filter residue；
2) then spiral shell is rubbed into spiral shell muddy flesh at -12 DEG C of quick-frozen 45min；
3) acid iodide and molar concentration is added into filter residue as the lactic acid of 5mol/L, is stirred at 70 DEG C, adjusting pH is
It is neutral；Aquatic animal muddy flesh, banana and water is added, papain and trypsase is added, adjusting pH is neutrality, at 33 DEG C
Filtrate is obtained by filtration in stirring enzymatic hydrolysis, sterilization；
4) fig is put into triangular flask, is added and is equivalent to 2 times of total mass of raw material of water, 121 DEG C of sterilizing 30min, so
Bacillus subtilis and Bifidobacterium bacterium solution are added afterwards, is carried out fermented and cultured 10 days at 30 DEG C after mixing, obtains tunning,
In tunning plus water, acetic acid is then added and sodium acetate solution adjusts pH, water is carried out at 60 DEG C and is mentioned, during Aqueous extracts are adjusted to
After property, fig extract is obtained；
5) extracting solution, filtrate and fig extract are mixed, concentration adds fermented glutinous rice, stirs evenly, dry, powder
It is broken, it sterilizes to get the water solube powder containing pearl.
Using the nutritive value highest for the water solube powder containing pearl that above-mentioned most preferred raw material and preparation method obtain,
Mouthfeel is best, is best able to be received and liked by the majority of consumers, best to the therapeutic effect of osteoporosis, and increases bone density effect
Fruit is the most significant, and the increment rate of bone density has reached 57%.
The beneficial effects of the present invention are:
1, the application refluxing extraction 3 times, and the volumetric concentration of refluxing extraction ethyl alcohol and Extracting temperature all become every time
Change, the part effective component in pearl powder can be made sufficiently to extract using the extracting method of the application, especially taurine,
The nutritive value of final drink is improved, supplementing calcium element can be avoided osteoporosis caused by calcium deficiency.
2, aquatic animal meat of the invention is in -15~-8 DEG C of quick-frozen 45-60min, so that internal protein, a variety of amino
Acid, lipopolysaccharides, multivitamin, microelement and the bioactive substances such as enzyme beneficial to human body maintain original activity, not by
It destroys.
3, acid iodide and lactic acid is added in the application in filter residue, and aquatic animal muddy flesh, banana and water are added after acidolysis, adds
Papain and trypsase, stirring enzymatic hydrolysis, add fermented glutinous rice, stir evenly, dry, pulverize, and sterilize up to containing pearl
Water solube powder.The present invention is retained in the nutriment of pearl and aquatic animal meat largely finally by above-mentioned way
Water solube powder in, be lost it is less, the water solube powder taste of preparation is dense, fragrant in taste, and very tasty and refreshing, nutritive value
Height, strong health-care function is deep to be liked by the majority of consumers, can treat osteoporosis.
4, acid iodide and lactic acid is added in the application in filter residue, is conducive to being fully hydrolyzed for pearl raw material, makes the degree of hydrolysis
It is higher, aquatic animal muddy flesh, banana and papain and trypsase is then added, it can not only will be effective in banana
Ingredient hydrolysis is come, and the nutritive value of final water solube powder is increased, additionally it is possible to be carried out using the enzyme wherein contained to pearl powder
It is fully hydrolyzed.
5, preparation method of the invention is simple, and process is short, and processing cost is low, reduces the battalion of nutriment in process
It supports and loses, so that forming interaction between raw material, and retain intact nutrition, retain original shape, color and construction,
It is not required to add any preservative, has fully ensured that the mouthfeel and nutriture value of the drink obtained after the water solube powder containing pearl brews
Value, gained drink are applicable in any crowd, and long-term reference can also beautifying face and moistering lotion.
Specific embodiment
To make the objectives, technical solutions, and advantages of the present invention clearer, below in conjunction with specific embodiment, to this hair
Bright further description.
Embodiment 1
Water solube powder containing pearl, including following component and respective mass percentage: fineness is the pearl powder of 300 mesh
35%, freshwater mussel meat muddy flesh 40%, banana 8%, fig 5%, fermented glutinous rice 12%.
Water solube powder containing pearl the preparation method is as follows:
1) pearl original powder crushes to obtain pearl powder, and with ethanol solution refluxing extraction 3 times, first time extraction is with volumetric concentration
35% ethanol solution, Extracting temperature are 90 DEG C, and the mass ratio of pearl powder and ethanol solution is 1:5, and I He of extracting solution is obtained by filtration
Extract slag I；The ethanol solution that it is 80% with volumetric concentration that second, which is extracted, Extracting temperature are 100 DEG C, pearl powder and ethanol solution
Mass ratio be 1:6, be obtained by filtration extracting solution II and extract slag II；The ethyl alcohol that it is 50% with volumetric concentration that third time, which is extracted, is molten
Liquid, Extracting temperature are 70 DEG C, and the mass ratio of pearl powder and ethanol solution is 1:6, and extracting solution III is obtained by filtration and extracts slag III；It will
Extracting solution I, extracting solution II and the merging of extracting solution III obtain extracting solution, and extracting slag III is filter residue；
2) then freshwater mussel meat is rubbed into freshwater mussel meat muddy flesh at -8 DEG C of quick-frozen 60min；
3) lactic acid that the molar concentration of acid iodide and 4 times of quality that 0.3 times of quality is added into filter residue is 6mol/L, at 60 DEG C
Under be stirred 40h, adjusting pH is neutrality；Freshwater mussel meat muddy flesh, banana and water is added, papain and trypsase is added, adjusts
Saving pH is neutrality, and filtrate is obtained by filtration in stirring enzymatic hydrolysis 2.5h, sterilization at 35 DEG C；
4) fig is put into triangular flask, is added and is equivalent to 2 times of total mass of raw material of water, 121 DEG C of sterilizing 30min, so
It is added afterwards and accounts for the bacillus subtilis of fig quality 1/5 and account for the Bifidobacterium bacterium solution of fig quality 1/5,30 after mixing
It is carried out fermented and cultured 10 days at DEG C, obtains tunning, add water in tunning, acetic acid is then added and sodium acetate solution is adjusted
PH is 3, and water is carried out at 60 DEG C and is mentioned, after Aqueous extracts are adjusted to neutrality, obtains fig extract；
5) extracting solution, filtrate and fig extract are mixed, concentration adds fermented glutinous rice, stirs evenly, dry, powder
It is broken, it sterilizes to get the water solube powder containing pearl.
Embodiment 2
Water solube powder containing pearl, including following component and respective mass percentage: fineness is the pearl powder of 400 mesh
40%, spiral shell muddy flesh 34%, banana 8%, fig 8%, fermented glutinous rice 10%.
Water solube powder containing pearl the preparation method is as follows:
1) pearl original powder crushes to obtain pearl powder, and with ethanol solution refluxing extraction 3 times, first time extraction is with volumetric concentration
30% ethanol solution, Extracting temperature are 85 DEG C, and the mass ratio of pearl powder and ethanol solution is 1:6, and I He of extracting solution is obtained by filtration
Extract slag I；The ethanol solution that it is 80% with volumetric concentration that second, which is extracted, Extracting temperature are 100 DEG C, pearl powder and ethanol solution
Mass ratio be 1:5, be obtained by filtration extracting solution II and extract slag II；The ethyl alcohol that it is 55% with volumetric concentration that third time, which is extracted, is molten
Liquid, Extracting temperature are 70 DEG C, and the mass ratio of pearl powder and ethanol solution is 1:8, and extracting solution III is obtained by filtration and extracts slag III；It will
Extracting solution I, extracting solution II and the merging of extracting solution III obtain extracting solution, and extracting slag III is filter residue；
2) then spiral shell is rubbed into spiral shell muddy flesh at -12 DEG C of quick-frozen 45min；
3) lactic acid that the molar concentration of acid iodide and 3 times of quality that 0.2 times of quality is added into filter residue is 5mol/L, at 70 DEG C
Under be stirred 48h, adjusting pH is neutrality；Spiral shell muddy flesh, banana and water is added, papain and trypsase is added,
Adjusting pH is neutrality, and filtrate is obtained by filtration in stirring enzymatic hydrolysis 2h, sterilization at 33 DEG C；
4) fig is put into triangular flask, is added and is equivalent to 2 times of total mass of raw material of water, 121 DEG C of sterilizing 30min, so
It is added afterwards and accounts for the bacillus subtilis of fig quality 1/5 and account for the Bifidobacterium bacterium solution of fig quality 1/5,30 after mixing
It is carried out fermented and cultured 10 days at DEG C, obtains tunning, add water in tunning, acetic acid is then added and sodium acetate solution is adjusted
PH is 3, and water is carried out at 60 DEG C and is mentioned, after Aqueous extracts are adjusted to neutrality, obtains fig extract；
5) extracting solution, filtrate and fig extract are mixed, concentration adds fermented glutinous rice, stirs evenly, dry, powder
It is broken, it sterilizes to get the water solube powder containing pearl.
Embodiment 3
Water solube powder containing pearl, including following component and respective mass percentage: fineness is the pearl powder of 350 mesh
45%, spiral shell muddy flesh 25%, banana 13%, fig 10%, fermented glutinous rice 7%.
Water solube powder containing pearl the preparation method is as follows:
1) pearl original powder crushes to obtain pearl powder, and with ethanol solution refluxing extraction 3 times, first time extraction is with volumetric concentration
40% ethanol solution, Extracting temperature are 80 DEG C, and the mass ratio of pearl powder and ethanol solution is 1:8, and I He of extracting solution is obtained by filtration
Extract slag I；The ethanol solution that it is 80% with volumetric concentration that second, which is extracted, Extracting temperature are 100 DEG C, pearl powder and ethanol solution
Mass ratio be 1:8, be obtained by filtration extracting solution II and extract slag II；The ethyl alcohol that it is 60% with volumetric concentration that third time, which is extracted, is molten
Liquid, Extracting temperature are 70 DEG C, and the mass ratio of pearl powder and ethanol solution is 1:5, and extracting solution III is obtained by filtration and extracts slag III；It will
Extracting solution I, extracting solution II and the merging of extracting solution III obtain extracting solution, and extracting slag III is filter residue；
2) then spiral shell is rubbed into spiral shell muddy flesh at -15 DEG C of quick-frozen 50min；
3) lactic acid that the molar concentration of acid iodide and 2 times of quality that 0.4 times of quality is added into filter residue is 4mol/L, at 65 DEG C
Under be stirred 46h, adjusting pH is neutrality；Spiral shell muddy flesh, banana and water is added, papain and trypsase is added,
Adjusting pH is neutrality, and filtrate is obtained by filtration in stirring enzymatic hydrolysis 3h, sterilization at 30 DEG C；
4) fig is put into triangular flask, is added and is equivalent to 2 times of total mass of raw material of water, 121 DEG C of sterilizing 30min, so
It is added afterwards and accounts for the bacillus subtilis of fig quality 1/5 and account for the Bifidobacterium bacterium solution of fig quality 1/5,30 after mixing
It is carried out fermented and cultured 10 days at DEG C, obtains tunning, add water in tunning, acetic acid is then added and sodium acetate solution is adjusted
PH is 3, and water is carried out at 60 DEG C and is mentioned, after Aqueous extracts are adjusted to neutrality, obtains fig extract；
5) extracting solution, filtrate and fig extract are mixed, concentration adds fermented glutinous rice, stirs evenly, dry, powder
It is broken, it sterilizes to get the water solube powder containing pearl.
Comparative example 1
Water solube powder containing pearl, including following component and respective mass percentage: fineness is the pearl powder of 400 mesh
55%, spiral shell muddy flesh 45%.
Water solube powder containing pearl the preparation method is as follows:
1) pearl original powder crushes to obtain pearl powder, and with ethanol solution refluxing extraction 3 times, first time extraction is with volumetric concentration
30% ethanol solution, Extracting temperature are 85 DEG C, and the mass ratio of pearl powder and ethanol solution is 1:6, and I He of extracting solution is obtained by filtration
Extract slag I；The ethanol solution that it is 80% with volumetric concentration that second, which is extracted, Extracting temperature are 100 DEG C, pearl powder and ethanol solution
Mass ratio be 1:5, be obtained by filtration extracting solution II and extract slag II；The ethyl alcohol that it is 55% with volumetric concentration that third time, which is extracted, is molten
Liquid, Extracting temperature are 70 DEG C, and the mass ratio of pearl powder and ethanol solution is 1:8, and extracting solution III is obtained by filtration and extracts slag III；It will
Extracting solution I, extracting solution II and the merging of extracting solution III obtain extracting solution, and extracting slag III is filter residue；
2) then spiral shell is rubbed into spiral shell muddy flesh at -12 DEG C of quick-frozen 45min；
3) lactic acid that the molar concentration of acid iodide and 3 times of quality that 0.2 times of quality is added into filter residue is 5mol/L, at 70 DEG C
Under be stirred 48h, adjusting pH is neutrality；Spiral shell muddy flesh and water is added, is stirred evenly at 50 DEG C, adds Papain
Enzyme and trypsase, adjusting pH is neutrality, and filtrate is obtained by filtration in stirring enzymatic hydrolysis 2h, sterilization at 33 DEG C；
4) extracting solution, filtrate are mixed, stirs evenly, dry, pulverize, sterilized to get the water solube powder containing pearl.
Comparative example 2
Water solube powder containing pearl, including following component and respective mass percentage: fineness is the pearl powder of 400 mesh
55%, spiral shell muddy flesh 45%.
Water solube powder containing pearl the preparation method is as follows:
1) pearl original powder crushes to obtain pearl powder, and the lactic acid that molar concentration is 5mol/L is added, and the additional amount of lactic acid is treasure
3 times of pearl silty amount, are stirred at 70 DEG C, and it is neutrality that pH is adjusted after 40h, and spiral shell muddy flesh is added, and after mixing evenly, adjust
Saving pH is neutrality, and the papain for accounting for both pearl powder and spiral shell muddy flesh quality sum 0.2% is added, stirs at 33 DEG C
It mixes, filters, dry, pulverize after 2.5h, sterilize to get the water solube powder containing pearl.
Comparative example 3
Water solube powder containing pearl, including following component and respective mass percentage: fineness is the pearl powder of 400 mesh
40%, spiral shell muddy flesh 34%, banana 8%, fig 8%, fermented glutinous rice 10%.
Water solube powder containing pearl the preparation method is as follows:
1) then spiral shell is rubbed into spiral shell muddy flesh at -12 DEG C of quick-frozen 45min；
2) pearl original powder crushes to obtain pearl powder, and the acid iodide of 0.2 times of quality and mole of 3 times of quality are added into pearl powder
Concentration is the lactic acid of 5mol/L, and 48h is stirred at 70 DEG C, and adjusting pH is neutrality；Spiral shell muddy flesh, banana and water is added,
Papain and trypsase is added, adjusting pH is neutrality, and filtrate is obtained by filtration in stirring enzymatic hydrolysis 2h, sterilization at 33 DEG C；
3) fig is put into triangular flask, is added and is equivalent to 2 times of total mass of raw material of water, 121 DEG C of sterilizing 30min, so
It is added afterwards and accounts for the bacillus subtilis of fig quality 1/5 and account for the Bifidobacterium bacterium solution of fig quality 1/5,30 after mixing
It is carried out fermented and cultured 10 days at DEG C, obtains tunning, add water in tunning, acetic acid is then added and sodium acetate solution is adjusted
PH is 3, and water is carried out at 60 DEG C and is mentioned, after Aqueous extracts are adjusted to neutrality, obtains fig extract；
4) filtrate and fig extract being mixed, concentration adds fermented glutinous rice, stirs evenly, dry, pulverize, it sterilizes,
Up to the water solube powder containing pearl.
Comparative example 4
Water solube powder containing pearl, including following component and respective mass percentage: fineness is the pearl powder of 400 mesh
40%, spiral shell muddy flesh 34%, banana 8%, fig 8%, fermented glutinous rice 10%.
Water solube powder containing pearl the preparation method is as follows:
1) pearl original powder crushes to obtain pearl powder, and with ethanol solution refluxing extraction 3 times, first time extraction is with volumetric concentration
80% ethanol solution, Extracting temperature are 85 DEG C, and the mass ratio of pearl powder and ethanol solution is 1:6, and I He of extracting solution is obtained by filtration
Extract slag I；The ethanol solution that it is 80% with volumetric concentration that second, which is extracted, Extracting temperature are 85 DEG C, pearl powder and ethanol solution
Mass ratio be 1:6, be obtained by filtration extracting solution II and extract slag II；The ethyl alcohol that it is 80% with volumetric concentration that third time, which is extracted, is molten
Liquid, Extracting temperature are 85 DEG C, and the mass ratio of pearl powder and ethanol solution is 1:6, and extracting solution III is obtained by filtration and extracts slag III；It will
Extracting solution I, extracting solution II and the merging of extracting solution III obtain extracting solution, and extracting slag III is filter residue；
2) spiral shell is rubbed into spiral shell muddy flesh；
3) pearl original powder crushes to obtain pearl powder, and the acid iodide of 0.2 times of quality and mole of 3 times of quality are added into pearl powder
Concentration is the lactic acid of 5mol/L, and 48h is stirred at 70 DEG C, and adjusting pH is neutrality；Spiral shell muddy flesh, banana and water is added,
Papain and trypsase is added, adjusting pH is neutrality, and filtrate is obtained by filtration in stirring enzymatic hydrolysis 2h, sterilization at 33 DEG C；
4) fig is put into triangular flask, is added and is equivalent to 2 times of total mass of raw material of water, 121 DEG C of sterilizing 30min, so
It is added afterwards and accounts for the bacillus subtilis of fig quality 1/5 and account for the Bifidobacterium bacterium solution of fig quality 1/5,30 after mixing
It is carried out fermented and cultured 10 days at DEG C, obtains tunning, add water in tunning, acetic acid is then added and sodium acetate solution is adjusted
PH is 3, and water is carried out at 60 DEG C and is mentioned, after Aqueous extracts are adjusted to neutrality, obtains fig extract；
5) extracting solution, filtrate and fig extract are mixed, concentration adds fermented glutinous rice, stirs evenly, dry, powder
It is broken, it sterilizes to get the water solube powder containing pearl.
Water is added to brew into liquid beverage the obtained water solube powder containing pearl of embodiment 1-3 and comparative example 1-4, often
The warm water that 150mL is added in 0.6g pulvis brews into pearl beverage, carries out mouthfeel experiment and treats the health-care efficacies such as osteoporosis
Experiment.
Mouthfeel experiment: selecting 100 volunteers to drink the pearl beverage that embodiment 1-3 and comparative example 1-4 are obtained, and records will
View of the hope person about mouthfeel, as a result such as table 1, the age range of this 100 volunteers is 10-65 years old, and men and women is fifty-fifty.
The experiment for treating osteoporosis: it selects 700 patients with osteoporosis to investigate, is divided into 7 groups, every group
100 people, every group of experimenter drink the pearl beverage that embodiment 1-3 and comparative example 1-4 are obtained respectively, drink 300mL daily, drink
After 4 months, the bone density of patient is measured, as a result such as table 2, using XR-36 type Study of bone mineral density instrument (U.S. NORLAND
Company) carry out Bone mineral density.
Water solube powder of the table 1 containing pearl brews into the mouthfeel experimental result of pearl beverage
The treatment osteoporosis effect experiment result of water solube powder of the table 2 containing pearl
| Embodiment | Drink preceding bone density (g/cm2) | Drink rear bone density (g/cm2) |
| Embodiment 1 | 0.74±0.13 | 1.04±0.10** |
| Embodiment 2 | 0.72±0.10 | 1.13±0.09**# |
| Embodiment 3 | 0.75±0.15 | 1.05±0.11** |
| Comparative example 1 | 0.77±0.09 | 0.92±0.09* |
| Comparative example 2 | 0.73±0.10 | 0.89±0.09* |
| Comparative example 3 | 0.78±0.12 | 0.98±0.13* |
| Comparative example 4 | 0.75±0.13 | 0.96±0.12** |
Note: compared with before treatment,*P < 0.05,**P<0.01；Compared with the control group,#P<0.05。
From the data in Tables 1 and 2 it is found that the water solube powder containing pearl obtained using raw material and method of the invention
There is certain therapeutic effect to osteoporosis, volunteer patients' bone density can be dramatically increased, and water is added to brew into drink deutostoma
Feel, be easier to be esthetically acceptable to the consumers and like.The water solube powder containing pearl that embodiment 2 obtains controls osteoporosis
Therapeutic effect is best, and increase bone density effect is the most significant, and the increment rate of bone density has reached 57%, and the mouthfeel of drink is best；
The water solube powder containing pearl that embodiment 1-3 is obtained is noticeably greater than comparative example 1-4 to the incrementss of volunteer's bone density and obtains
Incrementss of the pearl beverage arrived to volunteer's bone density.
The water solube powder containing pearl that comparative example 1,2 obtains lacks banana, fig and fermented glutinous rice, and comparative example 2
Preparation method in pearl powder do not have alcohol extracting be directly added into lactic acid carry out acidolysis, add papain and digested.Comparison
The pearl beverage mouthfeel that example 1 and 2 obtains is poor, has 23% and 33% volunteer that cannot receive the mouthfeel of this drink respectively, and
And the increase for drinking the bone density of rear volunteer is smaller, the increment rate of bone density is respectively 19% and 22%, is much smaller than embodiment 2
The water solube powder containing pearl to the increment rate of volunteer's bone density, illustrate that acid iodide and lactic acid is added in the application in filter residue,
Be conducive to being fully hydrolyzed for pearl raw material, keep the degree of hydrolysis higher, aquatic animal muddy flesh, banana and pawpaw egg is then added
Effective component hydrolysis in banana can not only be come, increase the battalion of the water solube powder containing pearl by white enzyme and trypsase
Support value, additionally it is possible to be fully hydrolyzed using the TYR enzyme wherein contained to pearl powder, such enzyme pair is found by research
The specificity of pearl is stronger.
Pearl powder in comparative example 3 does not pass through alcohol extracting；The volume of ethyl alcohol used in 3 alcohol extractings of pearl powder in comparative example 4
Concentration is constant, and aquatic animal does not pass through freezing and is directly ground to meat gruel；What comparative example 3 and comparative example 4 obtained contains pearl
Water solube powder brew into pearl beverage mouthfeel it is poor, have 18% and 14% volunteer that cannot receive its mouth completely respectively
Sense, and the increase for drinking the bone density of rear volunteer is smaller, and the increment rate of bone density is respectively 26% and 28%, much smaller than real
Increment rate of the pearl beverage to volunteer's bone density for applying example 2 illustrates the application refluxing extraction 3 times, and each refluxing extraction
The volumetric concentration and Extracting temperature of ethyl alcohol all change, and the part in pearl powder can be made to have using the extracting method of the application
Effect ingredient sufficiently extracts, especially taurine, improves the nutritive value of the finally water solube powder containing pearl, supplements calcium
Element can be avoided osteoporosis caused by calcium deficiency, improve mouthfeel, and aquatic animal meat of the invention is in -15~-8 DEG C of speed
Freeze 45-60min, so that internal protein, a variety of amino acid, lipopolysaccharides, multivitamin, microelement and beneficial to human body
The bioactive substances such as enzyme maintain original activity, are not destroyed.
Claims (10)
1. a kind of water solube powder containing pearl, which is characterized in that including following component and respective mass percentage: pearl powder
35-45%, aquatic animal muddy flesh 25-40%, banana 8-13%, fig 5-10%, fermented glutinous rice 7-12%.
2. as described in claim 1 containing the water solube powder of pearl, which is characterized in that including following component and respective quality hundred
Divide content: pearl powder 40%, aquatic animal muddy flesh 34%, banana 8%, fig 8%, fermented glutinous rice 10%.
3. a kind of preparation method of the water solube powder containing pearl as described in claim 1, which is characterized in that including following step
It is rapid:
1) pearl original powder crushes to obtain pearl powder, and ethanol solution is added into pearl powder, be warming up to 70-100 DEG C carry out reflux mention
It takes, extracting solution and filter residue is obtained by filtration；
2) aquatic animal meat is quick-frozen at -15~-8 DEG C, then rub into aquatic animal muddy flesh；
3) acid iodide and lactic acid are added into filter residue, is stirred at 60-70 DEG C, adjusting pH is neutrality；Aquatic animal meat is added
Papain and trypsase is added in mud, banana and water, and adjusting pH is neutrality, and enzymatic hydrolysis, sterilization, mistake are stirred at 30-35 DEG C
Filter obtains filtrate；
4) fig is put into triangular flask, is added and is equivalent to 2 times of total mass of raw material of water, 121 DEG C of sterilizing 30min, then plus
Enter bacillus subtilis and Bifidobacterium bacterium solution, carried out fermented and cultured 10 days at 30 DEG C after mixing, obtain tunning, ferments
Add water in product, acetic acid is then added and sodium acetate solution adjusts pH, water is carried out at 60 DEG C and is mentioned, Aqueous extracts are adjusted to neutrality
Afterwards, fig extract is obtained；
5) extracting solution, filtrate and fig extract are mixed, concentration adds fermented glutinous rice, stirs evenly, dry, pulverize, kills
Bacterium is to get the water solube powder containing pearl.
4. the preparation method of the water solube powder containing pearl as claimed in claim 3, which is characterized in that pearl described in step 1)
The fineness of powder is 300-400 mesh.
5. the preparation method of the water solube powder containing pearl as claimed in claim 3, which is characterized in that ethyl alcohol described in step 1)
The volumetric concentration of solution is 30-80%.
6. the preparation method of the water solube powder containing pearl as claimed in claim 3, which is characterized in that pearl described in step 1)
The mass ratio of powder and ethanol solution is 1:5-8.
7. the preparation method of the water solube powder containing pearl as described in claim 3 or 4, which is characterized in that described in step 2)
Aquatic animal meat is freshwater mussel meat or spiral shell.
8. the preparation method of the water solube powder containing pearl as described in claim 3 or 4, which is characterized in that the step 2) speed
The jelly time is 45-60min.
9. the preparation method of the water solube powder containing pearl as described in claim 3 or 4, which is characterized in that the step 3) cream
The additional amount of acid is 2-4 times of filter residue quality, and the additional amount of acid iodide is 0.2-0.4 times of filter residue quality.
10. the preparation method of the water solube powder containing pearl as described in claim 3 or 4, which is characterized in that the step 3) cream
The molar concentration of acid is 5-8mol/L.
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| CN1666673A (en) * | 2005-04-06 | 2005-09-14 | 湖南洞庭水殖股份有限公司 | Pearl beverage raw material and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1666673A (en) * | 2005-04-06 | 2005-09-14 | 湖南洞庭水殖股份有限公司 | Pearl beverage raw material and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 卢传功等: "微生物发酵中药功效浅析", 《生物技术世界》 * |
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