CN109554923A - A kind of digit printing fabric flame-proof antibiotic coating - Google Patents
A kind of digit printing fabric flame-proof antibiotic coating Download PDFInfo
- Publication number
- CN109554923A CN109554923A CN201811405242.3A CN201811405242A CN109554923A CN 109554923 A CN109554923 A CN 109554923A CN 201811405242 A CN201811405242 A CN 201811405242A CN 109554923 A CN109554923 A CN 109554923A
- Authority
- CN
- China
- Prior art keywords
- parts
- digit printing
- printing fabric
- proof antibiotic
- hexamethylene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 239000004744 fabric Substances 0.000 title claims abstract description 29
- 238000000576 coating method Methods 0.000 title claims abstract description 28
- 239000011248 coating agent Substances 0.000 title claims abstract description 27
- 230000003115 biocidal effect Effects 0.000 title claims abstract description 26
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 35
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 30
- 125000004836 hexamethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[*:1] 0.000 claims abstract description 27
- 239000002270 dispersing agent Substances 0.000 claims abstract description 20
- 239000003755 preservative agent Substances 0.000 claims abstract description 20
- 230000002335 preservative effect Effects 0.000 claims abstract description 20
- 239000002518 antifoaming agent Substances 0.000 claims abstract description 16
- YEVQZPWSVWZAOB-UHFFFAOYSA-N 2-(bromomethyl)-1-iodo-4-(trifluoromethyl)benzene Chemical compound FC(F)(F)C1=CC=C(I)C(CBr)=C1 YEVQZPWSVWZAOB-UHFFFAOYSA-N 0.000 claims abstract description 15
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 claims abstract description 15
- 239000004354 Hydroxyethyl cellulose Substances 0.000 claims abstract description 15
- 239000000440 bentonite Substances 0.000 claims abstract description 15
- 229910000278 bentonite Inorganic materials 0.000 claims abstract description 15
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims abstract description 15
- TVZPLCNGKSPOJA-UHFFFAOYSA-N copper zinc Chemical compound [Cu].[Zn] TVZPLCNGKSPOJA-UHFFFAOYSA-N 0.000 claims abstract description 15
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 claims abstract description 15
- MTNDZQHUAFNZQY-UHFFFAOYSA-N imidazoline Chemical compound C1CN=CN1 MTNDZQHUAFNZQY-UHFFFAOYSA-N 0.000 claims abstract description 15
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000003208 petroleum Substances 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- UXJMXERXJQAWSP-UHFFFAOYSA-N 2-pentylcyclohexan-1-one Chemical compound CCCCCC1CCCCC1=O UXJMXERXJQAWSP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 125000002947 alkylene group Chemical group 0.000 claims abstract description 13
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims abstract description 13
- 229910021502 aluminium hydroxide Inorganic materials 0.000 claims abstract description 13
- 229940043810 zinc pyrithione Drugs 0.000 claims abstract description 13
- MCMNRKCIXSYSNV-UHFFFAOYSA-N ZrO2 Inorganic materials O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims abstract description 12
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 claims abstract description 12
- RCEAADKTGXTDOA-UHFFFAOYSA-N OS(O)(=O)=O.CCCCCCCCCCCC[Na] Chemical compound OS(O)(=O)=O.CCCCCCCCCCCC[Na] RCEAADKTGXTDOA-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229920002681 hypalon Polymers 0.000 claims abstract description 11
- 235000015511 Liquidambar orientalis Nutrition 0.000 claims abstract description 9
- 239000004870 Styrax Substances 0.000 claims abstract description 9
- 235000000126 Styrax benzoin Nutrition 0.000 claims abstract description 9
- 239000010439 graphite Substances 0.000 claims description 20
- 229910002804 graphite Inorganic materials 0.000 claims description 20
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 claims description 18
- 238000003756 stirring Methods 0.000 claims description 15
- QFOHBWFCKVYLES-UHFFFAOYSA-N Butylparaben Chemical compound CCCCOC(=O)C1=CC=C(O)C=C1 QFOHBWFCKVYLES-UHFFFAOYSA-N 0.000 claims description 10
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 claims description 10
- 229960001617 ethyl hydroxybenzoate Drugs 0.000 claims description 10
- 235000010228 ethyl p-hydroxybenzoate Nutrition 0.000 claims description 10
- 239000004403 ethyl p-hydroxybenzoate Substances 0.000 claims description 10
- NUVBSKCKDOMJSU-UHFFFAOYSA-N ethylparaben Chemical compound CCOC(=O)C1=CC=C(O)C=C1 NUVBSKCKDOMJSU-UHFFFAOYSA-N 0.000 claims description 10
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 claims description 10
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 claims description 9
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 claims description 9
- OLXYLDUSSBULGU-UHFFFAOYSA-N methyl pyridine-4-carboxylate Chemical compound COC(=O)C1=CC=NC=C1 OLXYLDUSSBULGU-UHFFFAOYSA-N 0.000 claims description 9
- 229960002216 methylparaben Drugs 0.000 claims description 9
- 238000002360 preparation method Methods 0.000 claims description 9
- 241000736148 Styrax Species 0.000 claims description 8
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 6
- 229910052708 sodium Inorganic materials 0.000 claims description 6
- 239000011734 sodium Substances 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 5
- 229910052754 neon Inorganic materials 0.000 claims description 5
- GKAOGPIIYCISHV-UHFFFAOYSA-N neon atom Chemical compound [Ne] GKAOGPIIYCISHV-UHFFFAOYSA-N 0.000 claims description 5
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims 3
- 239000004411 aluminium Substances 0.000 claims 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims 2
- 229910052782 aluminium Inorganic materials 0.000 claims 2
- 150000002148 esters Chemical class 0.000 claims 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims 2
- 241000259759 Cassida nobilis Species 0.000 claims 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 1
- 229920000388 Polyphosphate Polymers 0.000 claims 1
- 229910052799 carbon Inorganic materials 0.000 claims 1
- 239000001205 polyphosphate Substances 0.000 claims 1
- 235000011176 polyphosphates Nutrition 0.000 claims 1
- 238000005516 engineering process Methods 0.000 abstract description 6
- 244000028419 Styrax benzoin Species 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 8
- SNRUBQQJIBEYMU-UHFFFAOYSA-N dodecane Chemical compound CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 description 7
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 6
- 150000001336 alkenes Chemical class 0.000 description 4
- 238000001354 calcination Methods 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- 239000001488 sodium phosphate Substances 0.000 description 4
- 229910000162 sodium phosphate Inorganic materials 0.000 description 4
- 229910052938 sodium sulfate Inorganic materials 0.000 description 4
- 235000011152 sodium sulphate Nutrition 0.000 description 4
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 4
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 3
- 239000004408 titanium dioxide Substances 0.000 description 3
- 229910052726 zirconium Inorganic materials 0.000 description 3
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 230000000979 retarding effect Effects 0.000 description 2
- QQZOPKMRPOGIEB-UHFFFAOYSA-N 2-Oxohexane Chemical compound CCCCC(C)=O QQZOPKMRPOGIEB-UHFFFAOYSA-N 0.000 description 1
- ATWGHWZRHOJITC-UHFFFAOYSA-N [S].C1=CC=NC=C1 Chemical compound [S].C1=CC=NC=C1 ATWGHWZRHOJITC-UHFFFAOYSA-N 0.000 description 1
- 230000000845 anti-microbial effect Effects 0.000 description 1
- 239000013065 commercial product Substances 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
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- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/04—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06N3/045—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds with polyolefin or polystyrene (co-)polymers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/30—Flame or heat resistance, fire retardancy properties
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N2209/00—Properties of the materials
- D06N2209/06—Properties of the materials having thermal properties
- D06N2209/067—Flame resistant, fire resistant
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N2209/00—Properties of the materials
- D06N2209/16—Properties of the materials having other properties
- D06N2209/1671—Resistance to bacteria, mildew, mould, fungi
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Abstract
The application belongs to fabric coating technology, specially a kind of digit printing fabric flame-proof antibiotic coating, raw material including following portions by weight, 20 parts of hydroxyethyl cellulose, 16 parts of chlorosulfonated polyethylene, 13 parts of trioctyl phosphate, 25 parts of hexamethylene alkylene pentylcyclohexanone, 30 parts of petroleum ether, 10 parts of stearate, 24 parts of sorbierite, 6 parts of hexamethylene, 18 parts of lauryl sodium sulfate, 25 parts of copper zinc pyrithione, 5 parts of imidazoline, 1000 parts of water, 5 parts of graphite powder, 15 parts of aluminium hydroxide, 25 parts of zirconium dioxide, 15 parts of bentonite, 5 parts of styrax, 5 parts of defoaming agent, 3 parts of dispersing agent, 2 parts of preservative.
Description
Technical field
The application belongs to fabric coating technology, specially a kind of preparation method of digit printing fabric flame-proof antibiotic coating.
Background technique
Digit printing is the stamp carried out with digital technology.Digital printing technology is as computer technology continues to develop
And a kind of new high-tech product for integrating machinery, computer machine electronic information technology gradually formed.And now with life
The raising of bioplasm amount, people more and more select outdoor sports, such as mountain-climbing, rock-climbing, and movement can generate a large amount of outdoors
Sweat, this requires fabrics to have antibacterial, fire-retardant excellent function.
Summary of the invention
In order to solve the above-mentioned technical problem, this application provides a kind of preparation sides of digit printing fabric flame-proof antibiotic coating
Method, the application are realized by following proposal:
A kind of digit printing fabric flame-proof antibiotic coating, 20 parts of hydroxyethyl cellulose, 16 parts of chlorosulfonated polyethylene, trioctyl phosphate
13 parts, 25 parts of hexamethylene alkylene pentylcyclohexanone, 30 parts of petroleum ether, 10 parts of stearate, 24 parts of sorbierite, 6 parts of hexamethylene, dodecane
18 parts of base sodium sulphate, 25 parts of copper zinc pyrithione, 5 parts of imidazoline, 1000 parts of water, 5 parts of graphite powder, 15 parts of aluminium hydroxide, titanium dioxide
25 parts of zirconium, 15 parts of bentonite, 5 parts of styrax, 5 parts of defoaming agent, 3 parts of dispersing agent, 2 parts of preservative.
Preferably, 18 parts of hydroxyethyl cellulose, 14 parts of chlorosulfonated polyethylene, 11 parts of trioctyl phosphate, hexamethylene alkylene basic ring
23 parts of hexanone, 28 parts of petroleum ether, 8 parts of stearate, 22 parts of sorbierite, 4 parts of hexamethylene, 16 parts of lauryl sodium sulfate, pyridine
23 parts of sulfidion copper zinc, 3 parts of imidazoline, 1000 parts of water, 4 parts of graphite powder, 13 parts of aluminium hydroxide, 23 parts of zirconium dioxide, 13 parts of bentonite,
4 parts of styrax, 4 parts of defoaming agent, 2 parts of dispersing agent, 1.5 parts of preservative.
Preferably, 16 parts of hydroxyethyl cellulose, 12 parts of chlorosulfonated polyethylene, 9 parts of trioctyl phosphate, hexamethylene alkylidene hexamethylene
20 parts of ketone, 22 parts of petroleum ether, 6 parts of stearate, 20 parts of sorbierite, 2 parts of hexamethylene, 13 parts of lauryl sodium sulfate, pyridine sulphur
20 parts of copper zinc, 3 parts of imidazoline, 1000 parts of water, 3 parts of graphite powder, 10 parts of aluminium hydroxide, 20 parts of zirconium dioxide, 11 parts of bentonite, peace
Breath is 2 parts, 2 parts of defoaming agent, 2 parts of dispersing agent, 1 part of preservative fragrant.
Preferably, the defoaming agent is BYK057.
Preferably, the dispersing agent is sodium tetrapolyphosphate, and the mixture of calgon and modified siloxane, described four is poly-
The mass ratio of sodium phosphate, calgon and modified siloxane is 1:2:1.
Preferably, the preservative be methylparaben, ethylparaben, propylben and butyl hydroxybenzoate, it is described
Methylparaben, ethylparaben, propylben and butyl hydroxybenzoate mass ratio be 1:4:2:3.
A kind of preparation method of digit printing fabric flame-proof antibiotic coating, (1) is by hydroxyethyl cellulose, the poly- second of chlorosulfonation
Alkene, trioctyl phosphate, hexamethylene alkylene pentylcyclohexanone, petroleum ether, stearate, sorbierite, hexamethylene, lauryl sodium sulfate,
Copper zinc pyrithione, imidazoline and water are placed in reaction kettle, and stir 3h at 55 DEG C；(2) continue that defoaming is added into reaction kettle
Agent, dispersing agent and preservative simultaneously stir 4h at 70 DEG C；(3) by graphite powder, aluminium hydroxide, zirconium dioxide and bentonite are in 500
Calcining 2h is placed on machinery spheroidal graphite 8h in spheroidal graphite tank and obtains premix at DEG C；(4) step (2) are added in premix obtained by step (3)
Reaction kettle at 60 DEG C stir 2h up to digit printing fabric flame-proof antibiotic coating.
Preferably, the revolving speed of the spheroidal graphite is 600r/min, and spheroidal graphite atmosphere is under neon atmosphere.
The application's, the utility model has the advantages that the application preparation process is simple, has high fire-retardance, high anti-microbial property, is suitble in face
Material field uses, and improves the performance of product.
Specific embodiment
Embodiment 1
A kind of digit printing fabric flame-proof antibiotic coating, 20 parts of hydroxyethyl cellulose, 16 parts of chlorosulfonated polyethylene, trioctyl phosphate
13 parts, 25 parts of hexamethylene alkylene pentylcyclohexanone, 30 parts of petroleum ether, 10 parts of stearate, 24 parts of sorbierite, 6 parts of hexamethylene, dodecane
18 parts of base sodium sulphate, 25 parts of copper zinc pyrithione, 5 parts of imidazoline, 1000 parts of water, 5 parts of graphite powder, 15 parts of aluminium hydroxide, titanium dioxide
25 parts of zirconium, 15 parts of bentonite, 5 parts of styrax, 5 parts of defoaming agent, 3 parts of dispersing agent, 2 parts of preservative.
Preferably, the defoaming agent is BYK057.
Preferably, the dispersing agent is sodium tetrapolyphosphate, and the mixture of calgon and modified siloxane, described four is poly-
The mass ratio of sodium phosphate, calgon and modified siloxane is 1:2:1.
Preferably, the preservative be methylparaben, ethylparaben, propylben and butyl hydroxybenzoate, it is described
Methylparaben, ethylparaben, propylben and butyl hydroxybenzoate mass ratio be 1:4:2:3.
A kind of preparation method of digit printing fabric flame-proof antibiotic coating, (1) is by hydroxyethyl cellulose, the poly- second of chlorosulfonation
Alkene, trioctyl phosphate, hexamethylene alkylene pentylcyclohexanone, petroleum ether, stearate, sorbierite, hexamethylene, lauryl sodium sulfate,
Copper zinc pyrithione, imidazoline and water are placed in reaction kettle, and stir 3h at 55 DEG C；(2) continue that defoaming is added into reaction kettle
Agent, dispersing agent and preservative simultaneously stir 4h at 70 DEG C；(3) by graphite powder, aluminium hydroxide, zirconium dioxide and bentonite are in 500
Calcining 2h is placed on machinery spheroidal graphite 8h in spheroidal graphite tank and obtains premix at DEG C；(4) step (2) are added in premix obtained by step (3)
Reaction kettle at 60 DEG C stir 2h up to digit printing fabric flame-proof antibiotic coating.
Preferably, the revolving speed of the spheroidal graphite is 600r/min, and spheroidal graphite atmosphere is under neon atmosphere.
Embodiment 2
A kind of digit printing fabric flame-proof antibiotic coating, 18 parts of hydroxyethyl cellulose, 14 parts of chlorosulfonated polyethylene, trioctyl phosphate
11 parts, 23 parts of hexamethylene alkylene pentylcyclohexanone, 28 parts of petroleum ether, 8 parts of stearate, 22 parts of sorbierite, 4 parts of hexamethylene, dodecane
16 parts of base sodium sulphate, 23 parts of copper zinc pyrithione, 3 parts of imidazoline, 1000 parts of water, 4 parts of graphite powder, 13 parts of aluminium hydroxide, titanium dioxide
23 parts of zirconium, 13 parts of bentonite, 4 parts of styrax, 4 parts of defoaming agent, 2 parts of dispersing agent, 1.5 parts of preservative.
Preferably, the defoaming agent is BYK057.
Preferably, the dispersing agent is sodium tetrapolyphosphate, and the mixture of calgon and modified siloxane, described four is poly-
The mass ratio of sodium phosphate, calgon and modified siloxane is 1:2:1.
Preferably, the preservative be methylparaben, ethylparaben, propylben and butyl hydroxybenzoate, it is described
Methylparaben, ethylparaben, propylben and butyl hydroxybenzoate mass ratio be 1:4:2:3.
A kind of preparation method of digit printing fabric flame-proof antibiotic coating, (1) is by hydroxyethyl cellulose, the poly- second of chlorosulfonation
Alkene, trioctyl phosphate, hexamethylene alkylene pentylcyclohexanone, petroleum ether, stearate, sorbierite, hexamethylene, lauryl sodium sulfate,
Copper zinc pyrithione, imidazoline and water are placed in reaction kettle, and stir 3h at 55 DEG C；(2) continue that defoaming is added into reaction kettle
Agent, dispersing agent and preservative simultaneously stir 4h at 70 DEG C；(3) by graphite powder, aluminium hydroxide, zirconium dioxide and bentonite are in 500
Calcining 2h is placed on machinery spheroidal graphite 8h in spheroidal graphite tank and obtains premix at DEG C；(4) step (2) are added in premix obtained by step (3)
Reaction kettle at 60 DEG C stir 2h up to digit printing fabric flame-proof antibiotic coating.
Preferably, the revolving speed of the spheroidal graphite is 600r/min, and spheroidal graphite atmosphere is under neon atmosphere.
Embodiment 3
A kind of digit printing fabric flame-proof antibiotic coating, 16 parts of hydroxyethyl cellulose, 12 parts of chlorosulfonated polyethylene, trioctyl phosphate
9 parts, 20 parts of hexamethylene alkylene pentylcyclohexanone, 22 parts of petroleum ether, 6 parts of stearate, 20 parts of sorbierite, 2 parts of hexamethylene, dodecyl
13 parts of sodium sulphate, 20 parts of copper zinc pyrithione, 3 parts of imidazoline, 1000 parts of water, 3 parts of graphite powder, 10 parts of aluminium hydroxide, zirconium dioxide
20 parts, 11 parts of bentonite, 2 parts of styrax, 2 parts of defoaming agent, 2 parts of dispersing agent, 1 part of preservative.
Preferably, the defoaming agent is BYK057.
Preferably, the dispersing agent is sodium tetrapolyphosphate, and the mixture of calgon and modified siloxane, described four is poly-
The mass ratio of sodium phosphate, calgon and modified siloxane is 1:2:1.
Preferably, the preservative be methylparaben, ethylparaben, propylben and butyl hydroxybenzoate, it is described
Methylparaben, ethylparaben, propylben and butyl hydroxybenzoate mass ratio be 1:4:2:3.
A kind of preparation method of digit printing fabric flame-proof antibiotic coating, (1) is by hydroxyethyl cellulose, the poly- second of chlorosulfonation
Alkene, trioctyl phosphate, hexamethylene alkylene pentylcyclohexanone, petroleum ether, stearate, sorbierite, hexamethylene, lauryl sodium sulfate,
Copper zinc pyrithione, imidazoline and water are placed in reaction kettle, and stir 3h at 55 DEG C；(2) continue that defoaming is added into reaction kettle
Agent, dispersing agent and preservative simultaneously stir 4h at 70 DEG C；(3) by graphite powder, aluminium hydroxide, zirconium dioxide and bentonite are in 500
Calcining 2h is placed on machinery spheroidal graphite 8h in spheroidal graphite tank and obtains premix at DEG C；(4) step (2) are added in premix obtained by step (3)
Reaction kettle at 60 DEG C stir 2h up to digit printing fabric flame-proof antibiotic coating.
Preferably, the revolving speed of the spheroidal graphite is 600r/min, and spheroidal graphite atmosphere is under neon atmosphere.
Performance measurement, the data obtained such as following table, fire protection flame retarding accreditation are carried out for embodiment 1-3 and certain commercial product
Using UL94 standard.
As it can be seen that the application has good corrosion-resistant, fire protection flame retarding, anti-mildew and antibacterial performance.
Claims (8)
1. kind of digit printing fabric flame-proof antibiotic coating, which is characterized in that 20 parts of hydroxyethyl cellulose, chlorosulfonated polyethylene 16
Part, 13 parts of trioctyl phosphate, 25 parts of hexamethylene alkylene pentylcyclohexanone, 30 parts of petroleum ether, 10 parts of stearate, 24 parts of sorbierite, ring
6 parts of hexane, 18 parts of lauryl sodium sulfate, 25 parts of copper zinc pyrithione, 5 parts of imidazoline, 1000 parts of water, 5 parts of graphite powder, hydroxide
15 parts of aluminium, 25 parts of zirconium dioxide, 15 parts of bentonite, 5 parts of styrax, 5 parts of defoaming agent, 3 parts of dispersing agent, 2 parts of preservative.
2. a kind of digit printing fabric flame-proof antibiotic coating as described in claim 1, which is characterized in that hydroxyethyl cellulose 18
Part, 14 parts of chlorosulfonated polyethylene, 11 parts of trioctyl phosphate, 23 parts of hexamethylene alkylene pentylcyclohexanone, 28 parts of petroleum ether, stearate 8
Part, 22 parts of sorbierite, 4 parts of hexamethylene, 16 parts of lauryl sodium sulfate, 23 parts of copper zinc pyrithione, 3 parts of imidazoline, 1000 parts of water,
4 parts of graphite powder, 13 parts of aluminium hydroxide, 23 parts of zirconium dioxide, 13 parts of bentonite, 4 parts of styrax, 4 parts of defoaming agent, dispersing agent 2
Part, 1.5 parts of preservative.
3. a kind of digit printing fabric flame-proof antibiotic coating as described in claim 1, which is characterized in that hydroxyethyl cellulose 16
Part, 12 parts of chlorosulfonated polyethylene, 9 parts of trioctyl phosphate, 20 parts of hexamethylene alkylene pentylcyclohexanone, 22 parts of petroleum ether, stearate 6
Part, 20 parts of sorbierite, 2 parts of hexamethylene, 13 parts of lauryl sodium sulfate, 20 parts of copper zinc pyrithione, 3 parts of imidazoline, 1000 parts of water,
3 parts of graphite powder, 10 parts of aluminium hydroxide, 20 parts of zirconium dioxide, 11 parts of bentonite, 2 parts of styrax, 2 parts of defoaming agent, dispersing agent 2
Part, 1 part of preservative.
4. a kind of digit printing fabric flame-proof antibiotic coating as described in claim 1, which is characterized in that the defoaming agent is
BYK057。
5. a kind of digit printing fabric flame-proof antibiotic coating as described in claim 1, which is characterized in that the dispersing agent is four
The mixture of polyphosphate sodium, calgon and modified siloxane, the sodium tetrapolyphosphate, calgon and modified siloxane
Mass ratio be 1:2:1.
6. a kind of digit printing fabric flame-proof antibiotic coating as described in claim 1, which is characterized in that the preservative is Buddhist nun
Moor tortoise beetle ester, ethylparaben, propylben and butyl hydroxybenzoate, the methylparaben, ethylparaben, nipalgin third
The mass ratio of ester and butyl hydroxybenzoate is 1:4:2:3.
7. a kind of preparation method of digit printing fabric flame-proof antibiotic coating as described in claim 1, which is characterized in that (1)
By hydroxyethyl cellulose, chlorosulfonated polyethylene, trioctyl phosphate, hexamethylene alkylene pentylcyclohexanone, petroleum ether, stearate, sorb
Alcohol, hexamethylene, lauryl sodium sulfate, copper zinc pyrithione, imidazoline and water are placed in reaction kettle, and stir 3h at 55 DEG C；
(2) continue that defoaming agent, dispersing agent and preservative are added into reaction kettle and stir 4h at 70 DEG C；(3) by graphite powder, hydroxide
Aluminium, zirconium dioxide and bentonite, which calcine 2h at 500 DEG C and be placed on machinery spheroidal graphite 8h in spheroidal graphite tank, obtains premix；(4) by step
(3) gained premix, which is added in the reaction kettle of step (2) at 60 DEG C, stirs 2h up to digit printing fabric flame-proof antibiotic coating.
8. a kind of preparation method of digit printing fabric flame-proof antibiotic coating as claimed in claim 7, which is characterized in that described
The revolving speed of spheroidal graphite is 600r/min, and spheroidal graphite atmosphere is under neon atmosphere.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811405242.3A CN109554923A (en) | 2018-11-23 | 2018-11-23 | A kind of digit printing fabric flame-proof antibiotic coating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811405242.3A CN109554923A (en) | 2018-11-23 | 2018-11-23 | A kind of digit printing fabric flame-proof antibiotic coating |
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| Publication Number | Publication Date |
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| CN109554923A true CN109554923A (en) | 2019-04-02 |
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| CN201811405242.3A Pending CN109554923A (en) | 2018-11-23 | 2018-11-23 | A kind of digit printing fabric flame-proof antibiotic coating |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113308875A (en) * | 2021-06-07 | 2021-08-27 | 宜禾股份有限公司 | High-acid-alkali-resistance flame-retardant fabric for work clothes |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105696346A (en) * | 2016-03-08 | 2016-06-22 | 杨超 | Antibacterial and flame-retardant coating for garment fabric |
-
2018
- 2018-11-23 CN CN201811405242.3A patent/CN109554923A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105696346A (en) * | 2016-03-08 | 2016-06-22 | 杨超 | Antibacterial and flame-retardant coating for garment fabric |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113308875A (en) * | 2021-06-07 | 2021-08-27 | 宜禾股份有限公司 | High-acid-alkali-resistance flame-retardant fabric for work clothes |
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Application publication date: 20190402 |